CN104450232B - A kind of preparation method of jeans scavenger specially - Google Patents
A kind of preparation method of jeans scavenger specially Download PDFInfo
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- CN104450232B CN104450232B CN201410660800.6A CN201410660800A CN104450232B CN 104450232 B CN104450232 B CN 104450232B CN 201410660800 A CN201410660800 A CN 201410660800A CN 104450232 B CN104450232 B CN 104450232B
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- jeans
- cedarleaves
- preparation
- extract
- surfactant
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Abstract
The invention provides a kind of preparation method of jeans scavenger specially, including step：The sucrose fatty ester of the preparation of surfactant, plus ionized water, gluconic acid, EDTA obtain surfactant；The preparation of CedarLeaves extract：CedarLeaves extract is obtained after the multiple alcohol extracting of CedarLeaves；The preparation of auxiliary agent：Sodium citrate, calcium soap and deionized water are mixed in proportion；Deionized water is heated to 55 DEG C, surfactant is added while stirring, until whole dissolvings, CedarLeaves extract, natural essence and auxiliary agent is added after cooling to 40 DEG C, the solution of stabilization is formed after being sufficiently stirred for, salt adjustment viscosity is added and is obtained jeans special cleaning.The CedarLeaves extract that spy adds can carry out fixation to the dyeing of jeans, be greatly reduced the phenomenon that fades of jeans；CedarLeaves extract is capable of the skin-friction force increase of jeans fabric fibre simultaneously, jeans is hardened, and keeps jeans pants type.
Description
Technical field
The present invention relates to a kind of clothes detergent, more particularly to a kind of preparation method of jeans cleaning agent.
Background technology
Jeans are a kind of currently a popular dress ornaments, and almost each young man has a jeans.Due to jeans certainly
The dyeing of body, causes jeans and is particularly easy to fade when washing, and a good jeans are often over washing
Color just changes completely after several times, and this problem strong influence that fades jeans wear the life-span.At present all using washing
Clothing liquid is cleaned to jeans, but existing liquid detergent has submissive effect to clothing, clothes is limbered up after exactly washing,
Make comfortable and easy to wear.And jeans, in order to keep pants type, generally requiring need not be submissive, therefore, liquid detergent of the prior art etc.
It is not appropriate for the washing of jeans.
The content of the invention
It is an object of the invention to provide a kind of preparation method of jeans scavenger specially, the preparation method is simple and easy to apply,
Do not faded during washing during the jeans cleaning agent cleaning jeans of acquisition, the advantages of maintain type after drying.
The technical solution adopted for the present invention to solve the technical problems is：
1st, a kind of preparation method of jeans scavenger specially, it is characterised in that comprise the following steps：
1) preparation of surfactant：Take the sucrose fatty ester of 1 weight portion, plus 3.5 weight portions ionized water, magnetic force stirs
Mix down, sequentially add the gluconic acid of 0.2 weight portion, the EDTA of 0.6 weight portion and keep the transparency of solution, maintain the temperature at 43
DEG C, obtain surfactant after stirring 1-1.5h；
2) preparation of CedarLeaves extract：The fresh CedarLeaves of 1 weight portion are taken, the 95% of 5 weight portions is added after CedarLeaves are crushed
Ethanol, extracts 2h at 65 DEG C, after filtering, recrement is extracted 3 hours at adding 65 DEG C of 95% ethanol of 3 weight portions；It is then combined with
Ethanol extract twice, after ethanol is reclaimed in evaporation, the solubility for adding 4 weight portions is 99% ethanol, is heated at 50 DEG C molten
Solution 1h, is cooled to 20 DEG C of stratification, removes a layer solution, then after evaporating and reclaiming ethanol, obtain CedarLeaves extract；
3) preparation of auxiliary agent：Sodium citrate, calcium soap and deionized water are pressed 1:5:12 part by weight mixing, is maintained at temperature
38 DEG C or so of degree, magnetic agitation 1h；
4) deionized water is heated to 55 DEG C, surfactant is added while stirring, until whole dissolvings, cool to 40 DEG C
After add CedarLeaves extract, natural essence and auxiliary agent, the solution of stabilization, wherein deionized water, surface are formed after being sufficiently stirred for
Activating agent, CedarLeaves extract, natural essence, the weight ratio of auxiliary agent are 100:20：12:2::25；
5) obtain adding the salt for accounting for deionized water weight 0.2-1% to adjust the viscosity of solution in solution in step 4, after
Continuous stirring obtains jeans scavenger specially to well mixed；
6) pack.
The distinctive technique effect of the present invention is：
1) proved by experimental verification, the CedarLeaves extract that uniqueness is added can carry out fixation to the dyeing of jeans, make
The phenomenon that fades of jeans is greatly reduced；CedarLeaves extract is capable of the skin-friction force increase of jeans fabric fibre simultaneously, makes
Jeans harden, keep jeans pants type, while it is this harden do not interfere with jeans dress it is comfortable；
2) low cost, safety non-toxic；
3) it is free from environmental pollution and with certain dirt-removing power, the special cleaning of present invention description compared with the prior art in
Liquid detergent and washing powder etc., dirt-removing power is general, but present cleaning clothes is rapid, and clothing will not be very dirty, should
Cleaning fluid tackles normal jeans cleaning enough, if increasing dirt-removing power, will certainly increase new chemical substance, can cause
The pollution of environment.
Specific embodiment
With reference to embodiment, the present invention will be further described：
Embodiment 1
A kind of preparation method of jeans scavenger specially, comprises the following steps：
1) preparation of surfactant：Take the sucrose fatty ester of 1 weight portion, plus 3.5 weight portions ionized water, magnetic force stirs
Mix down, sequentially add the gluconic acid of 0.2 weight portion, the EDTA of 0.6 weight portion and keep the transparency of solution, maintain the temperature at 43
DEG C, obtain surfactant after stirring 1-1.5h；
2) preparation of CedarLeaves extract：The fresh CedarLeaves of 1 weight portion are taken, the 95% of 5 weight portions is added after CedarLeaves are crushed
Ethanol, extracts 2h at 65 DEG C, after filtering, recrement is extracted 3 hours at adding 65 DEG C of 95% ethanol of 3 weight portions；It is then combined with
Ethanol extract twice, after ethanol is reclaimed in evaporation, the solubility for adding 4 weight portions is 99% ethanol, is heated at 50 DEG C molten
Solution 1h, is cooled to 20 DEG C of stratification, removes a layer solution, then after evaporating and reclaiming ethanol, obtain CedarLeaves extract；
3) preparation of auxiliary agent：Sodium citrate, calcium soap and deionized water are pressed 1:5:12 part by weight mixing, is maintained at temperature
38 DEG C or so of degree, magnetic agitation 1h；
4) deionized water is heated to 55 DEG C, surfactant is added while stirring, until whole dissolvings, cool to 40 DEG C
After add CedarLeaves extract, natural essence and auxiliary agent, the solution of stabilization, wherein deionized water, surface are formed after being sufficiently stirred for
Activating agent, CedarLeaves extract, natural essence, the weight ratio of auxiliary agent are 100:20：12:2::25；
5) obtain adding the salt for accounting for deionized water weight 0.2% to adjust the viscosity of solution in solution in step 4, continue
Stirring obtains jeans scavenger specially to well mixed；
6) pack.
Embodiment 2
Jeans special cleaning to being prepared by the method carries out compliance test result, is tested as follows respectively
1) detergency test
Three pairs of jeans are taken, a piece of 5cm × 5cm regions are looked on the trouser legs of three, upper soil, oil stain and meal are infected with respectively
Stain, is then cleaned using cleaning agent of the present invention, it is found that the Polluted area of three pairs of jeans be can't see completely；
2) surface tension test
The surface tension of the cleaning fluid is tested using interfacial tensimeter, it is average repeatedly to obtain surface tension after test
Value is 34.8 × 10-3N/m, close to the 35.710 of liquid detergent-3N/m；
3) fixation aptitude tests
12 pairs of jeans of market stochastic buying, 12 pairs of jeans keep same brand, same producer, same batch to produce,
Then four in 12 pairs of trousers are put into and 3h is soaked in the water for be dissolved with ordinary liquid laundry detergent, another 4 are put into and are dissolved with washing powder
Water in soak 3h, last four are put into be dissolved with the water of scavenger specially of the present invention and soak 3h；
The water of ordinary liquid laundry detergent is dissolved with, the water for being dissolved with washing powder and the water for being dissolved with scavenger specially of the present invention
The weight of the liquid detergent, washing powder and cleaning agent of middle addition is consistent.
Then the water after immersion is taken, is respectively charged into 12 test tubes, then allow tester to the water in 12 pipes by color
Depth ranking, most deep is the 1st, and most shallow for last, tester does not know that corresponding is liquid detergent, laundry when test
Powder or scavenger specially of the invention.
Tested by least 20 people, the sequence for drawing all is that four test tubes soaked in scavenger specially are all discharged to
Four afterwards.
It is possible thereby to illustrate scavenger specially tint retention of the invention be it is stable, effectively.
4) soft right degree test
This experiment touches test using tester's hand, takes same batch, same to brand, with 10 pairs of jeans of factory, will wherein five
Bar is cleaned with ordinary liquid laundry detergent, and the scavenger specially cleaning of the invention of five strip adoptions, dries 10 pairs of trousers after washing, so in addition
Afterwards five testers everyone assign to two pairs of trousers, a kind of strip adoption liquid detergent washing, strip adoption scavenger specially washing,
Allow tester to judge the pliability of two jeans, choose relatively hard one.Test result is that five people select
The trousers washed using scavenger specially, illustrate the scavenger specially of the present invention to trousers with certain shield
Type is acted on.
It will be recognized by those skilled in the art, on the premise of without departing from protection scope of the present invention, can be to above-mentioned
Implementation method carries out various modifications, change and combination, and thinks that this modification, change and combination are the models in originality thought
Within enclosing.
Claims (1)
1. a kind of preparation method of jeans scavenger specially, it is characterised in that comprise the following steps：
1) preparation of surfactant：Take the sucrose fatty ester of 1 weight portion, plus 3.5 weight portions ionized water, magnetic agitation
Under, sequentially add the gluconic acid of 0.2 weight portion, the EDTA of 0.6 weight portion and keep the transparency of solution, maintain the temperature at 43
DEG C, obtain surfactant after stirring 1-1.5h；
2) preparation of CedarLeaves extract：The fresh CedarLeaves of 1 weight portion are taken, 95% ethanol of 5 weight portions are added after CedarLeaves are crushed,
2h is extracted at 65 DEG C, after filtering, recrement is extracted 3 hours at adding 65 DEG C of 95% ethanol of 3 weight portions；It is then combined with twice
Ethanol extract, after ethanol is reclaimed in evaporation, the concentration for adding 4 weight portions is 99% ethanol, and heating for dissolving 1h, cold at 50 DEG C
But to 20 DEG C of stratification, a layer solution is removed, then after evaporating and reclaiming ethanol, obtain CedarLeaves extract；
3) preparation of auxiliary agent：Sodium citrate, calcium soap and deionized water are pressed 1:5:12 part by weight mixing, is maintained at temperature 38
DEG C, magnetic agitation 1h；
4) deionized water is heated to 55 DEG C, step 1 is added while stirring) described in surfactant, until whole dissolvings, drop
Temperature is to adding step 2 after 40 DEG C) described in CedarLeaves extract, natural essence and step 3) described in auxiliary agent, after being sufficiently stirred for
The solution of stabilization is formed, wherein described deionized water, described surfactant, described CedarLeaves extract, described day
Right essence, the weight ratio of described auxiliary agent are 100:20: 12:2:25；
5) in step 4) add in the solution that obtains the deionized water weight 0.2-1% for accounting for described salt adjustment solution it is viscous
Degree, it is to obtain jeans scavenger specially to continue to stir to being well mixed；
6) pack.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410660800.6A CN104450232B (en) | 2014-11-19 | 2014-11-19 | A kind of preparation method of jeans scavenger specially |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410660800.6A CN104450232B (en) | 2014-11-19 | 2014-11-19 | A kind of preparation method of jeans scavenger specially |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104450232A CN104450232A (en) | 2015-03-25 |
| CN104450232B true CN104450232B (en) | 2017-06-06 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410660800.6A Expired - Fee Related CN104450232B (en) | 2014-11-19 | 2014-11-19 | A kind of preparation method of jeans scavenger specially |
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Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104862091A (en) * | 2015-06-03 | 2015-08-26 | 杜杭华 | Preparation method of special cleaning agent for jeans |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BR9714454A (en) * | 1996-12-31 | 2000-03-21 | Procter & Gamble | endo dye fixers |
| CN103343064A (en) * | 2013-07-22 | 2013-10-09 | 孙佳丽 | Fading resistant strong-detergency laundry detergent |
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2014
- 2014-11-19 CN CN201410660800.6A patent/CN104450232B/en not_active Expired - Fee Related
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| CN104450232A (en) | 2015-03-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB03 | Change of inventor or designer information | ||
| CB03 | Change of inventor or designer information |
Inventor after: Meng Sen Inventor after: Hua Jinghua Inventor after: Shen Hongya Inventor after: Wang Ximing Inventor after: Qi Jun Inventor after: Liu Bing Inventor before: Zhou Dasheng |
|
| TA01 | Transfer of patent application right | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20170511 Address after: 450016, Henan, Zhengzhou lofty ideal city, building 18, 3-1-2 Applicant after: Meng Sen Address before: Yuyao City, Zhejiang province 315400 Ningbo Yangming Street Road No. 42 South Applicant before: Zhou Dasheng |
|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170606 Termination date: 20171119 |