CN104877827A - Dry cleaning agent for clothes and preparation method thereof - Google Patents
Dry cleaning agent for clothes and preparation method thereof Download PDFInfo
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- CN104877827A CN104877827A CN201510259180.XA CN201510259180A CN104877827A CN 104877827 A CN104877827 A CN 104877827A CN 201510259180 A CN201510259180 A CN 201510259180A CN 104877827 A CN104877827 A CN 104877827A
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Abstract
The invention discloses a dry cleaning agent for clothes and a preparation method thereof. The dry cleaning agent for clothes comprises carnauba wax, diatomite, D-limonene, liquid carbon dioxide, chitosan, octyl phenol polyethenoxy ether, lactate, propylene glycol monomethyl ether, dioctyl sodium sulphosuccinate, sodium tripolyphosphate, sodium silicate and deionized water. The preparation method comprises the following steps: adding the carnauba wax, diatomite, D-limonene and chitosan into the liquid carbon dioxide, and stirring uniformly to obtain a mixed solution I; adding the octyl phenol polyethenoxy ether, lactate, propylene glycol monomethyl ether, dioctyl sodium sulphosuccinate, sodium tripolyphosphate and sodium silicate into the deionized water, and stirring uniformly to obtain a mixed solution II; and adding the mixed solution I into the mixed solution II while stirring, thereby obtaining the dry cleaning agent for clothes. The dry cleaning agent is convenient and quick to use, and has the advantages of favorable stain removal effect, no pollution and no toxicity.
Description
Technical field
The invention belongs to cosmetics of everyday use technical field, be specifically related to a kind of dry cleaning agent for clothes and preparation method thereof.
Background technology
Along with the development of society, improving constantly of people's living standard, the continuous quickening of rhythm of life, people require more and more higher to the dress of clothes and maintenance, continuous pursuit is convenient, healthy, quick, leisure, variation and personalized, and then drive the flourish of the industries such as garment dry cleaning, dyeing, renovation and perfuming beauty treatment.Dry-cleaning refers to and uses chemical solvents a kind of method of washing clothing, compensate for the defects such as the shrink of silk wool fabric in water washing process, fiber be hardening, thus obtains in recent decades and develop rapidly.
Up to now, dry cleaning composition mainly comprises following four classes: petroleum solvent dry cleaning composition, tetrafluoroethylene, Freon solvent dry cleaning composition and liquid carbon dioxide dry cleaning agent.In dry cleaning processes, oil soluble dirt, to the affinity interaction of oil stains dirt, can be dissolved out from fabric, be distributed in non-aqueous solvent under mechanical action by non-aqueous solvent relatively easily, and the solia particle be wrapped in wherein is come off.On the other hand, non-aqueous solvent is almost helpless to hydrophilic stains, in non-aqueous solvent, therefore add a small amount of water and appropriate tensio-active agent, reaches the object removing hydrophilic stains.Thus dry cleaning technology only uses petroleum hydrocarbon as the hand washing of solvent from initial, develop into the full-automatic mechanical cleaning adding tensio-active agent and auxiliary agent, cleaning performance is become better and better.
Although the dry cleaning composition such as zellon and petroleum solvent has certain decontamination, de-sludging, grease removal to clothing and goes the function of stain in prior art, but, more or less there is dyestuff by the phenomenon of dissolving in clothing, thus cause the lighter of clothing, wear after dry-cleaning.Especially when dry-clean frequency higher or dry-cleaning number of times be accumulated to a threshold quantity, the color of clothing can show as entirety and shoals or bleach, until wash old scrapping, have impact on the normal use of clothing.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art and provide a kind of dry cleaning agent for clothes and preparation method thereof, this dry cleaning composition is easy to use, quick, and clean effect is good, pollution-free, nontoxicity.
A kind of dry cleaning agent for clothes, comprises with parts by weight: CARNAUBA WAX 3 ~ 7 parts, 2 ~ 6 parts, diatomite, D-limonene 1 ~ 5 part, liquid carbon dioxide 3 ~ 8 parts, chitosan 4 ~ 9 parts, polyoxyethylene octylphenol ether 1 ~ 5 part, lactate 2 ~ 6 parts, propylene glycol monomethyl ether 3 ~ 7 parts, dioctyl sodium sulphosuccinate 1 ~ 6 part, tripoly phosphate sodium STPP 2 ~ 6 parts, water glass 3 ~ 7 parts and deionized water 5 ~ 10 parts.
As the further improvement of foregoing invention, described dry cleaning agent for clothes, comprises with parts by weight: CARNAUBA WAX 4 parts, 5 parts, diatomite, D-limonene 2 parts, liquid carbon dioxide 7 parts, chitosan 6 parts, polyoxyethylene octylphenol ether 4 parts, lactate 5 parts, propylene glycol monomethyl ether 5 parts, dioctyl sodium sulphosuccinate 3 parts, tripoly phosphate sodium STPP 4 parts, water glass 5 parts and deionized water 8 parts.
The preparation method of above-mentioned dry cleaning agent for clothes, comprises the following steps:
Step 1, is added in liquid carbon dioxide by CARNAUBA WAX, diatomite, D-limonene, chitosan, stirs, obtain mixed solution I;
Step 2, adds in deionized water by polyoxyethylene octylphenol ether, lactate, propylene glycol monomethyl ether, dioctyl sodium sulphosuccinate, tripoly phosphate sodium STPP, water glass, stirs, obtain mixed solution II;
Step 3, adds to step 1 gained mixed solution I in step 2 gained mixed solution II, and limit edged stirs, and to obtain final product.
As the further improvement of foregoing invention, in step 1, whipping process carries out under 40 ~ 50 DEG C of conditions, and churning time is 20 ~ 30min.
As the further improvement of foregoing invention, in step 3, whipping process carries out under 30 ~ 40 DEG C of conditions, and churning time is 20 ~ 30min.
Dry cleaning composition of the present invention is not only easy to use, quick, clean effect is good, pollution-free, nontoxicity, and, physical property on fabric, color fastness, fiber microstructure excellent on the clearing power of fabric almost without impact, be a kind of excellent environment-friendly dry lotion.
Embodiment
Embodiment 1
A kind of dry cleaning agent for clothes, comprises with parts by weight: CARNAUBA WAX 3 parts, 2 parts, diatomite, D-limonene 1 part, liquid carbon dioxide 3 parts, chitosan 4 parts, polyoxyethylene octylphenol ether 1 part, lactate 2 parts, propylene glycol monomethyl ether 3 parts, dioctyl sodium sulphosuccinate 1 part, tripoly phosphate sodium STPP 2 parts, water glass 3 parts and deionized water 5 parts.
The preparation method of above-mentioned dry cleaning agent for clothes, comprises the following steps:
Step 1, is added in liquid carbon dioxide by CARNAUBA WAX, diatomite, D-limonene, chitosan, under 40 DEG C of conditions, stirs 30min, obtain mixed solution I;
Step 2, adds in deionized water by polyoxyethylene octylphenol ether, lactate, propylene glycol monomethyl ether, dioctyl sodium sulphosuccinate, tripoly phosphate sodium STPP, water glass, under 30 DEG C of conditions, stirs 30min, obtain mixed solution II;
Step 3, adds to step 1 gained mixed solution I in step 2 gained mixed solution II, and limit edged stirs, and to obtain final product.
Embodiment 2
A kind of dry cleaning agent for clothes, comprises with parts by weight: CARNAUBA WAX 4 parts, 5 parts, diatomite, D-limonene 2 parts, liquid carbon dioxide 7 parts, chitosan 6 parts, polyoxyethylene octylphenol ether 4 parts, lactate 5 parts, propylene glycol monomethyl ether 5 parts, dioctyl sodium sulphosuccinate 3 parts, tripoly phosphate sodium STPP 4 parts, water glass 5 parts and deionized water 8 parts.
The preparation method of above-mentioned dry cleaning agent for clothes, comprises the following steps:
Step 1, is added in liquid carbon dioxide by CARNAUBA WAX, diatomite, D-limonene, chitosan, under 45 DEG C of conditions, stirs 25min, obtain mixed solution I;
Step 2, adds in deionized water by polyoxyethylene octylphenol ether, lactate, propylene glycol monomethyl ether, dioctyl sodium sulphosuccinate, tripoly phosphate sodium STPP, water glass, under 35 DEG C of conditions, stirs 25min, obtain mixed solution II;
Step 3, adds to step 1 gained mixed solution I in step 2 gained mixed solution II, and limit edged stirs, and to obtain final product.
Embodiment 3
A kind of dry cleaning agent for clothes, comprises with parts by weight: CARNAUBA WAX 7 parts, 6 parts, diatomite, D-limonene 5 parts, liquid carbon dioxide 8 parts, chitosan 9 parts, polyoxyethylene octylphenol ether 5 parts, lactate 6 parts, propylene glycol monomethyl ether 7 parts, dioctyl sodium sulphosuccinate 6 parts, tripoly phosphate sodium STPP 6 parts, water glass 7 parts and deionized water 10 parts.
The preparation method of above-mentioned dry cleaning agent for clothes, comprises the following steps:
Step 1, is added in liquid carbon dioxide by CARNAUBA WAX, diatomite, D-limonene, chitosan, under 50 DEG C of conditions, stirs 20min, obtain mixed solution I;
Step 2, adds in deionized water by polyoxyethylene octylphenol ether, lactate, propylene glycol monomethyl ether, dioctyl sodium sulphosuccinate, tripoly phosphate sodium STPP, water glass, under 40 DEG C of conditions, stirs 20min, obtain mixed solution II;
Step 3, adds to step 1 gained mixed solution I in step 2 gained mixed solution II, and limit edged stirs, and to obtain final product.
Embodiment 1 to 3 gained dry cleaning composition and commercially available prod (zellon) are made a service test,
(1) shrink simultaneous test
The wool shrink sample cloth 300*300mm size dimension adopting GB MLBT4288-2008 to require is as test sample cloth, be immersed in 30min in the beaker filling solvent, described solvent is uninterruptedly stir with glass stick, dries, measure distortion size after complete at 60 DEG C of temperature.
(2) detergency test
The cotton getting GB MLBT4288-2008 requirement, as the substrate of spot cloth, in its surface-coated soy sauce spot, for test after its drying, is cut into the spot cloth of 120*120mm size.
Make the keg of 2 liter capacity sizes, keg is fixed on the equipment of similar cylinder rotation, simulation drum wash mode carries out detergency ability test, get the soiled cotton of 1 piece of 120*120mm size, dry cleaning solvent 1kg, normal temperature washs, washing time is 30min, after take out spot cloth, naturally dry, test spot cloth whiteness.
(3) anti-colour contamination test
Make the keg of 2 liter capacity sizes, be fixed on by keg on the equipment of similar cylinder rotation, simulation drum wash mode carries out colourimetric number test, respectively get the red calico of 4 pieces of 120*120mm sizes, dry cleaning solvent 1kg, normal temperature washs, washing time is 30min, after take out cotton, naturally dry.
Before common silk cotton cloth and common white cotton read and wash, value is as standard value, after simulation dry cleaning processes terminates, reads the colourimetric number of red cloth and calico respectively.Colour fixation is by red cloth after measuring washing and do not wash the color distinction of red cloth, and namely Δ E represents, aberration is larger, illustrates that painting cloth fades more serious, the fixation of dry cleaning composition and the weak effect of anti-colour contamination, on the contrary then colour fixation.Dye transfer inhibition effect is then the value of chromatism with calico after washing, and Δ E value is lower shows that the dyestuff transferred on calico is less, and dye transfer inhibition effect is more obvious
Result is as follows:
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Zellon | Water | |
| Washing shrinkage (%) | 0.93 | 0.85 | 0.98 | 2.3 | 4.5 |
| Whiteness before cleaning | 28.5 | 28.5 | 28.5 | 28.5 | 28.5 |
| Whiteness after cleaning | 76.5 | 78.2 | 78.5 | 31.2 | 28.5 |
| Red cloth Δ E | 0.35 | 0.40 | 0.45 | 1.60 | 0.20 |
| Calico Δ E | 0.20 | 0.25 | 0.24 | 0.80 | 0.10 |
From above result, dry cleaning composition of the present invention is obviously better than the dry cleaning composition of prior art in dry cleaning processes to the anti-shrinkage of clothing, clearing power and effect of color protection.
Claims (5)
1. a dry cleaning agent for clothes, is characterized in that: comprise with parts by weight: CARNAUBA WAX 3 ~ 7 parts, 2 ~ 6 parts, diatomite, D-limonene 1 ~ 5 part, liquid carbon dioxide 3 ~ 8 parts, chitosan 4 ~ 9 parts, polyoxyethylene octylphenol ether 1 ~ 5 part, lactate 2 ~ 6 parts, propylene glycol monomethyl ether 3 ~ 7 parts, dioctyl sodium sulphosuccinate 1 ~ 6 part, tripoly phosphate sodium STPP 2 ~ 6 parts, water glass 3 ~ 7 parts and deionized water 5 ~ 10 parts.
2. dry cleaning agent for clothes according to claim 1, is characterized in that: comprise with parts by weight: CARNAUBA WAX 4 parts, 5 parts, diatomite, D-limonene 2 parts, liquid carbon dioxide 7 parts, chitosan 6 parts, polyoxyethylene octylphenol ether 4 parts, lactate 5 parts, propylene glycol monomethyl ether 5 parts, dioctyl sodium sulphosuccinate 3 parts, tripoly phosphate sodium STPP 4 parts, water glass 5 parts and deionized water 8 parts.
3. the preparation method of the dry cleaning agent for clothes described in claim 1 or 2, is characterized in that: comprise the following steps:
Step 1, is added in liquid carbon dioxide by CARNAUBA WAX, diatomite, D-limonene, chitosan, stirs, obtain mixed solution I;
Step 2, adds in deionized water by polyoxyethylene octylphenol ether, lactate, propylene glycol monomethyl ether, dioctyl sodium sulphosuccinate, tripoly phosphate sodium STPP, water glass, stirs, obtain mixed solution II;
Step 3, adds to step 1 gained mixed solution I in step 2 gained mixed solution II, and limit edged stirs, and to obtain final product.
4. the preparation method of dry cleaning agent for clothes according to claim 3, is characterized in that: in step 1, whipping process carries out under 40 ~ 50 DEG C of conditions, and churning time is 20 ~ 30min.
5. the preparation method of dry cleaning agent for clothes according to claim 3, is characterized in that: in step 3, whipping process carries out under 30 ~ 40 DEG C of conditions, and churning time is 20 ~ 30min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510259180.XA CN104877827A (en) | 2015-05-20 | 2015-05-20 | Dry cleaning agent for clothes and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510259180.XA CN104877827A (en) | 2015-05-20 | 2015-05-20 | Dry cleaning agent for clothes and preparation method thereof |
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| CN104877827A true CN104877827A (en) | 2015-09-02 |
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| CN201510259180.XA Pending CN104877827A (en) | 2015-05-20 | 2015-05-20 | Dry cleaning agent for clothes and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105647709A (en) * | 2016-02-01 | 2016-06-08 | 东莞品派实业投资有限公司 | Dry cleaning agent for removing yellow spots on clothes and preparation method thereof |
| CN108300604A (en) * | 2018-02-10 | 2018-07-20 | 蒋春霞 | A kind of preparation method of dry cleaning agent |
Citations (4)
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| CN1095413A (en) * | 1993-05-10 | 1994-11-23 | 崔岚 | Multipurpose spraying agent for removing greasy dirt |
| US5858022A (en) * | 1997-08-27 | 1999-01-12 | Micell Technologies, Inc. | Dry cleaning methods and compositions |
| US6461384B1 (en) * | 1999-06-17 | 2002-10-08 | Bausch & Lomb Incorporated | Intraocular lenses |
| CN102618403A (en) * | 2012-03-13 | 2012-08-01 | 宋子奎 | Color-increasing dry cleaning agent composition and preparation method thereof |
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2015
- 2015-05-20 CN CN201510259180.XA patent/CN104877827A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1095413A (en) * | 1993-05-10 | 1994-11-23 | 崔岚 | Multipurpose spraying agent for removing greasy dirt |
| US5858022A (en) * | 1997-08-27 | 1999-01-12 | Micell Technologies, Inc. | Dry cleaning methods and compositions |
| US6461384B1 (en) * | 1999-06-17 | 2002-10-08 | Bausch & Lomb Incorporated | Intraocular lenses |
| CN102618403A (en) * | 2012-03-13 | 2012-08-01 | 宋子奎 | Color-increasing dry cleaning agent composition and preparation method thereof |
Non-Patent Citations (2)
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| 彭明丽等: "<<小化工产品配方与工艺>>", 31 January 2010, 化学工业出版社 * |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105647709A (en) * | 2016-02-01 | 2016-06-08 | 东莞品派实业投资有限公司 | Dry cleaning agent for removing yellow spots on clothes and preparation method thereof |
| CN108300604A (en) * | 2018-02-10 | 2018-07-20 | 蒋春霞 | A kind of preparation method of dry cleaning agent |
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Application publication date: 20150902 |
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