CN111471534A - Quick-drying efficient down jacket spray cleaning agent without leaving marks and preparation method thereof - Google Patents
Quick-drying efficient down jacket spray cleaning agent without leaving marks and preparation method thereof Download PDFInfo
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- CN111471534A CN111471534A CN202010363608.6A CN202010363608A CN111471534A CN 111471534 A CN111471534 A CN 111471534A CN 202010363608 A CN202010363608 A CN 202010363608A CN 111471534 A CN111471534 A CN 111471534A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
- C11D1/831—Mixtures of non-ionic with anionic compounds of sulfonates with ethers of polyoxyalkylenes without phosphates
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2006—Monohydric alcohols
- C11D3/201—Monohydric alcohols linear
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2041—Dihydric alcohols
- C11D3/2044—Dihydric alcohols linear
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2041—Dihydric alcohols
- C11D3/2048—Dihydric alcohols branched
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/33—Amino carboxylic acids
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/34—Organic compounds containing sulfur
- C11D3/349—Organic compounds containing sulfur additionally containing nitrogen atoms, e.g. nitro, nitroso, amino, imino, nitrilo, nitrile groups containing compounds or their derivatives or thio urea
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38645—Preparations containing enzymes, e.g. protease or amylase containing cellulase
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/43—Solvents
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/28—Sulfonation products derived from fatty acids or their derivatives, e.g. esters, amides
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/29—Sulfates of polyoxyalkylene ethers
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
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Abstract
The invention relates to a quick-drying efficient down jacket spray cleaning agent without leaving marks and a preparation method thereof. The spray cleaning agent contains anionic surfactant, nonionic surfactant, biological enzyme, solvent, chelating agent, benzisothiazolinone, aromatherapy essential oil and deionized water. The spray cleaning agent has the advantages that local treatment is convenient for down jackets, and the spray cleaning agent has the characteristics of quick drying, no trace after use, no need of water, high-efficiency cleaning and the like by means of spraying, so that the down jackets can be cleaned without being wholly washed, and the problem of convenient and quick cleaning of people at any time and any place can be solved.
Description
Technical Field
The invention relates to the field of detergents, in particular to a quick-drying efficient down jacket spray cleaning agent without leaving marks and a preparation method thereof.
Background
With the improvement of the living quality and the consumption level of people, wearing down jackets in the north becomes a necessary warm-keeping garment in winter. However, down jackets are warm and annoying to people. For example, the gloves are stained carelessly or stained once or two days, especially the cuff part, the whole piece is troublesome to wash, uncomfortable to watch after not washing, and difficult to dry especially in winter due to cold weather. Meanwhile, due to the particularity of the down jacket, the down jacket is washed frequently or improperly, so that the fabric is faded, and the down hair plate, the down feather are hardened and the heat retention property is poor. More importantly, 90% of the down coats are marked to be washed by hands, and a washing solution or a washing powder solution special for the down coats is used. The warm-keeping material of the down jacket mainly uses feather, and is different from other warm-keeping clothes mainly made of materials such as cotton, silk fabrics or chemical fibers, the warm-keeping property of the down jacket can be influenced by liquid medicine for dry cleaning, cloth can be aged, and fillers of the down jacket are uneven in thickness and easy to deform due to machine washing and spin-drying, so that the attractiveness and the warm-keeping property are influenced. This causes problems of inconvenient and difficult washing, such as machine washing, dry washing, and hand washing.
The patent application with the publication number CN102051276B and the invention name 'Down coat cleaning agent' discloses a cleaning agent for down coats, which comprises the components of anionic surfactant, nonionic surfactant, DP-3000, tea saponin, soya ethyl morpholine sulfate, colloid HSi0, essence, sodium citrate and deionized water. The cleaning agent of the technical scheme can integrate sterilization, deodorization and conditioning, and has the characteristics of good stability, both cold water and hot water, and no harm to hands. The patent application with the invention name of CN108085190A discloses a down jacket cleaning agent with an anti-fouling function. The technical scheme comprises a surfactant, an anti-fouling polymer and water. The technical scheme has the functions of decontamination and antibiosis, and has the characteristics of good filling power, good water solubility and good environmental protection property of the down feather. The technical scheme disclosed above is not ideal in effect for local cleaning and rapid drying of the down jacket.
Therefore, the down jacket user has a demand for removing the dirt without integral washing, and people need a detergent which can be used for efficiently cleaning the down jacket at any time, so that the problem of convenient and rapid cleaning of the down jacket at any time and any place is solved. In the prior art, a cleaning agent and a treatment method for local cleaning treatment by means of spraying or the like are lacked.
Disclosure of Invention
In order to overcome the defects in the prior art and improve the technology, the invention provides a quick-drying efficient down jacket spray cleaning agent without leaving marks and a preparation method thereof.
In order to realize the purpose of the invention, the invention provides the following technical scheme:
the technical scheme disclosed by the invention particularly relates to a quick-drying efficient down jacket spray cleaning agent without leaving marks and a preparation method thereof. The main raw materials of the quick-drying, trace-free and efficient cleaning spray cleaning agent for down jackets comprise: anionic surfactant, nonionic surfactant, biological enzyme, solvent, chelating agent, benzisothiazolinone, aromatherapy essential oil, and deionized water.
The invention is realized by the following technical scheme:
the invention discloses a quick-drying trace-free efficient down jacket spray cleaning agent and a preparation method thereof, wherein the raw materials of the spray cleaning agent for washing comprise an anionic surfactant, a nonionic surfactant, a biological enzyme, a solvent, a chelating agent, benzisothiazolinone, aromatherapy essential oil and deionized water, and in the technical scheme disclosed by the invention, the spray cleaning agent for the down jacket comprises the following raw materials in parts by weight:
in the quick-drying trace-free efficient down jacket spray cleaning agent disclosed by the technical scheme of the invention, the anionic surfactant is selected from one, two or more of fatty alcohol-polyoxyethylene ether sodium sulfate, fatty acid methyl ester ethoxylate sulfonate, fatty acid methyl ester sodium sulfonate and sodium lauroyl glutamate;
wherein, the carbon atom number of the fatty alcohol-polyoxyethylene ether sodium sulfate is preferably 10-18, and more preferably 12-14; the number of carbon atoms of the "fatty acid" group in the fatty acid methyl ester ethoxylate sulfonate or the fatty acid methyl ester sodium sulfonate is preferably 6 to 18, and more preferably 8 to 14.
The nonionic surfactant is one, two or more of fatty alcohol polyoxyethylene (3) ether, fatty alcohol polyoxyethylene (7) ether, fatty alcohol polyoxyethylene (9) ether, isomeric decyl alcohol oxidation nonionic surfactant and isomeric tridecyl alcohol oxidation nonionic surfactant; further, the isomeric decyl alcohol oxidizing nonionic surfactant is an isomeric decyl alcohol oxidizing nonionic surfactant (HIC 2109); the isomeric tridecanol alkoxylated nonionic surfactant is an isomeric tridecanol alkoxylated nonionic surfactant (HIF 4100);
among these, the "aliphatic alcohol" group preferably has 10 to 18 carbon atoms, and more preferably has 12 to 14 carbon atoms.
The biological enzyme is cellulase, preferably Novoxil cellulase (4500L);
the solvent is selected from one or more of tripropylene glycol methyl ether, 2-methyl-2, 4-pentanediol, diethylene glycol butyl ether, ethanol or propylene glycol;
the chelating agent is one or two of ethylenediaminetetraacetic acid tetrasodium salt, sodium citrate and glutamic diacetic acid tetrasodium salt.
In the technical scheme of the invention, the preparation method of the quick-drying efficient down jacket spray cleaning agent without leaving marks sequentially comprises the following steps:
the preparation method comprises the following steps:
A. according to the weight parts of the raw materials in the formula, firstly, 49.55 percent of the total weight is measured～Adding 92.4 percent of deionized water into the material kettle, and thenSequentially adding the anionic surfactant, the nonionic surfactant and the solvent according to the mixture ratio to obtain a mixed solution A;
B. adding the benzisothiazolinone, the chelating agent and the essence oil into the mixed solution A according to the weight ratio of the formula, and uniformly stirring to obtain a mixed solution B;
C. adding biological enzyme into the mixed solution B according to the weight ratio of the formula, and uniformly stirring to obtain a mixed solution C;
D. and filtering the mixed solution C to obtain the quick-drying efficient cleaning down feather spray cleaning agent without leaving marks.
Further, the quick-drying efficient spray cleaning agent without leaving traces for down jackets comprises the following preferable technical scheme:
wherein the spray cleaning agent comprises the following raw materials in parts by weight:
the anionic surfactant is a mixture consisting of fatty alcohol-polyoxyethylene ether sodium sulfate and fatty acid methyl ester ethoxylate sulfonate, and the weight part ratio of the fatty alcohol-polyoxyethylene ether sodium sulfate to the fatty acid methyl ester ethoxylate sulfonate is 6: 4; wherein, the carbon atom number of the fatty alcohol-polyoxyethylene ether sodium sulfate is preferably 10-18, and more preferably 12-14; the number of carbon atoms of the "fatty acid" group in the fatty acid methyl ester ethoxylate sulfonate is preferably 6 to 18, and more preferably 8 to 14.
The nonionic surfactant is a mixture consisting of fatty alcohol polyoxyethylene (9) ether and isomeric tridecanol alkoxy nonionic surfactant, and the weight part ratio of the fatty alcohol polyoxyethylene (9) ether to the isomeric tridecanol alkoxy is 2: 5; wherein the number of carbon atoms of the "aliphatic alcohol" group is preferably 10 to 18, and more preferably 12 to 14; further, the isomeric tridecanol alkoxylated nonionic surfactant is an isomeric tridecanol alkoxylated nonionic surfactant (HIF 4100).
The solvent is a mixture of diethylene glycol butyl ether, ethanol and propylene glycol, and the weight part ratio of the diethylene glycol butyl ether to the ethanol to the propylene glycol is 5:2: 3;
the chelating agent is tetrasodium glutamate diacetate;
the biological enzyme is cellulase (4500L).
Furthermore, the quick-drying efficient spray cleaning agent without leaving traces of the invention is the down coat spray cleaning agent, and the more preferable technical scheme is as follows:
wherein the spray cleaning agent comprises the following raw materials in parts by weight:
wherein the anionic surfactant is fatty alcohol-polyoxyethylene ether sodium sulfate;
the nonionic surfactant is a mixture composed of fatty alcohol polyoxyethylene (9) ether, fatty alcohol polyoxyethylene (7) ether and isomeric tridecanol alkoxy nonionic surfactant, and the weight part ratio of the fatty alcohol polyoxyethylene (9) ether, the fatty alcohol polyoxyethylene (7) ether and the isomeric tridecanol alkoxy nonionic surfactant is 2: 3: 5; wherein the number of carbon atoms of the "aliphatic alcohol" group is preferably 10 to 18, and more preferably 12 to 14; further, the isomeric tridecanol alkoxylated nonionic surfactant is an isomeric tridecanol alkoxylated nonionic surfactant (HIF 4100).
The solvent is 2-methyl-2, 4-pentanediol, ethanol and propylene glycol, and the weight part ratio of the 2-methyl-2, 4-pentanediol, the ethanol and the propylene glycol is 5:2: 3;
the chelating agent is tetrasodium glutamate diacetate and sodium citrate, and the weight part ratio of the tetrasodium glutamate diacetate to the sodium citrate is 5:5
The biological enzyme is cellulase.
Furthermore, the quick-drying efficient spray cleaning agent without leaving traces of the invention is the down coat spray cleaning agent, and the more preferable technical scheme is as follows:
wherein the spray cleaning agent comprises the following raw materials in parts by weight:
the anionic surfactant is a mixture consisting of fatty acid methyl ester ethoxylate sulfonate and fatty acid methyl ester sodium sulfonate, and the weight part ratio of the fatty acid methyl ester ethoxylate sulfonate to the fatty acid methyl ester sodium sulfonate is 7: 3; the number of carbon atoms of the "fatty acid" group is preferably 6 to 18, and more preferably 8 to 14.
The nonionic surfactant is a mixture consisting of fatty alcohol polyoxyethylene (7) ether and isomeric tridecanol alkoxylated nonionic surfactant, and the weight part ratio of the fatty alcohol polyoxyethylene (7) ether to the isomeric tridecanol alkoxylated nonionic surfactant is 5: 5; wherein the number of carbon atoms of the "aliphatic alcohol" group is preferably 10 to 18, and more preferably 12 to 14; further, the isomeric tridecanol alkoxylated nonionic surfactant is an isomeric tridecanol alkoxylated nonionic surfactant (HIF 4100).
The solvent is a mixture consisting of ethanol and propylene glycol, and the weight part ratio of the ethanol to the propylene glycol is 5: 5;
the chelating agent is tetrasodium glutamate diacetate;
the biological enzyme is cellulase (4500L).
Furthermore, the quick-drying efficient spray cleaning agent without leaving traces of the invention is the down coat spray cleaning agent, and the more preferable technical scheme is as follows:
wherein the spray cleaning agent comprises the following raw materials in parts by weight:
wherein the anionic surfactant is (C12-C14) sodium fatty acid methyl ester ethoxylate sulfonate;
the nonionic surfactant is a mixture consisting of (C12-C14) fatty alcohol polyoxyethylene (7) ether, isomeric decyl alcohol oxidation nonionic surfactant (HIC 2109) and isomeric tridecanol oxidation nonionic surfactant (HIF4100), and the weight part ratio of the fatty alcohol polyoxyethylene (7) ether, the isomeric decyl alcohol oxidation nonionic surfactant (HIC 2109) and the isomeric tridecanol oxidation nonionic surfactant (HIF4100) is 4:3: 3; among these, the "aliphatic alcohol" group preferably has 10 to 18 carbon atoms, and more preferably has 12 to 14 carbon atoms.
The solvent is a mixture consisting of ethanol and propylene glycol, and the weight part ratio of the ethanol to the propylene glycol is 5: 5;
the chelating agent is tetrasodium glutamate diacetate;
the biological enzyme is cellulase.
Compared with the prior art, the invention has the following advantages:
the spray cleaning agent has the characteristics of quick drying, no trace after use, no need of water, high-efficiency cleaning and the like, so that the down jacket can remove dirt without integral washing, and the problems of convenience and rapidness in cleaning at any time and any place of people are solved.
In order to make the purpose and technical solution of the embodiments of the present invention clearer, the technical solution of the embodiments of the present invention will be clearly and completely described below with reference to the implementation examples of the embodiments of the present invention. It is to be understood that the embodiments described are only a few embodiments of the present invention, and not all embodiments. All other embodiments, which can be made by a person skilled in the art without inventive effort based on the described embodiments of the invention, fall within the scope of protection of the invention.
Detailed Description
The following further describes a specific embodiment of the present invention with specific examples, which are intended to describe the technical solution in detail, but not to limit the technical solution.
The preparation method comprises the following steps:
A. according to the weight ratio of the formula, 49.55-92.4% of the total weight of the deionized water is added into a material melting kettle, and then the anionic surfactant, the nonionic surfactant and the solvent are sequentially added according to the ratio to obtain a mixed solution A;
B. adding the benzisothiazolinone, the chelating agent and the essence oil into the mixed solution A according to the weight ratio of the formula, and uniformly stirring to obtain a mixed solution B;
C. adding biological enzyme into the mixed solution B according to the weight ratio of the formula, and uniformly stirring to obtain a mixed solution C;
D. and filtering the mixed solution C to obtain the quick-drying efficient clean down feather cleaning agent without leaving marks.
The weight unit used in the embodiment is gram, and can also be kilogram; the essence essential oil in the embodiment is food-grade, and other raw materials are all industrial-grade; the respective raw materials described in this example were mass-produced.
Firstly, the use mode of the product is as follows: the down jacket spray cleaning agent is directly sprayed on the surface of the down jacket with stains, and then the down jacket is wiped by using a clean towel or a paper towel, and the operation is repeated for one time or two times.
Second, decontamination test method
1. Instrument and apparatus
A vertical decontamination machine: the rotating speed range is 30 r/min-200 r/min, and the temperature error is +/-0.5 ℃.
A whiteness meter: meets the requirements of JB/T9327 and JJG 512.
Large enamel plate: 46cmX36 cm.
A rinsing device: the structure is the same as that of a commercial vegetable dehydrator.
2. The method comprises the following steps: measured according to the test conditions for detergency (according to QB/T1224, 6.7.2 collar cuff pre-wash);
A. pretreating a dirty cloth test piece, namely taking 3 circular dirty cloth test pieces of JB-01, JB-02 and JB-03 with the diameter of 4cm, respectively stacking the circular dirty cloth test pieces in a culture dish (one dirty cloth is a group), weighing 2.0g of a sample in a beaker, adding 2m L of hard water with the concentration of 250mg/kg for dilution, uniformly dripping the uniformly mixed sample on each dirty cloth by using a dropper according to the sequence of the JB-01, JB-02 and JB-03 dirty cloth stacked test pieces, slightly turning the dirty cloth by using tweezers to completely moisten the dirty cloth, controlling the dripping time within 1min, placing the soaked dirty cloth test piece for 5min, respectively taking 200m L of 250mg/kg of hard water heated to 30 ℃, transferring the samples remained in the dropper, the beaker and the culture dish and the soaked dirty cloth test piece to an experimental bathtub, and adding 800m L of hard water with the concentration of 250mg/kg and 30 ℃.
B. And synchronously treating the stained cloth test piece by adopting the standard laundry detergent for comparison and measurement.
C. The pretreated soiled cloth was then tested for its cleaning performance in accordance with the method specified in GB/T13174.
Example 1
In this example, according to the above-described preparation method of the quick-drying efficient down jacket spray cleaning agent without leaving traces according to the technical scheme of the present invention, the down jacket spray cleaning agent of this example is prepared according to the following raw material mixture ratio.
In this embodiment, the weight parts of the raw materials of the quick-drying traceless efficient cleaning down feather cleaning agent are as follows:
anionic surfactant: sodium (C12-C14) fatty alcohol polyoxyethylene (3) ether sulfate
Nonionic surfactant: the weight part ratio of (C12-C14) fatty alcohol polyoxyethylene (9) ether, (C12-C14) fatty alcohol polyoxyethylene (7) ether and isomeric tridecanol alkoxy nonionic surfactant (HIF4100) is 2: 3: 5
Solvent: the weight part ratio of the 2-methyl-2, 4-pentanediol to the ethanol to the propylene glycol is 5:2:3
Chelating agent: the weight part ratio of the tetrasodium glutamate diacetate to the sodium citrate is 5:5
QB/T1224 is standard "liquid detergents for clothing", and is suitable for liquid detergent products for cleaning various fabrics, which are prepared from various surfactants and auxiliaries.
Detergency of the spray cleaners of this example, tested under the test conditions for detergency (according to QB/T1224, collar cuff pre-wash) and wash results are given in the following table:
the decontamination method comprises the following steps: the above-mentioned stain removal method is used to pretreat the stained cloth test piece, and then the pretreated stained cloth is tested for its washing performance according to the method specified in GB/T13174.
Marking liquid: the numerical representation of the detergency of the laundry detergent with a specific formula prepared from raw materials with certain specifications is usually taken as a reference and the washing performances of other detergents are compared and detected;
decontamination value of standard solution: the digital representation of the detergency of the standard liquid is expressed by the whiteness difference of the test piece;
and (3) detergency step: following the stain removal test method described above;
sample values: the ratio of the decontamination value of the sample to the decontamination value of the standard solution;
numerical measurement method: measuring with a whiteness meter;
JB-01: carbon black greasy dirt cloth;
JB-02: protein-contaminated cloth;
JB-03: sebum-stained cloth;
the down coat spray cleaning agent of the invention (40 ℃, 30 days): the stability of the down jacket spray cleaning agent sample is 30 days, and the conditions are as follows: the temperature of the oven is kept constant at 40 ℃;
control sample: youjieshi down jacket cleaning agent.
The experimental results are as follows: according to the experimental result, the cleaning effect of the down coat spray cleaning agent is obviously better than that of a control sample; after stability experiments, the product effect is better than that of a control sample, and the aim of high-efficiency decontamination is fulfilled.
Example 2
In this example, according to the preparation method of the spray cleaning agent for down jackets, which is described in example 1 and is a quick-drying efficient spray cleaning agent without leaving traces, the spray cleaning agent for down jackets of this example is prepared according to the following raw material proportions.
In this embodiment, the weight parts of the raw materials of the quick-drying traceless efficient cleaning down feather cleaning agent are as follows:
anionic surfactant: the weight part ratio of (C12-C14) sodium fatty acid methyl ester ethoxylate sulfonate to (C12-C14) sodium fatty acid methyl ester sulfonate is 7:3
Nonionic surfactant: (C12-C14) the weight portion ratio of fatty alcohol polyoxyethylene (7) ether to isomeric tridecanol alkoxy (HIF4100) is 5:5
Solvent: the weight portion ratio of the ethanol to the propylene glycol is 5:5
Chelating agent: glutamic acid diacetic acid tetrasodium salt
Detergency of spray cleaners of this example the following table shows the results of the washing according to the test conditions of detergency (according to QB/T1224, collar cuff pre-wash):
the experimental results are as follows: according to the experimental result, the cleaning effect of the down coat spray cleaning agent is obviously better than that of a control sample; after stability experiments, the product effect is better than that of a control sample, and the aim of high-efficiency decontamination is fulfilled.
Example 3
In this example, according to the preparation method of the spray cleaning agent for down jackets, which is described in example 1 and is a quick-drying efficient spray cleaning agent without leaving traces, the spray cleaning agent for down jackets of this example is prepared according to the following raw material proportions.
In this embodiment, the weight parts of the raw materials of the quick-drying traceless efficient cleaning down feather cleaning agent are as follows:
anionic surfactant: (C12-C14) sodium fatty acid methyl ester ethoxylate sulfonate
Nonionic surfactant: (C12-C14) fatty alcohol polyoxyethylene (7) ether, isomeric decyl alcohol oxidation
Nonionic surfactant (HIC 2109) and isomeric tridecanol alkoxylated nonionic surfactant
(HIF4100) weight ratio of 4:3
Solvent: the weight portion ratio of the ethanol to the propylene glycol is 5:5
Chelating agent: glutamic acid diacetic acid tetrasodium salt
Detergency of spray cleaners of this example the following table shows the results of the washing according to the test conditions of detergency (according to QB/T1224, collar cuff pre-wash):
the experimental results are as follows: according to the experimental result, the cleaning effect of the down coat spray cleaning agent is obviously better than that of a control sample; after stability experiments, the product effect is better than that of a control sample, and the aim of high-efficiency decontamination is fulfilled.
The present invention is further described in the embodiments above, which are intended to describe the technical solutions in detail, but not to limit the technical solutions. The above-mentioned embodiments are merely illustrative of the preferred embodiments of the present invention, and do not limit the technical concept and the protection scope of the present invention, and various modifications and improvements made to the technical scheme by those skilled in the art without departing from the design concept of the present invention shall fall within the protection scope of the present invention.
Claims (10)
1. A quick-drying efficient down jacket spray cleaning agent without leaving marks is characterized in that the spray comprises an anionic surfactant, a nonionic surfactant, a biological enzyme, a solvent, a chelating agent, benzisothiazolinone, aromatherapy essential oil and deionized water; the down jacket spray comprises the following components:
the above component values are all calculated by weight parts.
2. The quick-drying trace-free efficient spray cleaning agent for down jackets as claimed in claim 1, wherein the anionic surfactant is selected from one, two or more of sodium fatty alcohol polyoxyethylene ether sulfate, fatty acid methyl ester ethoxylate sulfonate, sodium fatty acid methyl ester sulfonate and sodium lauroyl glutamate; the nonionic surfactant is one, two or more of fatty alcohol polyoxyethylene (3) ether, fatty alcohol polyoxyethylene (7) ether, fatty alcohol polyoxyethylene (9) ether, isomeric decyl alcohol oxidation nonionic surfactant and isomeric tridecyl alcohol oxidation nonionic surfactant; preferably, the number of carbon atoms of the "fatty alcohol" group is 10 to 18, more preferably 12 to 14; the number of carbon atoms of the "fatty acid" group is preferably 6 to 18, and more preferably 8 to 14.
3. The quick-drying, non-marking and high-efficiency down jacket spray cleaning agent according to claim 1, characterized in that the biological enzyme is cellulase, preferably Novoxil cellulase; the solvent is selected from one or more of tripropylene glycol methyl ether, 2-methyl-2, 4-pentanediol, diethylene glycol butyl ether, ethanol or propylene glycol.
4. The quick-drying traceless high-efficiency down jacket spray cleaning agent according to claim 1, wherein the chelating agent is one or two of ethylenediaminetetraacetic acid tetrasodium salt, sodium citrate and glutamic diacetic acid tetrasodium salt.
5. The quick-drying efficient down jacket spray cleaning agent without leaving marks according to any one of claims 1 to 4, which is characterized by comprising the following raw materials in parts by weight:
the anionic surfactant is a mixture consisting of fatty alcohol-polyoxyethylene ether sodium sulfate and fatty acid methyl ester ethoxylate sulfonate, and the weight part ratio of the fatty alcohol-polyoxyethylene ether sodium sulfate to the fatty acid methyl ester ethoxylate sulfonate is 6: 4;
the nonionic surfactant is a mixture consisting of fatty alcohol polyoxyethylene (9) ether and isomeric tridecanol alkoxylated nonionic surfactant, and the weight part ratio of the fatty alcohol polyoxyethylene (9) ether to the isomeric tridecanol alkoxylated surfactant is 2: 5;
the solvent is a mixture consisting of diethylene glycol butyl ether, ethanol and propylene glycol, and the weight part ratio of the diethylene glycol butyl ether to the ethanol to the propylene glycol is 5:2: 3;
the chelating agent is tetrasodium glutamate diacetate;
the biological enzyme is cellulase.
6. The quick-drying efficient down jacket spray cleaning agent without leaving marks according to any one of claims 1 to 4, which is characterized by comprising the following raw materials in parts by weight:
the anionic surfactant is fatty alcohol-polyoxyethylene ether sodium sulfate;
the nonionic surfactant is a mixture consisting of fatty alcohol polyoxyethylene (9) ether, fatty alcohol polyoxyethylene (7) ether and isomeric tridecanol alkoxy nonionic surfactant, wherein the alkoxy part ratio of the fatty alcohol polyoxyethylene (9) ether, the fatty alcohol polyoxyethylene (7) ether and the isomeric tridecanol is 2: 3: 5;
the solvent is 2-methyl-2, 4-pentanediol, ethanol and propylene glycol, and the weight part ratio of the 2-methyl-2, 4-pentanediol, the ethanol and the propylene glycol is 5:2: 3;
the chelating agent is tetrasodium glutamate diacetate and sodium citrate, and the weight part ratio of the tetrasodium glutamate diacetate to the sodium citrate is 5:5
The biological enzyme is cellulase.
7. The quick-drying efficient down jacket spray cleaning agent without leaving marks according to any one of claims 1 to 4, which is characterized by comprising the following raw materials in parts by weight:
the anionic surfactant is a mixture consisting of fatty acid methyl ester ethoxylate sulfonate and fatty acid methyl ester sodium sulfonate, and the weight part ratio of the fatty acid methyl ester ethoxylate sulfonate to the fatty acid methyl ester sodium sulfonate is 7: 3;
the nonionic surfactant is a mixture consisting of fatty alcohol polyoxyethylene (7) ether and isomeric tridecanol alkoxylated nonionic surfactant, and the weight part ratio of the fatty alcohol polyoxyethylene (7) ether to the isomeric tridecanol alkoxylated nonionic surfactant (HIF4100) is 5: 5;
the solvent is a mixture consisting of ethanol and propylene glycol, and the weight part ratio of the ethanol to the propylene glycol is 5: 5;
the chelating agent is tetrasodium glutamate diacetate
The biological enzyme is cellulase.
8. The quick-drying efficient down jacket spray cleaning agent without leaving marks according to any one of claims 1 to 4, which is characterized by comprising the following raw materials in parts by weight:
the anionic surfactant is fatty acid methyl ester ethoxylate sulfonate;
the nonionic surfactant is a mixture consisting of fatty alcohol polyoxyethylene (7) ether, isomeric decyl alcohol oxidation nonionic surfactant and isomeric tridecyl alcohol oxidation nonionic surfactant, and the weight part ratio of the fatty alcohol polyoxyethylene (7) ether, the isomeric decyl alcohol oxidation nonionic surfactant and the isomeric tridecyl alcohol oxidation nonionic surfactant is 4:3: 3;
the solvent is ethanol and propylene glycol, and the weight part ratio of the ethanol to the propylene glycol is 5: 5;
the chelating agent is tetrasodium glutamate diacetate;
the biological enzyme is cellulase.
9. The quick-drying efficient down jacket spray cleaning agent without leaving marks according to any one of claims 1 to 4, which is characterized by comprising the following raw materials in parts by weight:
the anionic surfactant is (C12-C14) sodium fatty acid methyl ester ethoxylate sulfonate;
the nonionic surfactant is a mixture consisting of (C12-C14) fatty alcohol polyoxyethylene (7) ether, isomeric decyl alcohol oxidation nonionic surfactant and isomeric tridecanol oxidation nonionic surfactant, wherein the weight part ratio of the fatty alcohol polyoxyethylene (7) ether, the isomeric decyl alcohol oxidation nonionic surfactant and the isomeric tridecanol oxidation nonionic surfactant is 4:3: 3;
the solvent is ethanol and propylene glycol, and the weight part ratio of the ethanol to the propylene glycol is 5: 5;
the chelating agent is tetrasodium glutamate diacetate;
the biological enzyme is cellulase.
10. A preparation method of a quick-drying efficient down jacket spray cleaning agent without leaving marks is characterized in that
A. Firstly measuring 49.55 percent of the total weight of the deionized water～Adding 92.4% deionized water into a material dissolving kettle, and then sequentially adding the anionic surfactant, the nonionic surfactant and the solvent according to the weight parts of the raw materials to obtain a mixed solution A;
B. adding the benzisothiazolinone, the chelating agent and the essence oil into the mixed solution A according to the weight ratio of the formula, and uniformly stirring to obtain a mixed solution B;
C. adding biological enzyme into the mixed solution B according to the weight ratio of the formula, and uniformly stirring to obtain a mixed solution C;
D. and filtering the mixed solution C to obtain the quick-drying efficient clean down spray without leaving marks.
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| CN111961538A (en) * | 2020-08-31 | 2020-11-20 | 广东中联邦精细化工有限公司 | Antibacterial and peculiar smell-removing laundry detergent and preparation method thereof |
| CN113528252A (en) * | 2021-08-23 | 2021-10-22 | 安徽启威生物科技有限公司 | Down feather washing deodorant and preparation method thereof |
| CN113583757A (en) * | 2021-08-12 | 2021-11-02 | 湖北天喜达生物科技有限公司 | Spray type detergent |
| CN113605090A (en) * | 2021-09-06 | 2021-11-05 | 安徽高梵电子商务有限公司 | Odor-removing and refreshing spray for down jackets and preparation method thereof |
| CN116083171A (en) * | 2023-02-01 | 2023-05-09 | 重庆珍爱卫生用品有限责任公司 | Down jacket cleaning wet tissue formula and preparation method thereof |
| CN116463174A (en) * | 2023-03-10 | 2023-07-21 | 武汉超好生物科技股份有限公司 | Dry cleaning agent special for down jackets and preparation method thereof |
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| CN116083171A (en) * | 2023-02-01 | 2023-05-09 | 重庆珍爱卫生用品有限责任公司 | Down jacket cleaning wet tissue formula and preparation method thereof |
| CN116463174A (en) * | 2023-03-10 | 2023-07-21 | 武汉超好生物科技股份有限公司 | Dry cleaning agent special for down jackets and preparation method thereof |
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