CN102071112B - Stubborn stain decomposer - Google Patents
Stubborn stain decomposer Download PDFInfo
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- CN102071112B CN102071112B CN2011100336339A CN201110033633A CN102071112B CN 102071112 B CN102071112 B CN 102071112B CN 2011100336339 A CN2011100336339 A CN 2011100336339A CN 201110033633 A CN201110033633 A CN 201110033633A CN 102071112 B CN102071112 B CN 102071112B
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- decomposition agent
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Abstract
The invention relates to a stubborn stain decomposer and application thereof. The stubborn stain decomposer is particularly applicable to the decomposition of hair-dyeing stains on towels, clothes or textiles. The invention invents the stubborn stain decomposer, which belongs to a dual-release washing agent, dye, grease and protein on the towels are fast removed through fast-release parts containing organized enzymes, other stains on the towels are removed through slow-release parts containing polyethenoxy ether compounds, and plant saponin and plant volatile oil are also contained in the slow-release parts, so the stain removing capability and the antibacterium capability are enhanced.
Description
Technical field
The present invention relates to a kind of stain decomposition agent and uses thereof, be used in particular for the decomposition of hair dyeing spot on towel, clothes or the textiles.
Background technology
In when hair dyeing, because various dyestuffs, grease, sweat, make on the fiber of the towel, clothes or the textiles that cover on people's shoulder and be stained with a large amount of impurity, particularly water-fast dyestuff, wax, grease, protein.Use at present general washing methods, can only be with the dirt eccysis of textile surfaces such as towel, and the inner organism of textiless such as towel can't eccysis; The fiber generation chemical transformation of textiless such as towel; Towel is aging, and color is degraded, and the dirt of long-term accumulation will diminish HUMAN HEALTH.
Prior art when removing hair dyeing on towel dirt, the general alkalescence prescription that adopts, portioned product also is added with solvent, might cause the clothing part to fade.
Prior art utilizes enzyme to remove dirt, through increasing the activity of surfactant content with the stabilate enzyme, has caused cost higher.
Summary of the invention
For one of solving the problems of the technologies described above, the technical scheme that the present invention adopts is following:
The present invention develops a kind of stain decomposition agent, is a kind of two washing composition of releasing,
By the immediate release section that contains organized enzyme, dispel dyestuff, grease on the towel rapidly, protein,
By the slow-released part that contains the Soxylat A 25-7 compounds, dispel other spots on the towel,
Also contain in the slow-released part, plant saponins, plant volatile oil, thus increase dispel dirty ability and antibacterial ability.Concrete grammar is:
1. the stain decomposition agent is a kind of two washing composition of releasing,
The weight fraction of immediate release section is formed
Ionic surface active agent | 1-5 |
Organized enzyme | 0.01-0.5 |
The organized enzyme stablizer | 0.2-5 |
The quick-release auxiliary material | 0.1-2 |
Washing assistant | 1-10 |
The weight fraction of slow-released part is formed
The Soxylat A 25-7 compounds | 1-10 |
Slow-release auxiliary material | 0.5-15 |
Washing assistant | 0.5-10 |
Ionic surface active agent | 0.5-10 |
The plant saponin(e | In right amount |
Plant volatile oil | In right amount. |
2. the stain decomposition agent is a kind of two washing composition of releasing,
The weight fraction of immediate release section is formed
Sodium lauryl sulphate | 3 |
Proteolytic enzyme | 0.2 |
Ucar 35 | ?0.1 |
Polyacrylate | 5 |
Trisodium Citrate | 0.5 |
Calcium chloride | 1 |
Deionized water | 90 |
The weight fraction of slow-released part is formed
Ethoxylated dodecyl alcohol | 2 |
Vltra tears | 0.5 |
Alcohol | 10 |
Sodium sulfate | 1 |
Yellow soda ash | 2 |
The Chinese honey locust saponin(e | 0.01 |
Spearmint oil | 0.2 |
Deionized water | 95。 |
3. institute's stain decomposition agent is a kind of two washing composition of releasing,
The weight fraction of immediate release section is formed
Sodium palmityl sulfate | 4 |
Lypase | 0.1 |
Polyoxyethylene glycol | 0.2 |
ZX-I | 3 |
Trisodium Citrate | 0.3 |
Calcium chloride | 2 |
Deionized water | 95 |
The weight fraction of slow-released part is formed
The T 46155 cetyl ether | 3 |
CMC 99.5 | 0.8 |
Alcohol | 8 |
Sodium sulfate | 1.2 |
Water glass | 1.8 |
Silicone oil | 0.5 |
Soybean saponin | 0.02 |
Jasmin oil | 0.1 |
1,2-diperoxy dodecandioic acid | 0.5 |
Zeolite | 1 |
Deionized water | 95。 |
The preparation method of immediate release section is
(1) in whisking appliance, drops into earlier water; Drop into AS, stir, fully dissolving;
(2) drop into washing assistant, stir, be stirred to dissolving fully;
(3) adjustment pH value is to 6.8-8.0;
(4) drop into organized enzyme and quick-release auxiliary material, stir;
(5) vacuum-drying is prepared into particle, sieves, and forms immediate release section, and is subsequent use, and the temperature in these 5 steps is lower than 36 ℃;
Organized enzyme be proteolytic enzyme, lypase, laccase, cellulase, Rohapect MPE,
The organized enzyme stablizer is calcium chloride, ZX-I
The quick-release auxiliary material is: Ucar 35, pinakon, 1, and 2-pentanediol, polyoxyethylene glycol, dipropylene glycol, 1,3 butylene glycol, 2-ethyl-1,3-pinakon, glycol ether, Vinylpyrrolidone polymer or Sudan Gum-arabic,
AS is: soap, AS, sulfonated alkylbenzene, aliphatic alcohol sulfate, fatty alcohol polyoxyethylene ether sulfate, alkyl polyoxyethylene ether sulfate, N-N-oleoyl methyl taurocholate, succsinic acid ethylhexyl sulphonate, sulfated butyl oleate, alkylphosphonic acid carboxylic acid fat salt, alkyl polyoxyethylene ether phosphate ester salt or, TX10 phosphoric acid fat salt; These salt are sodium; The potassium metal-salt.As: sodium lauryl sulphate, Sodium palmityl sulfate, sodium stearyl sulfate or, sodium laurylsulfonate, X 2073, tetradecyl Supragil GN, dodecyl phenyl ether disodium sulfonate
2. stain decomposition agent:
The preparation method of slow-released part is
(7) Soxylat A 25-7 compounds, alcohol, Jia Shui, heated and stirred is miscible,
(8) add water simultaneously again, add slow-release auxiliary material, the heated and stirred pulp;
(9) then both are mixed an amount of plant saponins of adding, plant volatile oil,
(10) 30 ℃ are continued to stir vacuum-drying.
The Soxylat A 25-7 compounds comprises: polyoxyethylene nonylphenol, ethoxylated dodecyl alcohol, T 46155 hexadecyl stearyl ether, polyoxyethylene stearyl base ether, T 46155 cetyl ether, polyoxyethylene oleyl ether, polyoxyethylene octyl phenyl ether, T 46155 methyl ether, T 46155 butyl ether, T 46155 Octyl Ether or, the T 46155 tridecyl ether
Slow-release auxiliary material comprises: hydroxypropylcellulose, methylcellulose gum, Vltra tears, TKK 021, Natvosol, CMC 99.5, vinylformic acid polymer, silicone oil verivate or, guar gum positively charged ion polymer,
AS is: soap, AS, sulfonated alkylbenzene, aliphatic alcohol sulfate, fatty alcohol polyoxyethylene ether sulfate, alkyl polyoxyethylene ether sulfate, N-N-oleoyl methyl taurocholate, succsinic acid ethylhexyl sulphonate, sulfated butyl oleate, alkylphosphonic acid carboxylic acid fat salt, alkyl polyoxyethylene ether phosphate ester salt or, TX10 phosphoric acid fat salt; These salt are sodium; The potassium metal-salt.As: sodium lauryl sulphate, Sodium palmityl sulfate, sodium stearyl sulfate or, sodium laurylsulfonate.
Cats product is: the tensio-active agent of quaternary ammonium salt, two octadecyl ammonium chloride of dimethyl-for example, methyl ammonium halide; At least be associated with particularly two to three long carbochains of satisfying basically and closing on the nitrogen-atoms; The tallow base, the methylsulfuric acid salt anionic of hydrogenated-tallow group, above-mentioned substance, long-chain aminoderivative are like ermine oleoyl aminopropyl dimethyl--2-hydroxyethyl ammonium chloride; Quaternium26; Aromatic compound is like Permethyl 99A. base phenyl three ethanol ammonium chlorides, N-alkylation amphiprotic substance, like N-alkylation trimethyl-glycine.
Cats product also comprises the cats products such as amine of alkylamine, alkyl imidazoline, various ethoxylations.As, Quaternium-8 ,-14 ,-18 ,-24 ,-26 ,-27 ,-33 ,-43 ,-52 ,-53 ,-60 ,-62 ,-83 etc.
To be monomeric cats product have more meliority with comparing for the tensio-active agent of polymkeric substance to cats product.
Cationic polymers is like the polymkeric substance of some quaternary ammonium salt; The multipolymer of the quaternised quaternary ammonium salt of Dimethylsulfate of the multipolymer of the multipolymer of Natvosol and dialkyl dimethyl ammonium chloride, acrylic amide and Beta-methyl acrylyl oxy-ethyl-trimethyl (methylsulfuric acid) ammonium, methyl and octadecyl dimethyl-(aminoethyl) methylacrylic acid; Quaternary ammonium polymer is that the reaction through the ethyl-sulfide hydrochlorate obtains, V-Pyrol RC and dimethylaminoethyl methylacrylic acid salt copolymer, quaternised guar gum and melon that natural gum etc.
Washing assistant comprises: vitriol, carbonate, supercarbonate, acetate, aluminosilicate, silicate, phosphoric acid salt, borate, NTA salt, edetate, tartrate, Citrate trianion, vinylformic acid, these salt be sodium, potash metal-salt or, ammonium salt.
For example sodium sulfate, yellow soda ash, ammonium sulfate, sodium ethylene diamine tetracetate, or, Trisodium Citrate
The plant saponins is: soybean saponin, Chinese honey locust saponin(e or, dioscin,
Plant volatile oil be spearmint oil, jasmin oil, volatile oil extracted from eucalyptus' leaves or twigs, olium anisi, Rhizoma Chuanxiong oil, Oleum Viticis Negundo, PH 6968, Radix Angelicae Sinensis oil, sweetgum oil, turps, orange flower oil, Rhizoma Alpiniae Officinarum oil, Therapeutic Mineral Ice, ledum terpenes, borneol, Syzygium aromaticum stem oil, Oleum Cinnamomi, Oil&Ulan, nepeta oil or, Eugenol.。
Slow-released part can also add like organic peroxy acid, other SYNTHETIC OPTICAL WHITNER, foaming inhibitor, bright and new dose, pH regulator agent, hydrotropic solvent, zeolite or the like.
Organic peroxide acid is selected from: 4-amino in the ninth of the ten Heavenly Stems-4-oxo Perbutyric Acid, 6-amino in the ninth of the ten Heavenly Stems-own carboxylic of 6-oxo peroxide, 1; 12-diperoxy dodecandioic acid, heptyl alkylsulfonyl perpropionic acid, decyl alkylsulfonyl perpropionic acid; Heptyl, octyl group, nonyl and decyl alkylsulfonyl perbutyric acid, or, the mixture of said peroxy acid;
3. obstinate saponin(e stain decomposition agent: formulation is that particle, powder, color are white.
4. stain decomposition agent:
Be in the same place immediate release section and slowly-releasing are partially mixed.
Specific embodiment 1
The stain decomposition agent,
The preparation method of immediate release section is
(1) in whisking appliance, drops into earlier water; Drop into sodium lauryl sulphate, stir, fully dissolving;
(2) drop into Trisodium Citrate, stir, be stirred to dissolving fully;
(3) adjustment pH value is to 6.8-8.0;
(4) drop into proteolytic enzyme, Ucar 35, calcium chloride, ZX-I, stir;
(5) vacuum-drying is ground into particle, and 20 orders that sieve form immediate release section, and are subsequent use.The temperature in these 5 steps is 30 ℃;
The raw material of immediate release section is pressed its ratio of weight and number:
Sodium lauryl sulphate | 3 |
Proteolytic enzyme | 0.2 |
Ucar 35 | ?0.1 |
ZX-I | 5 |
Trisodium Citrate | 0.5 |
Calcium chloride | 1 |
Deionized water | 90 |
Specific embodiment 2
Gu spot decomposition agent:
The preparation method of slow-released part is
(7) ethoxylated dodecyl alcohol, alcohol, Jia Shui, heated and stirred is miscible,
(8) add water simultaneously again, add Vltra tears, sodium sulfate, yellow soda ash, heated and stirred pulp;
(9) then both are mixed an amount of Chinese honey locust saponin(e of adding, spearmint oil,
(10) 30 ℃ are continued to stir, and the vacuum-drying powder is broken into particle, and 20 orders that sieve form immediate release section, and are subsequent use.
The raw material of slow-released part is pressed its ratio of weight and number:
Ethoxylated dodecyl alcohol | ?2 |
Vltra tears | ?0.5 |
Alcohol | ?10 |
Sodium sulfate | 1 |
Yellow soda ash | 2 |
The Chinese honey locust saponin(e | 0.01 |
Spearmint oil | 0.2 |
Deionized water | 95 |
Specific embodiment 3
In a packing bag, place two little bands, the immediate release section of the dress stain decomposition agent of a harness body embodiment 1, the slow-released part of the stain decomposition agent of a harness body embodiment 2,
Specific embodiment 4
Slow-released part with the stain decomposition agent of the immediate release section of the dress stain decomposition agent of specific embodiment 1 and specific embodiment 2 mixes, and is placed in the packaging vessel.
Specific embodiment 5
The stain decomposition agent,
The preparation method of immediate release section is
(1) in whisking appliance, drops into earlier water; Drop into Sodium palmityl sulfate, stir, fully dissolving;
(2) drop into Trisodium Citrate, stir, be stirred to dissolving fully;
(3) adjustment pH value is to 6.8-8.0;
(4) drop into lypase, polyoxyethylene glycol, calcium chloride, ZX-I, stir;
(5) vacuum-drying is ground into particle, and 20 orders that sieve form immediate release section, and are subsequent use.The water temperature in these 5 steps is 30 ℃;
The raw material of immediate release section is pressed its ratio of weight and number:
Sodium palmityl sulfate | 4 |
Lypase | 0.1 |
Polyoxyethylene glycol | 0.2 |
ZX-I | 3 |
Trisodium Citrate | 0.3 |
Calcium chloride | 2 |
Deionized water | 95 |
Specific embodiment 6
The raw material of slow-released part is pressed its ratio of weight and number:
The T 46155 cetyl ether | 3 |
CMC 99.5 | 0.8 |
Alcohol | 8 |
Sodium sulfate | 1.2 |
Water glass | 1.8 |
Silicone oil | 0.5 |
Soybean saponin | 0.02 |
Jasmin oil | 0.1 |
1,2-diperoxy dodecandioic acid | 0.5 |
Zeolite | 1 |
Deionized water | 95 |
Gu spot decomposition agent:
The preparation method of slow-released part is
(7) T 46155 cetyl ether, alcohol, Jia Shui, heated and stirred is miscible,
(8) add water simultaneously again, add CMC 99.5, sodium sulfate, yellow soda ash, heated and stirred pulp;
(9) then both are mixed an amount of Chinese honey locust saponin(e of adding, spearmint oil,
(10) 30 ℃ are continued to stir, and the vacuum-drying powder is broken into particle, and 20 orders that sieve form immediate release section, and are subsequent use.
Specific embodiment 7
In a packing bag, place two little bands, the immediate release section of the dress stain decomposition agent of a harness body embodiment 5, the slow-released part of the stain decomposition agent of a harness body embodiment 6,
Specific embodiment 8
Slow-released part with the stain decomposition agent of the immediate release section of the dress stain decomposition agent of specific embodiment 5 and specific embodiment 6 mixes, and is placed in the packaging vessel.
Specific embodiment 9
The present invention adopts above-mentioned prescription, owing to adopt the quick decomposition of protein of enzyme ability in the immediate release section, greasy dirt, thus the consumption of chemical substance in the slow-released part reduced, reduced injury to the towel fiber, prolonged the working life of towel.
Cats product, plant volatile oil, plant saponin(e that the present invention adds make product of the present invention have the effect of neutrality, soft conditioning, fungi-proofing, causing resuscitation with aromatic drugs.The result of use of specific embodiment 3,4,7,8
Use the French hardness water of 30 degree to prepare material solution, this solution contains the product of 2g/l specific embodiment 3,4,7,8
Contrast product 1: domestic certain main flow degreasing washing liquid, use 30 degree hardness water to be prepared into 2g/l
Test for contamination cloth (clean and detect thing) | Reference substance cleaner assay cloth | |
10cm * 10cm side's cloth | 10cm * 10cm side's cloth | 10cm * 10cm side's cloth |
Fabric | Dirt | Fabric |
Cotton fabric | Cream rinse 1 g | Cotton fabric |
Cotton fabric | Meat soup 0.5 g, makeup 0.5 g | Cotton fabric |
Terylene | Tealeaves soup 0.5 g, eye shadow 0.5 g | Terylene |
Cotton fabric | Carbon black 0.1 g, shoe polish 0.5 g | Cotton fabric |
The test washing methods
Stirring formula detersive power determinator is canned to have test recipe, pollute with cleaner assay cloth under 25 ℃ with 90rpm stirring 15,30,60 minutes.Take out a bag fabric in then from jar, water (the French hardness of 30 degree) rinsing is twice again.These fabrics are drying at least 12 hours in the dark again.
Former cloth before and after the spectrophotometric determination washing and test for contamination cloth carry out the decontamination evaluation in the transparence at 580nm place.The transparence increase shows greasiness removal, and therefore, numerical value is the bigger the better.
Slow, the immediate release section of the stain decomposition agent in the specific embodiment 3,7 are used simultaneously.
Churning time | Reference substance | Contrast product | Specific embodiment 3 | Specific embodiment 4 | Specific embodiment 7 | Specific embodiment 8 | |
Concentration | Minute | 0g/L | 2g/L | 2g/L | 2g/L | 2g/L | 2g/L |
Transparence | 15 | 60% | 40% | 48% | 50% | 53% | 55% |
Transparence | 30 | 62% | 45% | 51% | 56% | 55% | 57% |
Transparence | 60 | 61% | 54% | 60% | 57% | 58% | 61% |
Specific embodiment 10
The result of use of specific embodiment specific embodiment 1,2,5,6
Use the French hardness water of 30 degree to prepare material solution, this solution contains 1g/l specific embodiment 3,7 slow-released part, immediate release section separately
Contrast product 1: domestic certain main flow degreasing washing liquid, use 30 degree hardness water to be prepared into 1g/l
According to the method preparation of specific embodiment 9, test for contamination cloth (clean and detect thing) reference substance cleaner assay cloth
Method according to specific embodiment 9 is washed, and measures the transparence at 580nm place
Churning time | Reference substance | Contrast product | Specific embodiment 1 | Specific embodiment 2 | Specific embodiment 5 | Specific embodiment 6 | |
Concentration | Minute | 0g/L | 1g/L | 1g/L | 1g/L | 1g/L | 1g/L |
Transparence | 15 | 60% | 30% | 35% | 41% | 38% | 39% |
Transparence | 30 | 62% | 41% | 44% | 40% | 39% | 47% |
Transparence | 60 | 61% | 42% | 47% | 45% | 43% | 47% |
Claims (5)
3. according to any described stain decomposition agent of claim 1-2, it is characterized in that: be in the same place immediate release section and slowly-releasing are partially mixed.
4. stain decomposition agent according to claim 3 is characterized in that: the formulation of described stain decomposition agent is a particle, and the formulation color is a white.
5. stain decomposition agent according to claim 3 is characterized in that: the formulation of described stain decomposition agent is a powder, and the formulation color is a white.
Priority Applications (1)
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CN2011100336339A CN102071112B (en) | 2011-01-31 | 2011-01-31 | Stubborn stain decomposer |
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CN2011100336339A CN102071112B (en) | 2011-01-31 | 2011-01-31 | Stubborn stain decomposer |
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CN102071112B true CN102071112B (en) | 2012-07-04 |
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Granted publication date: 20120704 Termination date: 20130131 |