CN105753425A - Graphene and aluminum oxide based far-infrared heating coating and method for preparing same - Google Patents
Graphene and aluminum oxide based far-infrared heating coating and method for preparing same Download PDFInfo
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- CN105753425A CN105753425A CN201610043028.2A CN201610043028A CN105753425A CN 105753425 A CN105753425 A CN 105753425A CN 201610043028 A CN201610043028 A CN 201610043028A CN 105753425 A CN105753425 A CN 105753425A
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Abstract
The invention discloses a graphene and aluminum oxide based far-infrared heating coating and a method for preparing the same.The method includes carrying out plasma spraying processes on oxidized graphene, nanometer aluminum oxide, bamboo coal powder, tourmaline, nanometer silver-silicon dioxide core-shell structures, calcite, hematite, zircon, medical stone, red mud, silica sol, eucalyptus leaf oil, kaolin, silicone acrylic emulsion and defoaming agent materials to obtain the graphene and aluminum oxide based far-infrared heating coating.The graphene and aluminum oxide based far-infrared heating coating and the method have the advantage that the graphene and aluminum oxide based far-infrared heating coating is environmentally friendly and healthful and is high in far-infrared heating capacity.
Description
Technical field
The invention belongs to far infrared heating coatings art, particularly to a kind of Graphene alumina base far infrared heating coating and preparation method thereof.
Background technology
Far infrared has stronger penetration and radiant force, has significant temperature control effect and resonance effects, and it is easily absorbed by object and is converted into the interior energy of object.After far infrared is absorbed by the body, internal water can be made to produce resonance, make water molecule activation, strengthen its intermolecular adhesion, thus the large biological molecules such as activation of protein, make biological cell be in the highest vibration level.Owing to biological cell produces resonance effects, far infrared heat energy can be delivered to the subcutaneous deeper part of human body, following deep layer temperature rises, and the warm of generation distributes from inside to outside.This action intensity, makes telangiectasis, stimulates circulation, and strengthens the metabolism between each tissue, increases the power of regeneration of tissue, improves the immunocompetence of body, the exaltation state of regulation spirit, thus plays the effect of health care.Also there is a lot of far infrared heating material, such as Far-infrared self heating waist support, Far-infrared self heating waist support now, also known as Tourmaline self-heating waist support, under the exciting of human body temperature, by shifting the effect of catalyst, thermoinduction material reacts releasing heat in time, and under the amplification of heat energy, far-infrared negative-ion penetrates to the skin depths, the harmful substances such as peroxynitrite decomposition lipid, and get rid of external by urine and sweat, expand blood vessel, stimulate circulation, activating cell, regulation nerve.The molecular vibration of effectively conversion and the heated material of other energy is absorbed by far-infrared radiation material, and reach purposes such as heating, be dried, it have energy-conservation, heat temperature raising is fast, pollution-free, thermal efficiency high, can be widely applied to the aspects such as weaving, printing and dyeing, electromechanics, printing, glass annealing, food processing and health care, civilian cooker, heating system.
Graphene (Graphene) is the two dimensional crystal of the only one layer of atomic thickness being stripped out from graphite material, being made up of carbon atom.Graphene oxide (graphene oxide) is the oxide of Graphene, and its color is brown color, and the most common product has powder, sheet and solution shape.After oxidized, on it, oxygen-containing functional group increases and makes character relatively Graphene more active, can improve nature via the various reactions with oxygen-containing functional group.It has stronger electric conductivity and thermal conductivity.Graphene has been widely used in a lot of field, but about the research of graphene-based far infrared heating coating or rather seldom.
Summary of the invention
It is an object of the invention to for the problems referred to above, develop a kind of environmental protection, health, Graphene alumina base far infrared heating coating that far infrared heating ability is strong and preparation method thereof.
A kind of Graphene alumina base far infrared heating coating, this coating includes the raw material of following weight portion:
Graphene oxide 20-30 part；
Nano aluminium oxide 20-30 part；
Bamboo carbon powder 10-15 part；
Tourmaline 10-15 part；
Nano Silver-silicon dixoide nucleocapsid structure 1-5 part；
Calcite 1-5 part；
Bloodstone 1-5 part；
Zircon 1-5 part；
Medical stone 1-5 part；
Red mud 1-5 part；
Ludox 1-5 part；
Eucalyptus oil 1-5 part；
Kaolin 1-5 part；
Silicone acrylic emulsion 1-5 part；
Defoamer 1-5 part；
Described graphene oxide is obtained by following preparation method:
Take 2 weight portion flaky graphites and 1 parts by weight of potassium nitrate is added in the 85 weight portion concentrated sulfuric acids, the mixture obtained is placed in a reservoir and cooled down in ice-water bath, keep violent stirring simultaneously, continue to be slowly added the potassium permanganate of 5 weight portions, obtain the suspension of brown；Add the hydrogen peroxide solution of the 2wt% of 5 weight portions subsequently, obtain jonquilleous suspension；Then wash suspension respectively with deionized water and ethanol, subsequently graphene oxide is dispersed in the extract of tarragon, stirring mixing 2h at 80 DEG C, it is thus achieved that the graphene oxide that Folium Artemisiae Argyi extractive liquid is modified.
As preferably, this coating includes the raw material of following weight portion:
Graphene oxide 25 parts；
Nano aluminium oxide 25 parts；
Bamboo carbon powder 12 parts；
12 parts of tourmaline；
Nano Silver-silicon dixoide nucleocapsid structure 3 parts；
3 parts of calcite；
Bloodstone 3 parts；
Zircon 3 parts；
Medical stone 3 parts；
Red mud 3 parts；
Ludox 3 parts；
Eucalyptus oil 3 parts；
Kaolin 3 parts；
Silicone acrylic emulsion 3 parts；
Defoamer 3 parts.
As preferably, described defoamer is dimethyl silicone polymer.
A kind of method preparing above-mentioned Graphene alumina base far infrared heating coating, comprises the steps:
(1) dispensing is carried out according to Graphene alumina base far infrared heating coating material composition；By raw material mixing wet ball-milling 12 hours, solvent was distilled water, and abrading-ball is aluminum oxide abrading-ball, dries at 50 DEG C again, obtain standby material after ball milling；
(2) substrate is pre-processed according to demand；Standby material plasma spray being applied in pretreated substrate subsequently, can obtain Graphene alumina base far infrared heating coating, the thickness of coating is 1-20mm.
Beneficial effects of the present invention:
(1) present invention uses graphene oxide, nano aluminium oxide, bamboo carbon powder, tourmaline, Nano Silver-silicon dixoide nucleocapsid structure, calcite, bloodstone, zircon, medical stone, red mud, Ludox, eucalyptus oil, kaolin, silicone acrylic emulsion and defoamer to be raw material, main component therein is graphene oxide and nano aluminium oxide, graphene oxide is the graphene oxide that Folium Artemisiae Argyi extractive liquid is modified, this Graphene is in addition to the function with far infrared heating, also there is effect of health environment-friendly, useful for human body；And graphene oxide and the compound use of nano aluminium oxide, the two collaborative enhancing far infrared heating effect；
(2) in order to optimize the performance of far infrared heating further, have selected bamboo carbon powder, tourmaline, Nano Silver-silicon dixoide nucleocapsid structure, calcite, bloodstone, zircon, medical stone, red mud, Ludox, eucalyptus oil, kaolin, silicone acrylic emulsion and defoamer is auxiliary element, these auxiliary materials, together with graphene oxide and nano aluminium oxide, work in coordination with the far infrared heating performance strengthening coating.The infrared emissivity of coating prepared by the present invention has exceeded 99.3%.
(4) this Graphene alumina base far infrared heating preparation technology of coating is simple, it is easy to industrialization, and raw material sources are extensive, is highly suitable to be applied for producing.
Detailed description of the invention
Below in conjunction with specific embodiment, and with reference to data, the present invention is described in further detail.Should be understood that these embodiments present invention solely for the purpose of illustration, rather than limit the scope of the present invention by any way.
Embodiment 1:
A kind of Graphene alumina base far infrared heating coating, this coating includes the raw material of following weight portion:
Graphene oxide 25 parts；
Nano aluminium oxide 25 parts；
Bamboo carbon powder 12 parts；
12 parts of tourmaline；
Nano Silver-silicon dixoide nucleocapsid structure 3 parts；
3 parts of calcite；
Bloodstone 3 parts；
Zircon 3 parts；
Medical stone 3 parts；
Red mud 3 parts；
Ludox 3 parts；
Eucalyptus oil 3 parts；
Kaolin 3 parts；
Silicone acrylic emulsion 3 parts；
Defoamer 3 parts；
Described graphene oxide is obtained by following preparation method:
Take 2 weight portion flaky graphites and 1 parts by weight of potassium nitrate is added in the 85 weight portion concentrated sulfuric acids, the mixture obtained is placed in a reservoir and cooled down in ice-water bath, keep violent stirring simultaneously, continue to be slowly added the potassium permanganate of 5 weight portions, obtain the suspension of brown；Add the hydrogen peroxide solution of the 2wt% of 5 weight portions subsequently, obtain jonquilleous suspension；Then wash suspension respectively with deionized water and ethanol, subsequently graphene oxide is dispersed in the extract of tarragon, stirring mixing 2h at 80 DEG C, it is thus achieved that the graphene oxide that Folium Artemisiae Argyi extractive liquid is modified.
Described defoamer is dimethyl silicone polymer.
A kind of method preparing above-mentioned Graphene alumina base far infrared heating coating, comprises the steps:
(1) dispensing is carried out according to Graphene alumina base far infrared heating coating material composition；By raw material mixing wet ball-milling 12 hours, solvent was distilled water, and abrading-ball is aluminum oxide abrading-ball, dries at 50 DEG C again, obtain standby material after ball milling；
(2) substrate is pre-processed according to demand；Standby material plasma spray being applied in pretreated substrate subsequently, can obtain Graphene alumina base far infrared heating coating, the thickness of coating is 10mm.The far infrared transmissivity of this coating is 99.3%.
Embodiment 2:
A kind of Graphene alumina base far infrared heating coating, this coating includes the raw material of following weight portion:
Graphene oxide 20 parts；
Nano aluminium oxide 20 parts；
Bamboo carbon powder 15 parts；
15 parts of tourmaline；
Nano Silver-silicon dixoide nucleocapsid structure 1 part；
1 part of calcite；
Bloodstone 1 part；
Zircon 1 part；
Medical stone 1 part；
Red mud 1 part；
Ludox 1 part；
Eucalyptus oil 1 part；
Kaolin 1 part；
Silicone acrylic emulsion 1 part；
Defoamer 1 part；
Described graphene oxide is obtained by following preparation method:
Take 2 weight portion flaky graphites and 1 parts by weight of potassium nitrate is added in the 85 weight portion concentrated sulfuric acids, the mixture obtained is placed in a reservoir and cooled down in ice-water bath, keep violent stirring simultaneously, continue to be slowly added the potassium permanganate of 5 weight portions, obtain the suspension of brown；Add the hydrogen peroxide solution of the 2wt% of 5 weight portions subsequently, obtain jonquilleous suspension；Then wash suspension respectively with deionized water and ethanol, subsequently graphene oxide is dispersed in the extract of tarragon, stirring mixing 2h at 80 DEG C, it is thus achieved that the graphene oxide that Folium Artemisiae Argyi extractive liquid is modified.
Described defoamer is dimethyl silicone polymer.
A kind of method preparing above-mentioned Graphene alumina base far infrared heating coating, comprises the steps:
(1) dispensing is carried out according to Graphene alumina base far infrared heating coating material composition；By raw material mixing wet ball-milling 12 hours, solvent was distilled water, and abrading-ball is aluminum oxide abrading-ball, dries at 50 DEG C again, obtain standby material after ball milling；
(2) substrate is pre-processed according to demand；Standby material plasma spray being applied in pretreated substrate subsequently, can obtain Graphene alumina base far infrared heating coating, the thickness of coating is 15mm.The far infrared transmissivity of this coating is 99.7%.
Embodiment 3:
A kind of Graphene alumina base far infrared heating coating, this coating includes the raw material of following weight portion:
Graphene oxide 20 parts；
Nano aluminium oxide 20 parts；
Bamboo carbon powder 15 parts；
15 parts of tourmaline；
Nano Silver-silicon dixoide nucleocapsid structure 2 parts；
2 parts of calcite；
Bloodstone 2 parts；
Zircon 2 parts；
Medical stone 2 parts；
Red mud 2 parts；
Ludox 2 parts；
Eucalyptus oil 2 parts；
Kaolin 2 parts；
Silicone acrylic emulsion 2 parts；
Defoamer 2 parts；
Described graphene oxide is obtained by following preparation method:
Take 2 weight portion flaky graphites and 1 parts by weight of potassium nitrate is added in the 85 weight portion concentrated sulfuric acids, the mixture obtained is placed in a reservoir and cooled down in ice-water bath, keep violent stirring simultaneously, continue to be slowly added the potassium permanganate of 5 weight portions, obtain the suspension of brown；Add the hydrogen peroxide solution of the 2wt% of 5 weight portions subsequently, obtain jonquilleous suspension；Then wash suspension respectively with deionized water and ethanol, subsequently graphene oxide is dispersed in the extract of tarragon, stirring mixing 2h at 80 DEG C, it is thus achieved that the graphene oxide that Folium Artemisiae Argyi extractive liquid is modified.
Described defoamer is dimethyl silicone polymer.
A kind of method preparing above-mentioned Graphene alumina base far infrared heating coating, comprises the steps:
(1) dispensing is carried out according to Graphene alumina base far infrared heating coating material composition；By raw material mixing wet ball-milling 12 hours, solvent was distilled water, and abrading-ball is aluminum oxide abrading-ball, dries at 50 DEG C again, obtain standby material after ball milling；
(2) substrate is pre-processed according to demand；Standby material plasma spray being applied in pretreated substrate subsequently, can obtain Graphene alumina base far infrared heating coating, the thickness of coating is 12mm.The far infrared transmissivity of this coating is 99.5%.
Embodiment 4:
A kind of Graphene alumina base far infrared heating coating, this coating includes the raw material of following weight portion:
Graphene oxide 30 parts；
Nano aluminium oxide 30 parts；
Bamboo carbon powder 10 parts；
10 parts of tourmaline；
Nano Silver-silicon dixoide nucleocapsid structure 3 parts；
2 parts of calcite；
Bloodstone 2 parts；
Zircon 3 parts；
Medical stone 2 parts；
Red mud 2 parts；
Ludox 2 parts；
Eucalyptus oil 2 parts；
Kaolin 3 parts；
Silicone acrylic emulsion 2 parts；
Defoamer 3 parts；
Described graphene oxide is obtained by following preparation method:
Take 2 weight portion flaky graphites and 1 parts by weight of potassium nitrate is added in the 85 weight portion concentrated sulfuric acids, the mixture obtained is placed in a reservoir and cooled down in ice-water bath, keep violent stirring simultaneously, continue to be slowly added the potassium permanganate of 5 weight portions, obtain the suspension of brown；Add the hydrogen peroxide solution of the 2wt% of 5 weight portions subsequently, obtain jonquilleous suspension；Then wash suspension respectively with deionized water and ethanol, subsequently graphene oxide is dispersed in the extract of tarragon, stirring mixing 2h at 80 DEG C, it is thus achieved that the graphene oxide that Folium Artemisiae Argyi extractive liquid is modified.
Described defoamer is dimethyl silicone polymer.
A kind of method preparing above-mentioned Graphene alumina base far infrared heating coating, comprises the steps:
(1) dispensing is carried out according to Graphene alumina base far infrared heating coating material composition；By raw material mixing wet ball-milling 12 hours, solvent was distilled water, and abrading-ball is aluminum oxide abrading-ball, dries at 50 DEG C again, obtain standby material after ball milling；
(2) substrate is pre-processed according to demand；Standby material plasma spray being applied in pretreated substrate subsequently, can obtain Graphene alumina base far infrared heating coating, the thickness of coating is 16mm.The far infrared transmissivity of this coating is 99.4%.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, and without departing from the spirit or essential characteristics of the present invention, it is possible to realize the present invention in other specific forms.Therefore, no matter from the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is limited by claims rather than described above, it is intended that all changes fallen in the implication of equivalency and scope of claim included in the present invention.
In addition, it is to be understood that, although this specification is been described by according to embodiment, but the most each embodiment only comprises an independent technical scheme, this narrating mode of specification is only for clarity sake, specification should can also be formed, through appropriately combined, other embodiments that it will be appreciated by those skilled in the art that as an entirety, the technical scheme in each embodiment by those skilled in the art.
Claims (4)
1. a Graphene alumina base far infrared heating coating, it is characterised in that: this coating includes the raw material of following weight portion:
Graphene oxide 20-30 part；
Nano aluminium oxide 20-30 part；
Bamboo carbon powder 10-15 part；
Tourmaline 10-15 part；
Nano Silver-silicon dixoide nucleocapsid structure 1-5 part；
Calcite 1-5 part；
Bloodstone 1-5 part；
Zircon 1-5 part；
Medical stone 1-5 part；
Red mud 1-5 part；
Ludox 1-5 part；
Eucalyptus oil 1-5 part；
Kaolin 1-5 part；
Silicone acrylic emulsion 1-5 part；
Defoamer 1-5 part；
Described graphene oxide is obtained by following preparation method:
Take 2 weight portion flaky graphites and 1 parts by weight of potassium nitrate is added in the 85 weight portion concentrated sulfuric acids, the mixture obtained is placed in a reservoir and cooled down in ice-water bath, keep violent stirring simultaneously, continue to be slowly added the potassium permanganate of 5 weight portions, obtain the suspension of brown；Add the hydrogen peroxide solution of the 2wt% of 5 weight portions subsequently, obtain jonquilleous suspension；Then wash suspension respectively with deionized water and ethanol, subsequently graphene oxide is dispersed in the extract of tarragon, stirring mixing 2h at 80 DEG C, it is thus achieved that the graphene oxide that Folium Artemisiae Argyi extractive liquid is modified.
2. a Graphene alumina base far infrared heating coating as claimed in claim 2, it is characterised in that:
This coating includes the raw material of following weight portion:
Graphene oxide 25 parts；
Nano aluminium oxide 25 parts；
Bamboo carbon powder 12 parts；
12 parts of tourmaline；
Nano Silver-silicon dixoide nucleocapsid structure 3 parts；
3 parts of calcite；
Bloodstone 3 parts；
Zircon 3 parts；
Medical stone 3 parts；
Red mud 3 parts；
Ludox 3 parts；
Eucalyptus oil 3 parts；
Kaolin 3 parts；
Silicone acrylic emulsion 3 parts；
Defoamer 3 parts.
3. a Graphene alumina base far infrared heating coating as claimed in claim 1 or 2, it is characterised in that: described defoamer is dimethyl silicone polymer.
4. the method preparing Graphene alumina base far infrared heating coating as claimed in claim 1, it is characterised in that: comprise the steps:
(1) dispensing is carried out according to Graphene alumina base far infrared heating coating material composition；By raw material mixing wet ball-milling 12 hours, solvent was distilled water, and abrading-ball is aluminum oxide abrading-ball, dries at 50 DEG C again, obtain standby material after ball milling；
(2) substrate is pre-processed according to demand；Standby material plasma spray being applied in pretreated substrate subsequently, can obtain Graphene alumina base far infrared heating coating, the thickness of coating is 1-20mm.
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| CN107500782A (en) * | 2017-09-19 | 2017-12-22 | 迟逞 | A kind of preparation method of increasing material manufacturing modified anti-friction wear-resistant nano-ceramic powder material against corrosion |
| CN109116887A (en) * | 2018-08-28 | 2019-01-01 | 深圳天元羲王材料科技有限公司 | Graphene pyrotoxin, the production method based on it and intelligent constant-temperature system |
| CN109793990A (en) * | 2019-01-16 | 2019-05-24 | 辽宁东戴河新区惠惠梦甜科技有限责任公司 | A kind of magnetic bed mattress |
| CN111351042A (en) * | 2020-04-09 | 2020-06-30 | 丁桂林 | Gas infrared catalytic fiber layer and preparation method thereof |
| US10927268B1 (en) * | 2016-08-04 | 2021-02-23 | Tevian Parnell | Coat max |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| US10927268B1 (en) * | 2016-08-04 | 2021-02-23 | Tevian Parnell | Coat max |
| CN107500782A (en) * | 2017-09-19 | 2017-12-22 | 迟逞 | A kind of preparation method of increasing material manufacturing modified anti-friction wear-resistant nano-ceramic powder material against corrosion |
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| CN109793990A (en) * | 2019-01-16 | 2019-05-24 | 辽宁东戴河新区惠惠梦甜科技有限责任公司 | A kind of magnetic bed mattress |
| CN111351042A (en) * | 2020-04-09 | 2020-06-30 | 丁桂林 | Gas infrared catalytic fiber layer and preparation method thereof |
| CN111351042B (en) * | 2020-04-09 | 2021-10-22 | 丁桂林 | Gas infrared catalytic fiber layer and preparation method thereof |
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