CN109116887A - Graphene pyrotoxin, the production method based on it and intelligent constant-temperature system - Google Patents
Graphene pyrotoxin, the production method based on it and intelligent constant-temperature system Download PDFInfo
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- CN109116887A CN109116887A CN201810990925.3A CN201810990925A CN109116887A CN 109116887 A CN109116887 A CN 109116887A CN 201810990925 A CN201810990925 A CN 201810990925A CN 109116887 A CN109116887 A CN 109116887A
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- G—PHYSICS
- G05—CONTROLLING; REGULATING
- G05D—SYSTEMS FOR CONTROLLING OR REGULATING NON-ELECTRIC VARIABLES
- G05D23/00—Control of temperature
- G05D23/19—Control of temperature characterised by the use of electric means
- G05D23/20—Control of temperature characterised by the use of electric means with sensing elements having variation of electric or magnetic properties with change of temperature
- G05D23/24—Control of temperature characterised by the use of electric means with sensing elements having variation of electric or magnetic properties with change of temperature the sensing element having a resistance varying with temperature, e.g. a thermistor
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2227—Oxides; Hydroxides of metals of aluminium
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/04—Carbon
- C08K3/042—Graphene or derivatives, e.g. graphene oxides
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
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Abstract
The invention discloses a kind of graphene pyrotoxin, the production method based on it and intelligent constant-temperature systems, wherein, the graphene pyrotoxin includes heating layer, detection layers and reflecting layer, the heating layer is bonded reflecting layer, the detection layers are arranged between heating layer and reflecting layer, and the heating layer is mixed with by packing material, graphene pulvis, medical stone pulvis, aluminium oxide pulvis and epoxy resin.The heating effect of graphene pyrotoxin gets well and has health-care effect in the present invention, intelligent constant-temperature system based on it can monitor heating temperature in real time, it maintains heating temperature at setting value, and can be automatically closed under unmanned state, achieved the purpose that energy saving.
Description
Technical field
The present invention relates to graphene heating technique field, in particular to a kind of graphene pyrotoxin, the producer based on it
Method and intelligent constant-temperature system.
Background technique
Currently, being to carry out central heating by hot water pipe net in the heating system that northern area generallys use.But this confession
The drawbacks of warm mode is to need to be laid with a large amount of hot water pipeline, and hot-water boiler whole day 24 hours heat, the more wasteful energy.
The heating modes such as house ornamentation floor heating or air-conditioning are then mostly used in southern area.Wherein, be the shortcomings that floor heating need to be laid with pipeline, and
Installation and operating process are more troublesome；And so that indoor environment is become drying by air-conditioning heating, reduce the comfort level of resident.
Therefore, for currently used various heating systems, the prior art could be improved and improve.
Summary of the invention
Place in view of above-mentioned deficiencies of the prior art, the purpose of the present invention is to provide a kind of graphene pyrotoxin, is based on
Its production method and intelligent constant-temperature system, the intelligent constant-temperature system is with easy for installation, heating effect is good and energy saving
The advantages that.
In order to achieve the above object, this invention takes following technical schemes:
A kind of graphene pyrotoxin, including heating layer, detection layers and reflecting layer, the heating layer are bonded reflecting layer, the detection
Layer is arranged between heating layer and reflecting layer, and the heating layer is by packing material, graphene pulvis, medical stone pulvis, aluminium oxide
Pulvis and epoxy resin are mixed with.
In the graphene pyrotoxin, the heating layer includes: packing material 20%-30%, stone by weight percentage
Black alkene pulvis 10%-20%, medical stone pulvis 1%, aluminium oxide pulvis 1%, epoxy resin 58%.
In the graphene pyrotoxin, the mesh number of the graphene pulvis is -3000 mesh of 300 mesh.
In the graphene pyrotoxin, the packing material includes sodium tripolyphosphate, calgon and sodium pyrophosphate
One of or it is a variety of.
In the graphene pyrotoxin, the detection layers include that multiple arrays are arranged between heating layer and reflecting layer
Thermistor.
A kind of production method according to above-mentioned graphene pyrotoxin, comprising steps of
Packing material, graphene pulvis, medical stone pulvis, aluminium oxide pulvis and epoxy resin are mixed to form mixture, use ball
Grinding machine stirs mixture and forms mixed solution；
Mixed solution is coated in the upper surface in reflecting layer and detection layers；
The heating layer for toasting mixed solution using predetermined temperature, mixed solution being made to form abutting reflecting layer and detection layers.
In the production method, the predetermined temperature is 80 DEG C.
A kind of intelligent constant-temperature system, including above-mentioned graphene pyrotoxin, and
Power supply；
Power switch；
For carrying out thermostatically controlled main control unit；
For carrying out the interactive unit of human-computer interaction；
For detecting the human monitoring unit of physical activity；
Power switch input power and it is separately connected main control unit and graphene pyrotoxin, it is single that main control unit is also connected with interaction
Member and human testing unit.
It further include measuring unit in the intelligent constant-temperature system, the measuring unit is separately connected main control unit and stone
The detection layers of black alkene pyrotoxin.
In the intelligent constant-temperature system, the man-machine interaction unit includes liquid crystal display and temperature setting switch.
Compared to the prior art, graphene pyrotoxin provided by the invention, the production method based on it and intelligent constant-temperature system
System, wherein the graphene pyrotoxin includes heating layer, detection layers and reflecting layer, and the heating layer is bonded reflecting layer, the inspection
It surveys layer to be arranged between heating layer and reflecting layer, the heating layer is by packing material, graphene pulvis, medical stone pulvis, oxidation
Aluminium powder agent and epoxy resin are mixed with.Health-care effect is got well and had to the heating effect of graphene pyrotoxin in the present invention,
Intelligent constant-temperature system based on it can monitor heating temperature in real time, maintain heating temperature at setting value, and can be
It is automatically closed, achievees the purpose that energy saving under unmanned state.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the preferred embodiment of graphene pyrotoxin provided by the invention.
Fig. 2 is the structural schematic diagram of the preferred embodiment of the detection layers of graphene pyrotoxin provided by the invention.
Fig. 3 is temperature-change in resistance figure of thermistor provided by the invention.
Fig. 4 is the structural block diagram of intelligent constant-temperature system provided by the invention.
Fig. 5 is the circuit diagram one of the preferred embodiment of CPU in main control unit provided by the invention.
Fig. 6 is the circuit diagram two of the preferred embodiment of CPU in main control unit provided by the invention.
Fig. 7 is the circuit theory of the preferred embodiment of power switch control mouth circuit in main control unit provided by the invention
Figure.
Fig. 8 is the circuit diagram of the preferred embodiment of sensor input port circuit in main control unit provided by the invention
One.
Fig. 9 is the circuit diagram of the preferred embodiment of sensor input port circuit in main control unit provided by the invention
Two.
Figure 10 is the circuit diagram of the preferred embodiment of main control unit medium-long range control interface provided by the invention
One.
Figure 11 is the circuit diagram of the preferred embodiment of main control unit medium-long range control interface provided by the invention
Two.
Figure 12 is the circuit diagram of the preferred embodiment of main control unit medium-long range control interface provided by the invention
Three.
Specific embodiment
The present invention provides a kind of graphene pyrotoxin, the production method based on it and intelligent constant-temperature system, to make the present invention
Purpose, technical solution and effect it is clearer, clear, as follows in conjunction with drawings and embodiments further specifically to the present invention
It is bright.It should be appreciated that described herein, specific examples are only used to explain the present invention, is not intended to limit the present invention.
Referring to Fig. 1, the structural schematic diagram of the preferred embodiment for graphene pyrotoxin provided by the invention, the graphite
Alkene pyrotoxin includes heating layer 1, detection layers 2 and reflecting layer 3, and the heating layer 1 is bonded reflecting layer 3, and the setting of detection layers 2 exists
Between heating layer 1 and reflecting layer 3, the heating layer 1 by packing material, graphene pulvis, medical stone pulvis, aluminium oxide pulvis and
Epoxy resin is mixed with.
Graphene in heating layer 1 can issue far infrared after being powered, while by the way that medical stone (scientific name: quartz two is added
Long rock), the far infrared of 1000 microns of above wavelength may finally be generated.Far infrared is the beneficial light of a kind of pair of human body,
Human body can be heated when it irradiates human body；Also, it while heating, more having improves micro- human recycle system, rush
Into the physiotherapy functions such as blood circulation and cosmetology.
The effect of aluminium oxide pulvis and medical stone pulvis is the radiation wavelength for increasing far infrared, makes graphene pyrotoxin
The far infrared spectrum radiated is broader.In the particular embodiment, the heating layer 1 includes: to fill out by weight percentage
Fill material 20%-30%, graphene pulvis 10%-20%, medical stone pulvis 1%, aluminium oxide pulvis 1%, epoxy resin 58%.
If it is desired to which the conductivity of heating layer 1 is high, then need to increase the content of graphene pulvis, specifically optional heating layer 1
Constituent be packing material 20%, graphene pulvis 20%, medical stone pulvis 1%, aluminium oxide pulvis 1%, epoxy resin 58%；
If it is desired to which the conductivity of heating layer 1 is low, then need to reduce the dosage of graphene pulvis, the composition of specific optional heating layer 1 at
It is divided into packing material 30%, graphene pulvis 10%, medical stone pulvis 1%, aluminium oxide pulvis 1%, epoxy resin 58%.Certainly, graphite
The specific dosage of alkene pulvis can determine according to actual needs.
The effects of packing material plays filling, adjusts.Preferably, in the present embodiment packing material include sodium tripolyphosphate,
One of calgon and sodium pyrophosphate are a variety of, are the common raw material of industry, are easily obtained and cost is relatively low.For
It is distributed in graphene pulvis preferably everywhere in heating layer 1 in the preparation process of graphene pyrotoxin and issues uniformly
Stable infrared high beam needs to prevent graphene pulvis excessively thick or meticulous.The mesh number for requiring graphene pulvis in the present embodiment is
300 mesh are between 3000 mesh, and heating layer can satisfy the requirement of emitting light and heat of graphene pyrotoxin under this mesh number.
The effect in reflecting layer 3 is that the infrared light for issuing graphene is preferably launched.In the present embodiment, selection it is anti-
Penetrating a layer solid material is glass fabric.The graphene far infrared transmission cloth made in this way can crimp folding.When heating layer 1
After both ends are powered, film will generate heat, and radiation infrared outward by reflecting layer 3.
The effect of detection layers 2 is the heating temperature in order to detect heating layer 1, consequently facilitating to the heating temperature of heating layer 1
It is controlled.In the particular embodiment, detection layers 2 include multiple temperature-sensitive electricity being arranged between heating layer 1 and reflecting layer 3
Resistance.Resistance characteristic based on thermistor can obtain the temperature change of heating layer 1 by the change in resistance of thermistor, and
Which very simple is reliable, and cost is relatively low.Since the appreciable temperature range of single thermistor is limited, such as Fig. 2 institute
Show, thermistor can select suitable array manner to arrange according to the size of its temperature sensing range and heating layer in the present embodiment
It is listed on heating layer.
Further, referring to Fig. 3, temperature-change in resistance of the thermistor for preferred embodiment provided by the invention
Figure.Lines A, B, C are respectively referred to for the thermistor that resistance value under room temperature (25 degrees Celsius) is 10k Ω, 66k Ω, 100k Ω in Fig. 3
Temperature-change in resistance curve.Product orientation based on graphene pyrotoxin is that family uses, it is therefore desirable to limit heating layer 1
Highest heating temperature is 60 hereinafter, the maximum operating temperature for the thermistor that the present embodiment selects is 120 degree centigrade, Ke Yiman
Foot requires.Also, in the particular embodiment, the present invention selects room temperature resistance value for the thermistor of 2.2k Ω.
The present invention also provides a kind of production methods based on above-mentioned graphene pyrotoxin, comprising the following steps:
S100, packing material, graphene pulvis, medical stone pulvis, aluminium oxide pulvis and epoxy resin are mixed to form mixture,
Mixed solution is formed with ball mill stirring mixture；
S200, the upper surface that mixed solution is coated in reflecting layer and detection layers；
S300, mixed solution is toasted using predetermined temperature, mixed solution is made to form the heating layer for being close to reflecting layer and detection layers.
Preferably, in the step s 100, it is preset as 30 minutes, can be sufficiently stirred mixed with the time of ball mill stirring mixture
Object is closed to avoid wasting time again.Step S200 is specially that after paving reflecting layer, thermistor array is placed on reflecting layer,
And after picking out the circuit connecting with thermistor, it is coated on mixed solution to reflecting layer and thermistor.
In step S300, mixed solution can be toasted with 80 degrees Celsius of temperature by electric oven, and toasted
Time may be configured as 40 minutes, and mixed solution is finally made to form the tunic for being close to reflecting layer and detection layers, i.e. heating layer.In film
Both ends be powered, film will generate heat, and radiation infrared outward.
In addition, as shown in figure 4, the present invention also provides a kind of intelligent constant-temperature system, including above-mentioned graphene pyrotoxin (figure
In it is unlabeled), and
Power supply 10；
Power switch 20；
For carrying out thermostatically controlled main control unit 30；
For carrying out the interactive unit 40 of human-computer interaction；
For detecting the human monitoring unit 50 of physical activity；
20 input power 10 of power switch and it is separately connected main control unit 30 and graphene pyrotoxin, main control unit 30 also connects
Connect interactive unit 40 and human testing unit.
Preferably, the microcontroller of STM32 series can be used in main control unit 30, to require high-performance, low based on aiming at
The ARM microcontroller that cost, the Embedded Application of low-power consumption specially design.In order to realize the thermostatic control function of main control unit 30
Can, intelligent constant-temperature system further includes measuring unit (unlabeled in figure), and the measuring unit is separately connected graphene pyrotoxin
Detection layers and main control unit 30.The real time temperature of graphene pyrotoxin can be supplied to main control unit 30 by measuring unit, it is main
The real-time temperature values that unit 30 compares desired temperature and graphene pyrotoxin that interactive unit 40 inputs are controlled, graphene is sent out
The temperature of heat source is adjusted, and maintains the real time temperature of graphene pyrotoxin at set temperature.
Please continue to refer to Fig. 4, in the particular embodiment, measuring unit includes temperature-sensitive electricity in detectable graphene pyrotoxin
Hinder the detection resistance R2 of the electric current of R1.Detection resistance R2 selects resistance value for the precision resistance of 1k Ω, in one end and heating layer 1
One end of thermistor R1 and the AD mouth connection of microcontroller, the other end ground connection of detection resistance R2.Meanwhile in thermistor
The other end of R1 accesses 5V voltage.
When thermistor R1 is by temperature change and when resistance value changes.The voltage value of P point also can be corresponding in entire circuit
It changes.The voltage value of P point can be reduced with the resistance value of thermistor R1 and be reduced；It is on the contrary then increase.CPU is carried out by AD mouthfuls
Analog signal is become digital signal by analog-to-digital conversion, according to the program compiled and edit in advance, so that it may determine the temperature of thermistor R1
It is how many.When thermistor R1 temperature is lower than setting value, CPU can adjust power switch 20, increase supply current；Instead
It, then CPU reduces supply current even cut-off current, to achieve the effect that constant temperature.
Further, the man-machine interaction unit 40 includes liquid crystal display and temperature setting switch.User passes through temperature
Configuration switch sets the thermostat temperature of intelligent constant-temperature system, and is shown on liquid crystal display, realizes the mistake of human-computer interaction
Journey.In addition, man-machine interaction unit 40 may also include the mode tuning of timing unit with timing function, adjustable heating mode
Unit etc., which is not limited by the present invention.
Further, the human monitoring unit 50 includes the Doppler's human body for being mounted on the top of graphene pyrotoxin
Proximity sensor.Doppler emits 10 10.525GHz microwaves human body proximity sensor each second, while receiving echo-signal,
Its principle and radar are similar.All discovery someone activities, including the vibration that sleep breathing is caused, Doppler's man body approaching sensing
Device can monitor.
Therefore, it is monitored by using Doppler's human body proximity sensor, main control unit 30 may determine that interior belongs to
Someone's state or unmanned state.When main control unit 30 is judged as unmanned state, then control intelligent constant-temperature system automatically into
Standby mode and energy-saving mode.And find to be in someone's state, then intelligent constant-temperature system is according to the work shapes of normal operational settings
State works normally.To enable intelligent constant-temperature system automatic open close, is brought convenience to user and save the energy.
Fig. 5-Figure 12 is please referred to, in order to preferably show the technical solution of intelligent constant-temperature system in the present invention, this hair
The bright control circuit schematic diagram for additionally providing main control unit.Main control unit specifically includes CPU, power switch control mouth circuit, passes
Sensor input port circuit and far distance control mouth circuit.
Fig. 5-Fig. 6 is the circuit diagram of the CPU of main control unit in preferred embodiment provided by the invention, wherein master control
For the chip model for the CPU that unit uses for STM32F4, CPU operating voltage is 3.3V.Fig. 7 is preferable implementation provided by the invention
The circuit diagram of power switch control mouth circuit in example, power switch control mouth circuit connection is silicon-controlled or relay, can
The electric current of power switch input is controlled.Fig. 8-Fig. 9 is sensor input port electricity in preferred embodiment provided by the invention
The circuit diagram on road, sensor input circuit mainly connect the thermistor in graphene pyrotoxin.Figure 10-Figure 12 is
The circuit diagram of preferred embodiment medium-long range control interface provided by the invention communicates to connect human body prison by UART
Survey unit, i.e. Doppler's human body proximity sensor.
The component and its connection relationship used about circuit each in Fig. 5-Figure 12, is existing technical solution, and
Related technical personnel can be used existing circuit and be designed replacement, therefore the present invention does not repeat them here this.Master provided by the invention
The characteristics of controlling the control circuit of unit is the heating temperature that can be monitored heating temperature in real time, and maintain graphene pyrotoxin, is made
The heating temperature of graphene pyrotoxin will not be too high and to people of catching fire or scald, will not the too low work to lose heating
With.Also, the fever of graphene pyrotoxin can be automatically closed in it under unmanned state, to reach the mesh of using electricity wisely
's.
In conclusion graphene pyrotoxin provided by the invention, the production method based on it and intelligent constant-temperature system,
In, the graphene pyrotoxin includes heating layer, detection layers and reflecting layer, and the heating layer is bonded reflecting layer, the detection layers
It is arranged between heating layer and reflecting layer, the heating layer is by packing material, graphene pulvis, medical stone pulvis, alumina powder
Agent and epoxy resin are mixed with.Health-care effect is got well and had to the heating effect of graphene pyrotoxin in the present invention, is based on
Its intelligent constant-temperature system can monitor heating temperature in real time, maintain heating temperature at setting value, and can be at nobody
It is automatically closed, achievees the purpose that energy saving under state.
It, can according to the technique and scheme of the present invention and its hair it is understood that for those of ordinary skills
Bright design is subject to equivalent substitution or change, and all these changes or replacement all should belong to the guarantor of appended claims of the invention
Protect range.
Claims (10)
1. a kind of graphene pyrotoxin, which is characterized in that including heating layer, detection layers and reflecting layer, the heating layer fitting is anti-
Layer is penetrated, the detection layers are arranged between heating layer and reflecting layer, and the heating layer is by packing material, graphene pulvis, wheat meal
Mountain flour agent, aluminium oxide pulvis and epoxy resin are mixed with.
2. graphene pyrotoxin according to claim 1, which is characterized in that the heating layer wraps by weight percentage
It includes: packing material 20%-30%, graphene pulvis 10%-20%, medical stone pulvis 1%, aluminium oxide pulvis 1%, epoxy resin 58%.
3. graphene pyrotoxin according to claim 2, which is characterized in that the mesh number of the graphene pulvis is 300 mesh-
3000 mesh.
4. graphene pyrotoxin according to claim 1, which is characterized in that the packing material include sodium tripolyphosphate,
One of calgon and sodium pyrophosphate are a variety of.
5. graphene pyrotoxin according to claim 1, which is characterized in that the detection layers include that multiple array settings exist
Thermistor between heating layer and reflecting layer.
6. a kind of production method of graphene pyrotoxin according to claim 1, which is characterized in that comprising steps of
Packing material, graphene pulvis, medical stone pulvis, aluminium oxide pulvis and epoxy resin are mixed to form mixture, use ball
Grinding machine stirs mixture and forms mixed solution；
Mixed solution is coated in the upper surface in reflecting layer and detection layers；
The heating layer for toasting mixed solution using predetermined temperature, mixed solution being made to form abutting reflecting layer and detection layers.
7. production method according to claim 6, which is characterized in that the predetermined temperature is 80 DEG C.
8. a kind of intelligent constant-temperature system, which is characterized in that including graphene pyrotoxin as described in claim 1, and
Power supply；
Power switch；
For carrying out thermostatically controlled main control unit；
For carrying out the interactive unit of human-computer interaction；
For detecting the human monitoring unit of physical activity；
Power switch input power and it is separately connected main control unit and graphene pyrotoxin, it is single that main control unit is also connected with interaction
Member and human testing unit.
9. intelligent constant-temperature system according to claim 8, which is characterized in that it further include measuring unit, the measuring unit
It is separately connected the detection layers of main control unit and graphene pyrotoxin.
10. intelligent constant-temperature system according to claim 8, which is characterized in that the man-machine interaction unit includes liquid crystal
Display screen and temperature setting switch.
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| CN113388314A (en) * | 2021-06-28 | 2021-09-14 | 广东骏丰频谱股份有限公司 | Far infrared spectrum generator and preparation method thereof |
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