CN105645899A - Graphene oxide silicon based far infrared heating coating and preparation method thereof - Google Patents
Graphene oxide silicon based far infrared heating coating and preparation method thereof Download PDFInfo
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- CN105645899A CN105645899A CN201610043029.7A CN201610043029A CN105645899A CN 105645899 A CN105645899 A CN 105645899A CN 201610043029 A CN201610043029 A CN 201610043029A CN 105645899 A CN105645899 A CN 105645899A
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- C04B20/00—Use of materials as fillers for mortars, concrete or artificial stone according to more than one of groups C04B14/00 - C04B18/00 and characterised by shape or grain distribution; Treatment of materials according to more than one of the groups C04B14/00 - C04B18/00 specially adapted to enhance their filling properties in mortars, concrete or artificial stone; Expanding or defibrillating materials
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Abstract
The invention discloses a graphene oxide silicon based far infrared heating coating and a preparation method thereof. Graphene oxide, nano silicon dioxide, cerium oxide, tremolite, nano-silver-silica core-shell structure, obsidian, hematite, magnalium spinel, medical stone, chlorite, a silica solution, eucalyptus oil, high-alumina bauxite, silicone acrylic emulsion and a defoaming agent serve as raw materials, and the graphene oxide silicon based far infrared heating coating which is environmentally friendly, healthy and high in far infrared heating capacity is prepared through a plasma spraying process.
Description
Technical field
The invention belongs to far infrared heating coatings art, aoxidize silica-based far infrared heating coating and preparation method thereof particularly to a kind of Graphene.
Background technology
Far infrared has stronger penetration and radiant force, has significant temperature control effect and resonance effect, and it is easily absorbed by object and is converted into the interior energy of object. After far infrared is absorbed by the body, internal water can be made to produce resonance, make water molecule activation, strengthen its intermolecular adhesion, thus biomacromolecules such as activation of protein, make biological cell be in the highest vibration level. Owing to biological cell produces resonance effect, far infrared heat energy can being delivered to the subcutaneous deeper part of human body, following deep layer temperature rises, and the warm of generation distributes from inside to outside. This action intensity, makes telangiectasis, blood circulation promoting, strengthens the metabolism between each tissue, increases the regeneration capacity of tissue, improves the immunocompetence of body, regulates the exaltation state of spirit, thus playing the effect of health care. Also there is a lot of far infrared heating material now, such as Far-infrared self heating waist support, Far-infrared self heating waist support, also known as tourmaline self-heating waist support, under the exciting of human body temperature, by shifting the effect of catalyst, thermoinduction material reacts releasing heat in time, and under the amplification of heat energy, far-infrared negative-ion penetrates to the skin depths, the harmful substances such as peroxynitrite decomposition lipid, and get rid of external by urine and sweat, expand blood vessel, blood circulation promoting, activating cell, regulates nerve. The molecular vibration of effectively conversion and the heated material of other energy is absorbed by far-infrared radiation material, and reach purposes such as heating, dry, it have energy-conservation, heat temperature raising is fast, pollution-free, thermal efficiency high, can be widely applied to the aspects such as weaving, printing and dyeing, electromechanics, printing, glass annealing, food processing and health care, civilian cooker, heating system.
Graphene (Graphene) is the two dimensional crystal of the only one layer of atomic thickness being stripped out from graphite material, being made up of carbon atom. Graphene oxide (grapheneoxide) is the oxide of Graphene, and its color is brown color, and product common on the market has Powdered, lamellar and solution shape. After oxidized, on it, oxygen-containing functional group increases and makes character relatively Graphene more active, can improve nature via various with the reaction of oxygen-containing functional group. It has stronger electric conductivity and heat conductivity. Graphene has been widely used in a lot of field, but about the research of graphene-based far infrared heating coating or rather seldom.
Summary of the invention
It is an object of the invention to for the problems referred to above, develop a kind of environmental protection, health, Graphene that far infrared heating ability is strong aoxidize silica-based far infrared heating coating and preparation method thereof.
A kind of Graphene aoxidizes silica-based far infrared heating coating, and this coating includes the raw material of following weight portion:
Graphene oxide 25-35 part;
Nano silicon oxide 25-35 part;
Cerium oxide 10-14 part;
Tremolite 10-14 part;
Nanometer silver-silicon dixoide nucleocapsid structure 1-5 part;
Obsidian 1-5 part;
Bloodstone 1-5 part;
Magnesium aluminate spinel 1-5 part;
Maifanitum 1-5 part;
Chlorite 1-5 part;
Ludox 1-5 part;
Eucalyptus oil 1-5 part;
Alumine 1-5 part;
Silicone acrylic emulsion 1-5 part;
Defoamer 1-5 part;
Described graphene oxide is obtained by being made by method:
Take 2 weight portion flaky graphites and 1 parts by weight of potassium nitrate is added in 85 weight portion concentrated sulphuric acids, the mixture obtained is placed in a reservoir and cooled down in ice-water bath, it is maintained with violent stirring, continues to be slowly added the potassium permanganate of 5 weight portions, obtain the suspension of brown; Add the hydrogen peroxide solution of the 2wt% of 5 weight portions subsequently, obtain jonquilleous suspension; Then wash suspension respectively with deionized water and ethanol, subsequently graphene oxide is dispersed in the extracting solution of Folium olive, stirring mixing 3h at 81 DEG C, it is thus achieved that the graphene oxide that Folium olive extracting solution is modified.
As preferably, this coating includes the raw material of following weight portion:
Graphene oxide 25 parts;
Nano silicon oxide 25 parts;
Cerium oxide 12 parts;
The tremolite 12 parts;
Nanometer silver-silicon dixoide nucleocapsid structure 3 parts;
Obsidian 3 parts;
Bloodstone 3 parts;
Magnesium aluminate spinel 3 parts;
Maifanitum 3 parts;
3 parts of chlorite;
Ludox 3 parts;
Eucalyptus oil 3 parts;
Alumine 3 parts;
Silicone acrylic emulsion 3 parts;
Defoamer 3 parts.
As preferably, described defoamer is polydimethylsiloxane.
A kind of method preparing the above-mentioned Graphene silica-based far infrared heating coating of oxidation, comprises the steps:
(1) aoxidize silica-based far infrared heating coating material composition according to Graphene and carry out dispensing; By raw material mixing wet ball-milling 12 hours, solvent was distilled water, and abrading-ball is silicon oxide abrading-ball, dries, obtain standby material after ball milling at 45 DEG C;
(2) by substrate pretreatment according to demand; Being applied in pretreated substrate by standby material plasma spray subsequently, can obtain Graphene and aoxidize silica-based far infrared heating coating, the thickness of coating is 1-25mm.
Beneficial effects of the present invention:
(1) present invention adopts graphene oxide, nano silicon oxide, cerium oxide, the tremolite, nanometer silver-silicon dixoide nucleocapsid structure, obsidian, bloodstone, magnesium aluminate spinel, Maifanitum, chlorite, Ludox, eucalyptus oil, alumine, silicone acrylic emulsion and defoamer to be raw material, main component therein is graphene oxide and nano silicon oxide, graphene oxide is the graphene oxide that Folium olive extracting solution is modified, this Graphene is except the function with far infrared heating, also there is effect of health environment-friendly, useful for human body; And the compound use of graphene oxide and nano silicon oxide, the two collaborative far infrared heating effect that strengthens;
(2) in order to optimize the performance of far infrared heating further, have selected cerium oxide, the tremolite, nanometer silver-silicon dixoide nucleocapsid structure, obsidian, bloodstone, magnesium aluminate spinel, Maifanitum, chlorite, Ludox, eucalyptus oil, alumine, silicone acrylic emulsion and defoamer is auxiliary element, these adjuvants, together with graphene oxide and nano silicon oxide, work in coordination with the far infrared heating performance strengthening coating. Such as the component such as nanometer silver-silicon dixoide nucleocapsid structure also has the effect of sterilizing;The infrared emissivity of coating prepared by the present invention has exceeded 99.2%.
(4) the silica-based far infrared heating preparation technology of coating of this Graphene oxidation is simple, it is easy to industrialization, and raw material sources are extensive, is highly suitable to be applied for producing.
Detailed description of the invention
Below in conjunction with specific embodiment, and with reference to data, the present invention is described in further detail. Should be understood that these embodiments present invention solely for the purpose of illustration, but not the scope being intended to limit the present invention in any manner.
Embodiment 1:
A kind of Graphene aoxidizes silica-based far infrared heating coating, and this coating includes the raw material of following weight portion:
Graphene oxide 25 parts;
Nano silicon oxide 25 parts;
Cerium oxide 12 parts;
The tremolite 12 parts;
Nanometer silver-silicon dixoide nucleocapsid structure 3 parts;
Obsidian 3 parts;
Bloodstone 3 parts;
Magnesium aluminate spinel 3 parts;
Maifanitum 3 parts;
3 parts of chlorite;
Ludox 3 parts;
Eucalyptus oil 3 parts;
Alumine 3 parts;
Silicone acrylic emulsion 3 parts;
Defoamer 3 parts;
Described graphene oxide is obtained by being made by method:
Take 2 weight portion flaky graphites and 1 parts by weight of potassium nitrate is added in 85 weight portion concentrated sulphuric acids, the mixture obtained is placed in a reservoir and cooled down in ice-water bath, it is maintained with violent stirring, continues to be slowly added the potassium permanganate of 5 weight portions, obtain the suspension of brown; Add the hydrogen peroxide solution of the 2wt% of 5 weight portions subsequently, obtain jonquilleous suspension; Then wash suspension respectively with deionized water and ethanol, subsequently graphene oxide is dispersed in the extracting solution of Folium olive, stirring mixing 3h at 81 DEG C, it is thus achieved that the graphene oxide that Folium olive extracting solution is modified.
Described defoamer is polydimethylsiloxane.
A kind of method preparing the above-mentioned Graphene silica-based far infrared heating coating of oxidation, comprises the steps:
(1) aoxidize silica-based far infrared heating coating material composition according to Graphene and carry out dispensing; By raw material mixing wet ball-milling 12 hours, solvent was distilled water, and abrading-ball is silicon oxide abrading-ball, dries, obtain standby material after ball milling at 45 DEG C;
(2) by substrate pretreatment according to demand; Being applied in pretreated substrate by standby material plasma spray subsequently, can obtain Graphene and aoxidize silica-based far infrared heating coating, the thickness of coating is 10mm. The far infrared transmissivity of this coating is 99.4%.
Embodiment 2:
A kind of Graphene aoxidizes silica-based far infrared heating coating, and this coating includes the raw material of following weight portion:
Graphene oxide 25 parts;
Nano silicon oxide 25 parts;
Cerium oxide 14 parts;
The tremolite 14 parts;
Nanometer silver-silicon dixoide nucleocapsid structure 1 part;
Obsidian 1 part;
Bloodstone 1 part;
Magnesium aluminate spinel 1 part;
Maifanitum 1 part;
1 part of chlorite;
Ludox 1 part;
Eucalyptus oil 1 part;
Alumine 1 part;
Silicone acrylic emulsion 1 part;
Defoamer 1 part;
Described graphene oxide is obtained by being made by method:
Take 2 weight portion flaky graphites and 1 parts by weight of potassium nitrate is added in 85 weight portion concentrated sulphuric acids, the mixture obtained is placed in a reservoir and cooled down in ice-water bath, it is maintained with violent stirring, continues to be slowly added the potassium permanganate of 5 weight portions, obtain the suspension of brown; Add the hydrogen peroxide solution of the 2wt% of 5 weight portions subsequently, obtain jonquilleous suspension; Then wash suspension respectively with deionized water and ethanol, subsequently graphene oxide is dispersed in the extracting solution of Folium olive, stirring mixing 3h at 81 DEG C, it is thus achieved that the graphene oxide that Folium olive extracting solution is modified.
Described defoamer is polydimethylsiloxane.
A kind of method preparing the above-mentioned Graphene silica-based far infrared heating coating of oxidation, comprises the steps:
(1) aoxidize silica-based far infrared heating coating material composition according to Graphene and carry out dispensing; By raw material mixing wet ball-milling 12 hours, solvent was distilled water, and abrading-ball is silicon oxide abrading-ball, dries, obtain standby material after ball milling at 45 DEG C;
(2) by substrate pretreatment according to demand; Being applied in pretreated substrate by standby material plasma spray subsequently, can obtain Graphene and aoxidize silica-based far infrared heating coating, the thickness of coating is 15mm. The far infrared transmissivity of this coating is 99.3%.
Embodiment 3:
A kind of Graphene aoxidizes silica-based far infrared heating coating, and this coating includes the raw material of following weight portion:
Graphene oxide 25 parts;
Nano silicon oxide 25 parts;
Cerium oxide 14 parts;
The tremolite 14 parts;
Nanometer silver-silicon dixoide nucleocapsid structure 2 parts;
Obsidian 2 parts;
Bloodstone 2 parts;
Magnesium aluminate spinel 2 parts;
Maifanitum 2 parts;
2 parts of chlorite;
Ludox 2 parts;
Eucalyptus oil 2 parts;
Alumine 2 parts;
Silicone acrylic emulsion 2 parts;
Defoamer 2 parts;
Described graphene oxide is obtained by being made by method:
Take 2 weight portion flaky graphites and 1 parts by weight of potassium nitrate is added in 85 weight portion concentrated sulphuric acids, the mixture obtained is placed in a reservoir and cooled down in ice-water bath, it is maintained with violent stirring, continues to be slowly added the potassium permanganate of 5 weight portions, obtain the suspension of brown; Add the hydrogen peroxide solution of the 2wt% of 5 weight portions subsequently, obtain jonquilleous suspension; Then wash suspension respectively with deionized water and ethanol, subsequently graphene oxide is dispersed in the extracting solution of Folium olive, stirring mixing 3h at 81 DEG C, it is thus achieved that the graphene oxide that Folium olive extracting solution is modified.
Described defoamer is polydimethylsiloxane.
A kind of method preparing the above-mentioned Graphene silica-based far infrared heating coating of oxidation, comprises the steps:
(1) aoxidize silica-based far infrared heating coating material composition according to Graphene and carry out dispensing; By raw material mixing wet ball-milling 12 hours, solvent was distilled water, and abrading-ball is silicon oxide abrading-ball, dries, obtain standby material after ball milling at 45 DEG C;
(2) by substrate pretreatment according to demand; Being applied in pretreated substrate by standby material plasma spray subsequently, can obtain Graphene and aoxidize silica-based far infrared heating coating, the thickness of coating is 12mm. The far infrared transmissivity of this coating is 99.5%.
Embodiment 4:
A kind of Graphene aoxidizes silica-based far infrared heating coating, and this coating includes the raw material of following weight portion:
Graphene oxide 35 parts;
Nano silicon oxide 35 parts;
Cerium oxide 10 parts;
The tremolite 10 parts;
Nanometer silver-silicon dixoide nucleocapsid structure 3 parts;
Obsidian 2 parts;
Bloodstone 2 parts;
Magnesium aluminate spinel 3 parts;
Maifanitum 2 parts;
2 parts of chlorite;
Ludox 2 parts;
Eucalyptus oil 2 parts;
Alumine 3 parts;
Silicone acrylic emulsion 2 parts;
Defoamer 3 parts;
Described graphene oxide is obtained by being made by method:
Take 2 weight portion flaky graphites and 1 parts by weight of potassium nitrate is added in 85 weight portion concentrated sulphuric acids, the mixture obtained is placed in a reservoir and cooled down in ice-water bath, it is maintained with violent stirring, continues to be slowly added the potassium permanganate of 5 weight portions, obtain the suspension of brown; Add the hydrogen peroxide solution of the 2wt% of 5 weight portions subsequently, obtain jonquilleous suspension; Then wash suspension respectively with deionized water and ethanol, subsequently graphene oxide is dispersed in the extracting solution of Folium olive, stirring mixing 3h at 81 DEG C, it is thus achieved that the graphene oxide that Folium olive extracting solution is modified.
Described defoamer is polydimethylsiloxane.
A kind of method preparing the above-mentioned Graphene silica-based far infrared heating coating of oxidation, comprises the steps:
(1) aoxidize silica-based far infrared heating coating material composition according to Graphene and carry out dispensing; By raw material mixing wet ball-milling 12 hours, solvent was distilled water, and abrading-ball is silicon oxide abrading-ball, dries, obtain standby material after ball milling at 45 DEG C;
(2) by substrate pretreatment according to demand; Being applied in pretreated substrate by standby material plasma spray subsequently, can obtain Graphene and aoxidize silica-based far infrared heating coating, the thickness of coating is 16mm. The far infrared transmissivity of this coating is 99.6%.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, and when without departing substantially from the spirit of the present invention or basic feature, it is possible to realize the present invention in other specific forms. Therefore, no matter from which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the invention rather than described above limits, it is intended that all changes in the implication of the equivalency dropping on claim and scope included in the present invention.
In addition, it is to be understood that, although this specification is been described by according to embodiment, but not each embodiment only comprises an independent technical scheme, this narrating mode of description is only for clarity sake, description should be made as a whole by those skilled in the art, and the technical scheme in each embodiment through appropriately combined, can also form other embodiments that it will be appreciated by those skilled in the art that.
Claims (4)
1. a Graphene aoxidizes silica-based far infrared heating coating, it is characterised in that: this coating includes the raw material of following weight portion:
Graphene oxide 25-35 part;
Nano silicon oxide 25-35 part;
Cerium oxide 10-14 part;
Tremolite 10-14 part;
Nanometer silver-silicon dixoide nucleocapsid structure 1-5 part;
Obsidian 1-5 part;
Bloodstone 1-5 part;
Magnesium aluminate spinel 1-5 part;
Maifanitum 1-5 part;
Chlorite 1-5 part;
Ludox 1-5 part;
Eucalyptus oil 1-5 part;
Alumine 1-5 part;
Silicone acrylic emulsion 1-5 part;
Defoamer 1-5 part;
Described graphene oxide is obtained by being made by method:
Take 2 weight portion flaky graphites and 1 parts by weight of potassium nitrate is added in 85 weight portion concentrated sulphuric acids, the mixture obtained is placed in a reservoir and cooled down in ice-water bath, it is maintained with violent stirring, continues to be slowly added the potassium permanganate of 5 weight portions, obtain the suspension of brown; Add the hydrogen peroxide solution of the 2wt% of 5 weight portions subsequently, obtain jonquilleous suspension; Then wash suspension respectively with deionized water and ethanol, subsequently graphene oxide is dispersed in the extracting solution of Folium olive, stirring mixing 3h at 81 DEG C, it is thus achieved that the graphene oxide that Folium olive extracting solution is modified.
2. a Graphene as claimed in claim 2 aoxidizes silica-based far infrared heating coating, it is characterised in that:
This coating includes the raw material of following weight portion:
Graphene oxide 25 parts;
Nano silicon oxide 25 parts;
Cerium oxide 12 parts;
The tremolite 12 parts;
Nanometer silver-silicon dixoide nucleocapsid structure 3 parts;
Obsidian 3 parts;
Bloodstone 3 parts;
Magnesium aluminate spinel 3 parts;
Maifanitum 3 parts;
3 parts of chlorite;
Ludox 3 parts;
Eucalyptus oil 3 parts;
Alumine 3 parts;
Silicone acrylic emulsion 3 parts;
Defoamer 3 parts.
3. a Graphene as claimed in claim 1 or 2 aoxidizes silica-based far infrared heating coating, it is characterised in that: described defoamer is polydimethylsiloxane.
4. prepare the method that Graphene as claimed in claim 1 aoxidizes silica-based far infrared heating coating for one kind, it is characterised in that: comprise the steps:
(1) aoxidize silica-based far infrared heating coating material composition according to Graphene and carry out dispensing; By raw material mixing wet ball-milling 12 hours, solvent was distilled water, and abrading-ball is silicon oxide abrading-ball, dries, obtain standby material after ball milling at 45 DEG C;
(2) by substrate pretreatment according to demand; Being applied in pretreated substrate by standby material plasma spray subsequently, can obtain Graphene and aoxidize silica-based far infrared heating coating, the thickness of coating is 1-25mm.
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| CN108030585A (en) * | 2018-01-24 | 2018-05-15 | 南通大学附属医院 | A kind of gynemetrics's special-purpose plaster pad and preparation method thereof |
| CN108892495A (en) * | 2018-08-08 | 2018-11-27 | 陕西新容康医疗器械有限公司 | A kind of clay granular materials and preparation method thereof that can generate far infrared |
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| CN108892495A (en) * | 2018-08-08 | 2018-11-27 | 陕西新容康医疗器械有限公司 | A kind of clay granular materials and preparation method thereof that can generate far infrared |
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