CN1931936A - Fuctional paint composition and its production process - Google Patents

Fuctional paint composition and its production process Download PDF

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Publication number
CN1931936A
CN1931936A CN 200610150709 CN200610150709A CN1931936A CN 1931936 A CN1931936 A CN 1931936A CN 200610150709 CN200610150709 CN 200610150709 CN 200610150709 A CN200610150709 A CN 200610150709A CN 1931936 A CN1931936 A CN 1931936A
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fuctional
paint composition
charcoal powder
agent
emulsion
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栗忠原
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Abstract

The present invention is one functional paint composition with the functions of adsorbing harmful gas, regulating humidity, deodorizing, radiating far infrared ray and generating negative ion. It features the composition comprising water-thinned polymer emulsion, charcoal powder and tourmaline particle.

Description

Fuctional paint composition and manufacture method thereof
Technical field
The present invention relates to Fuctional paint composition, the Fuctional paint composition of metope undercoat in being specifically related to be used for, it has functions such as absorption obnoxious flavour, damping, deodorizing, far infrared radiation and negative ion generation, also relates to the manufacture method of this coating composition.
Background technology
Latex coating is a requisite material in the modern Interior fitting-up, and is along with the raising of living standards of the people, also more and more diversified for the requirement of indoor paint.Not only require safety and quality, but also require to have additional function as much as possible.
For example, the various toxic volatile chemical substances that the interior decoration finishing material tends to produce, electromagnetic radiation, offending smell etc., this healthy existence to people greatly endangers.In order to address this problem, researched and developed the functional paint that is added with wood charcoal powder with adsorption function and/or nourishing function.
Charcoal is the sorbing material of using always, it has that specific surface area is big, high adsorption capacity and cheap advantage, wherein, especially bamboo charcoal is more and more paid attention to, this be because bamboo charcoal not only adsorptive power be more than 10 times of general charcoal, but also have that far infrared radiation, hertzian wave intercept and nourishing functions such as negative ion generation.Wood charcoal powder introduced has become the main path that preparation has the absorption and the functional paint of nourishing function in the coating.
Japanese patent gazette spy opens flat 11-29742 and discloses a kind of concurrent coating composition of waving the peculiar function of charcoal of charcoal powder that contains.Japanese patent gazette 2002-302635 discloses a kind of water-borne coatings with absorption property, and it adds charcoal powder and medical stone in water-base resin coating, make gained coating possess good distribution stability and high ductility.Japanese patent gazette 2003-336374 discloses a kind of paint for wall that comprises framework material, bamboo charcoal, tackiness agent and tinting material, and it has absorption and nourishing function.Chinese patent CN1733852A discloses a kind of charcoal base latex coating that is used for coat plastics film, paper etc. and is used for the silk screen printing of non-woven fabrics, film etc.Chinese patent CN1386804A discloses a kind of charcoal health paint, and it has the function of improving indoor environment.
Above prior art all relates to the functional paint of introducing the charcoal powder, and its purpose all is that coating is combined with the characteristic property of charcoal, to obtain having the composite coating of functions such as absorption obnoxious flavour, damping, deodorizing, health care.Yet, in the existing capability coating that adds wood charcoal powder, there are some problems, the one, because wood charcoal powder is that porosity and looseness material and general particle diameter are bigger, its continuity and compactness influence for emulsion film forming is bigger, thereby causes coating to become film toughness to decline to a great extent; The 2nd, ventilative usually relatively poor after the resin emulsion film forming in the coating with water vapour permeability, thereby greatly reduce the original adsorptive power of charcoal powder, thereby must strengthen the wood charcoal powder consumption in order to reach certain adsorption effect, this has further reduced the coating quality of forming film again conversely.
In addition, tourmalinite be a kind of be the silicate minerals of feature with the boracic.Its chemical general formula: XY 3Z 6[Si 6O 18] [BO 3] 3W 4(X is mainly Na +, Ca 2+, K +Y is mainly Mg 2+, Fe 3+, Al 3+W is mainly O -, OH -, F -).Tourmalinite has piezoelectricity, pyroelectricity, ir signature and adsorptivity, but and because the adsorbed water of surface electrostatic field height electrolysis, thereby produce the negative ion useful to HUMAN HEALTH.In healthcare field, tourmalinite is except increasing airborne negative oxygen ion number by the airborne water of electrolysis, the absorbable ir radiation consistent wavelength of the ir radiation wavelength of its generation and human body can be absorbed by human body, produces the reason heat effect, tissue temperature is raise, vasodilation, blood flow quickens, and local blood circulation improves, form the function of health-care physical therapy, have the wound healing of promotion, inflammation contraction, remove effects such as muscle spasm and analgesia.
The inventor finds to introduce wood charcoal powder and tourmaline particle simultaneously in resin emulsion, so both can work in coordination with performance absorption, far-infrared radiation and negative ion generating function that the two had, and can also effectively improve ventilation property, the water vapour permeability of coating and become film toughness simultaneously.
Summary of the invention
In order to solve an above-mentioned difficult problem of the prior art, the inventor finds to add simultaneously in resin emulsion wood charcoal powder and tourmaline particle can improve breathing freely of emulsion film forming greatly and thereby water vapour permeability can reduce the wood charcoal powder consumption, and improve the one-tenth film toughness of coating, strengthen the far-infrared radiation intensity and the negative ion incidence of gained functional paint simultaneously greatly.
The invention provides a kind of Fuctional paint composition, it comprises aqueous polymer emulsion, wood charcoal powder and tourmaline particle.
In Fuctional paint composition of the present invention, employed wood charcoal powder is selected from activity charcoal powder, low temperature bamboo charcoal powder, middle temperature bamboo charcoal powder, high temperature bamboo charcoal powder and combination thereof.In a preferred embodiment of the invention, wood charcoal powder is selected from the high temperature bamboo charcoal powder, i.e. the long powdered carbon of Bei.
Wherein, the particle size range of employed wood charcoal powder is 1 μ m-300 μ m, and the preferable particle size scope is 30 μ m-100 μ m.
In the Fuctional paint composition in the present invention, employed tourmaline particle is to be selected from magnesium iron elbaite, tsilaisite, uvite and the buergerite tourmaline particle of one at least, is preferably the tourmalinite nano particle.
In embodiments of the invention, the particle size range of described tourmaline particle is 20nm-100 μ m, and the preferable particle size scope is 50nm-30 μ m, more preferably 100nm-10 μ m.
Aqueous polymer emulsion in the Fuctional paint composition of the present invention is selected from benzene emulsion, acrylic ester emulsion, pure-acrylic emulsion, organosilicon crylic acid latex, polyurethane-acrylate copolymer emulsion and fluoropolymer emulsion.
In one embodiment of the invention, Fuctional paint composition of the present invention comprises the aqueous polymer emulsion of 50-95wt%, the wood charcoal powder of 5-50wt% and the tourmaline particle of 1-15wt%, aqueous polymer emulsion, the wood charcoal powder of 10-30wt% and the tourmaline particle of 2-10wt% of preferred 60-90wt%.
Fuctional paint composition of the present invention can also comprise processing aid, and this processing aid is selected from dispersion agent, weighting agent, thickening material, tackiness agent, defoamer, wetting agent, film coalescence aid, softening agent, stablizer, anti-aging agent, fire retardant, sanitas, antiseptic-germicide, UV light absorber, synthon and combination thereof.
The consumption of described processing aid is below the 50wt%, preferably is not higher than 40wt%, more preferably below the 35wt%, is benchmark with the weight of final coating composition.
Described thickening material is selected from high-shear thickening material, middle shear thickening agent, low shear thickening agent and combination thereof, and wherein this thickening material is polyacrylic acid sodium salt or ammonium polyacrylate salt.
Described defoamer is selected from mineral oil, organosilicon and composition thereof.
Membrane-forming agent is selected from alkyd 12.
Weighting agent is selected from diatomite, kaolin, talcum powder, lime carbonate, magnesiumcarbonate, vermiculite, silicon-dioxide etc.
The present invention also provides a kind of method for preparing Fuctional paint composition, comprises the wood charcoal powder and the tourmaline particle that are pre-mixed predetermined amount; Then evenly sneak into it in aqueous polymer emulsion; And add the processing aid of predetermined amount and mix.
The undercoat of metope in Fuctional paint composition of the present invention is preferably used as.
Embodiment
Embodiment
Among the present invention employed various raw materials be commercial, wherein wood charcoal powder, tourmaline particle and medical stone granule: available from Tianjin China through nanosecond science and technology company limited.
Embodiment 1
Prescription according to table 1, to mix in activity charcoal powder and magnesium iron elbaite (schorl) the particle adding suitable quantity of water in advance, then in the mixing vessel of band whipping appts, slowly add activity charcoal powder and schorl particulate suspension in the emulsion, opened the agitator stirring at low speed 1 hour, described mixture is fully disperseed in emulsion, then each processing aid is mixed the back with suitable quantity of water and add in the gained emulsion mixture, continue to stir 2 hours.Water is regulated gained coating composition viscosity to 35-40cP.
Table 1
Raw material Specification Consumption (kg)
Water 400
Benzene emulsion 7199 200
Wetting agent PE-100 1
Defoamer NXZ 2
Defoamer 154 2
Membrane-forming agent TXL 8
The high-shear thickening material DR-73 2
Middle shear thickening agent DR-1 6
Low shear thickening agent ASE60 5
Kaolin 100
Talcum powder 150
Dispersion agent 5040 4
Ethylene glycol 80
Activity charcoal powder 5 μ m particle diameters 100
Tourmaline particle 0.4 μ m particle diameter 50
Add up to 1110
The coating composition of embodiment 1 can utilize ordinary method constructions such as roller coat, brushing, spraying, but Air drying or oven dry under 60 ℃, and coating thickness is about 50 μ m-200 μ m.
Embodiment 2
According to the prescription of table 2, according to the method preparation of embodiment 1.
Table 2
Raw material Specification Consumption (kg)
Water 400
Benzene emulsion R-501 200
Wetting agent PE-100 1
Defoamer NXZ 2
Defoamer 154 2
Membrane-forming agent TXL 8
The high-shear thickening material DR-73 2
Middle shear thickening agent DR-1 6
Low shear thickening agent ASE60 5
Kaolin 100
Talcum powder 150
Dispersion agent 5040 4
Ethylene glycol 80
The long powdered carbon of Bei 30 μ m particle diameters 100
Tourmaline particle 0.4 μ m particle diameter 50
Add up to 1110
Embodiment 3
According to the prescription of table 3, according to the method preparation of embodiment 1.
Table 3
Raw material Specification Consumption (kg)
Water 400
Pure-acrylic emulsion 7199 200
Wetting agent PE-100 1
Defoamer NXZ 2
Defoamer 154 2
Membrane-forming agent TXL 8
The high-shear thickening material DR-73 2
Middle shear thickening agent DR-1 6
Low shear thickening agent ASE60 5
Kaolin 100
Talcum powder 150
Dispersion agent 5040 4
Ethylene glycol 80
In warm bamboo charcoal powder 30 μ m particle diameters 100
Tourmaline particle 0.4 μ m particle diameter 50
Add up to 1110
Embodiment 4
According to the prescription of table 4, according to the method preparation of embodiment 1.
Table 4
Raw material Specification Consumption (kg)
Water 400
Pure-acrylic emulsion 7199 200
Wetting agent PE-100 1
Defoamer NXZ 2
Defoamer 154 2
Membrane-forming agent TXL 8
The high-shear thickening material DR-73 2
Middle shear thickening agent DR-1 6
Low shear thickening agent ASE60 5
Kaolin 100
Talcum powder 150
Dispersion agent 5040 4
Ethylene glycol 80
The low temperature bamboo charcoal powder 30 μ m particle diameters 100
Tourmaline particle 0.4 μ m particle diameter 50
Add up to 1110
Embodiment 5
According to the prescription of table 5, according to the method preparation of embodiment 1.
Table 5
Raw material Specification Consumption (kg)
Water 400
Benzene emulsion 7199 200
Wetting agent PE-100 1
Defoamer NXZ 2
Defoamer 154 2
Membrane-forming agent TXL 8
The high-shear thickening material DR-73 2
Middle shear thickening agent DR-1 6
Low shear thickening agent ASE60 5
Kaolin 100
Talcum powder 150
Dispersion agent 5040 4
Ethylene glycol 80
Activity charcoal powder 5 μ m particle diameters 100
Tourmaline particle 10 μ m particle diameters 50
Add up to 1110
The comparative example 1
According to the prescription of table 6, wood charcoal powder and benzene emulsion are mixed, sneak into various processing aids subsequently, water is regulated viscosity and pH.
Table 6
Raw material Specification Consumption (kg)
Water 400
Benzene emulsion 7199 200
Wetting agent PE-100 1
Defoamer NXZ 2
Defoamer 154 2
Membrane-forming agent TXL 8
The high-shear thickening material DR-73 2
Middle shear thickening agent DR-1 6
Low shear thickening agent ASE60 5
Kaolin 100
Talcum powder 150
Dispersion agent 5040 4
Ethylene glycol 80
Activity charcoal powder 5 μ m particle diameters 200
Add up to 1160
The comparative example 2
According to the prescription of table 7, tourmaline particle and benzene emulsion are mixed, sneak into various processing aids subsequently, water is regulated viscosity and pH.
Table 7
Raw material Specification Consumption (kg)
Water 400
Benzene emulsion 7199 200
Wetting agent PE-100 1
Defoamer NXZ 2
Defoamer 154 2
Membrane-forming agent TXL 8
The high-shear thickening material DR-73 2
Middle shear thickening agent DR-1 6
Low shear thickening agent ASE60 5
Kaolin 100
Talcum powder 150
Dispersion agent 5040 4
Ethylene glycol 80
Tourmaline particle 0.4 μ m particle diameter 200
Add up to 1160
The comparative example 3
According to the prescription of table 8, according to the method preparation of embodiment 1.
Table 8
Raw material Specification Consumption (kg)
Water 400
Benzene emulsion 7199 200
Wetting agent PE-100 1
Defoamer NXZ 2
Defoamer 154 2
Membrane-forming agent TXL 8
The high-shear thickening material DR-73 2
Middle shear thickening agent DR-1 6
Low shear thickening agent ASE60 5
Kaolin 100
Talcum powder 150
Dispersion agent 5040 4
Ethylene glycol 80
Activity charcoal powder 5 μ m particle diameters 200
Medical stone granule: 100 μ m particle diameters 50
Add up to 1210
Test implementation example 1
On the cement plate of 6 * 5cm, coating thickness is about 50 μ m, 60 ℃ of following flash bakings with above each embodiment and comparative example's coating composition separate application.The plate that scribbles the coating composition of each embodiment is placed the absorption test box, and test the adsorption rate of the coating composition of each embodiment under the same conditions for formaldehyde, benzene and hydrogen sulfide.The results are shown in the table 9.
Table 9
Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5 The comparative example 1 The comparative example 2 The comparative example 3
Formaldehyde ＞99％ ＞99％ ＞99％ ＞99％ ＞99％ ＞99％ 80％ ＞99％
Benzene ＞99％ ＞99％ ＞99％ ＞99％ ＞99％ ＞99％ 71％ ＞99％
Hydrogen sulfide ＞99％ ＞99％ ＞99％ ＞99％ ＞99％ ＞99％ 90％ ＞99％
By table 9 as seen, the adsorption rate of embodiment 1-4 and comparative example 1 and 3 is all fine, and comparative example 2 adsorption rate is lower.Obviously, use tourmalinite can not obtain the good adsorption effect separately.
Test implementation example 2
Each embodiment and comparative example's coating composition is coated on the sheet glass that scribbles remover in advance, forms essentially identical coating thickness, take off gained after the oven dry and film, carry out Mechanics Performance Testing, that its result is divided into is excellent, good, medium, differ from four grades.The result is as shown in table 9.
Table 9
Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5 The comparative example 1 The comparative example 2 The comparative example 3
Tensile strength Excellent Excellent Excellent Excellent Very Medium Very Medium
Elongation at break Excellent Excellent Excellent Excellent Very Relatively poor Very Excellent
As seen, mechanical property the best of filming of embodiment 1-4, not only tensile strength height, and elongation at break is also high.
Test implementation example 3
To the measurement that lamina membranacea carries out far-infrared radiation intensity and negative ion incidence that is coated with of each embodiment and comparative example's coating composition, its result is divided into excellent, good, medium, weak four grades.The result is as shown in table 10.
Table 10
Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5 The comparative example 1 The comparative example 2 The comparative example 3
Far-infrared radiation intensity Medium Excellent Very Very Excellent A little less than Very Very
The negative ion incidence Very Excellent Very Very Excellent A little less than Very Medium
By table 10 as seen, embodiment 2 and 5 the far-infrared radiation intensity and the negative ion incidence of filming are the highest, and embodiment 1,3,4 all is higher than comparative example 1-3.
The present invention is not limited to the foregoing description, the scope that these embodiment do not limit the present invention in any way.Any change that those skilled in the art have done within the scope of the claims and adjust also should be thought and belongs to scope of the present invention.

Claims (15)

1. Fuctional paint composition, it has absorption obnoxious flavour, damping, deodorizing, far infrared radiation and negative ion generating function, it is characterized in that comprising aqueous polymer emulsion, wood charcoal powder and tourmaline particle.
2. the Fuctional paint composition of claim 1 is characterized in that described Fuctional paint composition comprises the tourmaline particle of wood charcoal powder and the 1-15wt% of the aqueous polymer emulsion of 50-95wt%, 5-50wt%.
3. the Fuctional paint composition of claim 1 is characterized in that described Fuctional paint composition comprises the tourmaline particle of wood charcoal powder and the 2-10wt% of the aqueous polymer emulsion of 60-90wt%, 10-30wt%.
4. any one Fuctional paint composition among the claim 1-3 is characterized in that described wood charcoal powder is selected from activity charcoal powder, low temperature bamboo charcoal powder, middle temperature bamboo charcoal powder, high temperature bamboo charcoal powder and combination thereof.
5. the Fuctional paint composition of claim 4, the particle size range that it is characterized in that described wood charcoal powder is 1 μ m-300 μ m.
6. the Fuctional paint composition of claim 5, the particle size range that it is characterized in that described wood charcoal powder is 30 μ m-100 μ m.
7. any one Fuctional paint composition among the claim 1-3 is characterized in that described tourmaline particle is to be selected from magnesium iron elbaite, tsilaisite, uvite and the buergerite tourmaline particle of one at least.
8. the Fuctional paint composition of claim 7, the particle size range that it is characterized in that described tourmaline particle is 20nm-100 μ m.
9. the Fuctional paint composition of claim 8, the particle size range that it is characterized in that described tourmaline particle is 100nm-10 μ m.
10. any one Fuctional paint composition among the claim 1-3 is characterized in that described aqueous polymer emulsion is selected from benzene emulsion, acrylic ester emulsion, pure-acrylic emulsion, organosilicon crylic acid latex, polyurethane-acrylate copolymer emulsion and fluoropolymer emulsion.
11. any one Fuctional paint composition among the claim 1-3, it can also comprise processing aid, and this processing aid is selected from dispersion agent, weighting agent, thickening material, tackiness agent, defoamer, wetting agent, film coalescence aid, softening agent, stablizer, anti-aging agent, fire retardant, sanitas, antiseptic-germicide, UV light absorber, synthon and combination thereof.
12. the Fuctional paint composition of claim 11 is characterized in that described thickening material is selected from high-shear thickening material, middle shear thickening agent, low shear thickening agent and combination thereof.
13. the Fuctional paint composition of claim 12 is characterized in that described thickening material is polyacrylic acid sodium salt or ammonium polyacrylate salt.
14. a method for preparing Fuctional paint composition comprises the wood charcoal powder and the tourmaline particle that are pre-mixed predetermined amount; Then evenly sneak into it in aqueous polymer emulsion; And add the processing aid of predetermined amount and mix.
The purposes of metope undercoat in 15. the Fuctional paint composition of claim 1 is used for.
CN 200610150709 2006-10-24 2006-10-24 Fuctional paint composition and its production process Pending CN1931936A (en)

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CN101974285A (en) * 2010-09-30 2011-02-16 江苏大象东亚制漆有限公司 Long-acting antibacterial polyurethane water-based wood paint composition
CN102304244A (en) * 2011-07-21 2012-01-04 惠州市鼎晨新材料有限公司 Bamboo plastic plate
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CN102304244A (en) * 2011-07-21 2012-01-04 惠州市鼎晨新材料有限公司 Bamboo plastic plate
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CN105669158A (en) * 2016-01-23 2016-06-15 王秋芹 Graphene far-infrared heating coating and preparation method thereof
CN105645899A (en) * 2016-01-23 2016-06-08 王秋芹 Graphene oxide silicon based far infrared heating coating and preparation method thereof
CN105803857A (en) * 2016-03-31 2016-07-27 自贡市华尔美科技有限公司 Environment-friendly wallpaper
CN108611869A (en) * 2017-01-19 2018-10-02 刘定安 Fibrofelt, plank and preparation method thereof
CN106752154A (en) * 2017-03-30 2017-05-31 深圳市赛玛仕科技有限公司 A kind of negative oxygen ion activated carbon
CN108003672A (en) * 2017-11-21 2018-05-08 广西武宣金牌防水材料科技有限公司 A kind of flame retardant type water-repellent paint used for building exterior wall and its production method
CN108914617A (en) * 2018-05-29 2018-11-30 太仓绒彩纺织品有限公司 A kind of textile fabric anti-static coatings
CN110670830A (en) * 2019-10-14 2020-01-10 广州市星乐家具有限公司 Customized environment-friendly veneer and manufacturing method thereof

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