CN105747270A - Electronic cigarette liquid and preparation method thereof - Google Patents
Electronic cigarette liquid and preparation method thereof Download PDFInfo
- Publication number
- CN105747270A CN105747270A CN201610163470.9A CN201610163470A CN105747270A CN 105747270 A CN105747270 A CN 105747270A CN 201610163470 A CN201610163470 A CN 201610163470A CN 105747270 A CN105747270 A CN 105747270A
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- CN
- China
- Prior art keywords
- parts
- electronic cigarette
- liquid
- grape
- cigarette liquid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0069—Heterocyclic compounds
- C11B9/0073—Heterocyclic compounds containing only O or S as heteroatoms
- C11B9/008—Heterocyclic compounds containing only O or S as heteroatoms the hetero rings containing six atoms
Abstract
The invention provides electronic cigarette liquid and a preparation method thereof. The grape-flavored electronic cigarette liquid provided by the invention is obtained after propylene glycol, glycerol. 1,3-butanediol, xylitol liquid, a grape juice concentrate, edible grape essence and the like are uniformly mixed in proportion, wherein the grape juice concentrate is obtained by pressing, extraction, reduced pressure rotary evaporation and concentration; the grape-flavored electronic cigarette liquid comprises the following components in parts by weight: 1-80 parts of the propylene glycol, 1-60 parts of the glycerol, 1-50 parts of 1,3-butanediol, 1-30 parts of the xylitol liquid, 5-10 parts of the grape juice concentrate and 0.1-2 parts of the edible grape flavor. The electronic cigarette liquid provided by the invention has better grape fragrance, is fresh and sweet in mouth feeling and can satisfy the smoking demands of consumers on fruit-flavored electronic cigarettes.
Description
Technical field
The invention belongs to flavouring essence for tobacco field, relate to a kind of electronic cigarette liquid and preparation method thereof, particularly relate to a kind of Portugal
Electronic cigarette liquid of grape local flavor and preparation method thereof.
Background technology
Electronic cigarette has another name called electronic cigarette, has the outward appearance similar to Medicated cigarette and the taste of medicated cigarette approximation, the same also like Medicated cigarette
Energy sucking-off cigarette, sucking-off taste and sensation are come.Electronic cigarette does not has other harmful components such as the tar in Medicated cigarette, suspended particulates, the most several
Do not produce second hand smoking.
The fragrance of electronic cigarette and mouthfeel derive from electronic cigarette liquid, and the composition of electronic cigarette liquid is mainly essence and flavoring agent, and Nicotiana tabacum L. carries
Take thing and propylene glycol, glycerol equal solvent.In order to cater to the consumption habit of consumer's diversification, during the electronic cigarette on market has
The brand cigarette tastes such as China, Yuxi, also have the non-tobacco tastes such as Herba Menthae, cocoa, Rhizoma et radix valerianae.At present, the fruity without nicotine
Electronic cigarette is quite welcome by consumer with its pure and fresh sweet mouthfeel.
Summary of the invention
Solve the technical problem that: fruity electronic cigarette mainly brings sense by its pure and fresh sweet mouthfeel to consumer
Pleasurable sensation on official, but the mouthfeel of fruity electronic cigarette in the market is universal sweet greasy, and pleasant impression is the cleanest, it is impossible to meets and disappears
The requirement of sense of the person of expense.
Technical scheme: for above-mentioned technical problem, the invention discloses the electronic cigarette liquid of a kind of grape flavor, described Portugal
The electronic cigarette liquid of grape local flavor consists of the following composition: propylene glycol, glycerol, 1,3 butylene glycol, xylitol liquid, Sucus Vitis viniferae concentrated solution and
Table grapes essence.
Preferably, in the electronic cigarette liquid of described a kind of grape flavor, the parts by weight of each component are: propylene glycol is 1-80
Part, glycerol be 1-60 part, 1,3 butylene glycol be 1-50 part, xylitol liquid be 1-30 part, Sucus Vitis viniferae concentrated solution be 5-10 part, edible
Grape essence is 0.1-2 part.
Preferably, the electronic cigarette liquid of described a kind of grape flavor is sundown.
Preferably, the electronic cigarette liquid of described a kind of grape flavor, described table grapes essence is composed of the following components:
Methyl 2-aminobenzoate, N-methyl anthranilic acid methyl ester, ethyl acetate, ethyl n-butyrate., isoamyl acetate, 2-methyl fourth
Acetoacetic ester, maltol, 2-methyl butanol, phenethanol, trans-2-hexenol, citral, Alcohols,fusel, white lemon oil, oranger terpene,
Cognac green oil and propylene glycol.
Preferably, the electronic cigarette liquid of described a kind of grape flavor, the weight of each component in described table grapes essence
Number is: methyl 2-aminobenzoate be 3-6 part, N-methyl anthranilic acid methyl ester be 2-7 part, ethyl acetate be 1-5 part,
Ethyl n-butyrate. be 0.1-1 part, isoamyl acetate be 0.1-1 part, ethyl 2-methylbutyrate be 0.1-1 part, maltol be 0.1-1
Part, 2-methyl butanol be 1-5 part, phenethanol be 0.1-1 part, trans-2-hexenol be 0.01-1 part, citral be 0.01-1 part,
Alcohols,fusel be 1-5 part, white lemon oil be 0.1-1 part, oranger terpene be 0.1-1 part, cognac green oil be 0.1-1 part, propylene glycol
For 70-90 part.
Preferably, the electronic cigarette liquid of described a kind of grape flavor, described Sucus Vitis viniferae concentrated solution is that Fructus Vitis viniferae squeezing is extracted
After the Sucus Vitis viniferae concentrated solution that is concentrated to give.
Preferably, described Sucus Vitis viniferae concentrated solution preparation method comprises the following steps: (1) weighs clean Fructus Vitis viniferae, uses group
Knit bruisher to smash to pieces；(2) carry out squeezing with small-sized basket squeezer and obtain original grape juice；(3) original grape juice decompression is rotated
Evaporation and concentration becomes thick liquid, standby.
Preferably, the temperature that the rotary evaporation that reduces pressure in the preparation method of described Sucus Vitis viniferae concentrated solution concentrates is 50 DEG C, very
Reciprocal of duty cycle is 0.095 Mpa, and the Baume degrees of final gained Sucus Vitis viniferae concentrated solution is at 50-55 ° of Bx.
The preparation method of the electronic cigarette liquid of a kind of grape flavor, comprises the steps: that (1) weighs clean Fructus Vitis viniferae, uses group
Knit bruisher to smash to pieces；(2) carry out squeezing with small-sized basket squeezer and obtain original grape juice；(3) original grape juice decompression is rotated
Evaporation and concentration becomes thick liquid, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095 Mpa, is concentrated into Baume degrees and reaches 50-
After 55 ° of Bx standby；(4) methyl 2-aminobenzoate 3-6 part, N-methyl anthranilic acid methyl ester 2-7 part, ethyl acetate 1-are taken
5 parts, ethyl n-butyrate. 0.1-1 part, isoamyl acetate 0.1-1 part, ethyl 2-methylbutyrate 0.1-1 part, maltol 0.1-1 part, 2-
Methyl butanol 1-5 part, phenethanol 0.1-1 part, trans-2-hexenol 0.01-1 part, citral 0.01-1 part, Alcohols,fusel 1-5 part, white
Fructus Citri Limoniae oil 0.1-1 part, oranger terpene 0.1-1 part, cognac green oil 0.1-1 part, propylene glycol 70-90 part, mix mentioned component
After obtain table grapes essence；(5) propylene glycol 1-80 part, glycerol 1-60 part, 1,3 butylene glycol 1-50 part, xylitol liquid 1-30 are taken
Part, Sucus Vitis viniferae concentrated solution 5-10 part, Fructus Vitis viniferae edible essence 0.1-2 part, prepare grape flavor after being mixed by mentioned component
Electronic cigarette liquid.
The described xylitol aqueous solution that xylitol liquid is 20wt% to 50wt%.
Beneficial effect: the electronic cigarette liquid of the grape flavor prepared by the preparation method of the present invention is sundown,
Overcome fruity electronic cigarette mouthfeel universal sweet greasy, pleasant impression is the cleanest, it is impossible to the shortcoming meeting consumer sensory's demand, the present invention
Electronic cigarette liquid suction time be provided that fresh and sweet Fructus Vitis viniferae fragrance, mouthfeel is soft and moist and pleasant impression is the most comfortable, and described electronic cigarette
The preparation method of liquid is easy, and constant product quality can be widely applied in electronic cigarette product.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further described.
Embodiment 1
(1) weigh clean Fructus Vitis viniferae, smash to pieces with tissue mashing machine；Carry out squeezing with small-sized basket squeezer and obtain original grape juice；
Original grape juice decompression rotary evaporation is condensed into thick liquid, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095
Mpa, is concentrated into after Baume degrees reaches 50-55 ° of Bx standby；
(2) methyl 2-aminobenzoate 4 parts, N-methyl anthranilic acid methyl ester 5 parts, ethyl acetate 2 parts, butanoic acid are taken by weight
Ethyl ester 0.4 part, isoamyl acetate 0.5 part, ethyl 2-methylbutyrate 0.5 part, maltol 0.6 part, 2-methyl butanol 1 part, benzene second
Alcohol 0.1 part, trans-2-hexenol 0.05 part, citral 0.01 part, Alcohols,fusel 1 part, white lemon oil 0.1 part, oranger terpene 0.1 part,
Cognac green oil 0.1 part, propylene glycol 80 parts, obtain table grapes essence after being mixed by mentioned component；
(3) propylene glycol 50 parts, glycerol 20 parts, 1,3 butylene glycol 10 parts, the xylitol liquid 5 parts of 20wt%, Sucus Vitis viniferae are taken by weight dense
Contracting liquid 9.5 parts, 0.5 part of mix homogeneously of table grapes essence, obtain the electronic cigarette liquid of grape flavor.
Embodiment 2
(1) weigh clean Fructus Vitis viniferae, smash to pieces with tissue mashing machine；Carry out squeezing with small-sized basket squeezer and obtain original grape juice；
Original grape juice decompression rotary evaporation is condensed into thick liquid, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095
Mpa, is concentrated into after Baume degrees reaches 50-55 ° of Bx standby；
(2) methyl 2-aminobenzoate 3 parts, N-methyl anthranilic acid methyl ester 7 parts, ethyl acetate 5 parts, butanoic acid are taken by weight
Ethyl ester 0.1 part, isoamyl acetate 0.1 part, ethyl 2-methylbutyrate 0.1 part, maltol 0.1 part, 2-methyl butanol 2.5 parts, benzene
Ethanol 0.5 part, trans-2-hexenol 0.01 part, citral 0.03 part, Alcohols,fusel 2 parts, white lemon oil 0.4 part, oranger terpene 0.2
Part, cognac green oil 0.5 part, propylene glycol 70 parts, obtain table grapes essence after being mixed by mentioned component；
(3) propylene glycol 80 parts, glycerol 1 part, 1,3 butylene glycol 1 part, the xylitol liquid 30 parts of 40wt%, Sucus Vitis viniferae are taken by weight dense
Contracting liquid 10 parts, 0.1 part of mix homogeneously of table grapes essence, obtain the electronic cigarette liquid of grape flavor.
Embodiment 3
(1) weigh clean Fructus Vitis viniferae, smash to pieces with tissue mashing machine；Carry out squeezing with small-sized basket squeezer and obtain original grape juice；
Original grape juice decompression rotary evaporation is condensed into thick liquid, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095
Mpa, is concentrated into after Baume degrees reaches 50-55 ° of Bx standby；
(2) methyl 2-aminobenzoate 6 parts, N-methyl anthranilic acid methyl ester 2 parts, ethyl acetate 1 part, butanoic acid are taken by weight
Ethyl ester 1 part, isoamyl acetate 1 part, ethyl 2-methylbutyrate 1 part, maltol 1 part, 2-methyl butanol 5 parts, phenethanol 1 part, trans-
2-hexenol 1 part, citral 1 part, Alcohols,fusel 5 parts, white lemon oil 1 part, oranger terpene 1 part, cognac green oil 1 part, propylene glycol
90 parts, after being mixed by mentioned component, obtain table grapes essence；
(3) propylene glycol 1 part, glycerol 60 parts, 1,3 butylene glycol 50 parts, the xylitol liquid 1 part of 50wt%, Sucus Vitis viniferae are taken by weight dense
Contracting liquid 5 parts, 2 parts of mix homogeneously of table grapes essence, obtain the electronic cigarette liquid of grape flavor.
The embodiment 1 prepared, embodiment 2, the grape flavor electronic cigarette liquid of embodiment 3 are taken 0.5mL and add to electricity
In sub-cigarette, and separately take after commercially available table grapes essence propylene glycol is diluted to 0.3wt%, take the commercially available edible Portugal of 0.3wt% of 0.5mL
Grape essence diluent adds to electronic cigarette, as a comparison case, carries out integrated sensory's quality evaluation.Result is as follows:
Embodiment 1: flue gas is full, Fructus Vitis viniferae gives off a strong fragrance, mouthfeel is soft, pleasant impression is comfortable.
Embodiment 2: exquisiteness that flue gas is strong, Fructus Vitis viniferae fragrance is soft and moist, mouthfeel is fresh and sweet, pleasant impression are clean.
Embodiment 3: flue gas is strong, Fructus Vitis viniferae soft aroma and, delicate mouthfeel, pleasant impression clean.
Comparative example: flue gas is strong, Fructus Vitis viniferae fragrance coordinate, mouthfeel sweet greasy, pleasant impression is not good enough.
Can be seen that from result, the electronic cigarette liquid of the grape flavor prepared by the preparation method of the present invention is had clearly
Sweet Fructus Vitis viniferae fragrance, mouthfeel is soft and moist and pleasant impression is the most comfortable, and the preparation method of described electronic cigarette liquid is easy, and product quality is steady
Fixed, can be widely applied in electronic cigarette product.
Claims (1)
1. the preparation method of the electronic cigarette liquid of a grape flavor, it is characterised in that comprise the steps:
(1) weigh clean Fructus Vitis viniferae, smash to pieces with tissue mashing machine；Carry out squeezing with small-sized basket squeezer and obtain original grape juice；
Original grape juice decompression rotary evaporation is condensed into thick liquid, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095
Mpa, is concentrated into after Baume degrees reaches 50-55 ° of Bx standby；
(2) methyl 2-aminobenzoate 3 parts, N-methyl anthranilic acid methyl ester 7 parts, ethyl acetate 5 parts, butanoic acid are taken by weight
Ethyl ester 0.1 part, isoamyl acetate 0.1 part, ethyl 2-methylbutyrate 0.1 part, maltol 0.1 part, 2-methyl butanol 2.5 parts, benzene
Ethanol 0.5 part, trans-2-hexenol 0.01 part, citral 0.03 part, Alcohols,fusel 2 parts, white lemon oil 0.4 part, oranger terpene 0.2
Part, cognac green oil 0.5 part, propylene glycol 70 parts, obtain table grapes essence after being mixed by mentioned component；
(3) propylene glycol 80 parts, glycerol 1 part, 1,3 butylene glycol 1 part, the xylitol liquid 30 parts of 40wt%, Sucus Vitis viniferae are taken by weight dense
Contracting liquid 10 parts, 0.1 part of mix homogeneously of table grapes essence, obtain the electronic cigarette liquid of grape flavor.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610163470.9A CN105747270A (en) | 2014-07-28 | 2014-07-28 | Electronic cigarette liquid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610163470.9A CN105747270A (en) | 2014-07-28 | 2014-07-28 | Electronic cigarette liquid and preparation method thereof |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410360460.5A Division CN104087415B (en) | 2014-07-28 | 2014-07-28 | Electronic cigarette liquid of a kind of grape flavor and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105747270A true CN105747270A (en) | 2016-07-13 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201610163470.9A Pending CN105747270A (en) | 2014-07-28 | 2014-07-28 | Electronic cigarette liquid and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106235258A (en) * | 2016-08-11 | 2016-12-21 | 广东铭康香精香料有限公司 | A kind of natural grape essence |
| CN115463167A (en) * | 2022-09-07 | 2022-12-13 | 东莞百优百科技有限公司 | Grape-flavored anti-alcohol maintenance atomized liquid and preparation method thereof |
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| CN103404965A (en) * | 2012-12-28 | 2013-11-27 | 昌宁德康生物科技有限公司 | Method for producing pulp applied to electronic smoking set and traditional water pipe with shredded tobacco |
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| CN103876274A (en) * | 2014-03-18 | 2014-06-25 | 黄金珍 | Electronic cigarette atomization liquid and preparing method of electronic cigarette atomization liquid |
| CN103892454A (en) * | 2014-03-18 | 2014-07-02 | 黄金珍 | Pressure lowering and lipid lowering electronic cigarette atomized liquid and preparation method thereof |
-
2014
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Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1377237A (en) * | 1999-09-30 | 2002-10-30 | 宝洁公司 | Method for extending the flavor shelf life of aqueous compositions flavored with moisture and acid sensitive flavors and flavor compositions having extended flavor shelf lives |
| CN102240071A (en) * | 2011-07-02 | 2011-11-16 | 云南瑞升烟草技术（集团）有限公司 | Filter tip stick for low-tar cigarette |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106235258A (en) * | 2016-08-11 | 2016-12-21 | 广东铭康香精香料有限公司 | A kind of natural grape essence |
| CN115463167A (en) * | 2022-09-07 | 2022-12-13 | 东莞百优百科技有限公司 | Grape-flavored anti-alcohol maintenance atomized liquid and preparation method thereof |
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Application publication date: 20160713 |
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