CN105699578A - 一种玻璃酸钠组成糖型指纹图谱分析方法 - Google Patents
一种玻璃酸钠组成糖型指纹图谱分析方法 Download PDFInfo
- Publication number
- CN105699578A CN105699578A CN201610255322.XA CN201610255322A CN105699578A CN 105699578 A CN105699578 A CN 105699578A CN 201610255322 A CN201610255322 A CN 201610255322A CN 105699578 A CN105699578 A CN 105699578A
- Authority
- CN
- China
- Prior art keywords
- hyaluronic acid
- acid sodium
- hyaluronidase
- mobile phase
- enzymolysis
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/86—Signal analysis
- G01N30/8675—Evaluation, i.e. decoding of the signal into analytical information
- G01N30/8686—Fingerprinting, e.g. without prior knowledge of the sample components
Landscapes
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Engineering & Computer Science (AREA)
- Library & Information Science (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
- Measuring Or Testing Involving Enzymes Or Micro-Organisms (AREA)
Abstract
Description
Claims (4)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610255322.XA CN105699578B (zh) | 2016-04-22 | 2016-04-22 | 一种玻璃酸钠组成糖型指纹图谱分析方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610255322.XA CN105699578B (zh) | 2016-04-22 | 2016-04-22 | 一种玻璃酸钠组成糖型指纹图谱分析方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN105699578A true CN105699578A (zh) | 2016-06-22 |
CN105699578B CN105699578B (zh) | 2017-07-07 |
Family
ID=56217414
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610255322.XA Expired - Fee Related CN105699578B (zh) | 2016-04-22 | 2016-04-22 | 一种玻璃酸钠组成糖型指纹图谱分析方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN105699578B (zh) |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107561179A (zh) * | 2017-08-18 | 2018-01-09 | 上海景峰制药有限公司 | 一种交联透明质酸或其盐的交联度的测定方法 |
CN109298113A (zh) * | 2018-12-11 | 2019-02-01 | 华熙福瑞达生物医药有限公司 | 一种测定包含有柠檬酸的溶液中的透明质酸含量的方法 |
CN111562231A (zh) * | 2020-06-22 | 2020-08-21 | 华熙生物科技股份有限公司 | 一种透明质酸分子量的测定方法 |
CN113287708A (zh) * | 2021-07-12 | 2021-08-24 | 千世泰生物科技(青岛)有限公司 | 一种含透明质酸钠的固体饮料及其中透明质酸钠含量检测方法 |
CN114236014A (zh) * | 2021-12-27 | 2022-03-25 | 珠海溪谷医疗科技有限公司 | 隐形眼镜的护理液中透明质酸钠的含量的检测方法 |
CN114609296A (zh) * | 2022-03-29 | 2022-06-10 | 水羊化妆品制造有限公司 | 一种酶解透明质酸寡糖混合物的检测方法 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6279790A (ja) * | 1985-09-30 | 1987-04-13 | Toyo Jozo Co Ltd | 改質されたヒアルロン酸の製造法 |
JP3932348B2 (ja) * | 2001-03-28 | 2007-06-20 | 独立行政法人産業技術総合研究所 | オリゴ糖の製造方法 |
CN102323344A (zh) * | 2011-07-20 | 2012-01-18 | 山东福瑞达生物医药有限公司 | 一种定量检测透明质酸片段结构变化的方法 |
CN102645504A (zh) * | 2012-05-10 | 2012-08-22 | 江南大学 | 一种灵芝孢子粉多糖离子色谱指纹图谱的构建方法 |
CN104215704A (zh) * | 2013-06-05 | 2014-12-17 | 江苏中谱检测有限公司 | 掺假蜂蜜中寡糖的快速检测方法 |
-
2016
- 2016-04-22 CN CN201610255322.XA patent/CN105699578B/zh not_active Expired - Fee Related
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6279790A (ja) * | 1985-09-30 | 1987-04-13 | Toyo Jozo Co Ltd | 改質されたヒアルロン酸の製造法 |
JP3932348B2 (ja) * | 2001-03-28 | 2007-06-20 | 独立行政法人産業技術総合研究所 | オリゴ糖の製造方法 |
CN102323344A (zh) * | 2011-07-20 | 2012-01-18 | 山东福瑞达生物医药有限公司 | 一种定量检测透明质酸片段结构变化的方法 |
CN102645504A (zh) * | 2012-05-10 | 2012-08-22 | 江南大学 | 一种灵芝孢子粉多糖离子色谱指纹图谱的构建方法 |
CN104215704A (zh) * | 2013-06-05 | 2014-12-17 | 江苏中谱检测有限公司 | 掺假蜂蜜中寡糖的快速检测方法 |
Non-Patent Citations (5)
Title |
---|
JEFFREY A.CRAMER 等: "A reversed-phase ion-pair high-performance liquid chromatography method for bovine testicular hyaluronidase digests using postcolumn derivatization with 2-cyanoacetamide and ultraviolet detection", 《ANALYTICAL BIOCHEMISTRY》 * |
MARCO VIGLIANO 等: "Determination of Hyaluronic Acid in a Chitosan-Based Formulation by RP C18 and HILIC LC–ESI-MS: an Evaluation of Matrix Effect", 《CHROMATOGRAPHIA》 * |
P.J. KNUDSEN 等: "High-performance liquid chromatography of hyaluronic acid and oligosaccharides produced by bovine testes hyaluronidase", 《JOURNAL OF CHROMATOGRAPHY A》 * |
王海英 等: "高效液相色谱法测定玻璃酸钠的含量", 《中国药学杂志》 * |
鲍伦军 等: "软骨素酶 ABC酶解-高效液相色谱法测定鱼翅中的透明质酸", 《色谱》 * |
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107561179A (zh) * | 2017-08-18 | 2018-01-09 | 上海景峰制药有限公司 | 一种交联透明质酸或其盐的交联度的测定方法 |
CN107561179B (zh) * | 2017-08-18 | 2020-12-04 | 上海景峰制药有限公司 | 一种交联透明质酸或其盐的交联度的测定方法 |
CN109298113A (zh) * | 2018-12-11 | 2019-02-01 | 华熙福瑞达生物医药有限公司 | 一种测定包含有柠檬酸的溶液中的透明质酸含量的方法 |
CN109298113B (zh) * | 2018-12-11 | 2021-06-18 | 华熙生物科技股份有限公司 | 一种测定包含有柠檬酸的溶液中的透明质酸含量的方法 |
CN111562231A (zh) * | 2020-06-22 | 2020-08-21 | 华熙生物科技股份有限公司 | 一种透明质酸分子量的测定方法 |
CN111562231B (zh) * | 2020-06-22 | 2023-09-15 | 华熙生物科技股份有限公司 | 一种透明质酸分子量的测定方法 |
CN113287708A (zh) * | 2021-07-12 | 2021-08-24 | 千世泰生物科技(青岛)有限公司 | 一种含透明质酸钠的固体饮料及其中透明质酸钠含量检测方法 |
CN114236014A (zh) * | 2021-12-27 | 2022-03-25 | 珠海溪谷医疗科技有限公司 | 隐形眼镜的护理液中透明质酸钠的含量的检测方法 |
CN114609296A (zh) * | 2022-03-29 | 2022-06-10 | 水羊化妆品制造有限公司 | 一种酶解透明质酸寡糖混合物的检测方法 |
CN114609296B (zh) * | 2022-03-29 | 2024-01-05 | 水羊化妆品制造有限公司 | 一种酶解透明质酸寡糖混合物的检测方法 |
Also Published As
Publication number | Publication date |
---|---|
CN105699578B (zh) | 2017-07-07 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN105699578A (zh) | 一种玻璃酸钠组成糖型指纹图谱分析方法 | |
Hofmann et al. | Identification of carbohydrate anomers using ion mobility–mass spectrometry | |
Kailemia et al. | Oligosaccharide analysis by mass spectrometry: a review of recent developments | |
CN105699478B (zh) | 一种识别糖的快速方法 | |
Thanawiroon et al. | Liquid chromatography/mass spectrometry sequencing approach for highly sulfated heparin-derived oligosaccharides | |
Yang et al. | Hyphenated techniques for the analysis of heparin and heparan sulfate | |
Li et al. | Separation of chito-oligomers with several degrees of polymerization and study of their antioxidant activity | |
Doneanu et al. | Analysis of oligosaccharides derived from heparin by ion-pair reversed-phase chromatography/mass spectrometry | |
Hsu et al. | Simple method for de novo structural determination of underivatised glucose oligosaccharides | |
Liu et al. | Global characterization of neutral saccharides in crude and processed Radix Rehmanniae by hydrophilic interaction liquid chromatography tandem electrospray ionization time-of-flight mass spectrometry | |
Turnipseed et al. | Analysis of avermectin and moxidectin residues in milk by liquid chromatography–tandem mass spectrometry using an atmospheric pressure chemical ionization/atmospheric pressure photoionization source | |
Tolonen et al. | Comparison of electrospray ionization and atmospheric pressure chemical ionization techniques in the analysis of the main constituents from Rhodiola rosea extracts by liquid chromatography/mass spectrometry | |
Chen et al. | Optimized hydrolysis and analysis of Radix Asparagi polysaccharide monosaccharide composition by capillary zone electrophoresis | |
Ma et al. | Identification of chemical constituents in extracts and rat plasma from Fructus Aurantii by UPLC‐PDA‐Q‐TOF/MS | |
Zhao et al. | Screening and determination for potential α‐glucosidase inhibitory constituents from Dalbergia odorifera T. Chen using ultrafiltration‐LC/ESI‐MSn | |
CN105527350A (zh) | 细胞胞内氨基酸代谢轮廓分析方法 | |
Zhao et al. | Simultaneous determination of 13 carbohydrates using high‐performance anion‐exchange chromatography coupled with pulsed amperometric detection and mass spectrometry | |
Bielik et al. | Historical overview of glycoanalysis | |
Guo et al. | Simultaneous determination of linarin, naringenin and formononetin in rat plasma by LC‐MS/MS and its application to a pharmacokinetic study after oral administration of Bushen Guchi Pill | |
Li et al. | Analysis of monosaccharide composition of water‐soluble polysaccharides from Codium fragile by ultra‐performance liquid chromatography‐tandem mass spectrometry | |
Grundmann et al. | Fast counter-electroosmotic capillary electrophoresis–time-of-flight mass spectrometry of hyaluronan oligosaccharides | |
Jiang et al. | Combining online size exclusion chromatography and electrospray ionization mass spectrometry to characterize plant polysaccharides | |
CN104764847B (zh) | 含n-乙酰化结构肝素寡糖的制备方法 | |
CN102936235B (zh) | 葡萄糖醛酸缩硫醇-乙酸酯衍生物及其制备方法和应用 | |
Cao et al. | Screening of glycoside isomers in P. scrophulariiflora using ionic liquid‐based ultrasonic‐assisted extraction and ultra‐performance liquid chromatography/electrospray ionization quadrupole time‐of‐flight tandem mass spectrometry |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20200528 Address after: 523871 room 114, building 3, No. 368, middle Zhen'an Road, Chang'an Town, Dongguan City, Guangdong Province Patentee after: Dongguan dongyangguang biosynthetics Co., Ltd Address before: 523808 Guangdong city of Dongguan province Hubei Songshan Industrial Park Industrial Road No. 1 Patentee before: SUNSHINE LAKE PHARMA Co.,Ltd. |
|
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20200922 Address after: No.62, Lucheng Binjiang Road, Yidu City, Yichang City, Hubei Province Patentee after: Yichang dongyangguang Biochemical Pharmaceutical Co., Ltd Address before: 523871 room 114, building 3, No. 368, middle Zhen'an Road, Chang'an Town, Dongguan City, Guangdong Province Patentee before: Dongguan dongyangguang biosynthetics Co.,Ltd. |
|
TR01 | Transfer of patent right | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170707 Termination date: 20210422 |
|
CF01 | Termination of patent right due to non-payment of annual fee |