CN105662924A - Anti-aging microemulsion - Google Patents
Anti-aging microemulsion Download PDFInfo
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- CN105662924A CN105662924A CN201610070602.3A CN201610070602A CN105662924A CN 105662924 A CN105662924 A CN 105662924A CN 201610070602 A CN201610070602 A CN 201610070602A CN 105662924 A CN105662924 A CN 105662924A
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- oil
- microemulsion
- ageing
- methyl glucose
- laurin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
- A61K8/068—Microemulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
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- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Dispersion Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses an anti-aging microemulsion and particularly discloses an anti-aging microemulsion containing geranium essential oil, laurel essential oil and cinnamon essential oil. The prepared anti-aging microemulsion is not found irritant to skin, can promote skin to become tender, smooth and full of elasticity and has an excellent anti-ageing effect.
Description
Technical field
The invention belongs to cosmetic technical field, it is specifically related to a kind of anti-ageing microemulsion.
Background technology
In the today in 21st century, people, after enjoying progressive achievement, but gradually find that the science and technology of civilization is except bringing social prosperity and life convenient, also makes our environment start to worsen. Before long, the various pollutions that are inferior and that be seen everywhere of air quality occupy the living space of our major part, civilized sequela of all kinds has started to corrode our health and soul, the too early aging phenomenons such as the colour of skin is obscure, pigmentation, skin lose elasticity become common problem, how anti-ageing has been an important problem, and " back to nature " is the initial approach to become a Buddhist believer addressed this problem.
Under the new life idea trend of back to nature affects, the volatile oils adding some plant extract more and more in makeup reaches anti-ageing, recovers the object of physical and mental health. Obtained it is to be noted that, essence oil is a kind of Oil soluble materials, convenient in finish class cosmetic applications, but but be difficult to use in the water aqua type product such as astringent, facial mask essence, method usual in industry is that the solubilizing agent with about 10 times of essence oil consumptions is in advance by essence oil solubilising, solubilizing agent be a class high hlb (hydrophile-lipophile balance value) there is irritating tensio-active agent, in cosmetics series, the introducing of excessive solubilizing agent causes easy sensitization and the pungency of product.
Summary of the invention
Based on this, it is an object of the invention to provide a kind of anti-ageing microemulsion, the emulsifier hlb value adopted is on the low side, and adding proportion is low, not yet finds skin irritant; It makes skin become delicate, smooth, flexible, has excellent anti-ageing effect.
In order to solve the problems of the technologies described above, the present invention is achieved through the following technical solutions:
A kind of anti-ageing microemulsion, containing massfraction in this microemulsion formula is the anti-apolexis composition of 0.03-1.5%, and described anti-apolexis composition is containing, for example each component of lower mass parts: Geranium Essential 0.01-0.5 part, laurin oil 0.01-0.5 part and cinnamon essential oil 0.01-0.5 part.
Further, described anti-ageing microemulsion comprises the component of following mass percent:
Methyl glucose sesquialter stearate 1-2%
PEG-20 methyl glucose sesquialter stearate 1-3%
Chinese gooseberry seed oil 2.5-5%
Linseed oil 2.5-5%
Geranium Essential 0.01-0.5%
Laurin oil 0.01-0.5%
Cinnamon essential oil 0.01-0.5%
Vitamin E acetate 0.1-0.5%
VCE 0.1-0.5%
Troxerutin 0.1-0.5%
Butyleneglycol 15-30%
Carbomer 0.1-0.2%
Arginine 0.1-0.2%
Rhizoma Polygonati extract 0.1-1%
Wax gourd seed extract 0.1-1%
Water surplus.
Wherein in an embodiment, described anti-ageing microemulsion comprises the component of following mass percent:
Methyl glucose sesquialter stearate 1.5%
PEG-20 methyl glucose sesquialter stearate 2%
Chinese gooseberry seed oil 3%
Linseed oil 3%
Geranium Essential 0.2%
Laurin oil 0.2%
Cinnamon essential oil 0.2%
Vitamin E acetate 0.2%
VCE 0.2%
Troxerutin 0.2%
Butyleneglycol 20%
Carbomer 0.15%
Arginine 0.15%
Rhizoma Polygonati extract 0.5%
Wax gourd seed extract 0.5%
Water surplus.
Anti-ageing microemulsion prepared by the present invention has good water soluble/dispersible, both can directly use as astringent, it is possible to adding in cosmetic product as a kind of senile-resistant efficacy additive, application is convenient.
When anti-ageing microemulsion of the present invention joins cosmetic product as functional additive, it is preferable that, the addition of described anti-ageing microemulsion in cosmetic product is 0.1-5wt%.
The microemulsion of the present invention can by the preparation of conventional production technique, preferred following preparation method, it comprises the following steps: methyl glucose sesquialter stearate, PEG-20 methyl glucose sesquialter stearate, Chinese gooseberry seed oil, linseed oil, Geranium Essential, laurin oil, cinnamon essential oil, Vitamin E acetate mixing are formed oil phase, oil phase is heated to 70-90 DEG C, stirring and dissolving; VCE, troxerutin, butyleneglycol, carbomer mixing are formed aqueous phase, by heated aqueous to 70-90 DEG C, stirring and dissolving; Pressurization 0.1-10Mpa, injects oil mixture by aqueous phase, homogeneous (homogeneous speed is 1000-5000rpm) after 3-5 minute insulated and stirred 15-45 minute; Relief pressure, cools to 45 DEG C, adds arginine, Rhizoma Polygonati extract and wax gourd seed extract successively, stirs evenly.
Conventional makeup emulsification method is vacuum emulsification method, i.e. homogenizing emulsifying under negative (0.1-0.5) Mpa pressure, and the preparation method of the present invention is just contrary with it, just have employed (0.1-10) Mpa pressure.
Compared with prior art, the present invention has following useful effect:
(1) anti-ageing microemulsion of the present invention with the addition of Geranium Essential part, laurin oil and cinnamon essential oil, arrange in pairs or groups according to specified proportion, the multiple efficacies composition being rich in is in harmonious proportion mutually, works in coordination with, and makes skin become delicate, smooth, flexible, has excellent anti-ageing effect.
(2) the present invention is composite with the addition of Vitamin E acetate, VCE and troxerutin, and these three kinds of raw materials have stronger antioxygenation, and after composite use, effect is better, and troxerutin can absorb ultraviolet in addition, can resist the photoaging of skin; Composite with the addition of Rhizoma Polygonati extract and wax gourd seed extract, sealwort and wax gourd seed belong to Chinese medicinal materials, the effect can play righting, consolidating; Composite Chinese gooseberry seed oil and linseed oil belong to polyenoic acid vegetables oil, mainly containing the polyenoic acid such as linolic acid, linolenic acid and VE, plant sterol, mineral element, squalene isoreactivity composition. Each composite component in formula is fully in harmonious proportion, works in coordination with, and plays the auxiliary anti-oxidant effect with delaying senility.
Embodiment
Below in conjunction with embodiment, the present invention is for a more detailed description, but embodiments of the present invention are not limited to this, for the processing parameter not indicated especially or condition, can refer to routine techniques and carry out.
Geranium Essential of the present invention, cosmetic material INCI name is called: Pelargonium gravelens (PELARGONIUMGRAVEOLENS) oil; Laurin oil of the present invention, cosmetic material INCI name is called: bay (LAURUSNOBILIS) leaf oil; Cinnamon essential oil of the present invention, cosmetic material INCI name is called: Chinese cassia tree (CINNAMOMUMCASSIA) oil.
Embodiment 1
A kind of anti-ageing microemulsion, comprises the component of following mass percent:
Methyl glucose sesquialter stearate 1%
PEG-20 methyl glucose sesquialter stearate 1%
Chinese gooseberry seed oil 2.5%
Linseed oil 2.5%
Geranium Essential 0.5%
Laurin oil 0.01%
Cinnamon essential oil 0.5%
Vitamin E acetate 0.1%
VCE 0.5%
Troxerutin 0.1%
Butyleneglycol 30%
Carbomer 0.1%
Arginine 0.1%
Rhizoma Polygonati extract 0.1%
Wax gourd seed extract 1%
Water surplus.
Preparation method: methyl glucose sesquialter stearate, PEG-20 methyl glucose sesquialter stearate, Chinese gooseberry seed oil, linseed oil, Geranium Essential, laurin oil, cinnamon essential oil, Vitamin E acetate mixing are formed oil phase, oil phase is heated to 70 DEG C, stirring and dissolving; VCE, troxerutin, butyleneglycol, carbomer mixing are formed aqueous phase, by heated aqueous to 90 DEG C, stirring and dissolving; Pressurization 0.1Mpa, injects oil mixture by aqueous phase, homogeneous (homogeneous speed is 5000rpm) insulated and stirred 45 minutes after 3 minutes; Relief pressure, cools to 45 DEG C, adds arginine, Rhizoma Polygonati extract and wax gourd seed extract successively, stirs evenly.
Embodiment 2
A kind of anti-ageing microemulsion, comprises the component of following mass percent:
Methyl glucose sesquialter stearate 1.5%
PEG-20 methyl glucose sesquialter stearate 2%
Chinese gooseberry seed oil 3%
Linseed oil 4%
Geranium Essential 0.2%
Laurin oil 0.2%
Cinnamon essential oil 0.2%
Vitamin E acetate 0.2%
VCE 0.2%
Troxerutin 0.2%
Butyleneglycol 20%
Carbomer 0.15%
Arginine 0.15%
Rhizoma Polygonati extract 0.5%
Wax gourd seed extract 0.5%
Water surplus.
Preparation method: methyl glucose sesquialter stearate, PEG-20 methyl glucose sesquialter stearate, Chinese gooseberry seed oil, linseed oil, Geranium Essential, laurin oil, cinnamon essential oil, Vitamin E acetate mixing are formed oil phase, oil phase is heated to 80 DEG C, stirring and dissolving; VCE, troxerutin, butyleneglycol, carbomer mixing are formed aqueous phase, by heated aqueous to 80 DEG C, stirring and dissolving; Pressurization 5Mpa, injects oil mixture by aqueous phase, homogeneous (homogeneous speed is 3000rpm) insulated and stirred 30 minutes after 4 minutes; Relief pressure, cools to 45 DEG C, adds arginine, Rhizoma Polygonati extract and wax gourd seed extract successively, stirs evenly.
Embodiment 3
A kind of anti-ageing microemulsion, comprises the component of following mass percent:
Methyl glucose sesquialter stearate 2%
PEG-20 methyl glucose sesquialter stearate 3%
Chinese gooseberry seed oil 5%
Linseed oil 5%
Geranium Essential 0.01%
Laurin oil 0.5%
Cinnamon essential oil 0.01%
Vitamin E acetate 0.5%
VCE 0.1%
Troxerutin 0.5%
Butyleneglycol 15%
Carbomer 0.2%
Arginine 0.2%
Rhizoma Polygonati extract 1%
Wax gourd seed extract 0.1%
Water surplus.
Preparation method: methyl glucose sesquialter stearate, PEG-20 methyl glucose sesquialter stearate, Chinese gooseberry seed oil, linseed oil, Geranium Essential, laurin oil, cinnamon essential oil, Vitamin E acetate mixing are formed oil phase, oil phase is heated to 90 DEG C, stirring and dissolving; VCE, troxerutin, butyleneglycol, carbomer mixing are formed aqueous phase, by heated aqueous to 70 DEG C, stirring and dissolving; Pressurization 10Mpa, injects oil mixture by aqueous phase, homogeneous (homogeneous speed is 1000rpm) insulated and stirred 15 minutes after 5 minutes; Relief pressure, cools to 45 DEG C, adds arginine, Rhizoma Polygonati extract and wax gourd seed extract successively, stirs evenly.
Embodiment 4
A kind of astringent, comprises the component of following mass percent:
Glycerine 5%
Sorbyl alcohol 5%
Methyl esters 0.1%
Hyaluronate sodium 0.02%
Scleroglucan 0.2%
Anti-ageing microemulsion 5% prepared by embodiment 2
Phenoxyethanol 0.35%
Water surplus;
Preparation method: by glycerine, sorbyl alcohol, methyl esters heating for dissolving, then add water, hyaluronate sodium, Scleroglucan, be heated to 85 DEG C, stirring and dissolving, is incubated 30 minutes, then cools to 45 DEG C, add the anti-ageing microemulsion prepared by embodiment 2, Phenoxyethanol, stir evenly.
Embodiment 5
A kind of astringent, comprises the component of following mass percent:
Glycerine 5%
Sorbyl alcohol 5%
Methyl esters 0.1%
Hyaluronate sodium 0.02%
Scleroglucan 0.2%
Anti-ageing microemulsion 0.1% prepared by embodiment 1
Phenoxyethanol 0.35%
Water surplus;
Preparation method is with embodiment 4.
Embodiment 6
Test effect evaluation
Anti-ageing microemulsion prepared by embodiment 1-3 being carried out effect evaluation, and arranges comparative example 1-3, wherein comparative example 1 is commercially available anti-ageing emulsion, and comparative example 2-3 is prepared as follows:
The preparation of comparative example 2: a kind of anti-ageing microemulsion, comprises the component of following mass percent:
Methyl glucose sesquialter stearate 1.5%
PEG-20 methyl glucose sesquialter stearate 2%
Chinese gooseberry seed oil 3%
Linseed oil 4%
Geranium Essential 0.6%
Laurin oil 0.6%
Vitamin E acetate 0.2%
VCE 0.2%
Troxerutin 0.2%
Butyleneglycol 20%
Carbomer 0.15%
Arginine 0.15%
Rhizoma Polygonati extract 0.5%
Wax gourd seed extract 0.5%
Water surplus;
Preparation method is with embodiment 1.
The preparation of comparative example 3: a kind of anti-ageing microemulsion, comprises the component of following mass percent:
Methyl glucose sesquialter stearate 1.5%
PEG-20 methyl glucose sesquialter stearate 2%
Chinese gooseberry seed oil 3%
Linseed oil 4%
Laurin oil 0.6%
Cinnamon essential oil 0.6%
Vitamin E acetate 0.2%
VCE 0.2%
Troxerutin 0.2%
Butyleneglycol 20%
Carbomer 0.15%
Arginine 0.15%
Rhizoma Polygonati extract 0.5%
Wax gourd seed extract 0.5%
Water surplus;
Preparation method is with embodiment 1.
The anti-aging cosmetics of embodiment of the present invention 1-3 and comparative example 1-3 is carried out crowd try out, to evaluate its senile-resistant efficacy. Tested object: each experimental group is 100 women, 30-50 year, it is possible to by Normalization rule makeup, and cooperating personnel complete appraisal on request, have certain expressive faculty, can actual response use after impression; Test zone: face; Use: every day uses twice, after using 30 days continuously; Test event: skin delicacy degree, skin elasticity, wrinkle depth (crows feet area). Concrete test result is in table 1.
The anti-ageing test evaluation table of table 1
As can be known from the above table, the embodiment 1-3 prepared by the present invention is compared with commercially available prod comparative group 1, and the anti-ageing effect of the anti-ageing microemulsion prepared by the present invention is better; Embodiment 2 is compared with comparative group 2-3, and when Geranium Essential part, laurin oil and cinnamon essential oil combinationally use, effect is better, it is achieved that the senile-resistant efficacy of synergetic property.
The above, it it is only the better embodiment of the present invention, not the present invention is done any restriction in form, therefore all contents not departing from technical solution of the present invention, the technical spirit of foundation the present invention, to any simple modification made for any of the above embodiments, equivalent variations and modification, all still belongs in the scope of technical solution of the present invention.
Claims (5)
1. an anti-ageing microemulsion, it is characterized in that, containing massfraction in described microemulsion formula is the anti-apolexis composition of 0.03-1.5wt%, and described anti-apolexis composition is containing, for example each component of lower mass parts: Geranium Essential 0.01-0.5 part, laurin oil 0.01-0.5 part and cinnamon essential oil 0.01-0.5 part.
2. anti-ageing microemulsion according to claim 1, it is characterised in that, described anti-ageing microemulsion comprises the component of following mass percent:
Methyl glucose sesquialter stearate 1-2%
PEG-20 methyl glucose sesquialter stearate 1-3%
Chinese gooseberry seed oil 2.5-5%
Linseed oil 2.5-5%
Geranium Essential 0.01-0.5%
Laurin oil 0.01-0.5%
Cinnamon essential oil 0.01-0.5%
Vitamin E acetate 0.1-0.5%
VCE 0.1-0.5%
Troxerutin 0.1-0.5%
Butyleneglycol 15-30%
Carbomer 0.1-0.2%
Arginine 0.1-0.2%
Rhizoma Polygonati extract 0.1-1%
Wax gourd seed extract 0.1-1%
Water surplus.
3. anti-ageing microemulsion according to claim 2, it is characterised in that, described anti-ageing microemulsion comprises the component of following mass percent:
Methyl glucose sesquialter stearate 1.5%
PEG-20 methyl glucose sesquialter stearate 2%
Chinese gooseberry seed oil 3%
Linseed oil 3%
Geranium Essential 0.2%
Laurin oil 0.2%
Cinnamon essential oil 0.2%
Vitamin E acetate 0.2%
VCE 0.2%
Troxerutin 0.2%
Butyleneglycol 20%
Carbomer 0.15%
Arginine 0.15%
Rhizoma Polygonati extract 0.5%
Wax gourd seed extract 0.5%
Water surplus.
4. anti-ageing microemulsion according to claim 1 and 2, it is characterised in that, when described anti-ageing microemulsion joins cosmetic product as functional additive, its addition is 0.1-5wt%.
5. anti-ageing microemulsion according to claim 1 and 2, it is characterized in that, the preparation method of described anti-ageing microemulsion is: methyl glucose sesquialter stearate, PEG-20 methyl glucose sesquialter stearate, Chinese gooseberry seed oil, linseed oil, Geranium Essential, laurin oil, cinnamon essential oil, Vitamin E acetate mixing are formed oil phase, oil phase is heated to 70-90 DEG C, stirring and dissolving; VCE, troxerutin, butyleneglycol, carbomer mixing are formed aqueous phase, by heated aqueous to 70-90 DEG C, stirring and dissolving; Pressurization 0.1-10Mpa, injects oil mixture by aqueous phase, homogeneous (homogeneous speed is 1000-5000rpm) after 3-5 minute insulated and stirred 15-45 minute; Relief pressure, cools to 45 DEG C, adds arginine, Rhizoma Polygonati extract and wax gourd seed extract successively, stirs evenly.
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CN106176458A (en) * | 2016-08-29 | 2016-12-07 | 秦艳红 | A kind of whitening emulsion |
CN112425648A (en) * | 2020-11-13 | 2021-03-02 | 广州市从化华隆果菜保鲜有限公司 | Fruit and vegetable preservative and preparation method thereof |
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CN103007104A (en) * | 2012-11-13 | 2013-04-03 | 唯美度科技(北京)有限公司 | Compound Chinese mugwort essential oil |
CN103816104A (en) * | 2014-02-26 | 2014-05-28 | 南通恒隆化工有限公司 | Anti-wrinkle moisturizing lotion |
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2016
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CN103007104A (en) * | 2012-11-13 | 2013-04-03 | 唯美度科技(北京)有限公司 | Compound Chinese mugwort essential oil |
CN103816104A (en) * | 2014-02-26 | 2014-05-28 | 南通恒隆化工有限公司 | Anti-wrinkle moisturizing lotion |
CN104352418A (en) * | 2014-10-20 | 2015-02-18 | 东莞市阿比亚能源科技有限公司 | Anti-ageing essence |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN106176458A (en) * | 2016-08-29 | 2016-12-07 | 秦艳红 | A kind of whitening emulsion |
CN112425648A (en) * | 2020-11-13 | 2021-03-02 | 广州市从化华隆果菜保鲜有限公司 | Fruit and vegetable preservative and preparation method thereof |
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