CN103830137A - Plant extract composition with whitening effect, preparation and preparation method thereof - Google Patents

Plant extract composition with whitening effect, preparation and preparation method thereof Download PDF

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Publication number
CN103830137A
CN103830137A CN201410025242.6A CN201410025242A CN103830137A CN 103830137 A CN103830137 A CN 103830137A CN 201410025242 A CN201410025242 A CN 201410025242A CN 103830137 A CN103830137 A CN 103830137A
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plant extract
raw material
preparation
extract compositions
phase
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CN201410025242.6A
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朱文斌
沈小龙
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SHANGHAI GREAF BIOTECH Co Ltd
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SHANGHAI GREAF BIOTECH Co Ltd
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Priority to CN201410025242.6A priority Critical patent/CN103830137A/en
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Abstract

The invention provides a plant extract composition with whitening effect, an external preparation and a preparation method thereof. The plant extract composition is prepared by the following raw material herbs by weight: 30-50 parts by weight of peony; 20-60 parts by weight of magnolia denudate; and 40-70 parts by weight of lily. Three kinds of petals of poney, magnolia denudate, and lily are selected, and the plant extract composition is prepared by a traditional cold pressing separating technology with original effective components being reserved. The plant extract composition has prominent effect on inhibiting the generation of skin melanin, and can be used for preparation of external skin-care preparations with whitening effect.

Description

There is plant extract compositions, preparation of white-skinned face function and preparation method thereof
Technical field
The present invention relates to a kind of plant extract compositions, specifically a kind of plant extract compositions with white-skinned face function, the present invention relates to the external preparation that contains this plant extract compositions simultaneously.
Background technology
Along with the raising of living standards of the people, beauty and skin care becomes the common thing of paying close attention to of numerous personages of liking to be beautiful, and the skin care item of pure natural are pursuing a goal of consumer always.
Usually there are the white hundred ugly ideas that hide in China, fair and clear for U.S. taking skin, therefore, work out the cosmetic material that a kind of pure plant origin has white-skinned face function simultaneously and just there is very strong current demand.
In the Chinese invention patent application that is 201310210916.5 at application number, a kind of the have vegetable composition of whitening function and the application in skin-lightening cosmetic thereof are disclosed.This vegetable composition by Cortex Mori extract, Radix Glycyrrhizae extract, Flos Moutan extract, Flos Bombacis Malabarici extract, Radix Angelicae Sinensis extract, Cortex Moutan extract is composite forms, can be used in whitening formula, there is the function of restraint of tyrosinase activity, removing free radical and skin whitening.
In addition, in the Chinese invention patent application that is 201310293696.7, disclosing a kind of topical composition with whitening and speckle dispelling effect at application number, is that Bulbus Lilii, Fructus Cucumidis sativi, leaf of elm tree are pulverized and squeezed the juice respectively, obtains Bulbus Lilii juice, Sucus Cucumidis sativi, leaf of elm tree juice; Herba bromi japonici, the Radix Angelicae Dahuricae, Herba Leonuri are ground into respectively to 80~120 object powder, make oatmeal, Radix Angelicae Dahuricae powder, motherwort powder; By Bulbus Lilii juice, Sucus Cucumidis sativi, leaf of elm tree juice, oatmeal, Radix Angelicae Dahuricae powder, motherwort powder mix homogeneously, obtain topical composition.This topical composition has effect of skin maintenance, anti-ageing anti-old, speckle dispelling detumescence.
Summary of the invention
Primary technical problem to be solved by this invention is to provide a kind of plant extract compositions with white-skinned face function.
Another technical problem to be solved by this invention is to provide a kind of preparation method of above-mentioned plant extract compositions.
Invention thinking of the present invention is as follows:
Magnolia denudata: (1) acrid in the mouth, temperature, have that expelling wind and cold is sensible, effect of lung qi dispersing stuffy nose relieving; (2) Magnolia denudata Desr. has inhibitory action to common dermatophytes.
Bulbus Lilii: (1) replenishing YIN and removing heat, clearing away heart-fire for tranquillization effect; (2) rich in proteins, mineral, vitamin, carotene and alkaloid etc.
Paeonia suffruticosa: there is clearing heat and moistening lung effect.
The present invention selects Magnolia denudata, Bulbus Lilii and three kinds of petals of Paeonia suffruticosa, utilizes traditional cold pressing isolation technics, retains original functional component, makes the plant extract compositions with white-skinned face function, and the external whitening that contains this plant extract compositions preparation is provided simultaneously.
For realizing above-mentioned goal of the invention, the present invention adopts following technical proposals:
A plant extract compositions with white-skinned face function, is made by the crude drug of following weight portion proportioning:
Paeonia suffruticosa: 30~50 weight portions; Magnolia denudata: 20~60 weight portions; Bulbus Lilii: 40~70 weight portions.
A preparation method for above-mentioned plant extract compositions, comprises the following steps:
(1) take Paeonia suffruticosa, Magnolia denudata and Bulbus Lilii petal by above-mentioned weight proportion, by washed with de-ionized water, and dry;
(2) material after drying in step (1) is pulverized, and squeezed out liquid;
(3) will after the liquid filtering squeezing out in step (2), obtain extracting solution;
(4) in the extracting solution obtaining in step (3), add antiseptic MTI, stir, obtain plant extract compositions.
The purposes of above-mentioned plant extract compositions in preparation whitening external-use skin care preparation.
There is an external-use skin care preparation for white-skinned face function, use plant extract compositions as raw material, and the weight ratio that described plant extract compositions accounts for raw material is between 1~8%.
An emulsion of being prepared as raw material by above-mentioned plant extract compositions, comprises the composition of following weight ratio:
A phase: EDTA-2Na0.1~0.3%, card aunt 0.2~1%, glycerol 1~5%, pantothenylol 0.1~1%, trehalose 1~2%, 1,3 butylene glycol 2~4%, plant extract compositions 1~8%, water 60~80%;
B phase: PEG-100 stearate 1~3%, cetearyl alcohol 0.5~1.5%, tristerin 0.5~1%, polyisobutylene 2~7%, sad capric acid triglyceride 1~5%, Butyrospermum parkii 0.5~3%, 2-Methylpentadecane 2~7%;
C phase: 10%NaOH0.4~2.5%, antiseptic 0.1~0.2%.
Wherein more preferably, above-mentioned emulsion raw material comprises that weight ratio is 5% plant extract compositions.
For the preparation of a preparation method for above-mentioned emulsion, comprise the steps:
(1) water is added in kettle, add card aunt, soak 10min, dissolve completely to raw material is whole heated and stirred to 80~85 DEG C;
(2) add A other raw materials mutually, be incubated 80~85 DEG C and be stirred to the whole dissolvings of raw material completely, after insulation 10min sterilizing, be incubated for subsequent use;
(3) B phase raw material is added in oil phase pot, 80~85 DEG C of dissolvings of agitating heating completely, are incubated for subsequent use;
(4), by A phase raw material suction emulsifying pot, under homogenizing stirs, by B phase raw material suction emulsifying pot, homogenizing 5min, starts cooling after stirring insulation 10min.
(5) in the time that temperature drops to 40~45 DEG C, add C phase raw material, discharging stirs.
Plant extract compositions provided by the invention, can effectively suppress dermal melanin, is a kind of natural inirritative whitening raw material, can be used for preparing the multiple external preparation with skin whitening efficacy.
According to use approach difference, the external-use skin care preparation that plant extract compositions provided by the invention is made as raw material, is not limited to emulsion, also can be made into cleansing milk, facial cream, facial film etc.Can, according to method known in skin care item industrial circle, above-mentioned plant extract compositions be made to various external preparation.
Brief description of the drawings
Fig. 1 adds the emulsion of 5% plant extract compositions and the dermal melanin changes of contents figure of blank group.
Detailed description of the invention
Foregoing invention content part has done detailed description to technical scheme of the present invention, and those skilled in the art can repeat the present invention and obtain technique effect of the present invention according to foregoing.Below by detailed description of the invention, the technology of the present invention content is further explained, understands content of the present invention so that those skilled in the art are clearer, not limitation of the present invention, any being equal to, replaces or known change all belongs to protection domain of the present invention.
The preparation of embodiment 1 plant extract compositions
The present invention selects Magnolia denudata, Paeonia suffruticosa, three kinds of petals of Bulbus Lilii, utilizes traditional cold pressing isolation technics, retains original functional component, makes the plant extract compositions with white-skinned face function.Concrete steps are as follows:
(1) take three kinds of petals by following weight proportion:
Paeonia suffruticosa: 30~50 weight portions; Magnolia denudata: 20~60 weight portions; Bulbus Lilii: 40~70 weight portions;
(2) mixture taking with deionized water cleaning step (1), and dry;
(3) material after drying in step (2) is pulverized, and squeezed out liquid;
(4) will after the liquid filtering squeezing out in step (3), obtain extracting solution;
(5) in the extracting solution obtaining in step (4), add antiseptic MTI, stir, obtain plant extract compositions.
Wherein, in step (2), preferably with three kinds of petals of the washed with de-ionized water more than 50 times.
The preparation of the emulsion that embodiment 2 contains plant extract compositions
The component of emulsion and consumption thereof
A phase: EDTA-2Na0.1~0.3%, card aunt 0.2~1%, glycerol 1~5%, pantothenylol 0.1~1%, trehalose 1~2%, 1,3 butylene glycol 2~4%, the plant extract compositions 1~8% of embodiment 1, water 60~80%;
B phase: PEG-100 stearate 1~3%, cetearyl alcohol 0.5~1.5%, tristerin 0.5~1%, polyisobutylene 2~7%, sad capric acid triglyceride 1~5%, Butyrospermum parkii 0.5~3%, 2-Methylpentadecane 2~7%;
C phase: 10%NaOH0.4~2.5%, antiseptic 0.1~0.2%.
Preparation method:
1) water is added in kettle, add card aunt, soak 10min, dissolve completely to raw material is whole heated and stirred to 80~85 DEG C;
2) add A other raw materials mutually, be incubated 80~85 DEG C and be stirred to the whole dissolvings of raw material completely, after insulation 10min sterilizing, be incubated for subsequent use;
3) B phase raw material is added in oil phase pot, 80~85 DEG C of dissolvings of agitating heating completely, are incubated for subsequent use;
4), by A phase raw material suction emulsifying pot, under stirring, homogenizing by B phase raw material suction emulsifying pot, in homogenizing 5min, after stirring insulation 10min, starts cooling.
5) in the time that temperature drops to 40~45 DEG C, add C phase raw material, discharging stirs.
The white-skinned face function test of the emulsion that embodiment 3 contains 5% plant extract compositions
Measure the impact of the emulsion that contains plant extract compositions on melanin content by contrast test.
Experimenter 30 people, wherein 15 of male volunteers, 15 of female volunteers, tested position is facial skin.Tested position can not be used any cosmetics or topical drug in 2~3 days before trial edition sample.The sample of experiment use is respectively the emulsion (experimental group) of adding 5.0% plant extract compositions and the emulsion (blank group) of not adding plant extract compositions.
Enjoin sooner or later clean skin rear left face use volunteer's every day experimental group sample, right face uses blank group sample.Use 28 days continuously, every a melanin content delta data of test in 7 days.Measure respectively 1 week (7 days), 2 weeks (14 days) on probation, 3 weeks (21 days), the tested region of 4 weeks (28 days) and the dermal melanin content in blank region.
Use dermal melanin and haemachrome tester to carry out the measurement of tested region and control zone, measure the variation of tested region melanin content, reaction white-skinned face function.Each region parallel assay 5 times.
Figure 1 shows that on-site measurement is used the emulsion that contains 5% plant extract compositions and the dermal melanin changes of contents figure that uses blank group.In Fig. 1, smooth broken line represents not contain the test result of the blank group of plant extract compositions; Represent the test result of the emulsion that contains 5% plant extract compositions with the broken line of stain.As seen from Figure 1, the trial zone of the emulsion that use contains 5% plant extract compositions is in the use procedure of 4 weeks, and compared with blank group, the black pigment of skin content progressively reduces, and it is larger to reduce Amplitude Ratio, shows that the emulsion that contains plant extract compositions has potent whitening function.
Can prove by above-mentioned experiment, plant extract compositions provided by the invention has excellent removing melanin effect, thereby has good white-skinned face function.According to use approach difference, can prepare using above-mentioned plant extract compositions as raw material the external-use skin care preparation with white-skinned face function.These external-use skin care preparations are not limited to emulsion, also can be made into cleansing milk, facial cream, facial film etc.Can be prepared according to method known in skin care item industrial circle.
Above plant extract compositions provided by the present invention, external preparation and preparation method thereof are had been described in detail.For one of ordinary skill in the art, any apparent change of under the prerequisite that does not deviate from connotation of the present invention, it being done, all will form infringement of patent right of the present invention, will bear corresponding legal responsibility.

Claims (8)

1. there is a plant extract compositions for white-skinned face function, it is characterized in that being made by the crude drug of following weight portion proportioning:
Paeonia suffruticosa: 30~50 weight portions; Magnolia denudata: 20~60 weight portions; Bulbus Lilii: 40~70 weight portions.
2. a preparation method for plant extract compositions as claimed in claim 1, comprises the following steps:
(1) take Paeonia suffruticosa, Magnolia denudata and Bulbus Lilii petal by the weight proportion in claim 1, by washed with de-ionized water, and dry;
(2) material after drying in step (1) is pulverized, and squeezed out liquid;
(3) will after the liquid filtering squeezing out in step (2), obtain extracting solution;
(4) in the extracting solution obtaining in step (3), add antiseptic MTI, stir, obtain plant extract compositions.
3. plant extract compositions as claimed in claim 1 is in the purposes of preparing in external-use skin care preparation.
4. have an external-use skin care preparation for white-skinned face function, use plant extract compositions as claimed in claim 1 as raw material, its weight ratio is raw material 1~8%.
5. external-use skin care preparation as claimed in claim 4, is characterized in that, described external-use skin care preparation is emulsion.
6. an emulsion of preparing as raw material using plant extract compositions claimed in claim 1, is characterized in that, comprises the composition of following weight ratio:
A phase: EDTA-2Na0.1~0.3%, card aunt 0.2~1%, glycerol 1~5%, pantothenylol 0.1~1%, trehalose 1~2%, 1,3 butylene glycol 2~4%, plant extract compositions 1~8% as claimed in claim 1, water 60~80%;
B phase: PEG-100 stearate 1~3%, cetearyl alcohol 0.5~1.5%, tristerin 0.5~1%, polyisobutylene 2~7%, sad capric acid triglyceride 1~5%, Butyrospermum parkii 0.5~3%, 2-Methylpentadecane 2~7%;
C phase: 10%NaOH0.4~2.5%, antiseptic 0.1~0.2%.
7. emulsion as claimed in claim 6, is characterized in that, raw material comprises that weight ratio is 5% plant extract compositions as claimed in claim 1.
8. for the preparation of a preparation method for the emulsion as described in claim 6 or 7, it is characterized in that, comprise the steps:
(1) water is added in kettle, add card aunt, soak 10min, dissolve completely to raw material is whole heated and stirred to 80~85 DEG C;
(2) add A other raw materials mutually, be incubated 80~85 DEG C and be stirred to the whole dissolvings of raw material completely, after insulation 10min sterilizing, be incubated for subsequent use;
(3) B phase raw material is added in oil phase pot, 80~85 DEG C of dissolvings of agitating heating completely, are incubated for subsequent use;
(4), by A phase raw material suction emulsifying pot, under homogenizing stirs, by B phase raw material suction emulsifying pot, homogenizing 5min, starts cooling after stirring insulation 10min.
(5) in the time that temperature drops to 40~45 DEG C, add C phase raw material, discharging stirs.
CN201410025242.6A 2014-01-20 2014-01-20 Plant extract composition with whitening effect, preparation and preparation method thereof Pending CN103830137A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104188863A (en) * 2014-08-28 2014-12-10 广州芭薇化妆品有限公司 Composition with anti-allergy soothing function, external preparations prepared from composition and preparation method thereof
CN104188864A (en) * 2014-08-28 2014-12-10 广州芭薇化妆品有限公司 Composition with cooling effect, externally applied preparation and preparation method thereof
CN106309244A (en) * 2016-10-09 2017-01-11 广州智媛生物科技有限公司 Whitening composition containing multiple fresh flowers and preparation method thereof
CN109846770A (en) * 2018-01-05 2019-06-07 上海珈凯生物科技有限公司 It is a kind of to have effects that slow down plant extract composition of skin irritatin and preparation method thereof, application
CN110573133A (en) * 2017-04-11 2019-12-13 宝洁公司 Cosmetic composition

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104188863A (en) * 2014-08-28 2014-12-10 广州芭薇化妆品有限公司 Composition with anti-allergy soothing function, external preparations prepared from composition and preparation method thereof
CN104188864A (en) * 2014-08-28 2014-12-10 广州芭薇化妆品有限公司 Composition with cooling effect, externally applied preparation and preparation method thereof
CN106309244A (en) * 2016-10-09 2017-01-11 广州智媛生物科技有限公司 Whitening composition containing multiple fresh flowers and preparation method thereof
CN106309244B (en) * 2016-10-09 2019-04-16 广州智媛生物科技有限公司 It is a kind of containing there are many lightening compositions of fresh flower and preparation method thereof
CN110573133A (en) * 2017-04-11 2019-12-13 宝洁公司 Cosmetic composition
CN109846770A (en) * 2018-01-05 2019-06-07 上海珈凯生物科技有限公司 It is a kind of to have effects that slow down plant extract composition of skin irritatin and preparation method thereof, application

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Application publication date: 20140604