CN104188864A - Composition with cooling effect, externally applied preparation and preparation method thereof - Google Patents
Composition with cooling effect, externally applied preparation and preparation method thereof Download PDFInfo
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- CN104188864A CN104188864A CN201410432810.4A CN201410432810A CN104188864A CN 104188864 A CN104188864 A CN 104188864A CN 201410432810 A CN201410432810 A CN 201410432810A CN 104188864 A CN104188864 A CN 104188864A
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Abstract
The invention discloses a composition with a cooling effect. The composition is prepared from the following raw materials in parts by weight: 30-50 parts of nicandra physaloides and 50-70 parts of mesona blume. The invention further provides an externally applied preparation using the composition as a raw material and a preparation method thereof. Experiments prove that the composition is a plant extract with a cooling effect, and is also a natural and non-irritative raw material for preparing a plurality of externally applied preparations with the cooling effect.
Description
Technical field
The present invention relates to a kind of compositions with refrigerant effect, relate to simultaneously and use said composition as external preparation of raw material and preparation method thereof.
Background technology
Along with the aggravation of environmental pollution, greenhouse effect is more obvious, under the impact constantly increasing, makes modern metropolitan cities people often in nervous state in operating pressure, causes skin scorching, irritated at heart.Therefore developing a product with refrigerant skin effect has Practical significance, can make user in refrigerant sensation, thereby by the refrigerant of skin, psychology be lowered the temperature.And the skin care item of pure natural are pursuing a goal of consumer always.Therefore, work out the cosmetic material that a kind of pure plant origin has refrigerant effect simultaneously and just there is profound significance.
In prior art, for refrigerant effect is provided, in external skin care, conventionally add Herba Menthae or other pennyroyal derivants as refrigerant composition, as the menthol derivative providing in Chinese patent ZL200580014806.5 and the coolant compositions that contains said components; The menthyl ester derivative gel factor and for example providing in Chinese patent application CN201210351979.8.Above-mentioned substance has refrigerant sensation, but also has the intrinsic pungent and bitter taste of Herba Menthae simultaneously, has zest.
Summary of the invention
Primary technical problem to be solved by this invention is to provide a kind of compositions with refrigerant effect.
Another technical problem to be solved by this invention is to provide a kind of preparation method of above-mentioned composition.
Invention thinking of the present invention is as follows:
Herba Nicandrae Physaloidis (another name crystal bean jelly < < Guizhou medical herbs > >, ice powder < < Yunnan Chinese herbal medicine select > >): all herbal medicine, has calmness, eliminates the phlegm, heat clearing away, removing toxic substances, cough-relieving effect.
Herba mesonae chinensis (having another name called Mesona chinensis Benth, Herba mesonae chinensis): sweet, light, cool.Clearing away heat-damp and promoting diuresis, removing heat from blood; There is clearing away summer-heat, quench one's thirst and pyretic toxicity effect.
The present invention selects above-mentioned two kinds of natural plants, utilizes modern biotechnology, makes compositions and the external preparation with refrigerant effect.
For achieving the above object, the present invention adopts following technical proposals:
A compositions with refrigerant effect, described compositions is made by the raw material of following weight portion proportioning: Herba Nicandrae Physaloidis: 30～50 weight portions; Herba mesonae chinensis: 50～70 weight portions.
The preparation method of above-mentioned composition, comprises the following steps:
(1) according to proportioning claimed in claim 1, take Herba Nicandrae Physaloidis and Herba mesonae chinensis;
(2) raw material taking with deionized water cleaning step (1), dries rear pulverizing;
(3) deionized water is mixed with taken raw material 20:1, then at 80 ℃, cool to 40 ℃ after extracting 30min;
(4) filter out extracting solution;
(5) add antiseptic, stir and be said composition.
Wherein more preferably, in step (5), antiseptic used is MTI.
Above-mentioned composition has the purposes in the external-use skin care preparation of refrigerant effect in preparation.
An external-use skin care preparation with refrigerant effect, is used above-mentioned composition as raw material, and its weight ratio is raw material 5～10%.
Use above-mentioned composition as an emulsion for raw material, comprise the composition of following weight ratio:
A phase: EDTA-2Na 0.1～0.3%, card aunt 0.2～1%, glycerol 1～5%, pantothenylol 0.1～1%, trehalose 1～2%, 1,3 butylene glycol 2～4%, above-mentioned cooling composition 5～10%, water 60～80%;
B phase: PEG-100 stearate 1～3%, cetearyl alcohol 0.5～1.5%, tristerin 0.5～1%, polyisobutylene 2～7%, sad capric acid triglyceride 1～5%, Butyrospermum parkii 0.5～3%, 2-Methylpentadecane 2～7%;
C phase: 10%NaOH 0.4～2.5%, antiseptic 0.1～0.2%.
A preparation method for above-mentioned emulsion, comprises the steps:
(1) water is added in kettle, add card aunt, soak 10min, dissolve completely to raw material is whole heated and stirred to 80～85 ℃;
(2) add A other raw materials mutually, be incubated 80～85 ℃ and be stirred to the whole dissolvings of raw material completely, after insulation 10min sterilizing, be incubated standby;
(3) B phase raw material is added in oil phase pot, 80～85 ℃ of dissolvings of agitating heating completely, are incubated standby;
(4), by A phase raw material suction emulsifying pot, under stirring, homogenizing by B phase raw material suction emulsifying pot, in homogenizing 5min, after stirring insulation 10min, starts cooling;
(5) when temperature drops to 40～45 ℃, add C phase raw material, discharging stirs.
Use above-mentioned composition as a facial film for raw material, comprise the composition of following weight ratio:
A group: EDTA-2Na 0.1%, HANSHENGJIAO 0.4%, glycerol 3%, pantothenylol 0.5%, trehalose 2%, 1,3 butylene glycol 3%, above-mentioned cooling composition 5%, hyaluronic acid 0.05%, water surplus;
B group: antiseptic 0.15%.
The preparation method of above-mentioned facial film, comprises the steps:
(1) A phase raw material is added in master cylinder, be incubated 80～85 ℃ and be stirred to the whole dissolvings of raw material completely, after insulation 10min sterilizing, start cooling;
(2) when temperature drops to 40～45 ℃, add B phase raw material, discharging stirs.
Compositions provided by the invention has refrigerant effect, is a kind of natural non-stimulated raw material, can be used for preparing the multiple external preparation with refrigerant effect.And different according to use approach, the external-use skin care preparation that the compositions with refrigerant effect provided by the invention is made as raw material, is not limited to emulsion, facial film, also can be made into cleansing milk, facial cream etc.Can, according to method known in skin care item industrial circle, above-mentioned composition be made to various external preparation.
The specific embodiment
Foregoing invention content part has been done detailed description to technical scheme of the present invention, and those skilled in the art can repeat the present invention and obtain technique effect of the present invention according to foregoing.Below by the specific embodiment, the technology of the present invention content is further explained, so that those skilled in the art are clearer, understands content of the present invention, limitation of the present invention not, any being equal to, replaces or known change all belongs to protection domain of the present invention.
Embodiment 1 has the preparation of the compositions of refrigerant effect
The present invention selects Herba Nicandrae Physaloidis, Herba mesonae chinensis two kind of plant, makes the compositions with refrigerant effect.Its concrete composition proportion and preparation process are as follows:
(1) by following weight proportion, take Herba Nicandrae Physaloidis and Herba mesonae chinensis: Herba Nicandrae Physaloidis: 30～50 weight portions; Herba mesonae chinensis: 50～70 weight portions.Herba Nicandrae Physaloidis and Herba mesonae chinensis are got herb as raw material.
(2) raw material taking by the washed with de-ionized water step (1) of 50 times, dries rear pulverizing;
(3) deionized water is mixed with taken raw material 20:1, then at 80 ℃, cool to 40 ℃ after extracting 30min;
(4) filter out extracting solution;
(5) add antiseptic, stir and be said composition.Antiseptic used can be selected MTI.
Embodiment 2 has the preparation of the emulsion of refrigerant effect
The component of emulsion and consumption thereof
A phase: EDTA-2Na 0.1～0.3%, card aunt 0.2～1%, glycerol 1～5%, pantothenylol 0.1～1%, trehalose 1～2%, 1,3 butylene glycol 2～4%, the cooling composition 5～10% of embodiment 1 preparation, water 60～80%;
B phase: PEG-100 stearate 1～3%, cetearyl alcohol 0.5～1.5%, tristerin 0.5～1%, polyisobutylene 2～7%, sad capric acid triglyceride 1～5%, Butyrospermum parkii 0.5～3%, 2-Methylpentadecane 2～7%;
C phase: 10%NaOH 0.4～2.5%, antiseptic 0.1～0.2%.
Preparation method:
(1) water is added in kettle, add card aunt, soak 10min, dissolve completely to raw material is whole heated and stirred to 80～85 ℃;
(2) add A other raw materials mutually, be incubated 80～85 ℃ and be stirred to the whole dissolvings of raw material completely, after insulation 10min sterilizing, be incubated standby;
(3) B phase raw material is added in oil phase pot, 80～85 ℃ of dissolvings of agitating heating completely, are incubated standby;
(4), by A phase raw material suction emulsifying pot, under stirring, homogenizing by B phase raw material suction emulsifying pot, in homogenizing 5min, after stirring insulation 10min, starts cooling;
(5) when temperature drops to 40～45 ℃, add C phase raw material, discharging stirs.
Embodiment 3 has the preparation of the emulsion of refrigerant effect
The component of emulsion and consumption thereof
A phase: EDTA-2Na 0.1%, card aunt 0.2%, glycerol 3%, pantothenylol 0.5%, trehalose 2%, 1,3 butylene glycol 3%, the cooling composition 5% of embodiment 1 preparation, water surplus;
B phase: PEG-100 stearate 2%, cetearyl alcohol 1%, tristerin 0.5%, polyisobutylene 4%, sad capric acid triglyceride 2%, Butyrospermum parkii 1%, 2-Methylpentadecane 2%;
C phase: 10%NaOH 0.4～2.5%, antiseptic 0.1～0.2%.
Preparation method:
(1) water is added in kettle, add card aunt, soak 10min, dissolve completely to raw material is whole heated and stirred to 80～85 ℃;
(2) add A other raw materials mutually, be incubated 80～85 ℃ and be stirred to the whole dissolvings of raw material completely, after insulation 10min sterilizing, be incubated standby;
(3) B phase raw material is added in oil phase pot, 80～85 ℃ of dissolvings of agitating heating completely, are incubated standby;
(4), by A phase raw material suction emulsifying pot, under stirring, homogenizing by B phase raw material suction emulsifying pot, in homogenizing 5min, after stirring insulation 10min, starts cooling;
(5) when temperature drops to 40～45 ℃, add C phase raw material, discharging stirs.
Embodiment 4 has the preparation of the facial film of refrigerant effect
The component of facial film and consumption thereof
A group: EDTA-2Na 0.1%, HANSHENGJIAO 0.4%, glycerol 3%, pantothenylol 0.5%, trehalose 2%, 1,3 butylene glycol 3%, the cooling composition 5% of embodiment 1 preparation, hyaluronic acid 0.05%, water surplus;
B group: antiseptic 0.15%.
Preparation method:
(1) A phase raw material is added in master cylinder, be incubated 80～85 ℃ and be stirred to the whole dissolvings of raw material completely, after insulation 10min sterilizing, start cooling;
(2) when temperature drops to 40～45 ℃, add B phase raw material, discharging stirs.
The refrigerant efficacy test of the emulsion that embodiment 5 contains 5% cooling composition
Experimental technique:
Volunteer is selected: the volunteer of participation experiment is totally 30 people, and wherein male is 8,22 of women, and the age was at 18～48 years old.
Evaluation methodology: experiment adopts the emulsion (emulsions of embodiment 2 preparations) of the cooling composition that contains 5.0% to smear volunteer's skin, and does not contrast containing cooling composition emulsion, allows volunteer perception cooling effect contrast.
Evaluation methodology: judge by the refrigerant degree of volunteer subjective sensation.Refrigerant degree is divided into following 3 grades:
0: there is no cooling effect.
1: there is slight cooling sensation.
2: cooling sensation is obvious.
Experimental result is as shown in table 1.
The refrigerant efficacy data of the emulsion that table 1 contains cooling composition
As can be seen from Table 1, the cooling effect of the emulsion of interpolation 5% cooling composition is significantly better than blank group emulsion.As can be seen here, compositions provided by the invention has good refrigerant effect, is a kind of natural non-stimulated natural material, can be used for making the multiple external preparation with refrigerant effect.
Above the compositions with refrigerant effect provided by the present invention, external preparation and preparation method thereof are had been described in detail.For one of ordinary skill in the art, any apparent change of under the prerequisite that does not deviate from connotation of the present invention, it being done, all will form infringement of patent right of the present invention, will bear corresponding legal responsibility.
Claims (9)
1. a compositions with refrigerant effect, is characterized in that: described compositions is made by the raw material of following weight portion proportioning:
Herba Nicandrae Physaloidis: 30～50 weight portions; Herba mesonae chinensis: 50～70 weight portions.
2. a preparation method for compositions as claimed in claim 1, is characterized in that comprising the following steps:
(1) according to proportioning claimed in claim 1, take Herba Nicandrae Physaloidis and Herba mesonae chinensis;
(2) raw material taking with deionized water cleaning step (1), dries rear pulverizing;
(3) deionized water is mixed with taken raw material 20:1, then at 80 ℃, cool to 40 ℃ after extracting 30min;
(4) filter out extracting solution;
(5) add antiseptic, stir and be said composition.
3. preparation method as claimed in claim 2, is characterized in that:
In step (5), antiseptic used is MTI.
4. compositions as claimed in claim 1 has the purposes in the external-use skin care preparation of refrigerant effect in preparation.
5. an external-use skin care preparation with refrigerant effect, is used compositions as claimed in claim 1 as raw material, and its weight ratio is raw material 5～10%.
6. use compositions as claimed in claim 1 as an emulsion for raw material, it is characterized in that comprising the composition of following weight ratio:
A phase: EDTA-2Na 0.1～0.3%, card aunt 0.2～1%, glycerol 1～5%, pantothenylol 0.1～1%, trehalose 1～2%, 1,3 butylene glycol 2～4%, cooling composition 5～10% as claimed in claim 1, water 60～80%;
B phase: PEG-100 stearate 1～3%, cetearyl alcohol 0.5～1.5%, tristerin 0.5～1%, polyisobutylene 2～7%, sad capric acid triglyceride 1～5%, Butyrospermum parkii 0.5～3%, 2-Methylpentadecane 2～7%;
C phase: 10%NaOH 0.4～2.5%, antiseptic 0.1～0.2%.
7. a preparation method for emulsion as claimed in claim 6, is characterized in that comprising the steps:
(1) water is added in kettle, add card aunt, soak 10min, dissolve completely to raw material is whole heated and stirred to 80～85 ℃;
(2) add A other raw materials mutually, be incubated 80～85 ℃ and be stirred to the whole dissolvings of raw material completely, after insulation 10min sterilizing, be incubated standby;
(3) B phase raw material is added in oil phase pot, 80～85 ℃ of dissolvings of agitating heating completely, are incubated standby;
(4), by A phase raw material suction emulsifying pot, under stirring, homogenizing by B phase raw material suction emulsifying pot, in homogenizing 5min, after stirring insulation 10min, starts cooling;
(5) when temperature drops to 40～45 ℃, add C phase raw material, discharging stirs.
8. use compositions as claimed in claim 1 as a facial film for raw material, it is characterized in that comprising the composition of following weight ratio:
A group: EDTA-2Na 0.1%, HANSHENGJIAO 0.4%, glycerol 3%, pantothenylol 0.5%, trehalose 2%, 1,3 butylene glycol 3%, cooling composition 5% as claimed in claim 1, hyaluronic acid 0.05%, water surplus;
B group: antiseptic 0.15%.
9. a preparation method for facial film as claimed in claim 8, is characterized in that comprising the steps:
(1) A phase raw material is added in master cylinder, be incubated 80～85 ℃ and be stirred to the whole dissolvings of raw material completely, after insulation 10min sterilizing, start cooling;
(2) when temperature drops to 40～45 ℃, add B phase raw material, discharging stirs.
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| CN201410432810.4A CN104188864B (en) | 2014-08-28 | 2014-08-28 | Composition with cooling effect, externally applied preparation and preparation method thereof |
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| CN201410432810.4A CN104188864B (en) | 2014-08-28 | 2014-08-28 | Composition with cooling effect, externally applied preparation and preparation method thereof |
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| CN104188864B CN104188864B (en) | 2017-05-03 |
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Cited By (1)
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| CN104546622A (en) * | 2015-02-04 | 2015-04-29 | 孙志平 | Pure natural plant skin-care product, and extraction process and extraction equipment thereof |
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| JPH11209262A (en) * | 1997-10-28 | 1999-08-03 | Kao Corp | Preparation for external use for skin |
| CN103462879A (en) * | 2013-09-27 | 2013-12-25 | 北京美丽铺化妆品有限公司 | Tremella mud with moisturizing effect, facial mask and preparation method thereof |
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| CN104546622A (en) * | 2015-02-04 | 2015-04-29 | 孙志平 | Pure natural plant skin-care product, and extraction process and extraction equipment thereof |
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