CN104188864B - Composition with cooling effect, externally applied preparation and preparation method thereof - Google Patents
Composition with cooling effect, externally applied preparation and preparation method thereof Download PDFInfo
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- CN104188864B CN104188864B CN201410432810.4A CN201410432810A CN104188864B CN 104188864 B CN104188864 B CN 104188864B CN 201410432810 A CN201410432810 A CN 201410432810A CN 104188864 B CN104188864 B CN 104188864B
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Abstract
The invention discloses a composition with a cooling effect. The composition is prepared from the following raw materials in parts by weight: 30-50 parts of nicandra physaloides and 50-70 parts of mesona blume. The invention further provides an externally applied preparation using the composition as a raw material and a preparation method thereof. Experiments prove that the composition is a plant extract with a cooling effect, and is also a natural and non-irritative raw material for preparing a plurality of externally applied preparations with the cooling effect.
Description
Technical field
The present invention relates to a kind of compositionss with refrigerant effect, while being directed to use with said composition as the external of raw material
Preparation and preparation method thereof.
Background technology
With the aggravation of environmental pollution, greenhouse effect is more obvious, under the influence of operating pressure constantly increases so that existing
For city people often in nervous state, cause skin scorching, it is irritated at heart.Therefore develop a with refrigerant skin effect
The product of fruit has Practical significance, can make user in refrigerant sensation, psychology be entered so as to pass through the refrigerant of skin
Row cooling.And the skin care item of pure natural are always pursuing a goal for consumer.Therefore, a kind of pure plant origin is worked out while tool
The cosmetic material for having refrigerant effect just has far-reaching significance.
In prior art, in order to provide refrigerant effect, generally add Herba Menthae or other Herba Menthaes in external skin care
Analog derivative is as cooling ingredient, the menthol derivative provided in such as Chinese patent ZL200580014806.5 and containing upper
State the coolant compositions of component；The menthyl ester derivative gel for and for example providing in Chinese patent application CN201210351979.8
The factor.Above-mentioned substance has a refrigerant sensation, but while the pungent and bitter taste for also having Herba Menthae intrinsic, with zest.
The content of the invention
Primary technical problem to be solved by this invention is to provide a kind of compositionss with refrigerant effect.
Another technical problem to be solved by this invention is to provide a kind of preparation method of above-mentioned composition.
The invention thinking of the present invention is as follows：
Herba Nicandrae Physaloidis (another name crystal bean jelly《Guizhou medical herbs》, ice powder《Yunnan Chinese herbal medicine choosing》)：All herbal medicine, with it is calm,
Eliminating the phlegm, heat clearing away, removing toxic substances, cough-relieving effect.
Herba mesonae chinensis (also known as Mesona chinensis Benth, Herba mesonae chinensiss)：It is sweet, light, it is cool.Clearing away heat-damp and promoting diuresis, removing heat from blood；With clearing away summer-heat, quench one's thirst and pyretic toxicity work(
Effect.
The present invention selects above two natural plants, using modern biotechnology, the compositionss with refrigerant effect is obtained
And external preparation.
For achieving the above object, the present invention adopts following technical proposals：
A kind of compositionss with refrigerant effect, the compositionss are obtained by the raw material of following weight：Herba Nicandrae Physaloidis：
30～50 weight portions；Herba mesonae chinensis：50～70 weight portions.
The preparation method of above-mentioned composition, comprises the following steps：
(1) Herba Nicandrae Physaloidis and Herba mesonae chinensis are weighed according to said ratio；
(2) raw material that deionized water cleaning step (1) is weighed, crushes after drying；
(3) by deionized water and the raw material 20 for being weighed:1 mixing, cools to 40 after then carrying out extraction 30min at 80 DEG C
℃；
(4) filter out extracting solution；
(5) preservative is added, is stirred as said composition.
Wherein more preferably, in step (5), preservative used is MTI.
Purposes of the above-mentioned composition in the external-use skin care preparation with refrigerant effect is prepared.
A kind of external-use skin care preparation with refrigerant effect, raw material include above-mentioned composition, and the compositionss account for raw material
The weight ratio of total amount is 5～10%.
A kind of emulsion for using above-mentioned composition as raw material, including the composition of following weight ratio：
A phases：EDTA-2Na 0.1～0.3%, carbomer 0.2～1%, glycerol 1～5%, pantothenylol 0.1～1%, trehalose
1～2%, 1,3 butylene glycol 2～4%, above-mentioned cooling composition 5～10%, water 60～80%；
B phases：PEG-100 stearates 1～3%, cetearyl alcohol 0.5～1.5%, tristerin 0.5～1%,
Polyisobutylene 2～7%, caprylic capric triglyceride 1～5%, Butyrospermum parkii fruit fat 0.5～3%, 2-Methylpentadecane 2～7%；
C phases：10%NaOH 0.4～2.5%, preservative 0.1～0.2%.
A kind of preparation method of above-mentioned emulsion, comprises the steps：
(1) add water in kettle, add carbomer, soak 10min, heated and stirred is all molten to raw material to 80～85 DEG C
Solution is complete；
(2) other raw materials of addition A phases, 80～85 DEG C of insulation are stirred to raw material and all dissolve complete, after being incubated 10min sterilizings
Insulation is standby；
(3) B phases raw material is added in oil phase pot, 80～85 DEG C of dissolvings of agitating heating are complete, are incubated standby；
(4) by A phase raw material suction emulsifying pots, by B phase raw material suction emulsifying pots under homogenizing stirring, homogenizing 5min
In, start cooling after stirring insulation 10min；
(5) C phase raw materials are added when temperature drops to 40～45 DEG C, stir discharging.
A kind of facial film for using above-mentioned composition as raw material, including the composition of following weight ratio：
A groups：EDTA-2Na 0.1%, HANSHENGJIAO 0.4%, glycerol 3%, pantothenylol 0.5%, trehalose 2%, 1,3 butylene glycol
3%, above-mentioned cooling composition 5%, hyaluronic acid 0.05%, water surplus；
B groups：Preservative 0.15%.
The preparation method of above-mentioned facial film, comprises the steps：
(1) A phases raw material is added in master cylinder, 80～85 DEG C of insulation is stirred to raw material and all dissolves complete, and insulation 10min goes out
Start cooling after bacterium；
(2) B phase raw materials are added when temperature drops to 40～45 DEG C, stir discharging.
The compositionss that the present invention is provided have refrigerant effect, are a kind of natural inirritative raw materials, can be used for preparation many
Plant the external preparation with refrigerant effect.Also, according to, combination with refrigerant effect that the present invention provide different using approach
Thing is used as external-use skin care preparation made by raw material, however it is not limited to emulsion, facial film, can also be fabricated to cleansing milk, facial cream etc..Can be according to
In skin care industry field, above-mentioned composition is made a variety of external preparation by known method.
Specific embodiment
Detailed description, those skilled in the art root have been done to technical scheme in foregoing invention content part
The present invention is repeated according to the above and technique effect of the present invention is obtained.Below by specific embodiment to this
Bright technology contents are further explained, so that those skilled in the art are clearer to understand present invention, not to this
Bright restriction, any equivalent or known change belong to the scope of the present invention.
Embodiment 1 has the preparation of the compositionss of refrigerant effect
The present invention selects Herba Nicandrae Physaloidis, two kinds of plants of Herba mesonae chinensis, and the compositionss with refrigerant effect are obtained.Its concrete composition proportion
And preparation process is as follows：
(1) Herba Nicandrae Physaloidis and Herba mesonae chinensis are weighed by following weight proportions：Herba Nicandrae Physaloidis：30～50 weight portions；Herba mesonae chinensis：50～70 weight
Part.Herba Nicandrae Physaloidis and Herba mesonae chinensis take herb as raw material.
(2) raw material weighed with 50 times of deionized water cleaning step (1), crushes after drying；
(3) by deionized water and the raw material 20 for being weighed:1 mixing, cools to 40 after then carrying out extraction 30min at 80 DEG C
℃；
(4) filter out extracting solution；
(5) preservative is added, is stirred as said composition.Preservative used can select MTI.
Embodiment 2 has the preparation of the emulsion of refrigerant effect
The component and its consumption of emulsion
A phases：EDTA-2Na 0.1～0.3%, carbomer 0.2～1%, glycerol 1～5%, pantothenylol 0.1～1%, trehalose
1～2%, 1,3 butylene glycol 2～4%, cooling composition 5～10% prepared by embodiment 1, water 60～80%；
B phases：PEG-100 stearates 1～3%, cetearyl alcohol 0.5～1.5%, tristerin 0.5～1%,
Polyisobutylene 2～7%, caprylic capric triglyceride 1～5%, Butyrospermum parkii fruit fat 0.5～3%, 2-Methylpentadecane 2～7%；
C phases：10%NaOH 0.4～2.5%, preservative 0.1～0.2%.
Preparation method：
(1) add water in kettle, add carbomer, soak 10min, heated and stirred is all molten to raw material to 80～85 DEG C
Solution is complete；
(2) other raw materials of addition A phases, 80～85 DEG C of insulation are stirred to raw material and all dissolve complete, after being incubated 10min sterilizings
Insulation is standby；
(3) B phases raw material is added in oil phase pot, 80～85 DEG C of dissolvings of agitating heating are complete, are incubated standby；
(4) by A phase raw material suction emulsifying pots, by B phase raw material suction emulsifying pots under homogenizing stirring, homogenizing 5min
In, start cooling after stirring insulation 10min；
(5) C phase raw materials are added when temperature drops to 40～45 DEG C, stir discharging.
Embodiment 3 has the preparation of the emulsion of refrigerant effect
The component and its consumption of emulsion
A phases：EDTA-2Na 0.1%, carbomer 0.2%, glycerol 3%, pantothenylol 0.5%, trehalose 2%, 1,3 butylene glycol
3%, cooling composition 5% prepared by embodiment 1, water surplus；
B phases：PEG-100 stearates 2%, cetearyl alcohol 1%, tristerin 0.5%, polyisobutylene 4% are pungent
Sour capric acid triglyceride 2%, Butyrospermum parkii fruit fat 1%, 2-Methylpentadecane 2%；
C phases：10%NaOH 0.4～2.5%, preservative 0.1～0.2%.
Preparation method：
(1) add water in kettle, add carbomer, soak 10min, heated and stirred is all molten to raw material to 80～85 DEG C
Solution is complete；
(2) other raw materials of addition A phases, 80～85 DEG C of insulation are stirred to raw material and all dissolve complete, after being incubated 10min sterilizings
Insulation is standby；
(3) B phases raw material is added in oil phase pot, 80～85 DEG C of dissolvings of agitating heating are complete, are incubated standby；
(4) by A phase raw material suction emulsifying pots, by B phase raw material suction emulsifying pots under homogenizing stirring, homogenizing 5min
In, start cooling after stirring insulation 10min；
(5) C phase raw materials are added when temperature drops to 40～45 DEG C, stir discharging.
Embodiment 4 has the preparation of the facial film of refrigerant effect
The component and its consumption of facial film
A groups：EDTA-2Na 0.1%, HANSHENGJIAO 0.4%, glycerol 3%, pantothenylol 0.5%, trehalose 2%, 1,3 butylene glycol
3%, cooling composition 5% prepared by embodiment 1, hyaluronic acid 0.05%, water surplus；
B groups：Preservative 0.15%.
Preparation method：
(1) A phases raw material is added in master cylinder, 80～85 DEG C of insulation is stirred to raw material and all dissolves complete, and insulation 10min goes out
Start cooling after bacterium；
(2) B phase raw materials are added when temperature drops to 40～45 DEG C, stir discharging.
The refrigerant efficacy test of emulsion of the embodiment 5 containing 5% cooling composition
Experimental technique：
Volunteer is selected：Participate in volunteer totally 30 people, wherein male 8 of experiment, women 22, the age is 18～48
Year.
Evaluation methodology：Experiment smears will using the emulsion containing 5.0% cooling composition (emulsion prepared by embodiment 2)
Hope person's skin, and contrast without cooling composition emulsion, allow volunteer to perceive cooling effect and contrast.
Evaluation methodology：Judged by the refrigerant degree of volunteer subjective sensation.Refrigerant degree is divided into following 3 grades：
0：Without cooling effect.
1：With slight cooling sensation.
2：Cooling sensation is obvious.
Experimental result is as shown in table 1.
The refrigerant efficacy data of emulsion of the table 1 containing cooling composition
As it can be seen from table 1 the cooling effect of the emulsion of 5% cooling composition of addition is significantly better than blank control group breast
Liquid.As can be seen here, the compositionss that the present invention is provided have good refrigerant effect, are a kind of natural inirritative natural materials,
Can be used to make various external preparation with refrigerant effect.
Above the compositionss with refrigerant effect provided by the present invention, external preparation and preparation method thereof have been carried out in detail
Thin explanation.For one of ordinary skill in the art, it is done on the premise of without departing substantially from true spirit
Any obvious change, all will constitute to infringement of patent right of the present invention, will undertake corresponding legal responsibility.
Claims (7)
1. a kind of compositionss with refrigerant effect, have the external-use skin care preparation of refrigerant effect for preparation, it is characterised in that：
The compositionss are obtained by the raw material of following weight：
Herba Nicandrae Physaloidis：30～50 weight portions；Herba mesonae chinensis：50～70 weight portions；
Also, the preparation method of the compositionss, comprises the following steps：
(1) Herba Nicandrae Physaloidis and Herba mesonae chinensis are weighed according to said ratio；
(2) raw material that deionized water cleaning step (1) is weighed, crushes after drying；
(3) by deionized water and the raw material 20 for being weighed:1 mixing, cools to 40 DEG C after then carrying out extraction 30min at 80 DEG C；
(4) filter out extracting solution；
(5) preservative is added, is stirred as said composition.
2. compositionss as claimed in claim 1, it is characterised in that：
In step (5), preservative used is MTI.
3. a kind of external-use skin care preparation with refrigerant effect, it is characterised in that raw material includes as claimed in claim 1 group
Compound, it is 5～10% that the compositionss account for the weight ratio of raw material total amount.
4. it is a kind of using compositionss as claimed in claim 1 as raw material emulsion, it is characterised in that including following weight ratio
Composition：
A phases：EDTA-2Na 0.1～0.3%, carbomer 0.2～1%, glycerol 1～5%, pantothenylol 0.1～1%, trehalose 1～
2%, 1,3 butylene glycol 2～4%, cooling composition as claimed in claim 1 5～10%, water 60～80%；
B phases：PEG-100 stearates 1～3%, cetearyl alcohol 0.5～1.5%, tristerin 0.5～1% gather different
Butylene 2～7%, caprylic capric triglyceride 1～5%, Butyrospermum parkii fruit fat 0.5～3%, 2-Methylpentadecane 2～7%；
C phases：10%NaOH 0.4～2.5%, preservative 0.1～0.2%.
5. a kind of preparation method of emulsion as claimed in claim 4, it is characterised in that comprise the steps：
(1) add water in kettle, add carbomer, soak 10min, heated and stirred to 80～85 DEG C to raw material has all dissolved
Entirely；
(2) other raw materials of addition A phases, 80～85 DEG C of insulation are stirred to raw material and all dissolve complete, are incubated after being incubated 10min sterilizings
It is standby；
(3) B phases raw material is added in oil phase pot, 80～85 DEG C of dissolvings of agitating heating are complete, are incubated standby；
(4) by A phase raw material suction emulsifying pots, by B phase raw material suction emulsifying pots under homogenizing stirring, in homogenizing 5min, stir
Start cooling after mixing insulation 10min；
(5) C phase raw materials are added when temperature drops to 40～45 DEG C, stir discharging.
6. it is a kind of using compositionss as claimed in claim 1 as raw material facial film, it is characterised in that including following weight ratio
Composition：
A groups：EDTA-2Na 0.1%, HANSHENGJIAO 0.4%, glycerol 3%, pantothenylol 0.5%, trehalose 2%, 1,3 butylene glycol 3%,
Cooling composition 5% as claimed in claim 1, hyaluronic acid 0.05%, water surplus；
B groups：Preservative 0.15%.
7. a kind of preparation method of facial film as claimed in claim 6, it is characterised in that comprise the steps：
(1) A phases raw material is added in master cylinder, 80～85 DEG C of insulation is stirred to raw material and all dissolves complete, after insulation 10min sterilizings
Start cooling；
(2) B phase raw materials are added when temperature drops to 40～45 DEG C, stir discharging.
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| CN201410432810.4A CN104188864B (en) | 2014-08-28 | 2014-08-28 | Composition with cooling effect, externally applied preparation and preparation method thereof |
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| CN201410432810.4A CN104188864B (en) | 2014-08-28 | 2014-08-28 | Composition with cooling effect, externally applied preparation and preparation method thereof |
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| CN104546622A (en) * | 2015-02-04 | 2015-04-29 | 孙志平 | Pure natural plant skin-care product, and extraction process and extraction equipment thereof |
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| JP2985083B2 (en) * | 1997-10-28 | 1999-11-29 | 花王株式会社 | External preparation for skin |
| CN103462879B (en) * | 2013-09-27 | 2016-03-30 | 北京美泥铺化妆品有限公司 | There is the tremella mud of moist effect, facial film and preparation method thereof |
| CN103830137A (en) * | 2014-01-20 | 2014-06-04 | 上海珈叶生物技术有限公司 | Plant extract composition with whitening effect, preparation and preparation method thereof |
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Non-Patent Citations (2)
| Title |
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| 《清凉化合物及其风味特性》;刘晓庚等;《粮食与油脂》;20081231(第11期);第44-47页，尤其是第44页左栏第1段，第45页左栏第1段和表1 * |
| 《超临界CO2萃取法与水蒸气蒸馏法提取凉粉草挥发油及其GC-MS分析》;陈飞龙等;《中药材》;20120831;第35卷(第8期);第1270-1273页，尤其是第1272页表1 * |
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Address after: 510440, 18, Luo Gang Industrial Area, Baiyun District, Guangdong, Guangzhou Applicant after: GUANGDONG BAWEI BIOLOGICAL TECHNOLOGY CO., LTD. Address before: 510440, 18, Luo Gang Industrial Area, Baiyun District, Guangdong, Guangzhou Applicant before: GUANGZHOU BAWEI COSMETICS CO., LTD. |
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