CN107157851A - A kind of preparation method of chamomile tearing facial mask - Google Patents

A kind of preparation method of chamomile tearing facial mask Download PDF

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Publication number
CN107157851A
CN107157851A CN201710485198.0A CN201710485198A CN107157851A CN 107157851 A CN107157851 A CN 107157851A CN 201710485198 A CN201710485198 A CN 201710485198A CN 107157851 A CN107157851 A CN 107157851A
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CN
China
Prior art keywords
chamomile
facial mask
parts
phase liquid
preparation
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201710485198.0A
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Chinese (zh)
Inventor
刘鹏飞
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Wuhu Dream Agel Ecommerce Ltd
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Wuhu Dream Agel Ecommerce Ltd
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Priority to CN201710485198.0A priority Critical patent/CN107157851A/en
Publication of CN107157851A publication Critical patent/CN107157851A/en
Withdrawn legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/74Biological properties of particular ingredients
    • A61K2800/78Enzyme modulators, e.g. Enzyme agonists
    • A61K2800/782Enzyme inhibitors; Enzyme antagonists

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Dermatology (AREA)
  • Epidemiology (AREA)
  • Engineering & Computer Science (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Biotechnology (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Cosmetics (AREA)

Abstract

A kind of preparation method of chamomile tearing facial mask, belongs to cosmetic technical field.The preparation method of the present invention includes:Poly-vinyl alcohol solution is prepared, camomile extract is prepared, prepares aqueous phase liquid, prepare oil phase liquid, prepare Essence, prepare tearing facial mask.Chamomile has effects that anti-oxidant and suppression tyrosinase activity, can be with whitening and anti-aging.Fibroin has effects that repairing skin tissue's cell.The facial mask natural component of the present invention is high, easily absorb, and preparation method is simple.

Description

A kind of preparation method of chamomile tearing facial mask
Technical field
The invention belongs to cosmetic technical field, and in particular to a kind of preparation method of chamomile tearing facial mask.
Background technology
Facial mask is a kind of cleaning, nursing, the cosmetics and skincare product of nutrition skin of face.Air-isolation and dirt in the facial mask short time Thing is contaminated, the surface temperature of skin of face is lifted, pore is expanded, promotes sweat gland secretion, accelerates metabolism, help excludes facial oil Fat and metabolin, so as to be penetrated into beneficial to the functional component in facial mask, are nourished skin, reach that tender skin, skin lightening, whitening are equivalent Really.Product function is segmented and product safety environmental protection is following development trend in facial mask market, and abstraction function is lived from natural materials Property material is as raw material by an importance as facial mask future development.It is more next on the basis of everybody has a love of beauty Trend is more inclined to naturally, the facial mask of natural environmental-protective enjoys consumers.The existing commercially available facial mask of current China has certain chemistry Composition, can be damaged to the skin of human body, and Essence is difficult to absorb.
The content of the invention
In order to solve problems of the prior art, the invention provides a kind of natural component it is high, easily absorb it is foreign sweet The preparation method of chrysanthemum tearing facial mask.
The present invention uses following technical scheme:
A kind of preparation method of chamomile tearing facial mask, comprises the following steps:
Step one:By 10g polyvinyl alcohol, 10g polyvinyl acetate, the ethanol that 10g volumetric concentrations are 75%, mixing is equal Even, 120W magnetic agitation 2h, obtain poly-vinyl alcohol solution;
Step 2:25kg chamomiles are taken, coarse powder is ground into, volatile ingredient is removed through steam distillation, ocean are obtained sweet Chrysanthemum residue, by solid-liquid ratio 1:5 add the ethanol that volumetric concentration is 95%, and 3h is extracted in stirring under the conditions of 50 DEG C, filters to take supernatant Liquid, repeats to extract 2 times;
Step 3:2 gained supernatants are merged, are concentrated under reduced pressure untill without ethanol, the extraction of chamomile ethanol is produced Thing;
Step 4:Suspension is made in the deionized water for taking chamomile ethanol extract to add 5 times of volumes thereto, to suspended Add the petroleum ether of 1 times of volume to extract 3h at room temperature in liquid, petroleum ether is mutually concentrated under reduced pressure after removal petroleum ether after layering, produced Camomile extract;
Step 5:According to the mass fraction, 10 parts of glycerine, 4 parts of propane diols, 1 part of fibroin, 0.4 part of triethanolamine are added Enter into 78 parts of deionized waters, 80 DEG C of heating stirrings are until dissolving, is made aqueous phase liquid;
Step 6:According to the mass fraction, by 2 parts of camomile extracts, 2 parts of methyl-silicone oils, 3 parts of monoglycerides, 1.2 parts of polyoxies Ethene Span 20,0.4 part of xanthan gum, stir under the conditions of 80 DEG C, oil phase liquid are made;
Step 7:Under conditions of being stirred continuously, oil phase liquid made from step 6 is added slowly to step 5 and is made Aqueous phase liquid in, described oil phase liquid and the mass ratio of aqueous phase liquid are 1:9,15min is stirred using high speed disperser, is cooled down out Material, both obtains Essence;
Step 8:By poly-vinyl alcohol solution and Essence in mass ratio 4:6 are mixed evenly, and obtain tearing facial mask.
It is preferred that, the mixing speed of the high speed disperser described in step 7 is 5000r/min.
It is preferred that, the crushing described in step 2 uses LD-Y400A high speed Universal pulverizers.
The beneficial effects of the present invention are:
1) chamomile has effects that anti-oxidant and suppresses tyrosinase activity, can be with whitening and anti-aging.
2) fibroin has effects that repairing skin tissue's cell.
3) facial mask natural component of the invention is high, easily absorb, and preparation method is simple.
Embodiment
Below with reference to specific embodiment, the present invention is described further.
Embodiment 1
A kind of preparation method of chamomile tearing facial mask, comprises the following steps:
Step one:By 10g polyvinyl alcohol, 10g polyvinyl acetate, the ethanol that 10g volumetric concentrations are 75%, mixing is equal Even, 120W magnetic agitation 2h, obtain poly-vinyl alcohol solution;
Step 2:25kg chamomiles are taken, coarse powder is ground into, volatile ingredient is removed through steam distillation, ocean are obtained sweet Chrysanthemum residue, by solid-liquid ratio 1:5 add the ethanol that volumetric concentration is 95%, and 3h is extracted in stirring under the conditions of 50 DEG C, filters to take supernatant Liquid, repeats to extract 2 times;
Step 3:2 gained supernatants are merged, are concentrated under reduced pressure untill without ethanol, the extraction of chamomile ethanol is produced Thing;
Step 4:Suspension is made in the deionized water for taking chamomile ethanol extract to add 5 times of volumes thereto, to suspended Add the petroleum ether of 1 times of volume to extract 3h at room temperature in liquid, petroleum ether is mutually concentrated under reduced pressure after removal petroleum ether after layering, produced Camomile extract;
Step 5:According to the mass fraction, 10 parts of glycerine, 4 parts of propane diols, 1 part of fibroin, 0.4 part of triethanolamine are added Enter into 78 parts of deionized waters, 80 DEG C of heating stirrings are until dissolving, is made aqueous phase liquid;
Step 6:According to the mass fraction, by 2 parts of camomile extracts, 2 parts of methyl-silicone oils, 3 parts of monoglycerides, 1.2 parts of polyoxies Ethene Span 20,0.4 part of xanthan gum, stir under the conditions of 80 DEG C, oil phase liquid are made;
Step 7:Under conditions of being stirred continuously, oil phase liquid made from step 6 is added slowly to step 5 and is made Aqueous phase liquid in, described oil phase liquid and the mass ratio of aqueous phase liquid are 1:9,15min is stirred using high speed disperser, is cooled down out Material, both obtains Essence;
Step 8:By poly-vinyl alcohol solution and Essence in mass ratio 4:6 are mixed evenly, and obtain tearing facial mask.
The mixing speed of high speed disperser described in step 7 is 5000r/min.
Crushing described in step 2 uses LD-Y400A high speed Universal pulverizers.
The performance comparison result of facial mask made from the embodiment of the present invention 1 and same type facial mask on the market see the table below 1.
Table 1
Sequence number Test event Embodiment 1 Same type facial mask
1 Essence infiltration rate Comparatively fast Typically
2 Moisture preserving time (h) 20h 18h
3 Glossiness It is glossy It is glossy

Claims (3)

1. a kind of preparation method of chamomile tearing facial mask, it is characterised in that comprise the following steps:
Step one:By 10g polyvinyl alcohol, 10g polyvinyl acetate, the ethanol that 10g volumetric concentrations are 75%, be well mixed, 120W magnetic agitation 2h, obtain poly-vinyl alcohol solution;
Step 2:25kg chamomiles are taken, coarse powder is ground into, volatile ingredient is removed through steam distillation, obtains chamomile residual Slag, by solid-liquid ratio 1:5 add the ethanol that volumetric concentration is 95%, and 3h is extracted in stirring under the conditions of 50 DEG C, filters to take supernatant, weight Extract 2 times again;
Step 3:2 gained supernatants are merged, is concentrated under reduced pressure untill without ethanol, produces chamomile ethanol extract;
Step 4:Suspension is made in the deionized water for taking chamomile ethanol extract to add 5 times of volumes thereto, into suspension Plus the petroleum ether of 1 times of volume extracts 3h at room temperature, petroleum ether is mutually concentrated under reduced pressure after removal petroleum ether after layering, ocean is produced sweet Chrysanthemum extract;
Step 5:According to the mass fraction, 10 parts of glycerine, 4 parts of propane diols, 1 part of fibroin, 0.4 part of triethanolamine are added to In 78 parts of deionized waters, 80 DEG C of heating stirrings are until dissolving, is made aqueous phase liquid;
Step 6:According to the mass fraction, by 2 parts of camomile extracts, 2 parts of methyl-silicone oils, 3 parts of monoglycerides, 1.2 parts of polyoxyethylene Span 20,0.4 part of xanthan gum, stir under the conditions of 80 DEG C, oil phase liquid are made;
Step 7:Under conditions of being stirred continuously, oil phase liquid made from step 6 is added slowly to water made from step 5 In phase liquid, described oil phase liquid and the mass ratio of aqueous phase liquid are 1:9, using high speed disperser stir 15min, cooling discharging, both Obtain Essence;
Step 8:By poly-vinyl alcohol solution and Essence in mass ratio 4:6 are mixed evenly, and obtain tearing facial mask.
2. a kind of preparation method of chamomile tearing facial mask according to claim 1, it is characterised in that:Described in step 7 High speed disperser mixing speed be 5000r/min.
3. a kind of preparation method of chamomile tearing facial mask according to claim 1, it is characterised in that:Described in step 2 Crushing use LD-Y400A high speed Universal pulverizers.
CN201710485198.0A 2017-06-23 2017-06-23 A kind of preparation method of chamomile tearing facial mask Withdrawn CN107157851A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107669550A (en) * 2017-10-31 2018-02-09 思拓科(上海)生物科技股份有限公司 Organic baby moistening frost and preparation method thereof
CN108096151A (en) * 2018-02-05 2018-06-01 上海绰然生物科技有限公司 A kind of facial mask liquid and preparation method thereof containing okra, roseleaf

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105147535A (en) * 2015-09-29 2015-12-16 丘桂荣 Essence capable of reducing wrinkles, compacting, repairing, whitening and removing freckles and preparing method thereof
CN105878158A (en) * 2016-04-15 2016-08-24 覃碧 Tearing pearl powder mask

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105147535A (en) * 2015-09-29 2015-12-16 丘桂荣 Essence capable of reducing wrinkles, compacting, repairing, whitening and removing freckles and preparing method thereof
CN105878158A (en) * 2016-04-15 2016-08-24 覃碧 Tearing pearl powder mask

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
王国林: "洋甘菊美白与保湿活性成分研究", 《中国优秀硕士学位论文全文数据库(电子期刊)工程科技I辑》 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107669550A (en) * 2017-10-31 2018-02-09 思拓科(上海)生物科技股份有限公司 Organic baby moistening frost and preparation method thereof
CN107669550B (en) * 2017-10-31 2019-08-16 思拓科(上海)生物科技股份有限公司 Organic baby moistening frost and preparation method thereof
CN108096151A (en) * 2018-02-05 2018-06-01 上海绰然生物科技有限公司 A kind of facial mask liquid and preparation method thereof containing okra, roseleaf

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Application publication date: 20170915