CN105641208A - Traditional Chinese medicine formula for nourishing liver and clearing away toxic materials and method for preparing traditional Chinese medicine granules with same - Google Patents
Traditional Chinese medicine formula for nourishing liver and clearing away toxic materials and method for preparing traditional Chinese medicine granules with same Download PDFInfo
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- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
- A61K36/287—Chrysanthemum, e.g. daisy
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
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- A61K36/725—Ziziphus, e.g. jujube
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/74—Rubiaceae (Madder family)
- A61K36/744—Gardenia
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- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
- A61K9/16—Agglomerates; Granulates; Microbeadlets ; Microspheres; Pellets; Solid products obtained by spray drying, spray freeze drying, spray congealing,(multiple) emulsion solvent evaporation or extraction
- A61K9/1605—Excipients; Inactive ingredients
- A61K9/1629—Organic macromolecular compounds
- A61K9/1652—Polysaccharides, e.g. alginate, cellulose derivatives; Cyclodextrin
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- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/39—Complex extraction schemes, e.g. fractionation or repeated extraction steps
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
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Abstract
The invention discloses a traditional Chinese medicine formula for nourishing the liver and clearing away toxic materials and a method for preparing traditional Chinese medicine granules with the traditional Chinese medicine formula. The traditional Chinese medicine is prepared from 3 parts of ginseng, 3 parts of gardenia, 3 parts of lycium barbarum, 3 parts of chrysanthemum flowers, 3 parts of jujube kernels, 3 parts of honeysuckle, 2 parts of auxiliary materials, 0.09 part of a flavoring agent and 0.18 part of a lubricating agent. The preparation method of traditional Chinese medicine granules includes the steps that raw materials are weighed; ginseng is extracted through an ultrasonic reverse flow method; mixtures of medicine residues generated after ginseng is extracted, gardenia, lycium barbarum, chrysanthemum flowers, jujube kernels and honeysuckle are extracted twice in an aqueous extraction mode; high-speed centrifuging impurity removal is performed; drying is performed; the auxiliary materials, the flavoring agent and the lubricating agent are added for preparing granules. The traditional Chinese medicine has the advantages that effective components in the traditional Chinese medicine formula can be extracted to the maximum extent, and the effects of nourishing the liver and clearing away toxic materials are well achieved.
Description
Technical field
The present invention relates to traditional Chinese medical science toxin expelling technical field, it particularly relates to the Chinese medicine formula of a kind of liver-nourishing, toxin-expelling and apply its method preparing Chinese medicinal granule.
Background technology
Everyone is required for health, and healthy physique needs to rely on liver care. At present, the liver protecting knowledge is understood very few by people, it is concerned about, love just less. The disastrous effect thus brought is, liver sickness rate remains high always. Development along with society, in the mankind, the sickness rate of liver is more and more higher, cause that the main cause of this phenomenon is after people's living standard improves, do not note science diet, like to eat the food of meat, fried class, sweet higher fatty acid, the high heat such as greasy, and that coarse grain, veterinary antibiotics are just eaten is less, in the course of time, bring out multiple disease.
The traditional Chinese medical science is thought, liver is human body " shield of toxin expelling ", and liver has three big physiological functions: a main store blood, two main catharsis, three main muscle. Strong liver, for human immunity and healthy important guarantee. If liver function declines, arising that store blood deficiency, catharsis imbalance, tendon and joint joint stuffiness, whole body is feeble, visual deterioration, blurred vision, and body disease-resistant power declines, and various diseases will be availed oneself of the opportunity to get in.
Therefore, market is needed badly a kind of can the traditional Chinese medicine reagent of liver-nourishing, toxin-expelling.
Summary of the invention
It is an object of the invention to provide Chinese medicinal granule of a kind of liver-nourishing, toxin-expelling and preparation method thereof, it is possible to extract the effective ingredient in this Chinese medicinal granule fully, thus reaching the effect of good liver-nourishing, toxin-expelling.
For realizing above-mentioned technical purpose, the technical scheme is that and be achieved in that:
A kind of Chinese medicine formula of liver-nourishing, toxin-expelling, including the raw material of following parts by weight:
Radix Ginseng 1 part, Fructus Gardeniae 1 part, Fructus Lycii 1 part, Flos Chrysanthemi 1 part, Semen Ziziphi Spinosae 1 part and Flos Lonicerae 1 part.
Further, the raw material of following parts by weight is also included:
Adjuvant 2 parts, correctives 0.09 part and lubricant 0.18 part.
Further, described adjuvant is dextrin, and described correctives is stevioside, and described lubricant is 95% ethanol.
A kind of method that Chinese medicine formula applying above-mentioned liver-nourishing, toxin-expelling prepares Chinese medicinal granule, comprises the steps:
1) raw material of above-mentioned each parts by weight is weighed;
2) described Radix Ginseng was pulverized 30 mesh sieves, adopt ultrasonic counter-current to extract Radix Ginseng, wherein, adopt 70% ethanol as solvent, solvent adverse current volume flow and feedstock quality flow-rate ratio are 8, Extracting temperature is 60 DEG C, and ultrasonic frequency is 30kHZ, and ultrasonic power is 20KW, obtain extracting solution and medicinal residues, from described extracting solution, reclaim ethanol, and the extracting solution eliminating ethanol is concentrated into relative density 1.10��1.12 under 60 DEG C of conditions, obtain alcohol-extracted extract;
3) with Fructus Gardeniae, Fructus Lycii, Flos Chrysanthemi, Semen Ziziphi Spinosae and Flos Lonicerae, described medicinal residues are merged water to carry, adopting the water boiling and extraction twice of boiling of 100 DEG C, first time adds the water extraction of 10 times of weight, and second time adds the water extraction of 8 times of weight, all extract 2h twice, obtain two parts of decocting liquids;
4) two parts of decocting liquids are adopted high speed centrifugation remove impurity, and merge two parts of decocting liquids after remove impurity;
5) filter, take filtrate and under 60 DEG C of conditions, filtrate decompression is compressed to relative density 1.10��1.12, obtaining the water extracted immersing paste, described the water extracted immersing paste is mixed with alcohol-extracted extract;
6) dry;
7) by dextrin, stevioside, ethanol, the water extracted immersing paste and alcohol-extracted extract mix homogeneously, No. 2 sieve series grains are crossed.
Further, step 6) in adopt spray drying method be dried.
Principles of the invention:
Radix Ginseng: Compendium of Material Medica: " controlling all deficiency syndrome, generate heat spontaneous perspiration, dizziness and headache, and food, Xuan malaria, sliding chronic dysentery of rushing down, frequent micturition are told in regurgitation, drench drop, overstrain internal injury, apoplexy, heatstroke, flaccidity syndrome and arthralgia syndrome, spit blood, hemoptysis, hematochezia, stranguria with blood, metrorrhagia, all diseases in puerperal before tire. "
Fructus Gardeniae: " China's book on Chinese herbal medicine ": pathogenic fire purging relieving restlessness; Clearing away heat-damp and promoting diuresis; Removing pathogenic heat from blood and toxic substance from the body. Main calentura is vexed; Liver-fire conjunctival congestion; Headache; Damp and hot yellow infantile malnutrition; Stranguria; Leaf blood epistaxis; Dysentery hematuria; Aphtha of the mouth and tongue; Sore swollen toxin; Sprain and swell and ache
Fructus Lycii: " China's book on Chinese herbal medicine ": nourishing the liver; Nourishing kidney; Lung moistening. Main caused by liver and kidney deficiency; Have a dizzy spell; Visual one clear; Soreness of the waist and knees; The expensive essence of sexual impotence; Cough due to consumptive disease; Quench one's thirst taking fluids profusely.
Flos Chrysanthemi: " China's book on Chinese herbal medicine ": wind and heat dispersing; Suppressing the hyperactive liver improving eyesight; Removing toxic substances and promoting subsidence of swelling.
Semen Ziziphi Spinosae: " Chinese Pharmacopoeia ": tonifying liver, mind calming, arresting sweating, promotes the production of body fluid. For restlessness of asrhenia type and insomnia, dreaminess of palpitating with fear, body void hyperhidrosis, Tianjin wound is thirsty.
Flos Lonicerae: " Chinese Pharmacopoeia ": heat-clearing and toxic substances removing, wind-heat dissipating. For carbuncle furuncle, sore throat, erysipelas, toxic-heat and blood stasis, anemopyretic cold, epidemic febrile disease is generated heat.
Radix Ginseng is dry root and the rhizome of Araliaceae Radix Ginseng (PanaxginsengC.A.Meyer), have that strongly invigorating primordial QI, multiple arteries and veins be admittedly de-, invigorating the spleen to benefit the lung, promote the production of body fluid nourish blood, effect of Fructus Alpiniae Oxyphyllae of calming the nerves, the main active of Radix Ginseng is ginsenoside. Current ginsenoside's extracting method mainly has decocting method, circumfluence method etc., but decocting method and circumfluence method heated time are long, temperature is high, effective ingredient is easily destroyed, for extracting in Radix Ginseng activity saponin component high, stay-in-grade better, the present invention adopts ultrasonic countercurrent extraction method, with ginsenoside Rb1, Rg1 and Re total extraction ratio for Testing index, investigate the extracting factor of Radix Ginseng, provide one new technology fast and efficiently for Radix Ginseng extracts active ingredients.
Set the ultrasonic frequency of experiment as 30kHZ, ultrasonic power is 20kW, study emphatically volume fraction of ethanol (A), pulverizing medicinal materials degree (B), solvent adverse current volume flow and feedstock quality flow-rate ratio (C), the impact on extraction effect of 4 factors of Extracting temperature (D) below, 3 levels of each selecting factors, experimental result is as shown in table 1:
Table 1
Wherein, extraction ratio is each component amount in each component amount/medical material in extract, total extraction ratio be ginsenoside Rb1 in extract, Rg1, Re amount sum/medical material in ginsenoside Rb1, Rg1, Re amount sum.
By table 1 it can be seen that the optimum extraction scheme of Radix Ginseng of the present invention is A2B2C2D3, namely use 70% ethanol, pulverizing medicinal materials crosses 30 mesh sieves, and the ratio of solvent adverse current volume flow and feedstock quality flow is 8, and Extracting temperature is 60 DEG C.
Adopt above-mentioned preferred plan that Radix Ginseng carries out 3 times to extract, extract result as shown in table 2:
Table 2
Conclusion: adopting optimum extraction scheme to extract Radix Ginseng, can make the extraction rate reached more than 94% of effective ingredient ginsenosides Rg1, Re and Rb1 in Radix Ginseng, total extraction ratio is more than 95%.
Beneficial effects of the present invention: the present invention can extract the effective ingredient of this Chinese medicine formula to greatest extent, reaches the effect of good liver-nourishing, toxin-expelling.
Detailed description of the invention
Technical scheme in the embodiment of the present invention will be clearly and completely described below, it is clear that described embodiment is only a part of embodiment of the present invention, rather than whole embodiments. Based on the embodiment in the present invention, the every other embodiment that those of ordinary skill in the art obtain, broadly fall into the scope of protection of the invention.
The Chinese medicine formula of a kind of liver-nourishing, toxin-expelling according to embodiments of the invention, including the raw material of following parts by weight:
Radix Ginseng 10g, Fructus Gardeniae 10g, Fructus Lycii 10g, Flos Chrysanthemi 10g, Semen Ziziphi Spinosae 10g, Flos Lonicerae 10g, dextrin, stevioside and 95% ethanol.
A kind of method that Chinese medicine formula applying liver-nourishing, toxin-expelling as above prepares Chinese medicinal granule, comprises the steps: 1) weigh the raw material of above-mentioned each parts by weight; 2) described Radix Ginseng was pulverized 30 mesh sieves, adopt ultrasonic counter-current to extract Radix Ginseng, wherein, adopt 70% ethanol as solvent, solvent adverse current volume flow and feedstock quality flow-rate ratio are 8, Extracting temperature is 60 DEG C, and ultrasonic frequency is 30kHZ, and ultrasonic power is 20kW, obtain extracting solution and medicinal residues, from described extracting solution, reclaim ethanol, and the extracting solution eliminating ethanol is concentrated into relative density 1.10��1.12 under 60 DEG C of conditions, obtain alcohol-extracted extract; 3) with Fructus Gardeniae, Fructus Lycii, Flos Chrysanthemi, Semen Ziziphi Spinosae and Flos Lonicerae, described medicinal residues are merged water to carry, adopting the water boiling and extraction twice of boiling of 100 DEG C, first time adds the water extraction of 10 times of weight, and second time adds the water extraction of 8 times of weight, all extract 2h twice, obtain two parts of decocting liquids; 4) two parts of decocting liquids are adopted high speed centrifugation remove impurity, and merge two parts of decocting liquids after remove impurity; 5) filter, take filtrate and under 60 DEG C of conditions, filtrate decompression is compressed to relative density 1.10��1.12, obtaining the water extracted immersing paste, described the water extracted immersing paste is mixed with alcohol-extracted extract; 6) spray drying method is adopted to be dried; 7) by dextrin, stevioside, ethanol, the water extracted immersing paste and alcohol-extracted extract mix homogeneously, No. 2 sieve series grains are crossed.
In sum, by means of the technique scheme of the present invention, the present invention can extract the effective ingredient of this Chinese medicine formula to greatest extent, reaches the effect of good liver-nourishing, toxin-expelling.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all within the spirit and principles in the present invention, any amendment of making, equivalent replacement, improvement etc., should be included within protection scope of the present invention.
Claims (5)
1. the Chinese medicine formula of a liver-nourishing, toxin-expelling, it is characterised in that include the raw material of following parts by weight:
Radix Ginseng 3 parts, Fructus Gardeniae 3 parts, Fructus Lycii 3 parts, Flos Chrysanthemi 3 parts, Semen Ziziphi Spinosae 3 parts and Flos Lonicerae 3 parts.
2. the Chinese medicine formula of liver-nourishing, toxin-expelling according to claim 1, it is characterised in that also include the raw material of following parts by weight:
Adjuvant 2 parts, correctives 0.09 part and lubricant 0.18 part.
3. the Chinese medicine formula of liver-nourishing, toxin-expelling according to claim 2, it is characterised in that described adjuvant is dextrin, described correctives is stevioside, and described lubricant is 95% ethanol.
4. the method that the Chinese medicine formula applying liver-nourishing, toxin-expelling as claimed in claim 3 prepares Chinese medicinal granule, it is characterised in that comprise the steps:
1) raw material of above-mentioned each parts by weight is weighed;
2) described Radix Ginseng was pulverized 30 mesh sieves, adopt ultrasonic counter-current to extract Radix Ginseng, wherein, adopt 70% ethanol as solvent, solvent adverse current volume flow and feedstock quality flow-rate ratio are 8, Extracting temperature is 60 DEG C, and ultrasonic frequency is 30kHZ, and ultrasonic power is 20KW, obtain extracting solution and medicinal residues, from described extracting solution, reclaim ethanol, and the extracting solution eliminating ethanol is concentrated into relative density 1.10 ~ 1.12 under 60 DEG C of conditions, obtain alcohol-extracted extract;
3) with Fructus Gardeniae, Fructus Lycii, Flos Chrysanthemi, Semen Ziziphi Spinosae and Flos Lonicerae, described medicinal residues are merged water to carry, adopting the water boiling and extraction twice of boiling of 100 DEG C, first time adds the water extraction of 10 times of weight, and second time adds the water extraction of 8 times of weight, all extract 2h twice, obtain two parts of decocting liquids;
4) two parts of decocting liquids are adopted high speed centrifugation remove impurity, and merge two parts of decocting liquids after remove impurity;
5) filter, take filtrate and under 60 DEG C of conditions, filtrate decompression is compressed to relative density 1.10 ~ 1.12, obtaining the water extracted immersing paste, described the water extracted immersing paste is mixed with alcohol-extracted extract;
6) dry;
7) by dextrin, stevioside, ethanol, the water extracted immersing paste and alcohol-extracted extract mix homogeneously, No. 2 sieve series grains are crossed.
5. the method that the Chinese medicine formula of application liver-nourishing, toxin-expelling according to claim 4 prepares Chinese medicinal granule, it is characterised in that adopt spray drying method to be dried in step 6).
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| CN108969689A (en) * | 2018-09-28 | 2018-12-11 | 李影 | A kind of health liquor of invigorating QI and blood and preparation method thereof |
| CN110074415A (en) * | 2019-06-13 | 2019-08-02 | 成都亮丽泉科技有限公司 | A kind of health food and preparation method thereof of internal organs expelling toxin opsonic |
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| CN102356895A (en) * | 2011-08-26 | 2012-02-22 | 吉林紫鑫药业股份有限公司 | Ginseng drink and its production technology |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108969689A (en) * | 2018-09-28 | 2018-12-11 | 李影 | A kind of health liquor of invigorating QI and blood and preparation method thereof |
| CN110074415A (en) * | 2019-06-13 | 2019-08-02 | 成都亮丽泉科技有限公司 | A kind of health food and preparation method thereof of internal organs expelling toxin opsonic |
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