CN105567354A - 水煤浆分散剂及其制备方法 - Google Patents
水煤浆分散剂及其制备方法 Download PDFInfo
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- CN105567354A CN105567354A CN201410538211.0A CN201410538211A CN105567354A CN 105567354 A CN105567354 A CN 105567354A CN 201410538211 A CN201410538211 A CN 201410538211A CN 105567354 A CN105567354 A CN 105567354A
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- Prior art keywords
- water slurry
- coal water
- humic acid
- acid
- dispersing agent
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 52
- 239000003245 coal Substances 0.000 title claims abstract description 48
- 239000002002 slurry Substances 0.000 title claims abstract description 45
- 239000002270 dispersing agent Substances 0.000 title claims abstract description 34
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 238000007613 slurry method Methods 0.000 title 1
- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 claims abstract description 44
- 239000004021 humic acid Substances 0.000 claims abstract description 44
- -1 sucrose ester Chemical class 0.000 claims abstract description 38
- 229920001732 Lignosulfonate Polymers 0.000 claims abstract description 23
- 235000019357 lignosulphonate Nutrition 0.000 claims abstract description 23
- 239000003999 initiator Substances 0.000 claims abstract description 21
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 19
- 229930006000 Sucrose Natural products 0.000 claims abstract description 19
- 239000005720 sucrose Substances 0.000 claims abstract description 19
- 239000007864 aqueous solution Substances 0.000 claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 14
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 38
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 36
- 238000006243 chemical reaction Methods 0.000 claims description 22
- 239000006185 dispersion Substances 0.000 claims description 22
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 19
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 19
- 238000009413 insulation Methods 0.000 claims description 18
- 239000003795 chemical substances by application Substances 0.000 claims description 16
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 claims description 12
- 238000010792 warming Methods 0.000 claims description 12
- 239000011260 aqueous acid Substances 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 9
- 239000000243 solution Substances 0.000 claims description 9
- 230000035484 reaction time Effects 0.000 claims description 8
- 239000003513 alkali Substances 0.000 claims description 6
- 239000012153 distilled water Substances 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 6
- 229950007687 macrogol ester Drugs 0.000 claims description 6
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinyl group Chemical group C1(O)=CC(O)=CC=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 claims description 6
- FOGYNLXERPKEGN-UHFFFAOYSA-N 3-(2-hydroxy-3-methoxyphenyl)-2-[2-methoxy-4-(3-sulfopropyl)phenoxy]propane-1-sulfonic acid Chemical compound COC1=CC=CC(CC(CS(O)(=O)=O)OC=2C(=CC(CCCS(O)(=O)=O)=CC=2)OC)=C1O FOGYNLXERPKEGN-UHFFFAOYSA-N 0.000 claims description 4
- LCPVQAHEFVXVKT-UHFFFAOYSA-N 2-(2,4-difluorophenoxy)pyridin-3-amine Chemical compound NC1=CC=CN=C1OC1=CC=C(F)C=C1F LCPVQAHEFVXVKT-UHFFFAOYSA-N 0.000 claims description 3
- JIGUICYYOYEXFS-UHFFFAOYSA-N 3-tert-butylbenzene-1,2-diol Chemical compound CC(C)(C)C1=CC=CC(O)=C1O JIGUICYYOYEXFS-UHFFFAOYSA-N 0.000 claims description 3
- 239000004160 Ammonium persulphate Substances 0.000 claims description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 3
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 3
- 239000004159 Potassium persulphate Substances 0.000 claims description 3
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 claims description 3
- 235000019395 ammonium persulphate Nutrition 0.000 claims description 3
- JXLHNMVSKXFWAO-UHFFFAOYSA-N azane;7-fluoro-2,1,3-benzoxadiazole-4-sulfonic acid Chemical compound N.OS(=O)(=O)C1=CC=C(F)C2=NON=C12 JXLHNMVSKXFWAO-UHFFFAOYSA-N 0.000 claims description 3
- 239000011575 calcium Substances 0.000 claims description 3
- 229910052791 calcium Inorganic materials 0.000 claims description 3
- 229940120693 copper naphthenate Drugs 0.000 claims description 3
- SEVNKWFHTNVOLD-UHFFFAOYSA-L copper;3-(4-ethylcyclohexyl)propanoate;3-(3-ethylcyclopentyl)propanoate Chemical compound [Cu+2].CCC1CCC(CCC([O-])=O)C1.CCC1CCC(CCC([O-])=O)CC1 SEVNKWFHTNVOLD-UHFFFAOYSA-L 0.000 claims description 3
- 229920005610 lignin Polymers 0.000 claims description 3
- 229910052700 potassium Inorganic materials 0.000 claims description 3
- 239000011591 potassium Substances 0.000 claims description 3
- USHAGKDGDHPEEY-UHFFFAOYSA-L potassium persulfate Chemical compound [K+].[K+].[O-]S(=O)(=O)OOS([O-])(=O)=O USHAGKDGDHPEEY-UHFFFAOYSA-L 0.000 claims description 3
- 235000019394 potassium persulphate Nutrition 0.000 claims description 3
- 229920005552 sodium lignosulfonate Polymers 0.000 claims description 3
- CHQMHPLRPQMAMX-UHFFFAOYSA-L sodium persulfate Substances [Na+].[Na+].[O-]S(=O)(=O)OOS([O-])(=O)=O CHQMHPLRPQMAMX-UHFFFAOYSA-L 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 239000002202 Polyethylene glycol Substances 0.000 abstract description 2
- 229920001223 polyethylene glycol Polymers 0.000 abstract description 2
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 abstract 1
- 238000010528 free radical solution polymerization reaction Methods 0.000 abstract 1
- 239000003112 inhibitor Substances 0.000 abstract 1
- 238000006116 polymerization reaction Methods 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- 239000002253 acid Substances 0.000 description 5
- 238000001556 precipitation Methods 0.000 description 5
- 239000002131 composite material Substances 0.000 description 3
- 239000013049 sediment Substances 0.000 description 3
- 150000001735 carboxylic acids Chemical class 0.000 description 2
- 238000007334 copolymerization reaction Methods 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- 239000010802 sludge Substances 0.000 description 2
- AGBXYHCHUYARJY-UHFFFAOYSA-N 2-phenylethenesulfonic acid Chemical compound OS(=O)(=O)C=CC1=CC=CC=C1 AGBXYHCHUYARJY-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000011362 coarse particle Substances 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 1
- 238000010907 mechanical stirring Methods 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- PSZYNBSKGUBXEH-UHFFFAOYSA-N naphthalene-1-sulfonic acid Chemical compound C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 PSZYNBSKGUBXEH-UHFFFAOYSA-N 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 229920000098 polyolefin Polymers 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- 238000002525 ultrasonication Methods 0.000 description 1
- 238000002604 ultrasonography Methods 0.000 description 1
Landscapes
- Liquid Carbonaceous Fuels (AREA)
- Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
Abstract
Description
Claims (10)
Priority Applications (1)
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CN201410538211.0A CN105567354B (zh) | 2014-10-13 | 2014-10-13 | 水煤浆分散剂及其制备方法 |
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CN201410538211.0A CN105567354B (zh) | 2014-10-13 | 2014-10-13 | 水煤浆分散剂及其制备方法 |
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CN105567354A true CN105567354A (zh) | 2016-05-11 |
CN105567354B CN105567354B (zh) | 2017-05-24 |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105542886A (zh) * | 2014-11-03 | 2016-05-04 | 太原市天鼎恒砼外加剂科技发展有限公司 | 水煤浆分散剂及其制备方法 |
CN108531231A (zh) * | 2018-04-24 | 2018-09-14 | 常州五荣化工有限公司 | 一种低金属敏感型水煤浆分散剂的制备方法 |
CN108913242A (zh) * | 2018-07-05 | 2018-11-30 | 王建东 | 一种水煤浆分散剂 |
CN110804122A (zh) * | 2019-11-19 | 2020-02-18 | 安徽鑫固环保股份有限公司 | 一种蔗糖酯合成疏型水煤浆分散剂的新方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102051242A (zh) * | 2010-12-17 | 2011-05-11 | 贵阳超群实业有限公司 | 一种油水煤浆及制备方法 |
CN103045317A (zh) * | 2012-12-26 | 2013-04-17 | 中国东方电气集团有限公司 | 一种木质素系水煤浆分散剂及其制备方法 |
EP2749547A1 (en) * | 2012-12-04 | 2014-07-02 | Services Pétroliers Schlumberger | Additive for well cementing applications |
-
2014
- 2014-10-13 CN CN201410538211.0A patent/CN105567354B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102051242A (zh) * | 2010-12-17 | 2011-05-11 | 贵阳超群实业有限公司 | 一种油水煤浆及制备方法 |
EP2749547A1 (en) * | 2012-12-04 | 2014-07-02 | Services Pétroliers Schlumberger | Additive for well cementing applications |
CN103045317A (zh) * | 2012-12-26 | 2013-04-17 | 中国东方电气集团有限公司 | 一种木质素系水煤浆分散剂及其制备方法 |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105542886A (zh) * | 2014-11-03 | 2016-05-04 | 太原市天鼎恒砼外加剂科技发展有限公司 | 水煤浆分散剂及其制备方法 |
CN108531231A (zh) * | 2018-04-24 | 2018-09-14 | 常州五荣化工有限公司 | 一种低金属敏感型水煤浆分散剂的制备方法 |
CN108913242A (zh) * | 2018-07-05 | 2018-11-30 | 王建东 | 一种水煤浆分散剂 |
CN108913242B (zh) * | 2018-07-05 | 2020-11-24 | 义乌市君胜科技有限公司 | 一种水煤浆分散剂 |
CN110804122A (zh) * | 2019-11-19 | 2020-02-18 | 安徽鑫固环保股份有限公司 | 一种蔗糖酯合成疏型水煤浆分散剂的新方法 |
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Publication number | Publication date |
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CN105567354B (zh) | 2017-05-24 |
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Address after: 030027 Shanxi Province, Taiyuan Jiufeng Jiancaoping District Binfeng garden road block A room 252 Applicant after: TAIYUAN CITY TIANDINGHENG CONCRETE ADMIXTURES TECHNOLOGY DEVELOPMENT Co.,Ltd. Address before: 030027 Shanxi Province, Taiyuan Jiufeng Jiancaoping District Binfeng garden road block A room 252 Applicant before: TAIYUAN TIANDING HENGQUAN ADMIXTURE TECHNOLOGY DEVELOPMENT Co.,Ltd. |
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Address after: 030027 Room 252, Building A, Binfengyuan, Jiufeng Road, Jiancaoping District, Taiyuan City, Shanxi Province Patentee after: Shanxi Tiandingheng Concrete Admixture Technology Development Co.,Ltd. Address before: 030027 Room 252, Building A, Binfengyuan, Jiufeng Road, Jiancaoping District, Taiyuan City, Shanxi Province Patentee before: TAIYUAN CITY TIANDINGHENG CONCRETE ADMIXTURES TECHNOLOGY DEVELOPMENT Co.,Ltd. |
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CP01 | Change in the name or title of a patent holder |