CN105560305A - Abelmoschus manihot flower product - Google Patents
Abelmoschus manihot flower product Download PDFInfo
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- CN105560305A CN105560305A CN201410623459.7A CN201410623459A CN105560305A CN 105560305 A CN105560305 A CN 105560305A CN 201410623459 A CN201410623459 A CN 201410623459A CN 105560305 A CN105560305 A CN 105560305A
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Abstract
The invention relates to an abelmoschus manihot flower product. Fresh abelmoschus manihot flowers and dry abelmoschus manihot flowers have specific chemical components and biological activity. The invention aims to achieve the effect that the active substances in the abelmoschus manihot flowers can be retained originally to the maximum extent and kept in stable state; therefore, the optimal control point for material temperature and material humidity can be calculated mechanically and physically; the abelmoschus manihot flowers in the ovary of a pistil seat are necessary, so that the content of biological flavones in a product is high, and the content of hyperoside serving as a labeling substance is twice or more of that of the pharmacopoeia criterion. The abelmoschus manihot flower product can be used as a raw material for production of traditional Chinese medicinal food products or medicinal, food and cosmetics.
Description
Technical field
The invention belongs to food development field and relate to a kind of JINHUA news of victory flower goods.
Background technology
The JINHUA news of victory is a kind of non-toxic herb, and the JINHUA news of victory is as botanical herbs material name, and be seen in " Chinese medicine voluminous dictionary " 2075 pages of 4252, No. 4254 items of nineteen ninety-five Shanghai science tech publishing house publication, formal name used at school is Abelmoschus manihot （L.） Medic
[Abelmoschusmanihot (L.) Medicus].6000010003 at the coding of National Botanical systematic name standard GB/T-93.
During JINHUA news of victory crude drug flower and dry product are spent, chemical composition and biological activity special, natural pharmacology system of College of Pharmacy, Beijing Univ, in state natural sciences fund key project 20432030 is reported, the active monomer compound of the JINHUA news of victory flower obtaining and study is 23.Military Medical Science Institute is in the research report of JINHUA news of victory flower, and the JINHUA news of victory contains the active component of 34 kinds of relative health in spending, what wherein belong to bioflavonoid reaches 30 kinds.Military medicine scientific radiology and radiation medicine institute, in the research report to JINHUA news of victory flower, special project is analyzed its liposoluble ingredient.
" PLA's medical journal " the 21st volume the 5th is interim has report to claim, and the JINHUA news of victory spends the content of middle hyperin to be 1.12%.
In Xi'an Communications University pharmacognosy master Cao Yong Xiang research report, containing a large amount of chromocor compounds in claiming the JINHUA news of victory to spend, and mostly these flavone compounds are aglycon and the glycosides of the multiple phenolic hydroxyl group of tool, and character is active, may have good antioxidation application prospect.Have a content higher building matter extremely unstable, failing separation all the time obtains.
Because the JINHUA news of victory has above-mentioned specific activity material in spending, place ensures that its active component does not lose, lose prerequisite less under, be processed into product application, people are seeking always.But the Report Publication over more than 20 year, authorize invention special literary composition in technical scheme and claim in product, on the contrary to active substance in well-known raw material, all the more work is fewer, even no more than 50% in products material.As the flavones content of product in 93110506.4 patents, by calculating, be only 20% of convenient source; Authoring program only 201201082553.7 patents of 11 months, in its product, flavone kind is five kinds, only quite convenient source contained amount 17%.
Relate to that material temperature in selection of the present invention and product forms, technological process controls, the ovary flower of gynoecium seat is selected, the information of corresponding JINHUA news of victory flower goods, there still is not information.
Summary of the invention
The object of the invention is to be intended to solve the JINHUA news of victory spend in active substance, ensured that ecosystem retains to greatest extent, and keep steady statue, for this reason on machinery, physics mode, try to achieve the optimum controlling point that material temperature material is wet, the JINHUA news of victory flower chosen in gynoecium end stand room is important document, and in product, biological flavone content is high, its marker substances Determination of Hyperoside, more than suitable standards of pharmacopoeia twice.
The invention provides a kind of JINHUA news of victory flower goods, it is characterized in that: select the JINHUA news of victory in gynoecium end stand room flower to do raw material, be processed as the material of dosage form goods; When producing tablet dosage form goods, graininess dosage form goods, adopt fresh goods flower material dewatering, to the disposal of dry product flower material humidification, make its moisture 17% to 39%; Control in the temperature this appropriate water content material being done to less than 99.8 DEG C, punching press obtains lamellar semi-finished product to be dried or the obtained graininess semi-finished product to be dried of extruding, and then use less than 148 DEG C temperature to do dry disposal respectively, obtained JINHUA news of victory flower sheet articles, JINHUA news of victory flower particle product respectively; During with JINHUA news of victory ovary flower slurry materiel machining goods, first add the water of three times to five times of flower slurry weight to flower slurry, spray after colloid mill centrifugal, obtained powdery JINHUA news of victory flower goods; In whole technological process, material does not contact acidity, alkalescence, organic solvent material, does not dose adjuvant in material.
As the JINHUA news of victory flower of food materials raw material, be called for short ovary flower, it is characterized in that: be the flowering time institute spewing flower bud centered by the ovary tissues of flower or open flower; This beggar room keeps completely, and ovary bottom is connected with anthocaulus base portion tissue and organizes organic all-in-one-piece calyx with base portion, and ovary top is organically connected with male flower stamen, and ovary round base portion is organically connected with whole petal; Be exactly for important document with beggar room, the flower of organic connected pistil, petal, calyx, anthocaulus base portion tissue, the gynoecium end seat of flower is at the ovary center of flower, and to be that 93110506.4 patents of inventor and lot of documents quote the character that relevant entry word describes far different to Xiong Ningning.
The harvesting of ovary flower is obtained is: colored gynoecium of gathering grows the flower being no more than 10 hours after not having the open flower of the alabastrum of Pollination Fertilization or gynoecium part Pollination Fertilization or gynoecium Pollination Fertilization, obtains by the dehydration technique of known flower.
JINHUA news of victory tablet half-finished drying time is within 2 hours, and granule half-finished drying time is within 1.5 hours, and flower serosity powdery half-finished drying time is within 58 minutes.
Product does Chinese crude drug food products or medicine, food, cosmetic material use.
That implements that the present invention needs to understand will have: except control temperature of charge mentioned above, humidity, material choice, dry humidity in time between etc. except node, the instrument and supplies operation of applying all adopts the conventional equipment and technique generally applied.
The material of JINHUA news of victory flower processing dosage form goods refers to: cut JINHUA news of victory ovary flower, pulverize, reach the rapidoprint of film-making agent routinely respectively, granule, powder requirement character.As for the processing of this respect, combustion etc., have known technology and Conventional wisdom in the industry.As, although do not have proposition to add any adjuvant of starch based to film-making, granule processed etc. in present invention process, but by phase data material handling in the present invention, the 16% high polysaccharide glue invariance that JINHUA news of victory ovary is contained in spending, can reach conventional film-making, granule processed doses the effect of adjuvant, in technological operation, adopt roughly the same Xiamen Chinese Medicine Co., Ltd, the equipment and process of production XINHUANGPIAN, comprise the requirement etc. to material, just.
For the restriction of the above-mentioned JINHUA news of victory, based in known references, when relating to JINHUA news of victory flower, mostly emphasize, JINHUA news of victory flower refers to crown portion, and general knowledge tells us, corolla person, and petal also, does not contain in other biological is not organized in naturally.The present invention is to the restriction of JINHUA news of victory flower; one is only in this way limit; the stable of flower Central Plains ecologic active material could be ensured; two is based on general knowledge; the sexual organ of plant; the expression focus of its efficacy performance often; the ovary of flower, pistil its sexual organ exactly; as only adopted corolla and abandoning ovary, pistil and need not; its effect is self-evident, and as above-mentioned restriction anthocaulus base portion and calyx, that is limit this could protect colored ovary and pistil is without prejudice completely; under the state that it keeps complete, just can reach and ensure that active component is stablized.Non-this, one is cannot imagine its efficiency and feasibility in actual operation of gathering, and the more important thing is colored ovary, pistil tears breakage certainly, be oxidized probability and increase, key active ingredient loss rate increases.
Gynoecium end seat, at the middle-end seat of ovary, is not adjective, is not more actor's part or lines libretto, and " Miss I sit up straight within young lady's bedchamber " sits up straight the meaning of a word.Seat, end press Chinese general knowledge, and what here express is shape localization quantificational word.At conventional florist's product, the gynoecium state related in flower Chinese crude drug, because Pollination Fertilization development time is longer, the non-end seat shape in irregular status, spends different from ovary of the present invention, therefore here to hold seat to state it.Gather gynoecium end stand room flower time, for alabastrum during flowering, although its stamen, gynoecium, ovary are grown completely, there is no Pollination Fertilization, because the stamen pollen now does not also eject from hole.To the flower after opening, be limited, after this for stamen part Pollination Fertilization, Pollination Fertilization grow the ovary flower being no more than 10 hours with the stamen pollen time of ejecting.Because of weather, season, concrete time of ejecting from hole lower than, the different stamen pollen such as seed, growth conditions, very different, the method determined is, holds high magnified glass, until the flowers are in blossom put time directly observe truth and determine.Gather after qualified fresh flower bud type flower, obtain dry product flower with known technology Dehydration.The technical scheme etc. that known technology is owner as described in 03106-267.3 patent documentation as Wang Li.All these, Xiong Ningning is 93110506.4 patents of inventor and to be expressly defined as by the JINHUA news of victory flower widely quoted be that " corolla of flower " grid also has its commodity picture, and outstanding in picture is only corolla.What corolla flower is, one of ingredient of " modern Chinese dictionary " 538 pages of (corolla) HuaGua flowers is made up of some petals.The general name of " simple and clear biology dictionary " 611 pages of corolla (Corolla) petals.Obviously, those limit popular JINHUA news of victory flower of corollas, just flower Petal and containing other, naturally also containing ovary, end seat gynoecium etc., also just therefore just appearance as the fact of background technology finally described in several sections.
The present invention, to the restriction of contact acid, alkali, organic solvent, except equipment, with except water, also comprises car to inside and outside environmental condition routinely naturally.
Data in the present invention only establish the upper limit not set limit, are because upper data is deisgn product character, the critical line of the combustion invariance namely in converted products flow process, and under this limits, without the worry of character change, only production efficiency difference.As: the high polysaccharide glue in material, under certain humidity, once temperature is more than 99.8 DEG C, namely degeneration is decomposed instantaneously.How not affect as dry humidity etc.? this is general knowledge, because of the control that dry humidity is dry environment humidity, under this environment, with the evaporative cooling of moisture in material, in the micro molecule part of material, temperature is another data, along with moisture evaporation, when heating up to micro molecule position, because temperature reduces, the condition that change is decomposed also is not present in, and its effect is well imagined.
Detailed description of the invention
Embodiment 1:
Get dry product JINHUA news of victory ovary flower alabastrum 30kg, be ground into beater grinder and be less than 1mm × 1.1mm.Be less than 1mm × 1.3mm mix broken sheet material.Detecting gained material is 29.7kg, and difference is material consumption, and because of small lot processing, therefore material consumption ratio is large; Material contains moisture 8%.Reach less than 38% with material moisture to calculate, 29.7kg deducts contained humidity number, and 38% deducts 8% equals 30%, then is multiplied by 29.7kg with 30% and equals 0.89kg, and this total needs amount of water exactly, and the water of this quantity is heated 98 DEG C.Adopt spraying humidification normal direction material to use the water of 98 DEG C of temperature, spraying humidification, then extrude material after humidification with the microminiature granulation machine of screw; obtained semi-finished product to be dried, are placed in small-sized drying baker to it, do not have 110 DEG C of humidity; after dry 23 minutes, obtain drying regime granule manufactured goods.
Embodiment 2:
Get 30kg open after JINHUA news of victory ovary flower dry product, adopt ball impact disintegrating mill, be ground into be less than 1mm × 0.5mm be less than 1mm × 1.6mm mix trickle fragment.In the manner of example 1, calculating is made into and adds wet stock, entrusts pharmaceutical factory, adjacent Guan Village, by its equipment, technique, stamps out semi-finished product to be dried, then carry out drying with its rolling chain type drying device, within dry 18 minutes, obtains sheet-like article.
Embodiment 3:
Hebei academy of agricultural sciences millet institute, has a set of spraying dry and colloid mill, filtration refining equipment that temporarily stop operation, is furnished with specific technique personnel, and they are by consigned processing.
The JINHUA news of victory ovary flower 300kg that the JINHUA news of victory ovary alabastrum mixing of gathering fresh is just open, with the obtained flower slurry of the beater of blade type device.Deliver millet institute in time specifically by entrusting technical staff, by its obtained powder-type JINHUA news of victory flower goods.
Claims (5)
1. the invention provides a kind of JINHUA news of victory flower goods, it is characterized in that: select the JINHUA news of victory in gynoecium end stand room flower to do raw material, be processed as the material of dosage form goods; When producing tablet dosage form goods, graininess dosage form goods, adopt fresh goods flower material dewatering, to the disposal of dry product flower material humidification, make its moisture 17% to 39%; The temperature this appropriate water content material being done to less than 99.8 DEG C controls, punching press obtains lamellar semi-finished product to be dried or the obtained graininess semi-finished product to be dried of extruding, and then use less than 148 DEG C temperature to do dry disposal respectively, obtained JINHUA news of victory flower sheet articles, JINHUA news of victory flower particle product respectively; During with JINHUA news of victory ovary flower slurry materiel machining goods, first add three times to five times water of flower slurry weight to flower slurry, spray after colloid mill centrifugal, obtained powdery JINHUA news of victory flower goods; In whole technological process, material does not contact acidity, alkalescence, organic solvent material, does not dose adjuvant in material.
2. described in claim 1 as the JINHUA news of victory flower of food materials raw material, be called for short ovary flower, it is characterized in that: be the flowering time institute spewing flower bud centered by the ovary tissues of flower or open flower; This beggar room keeps completely, and ovary bottom is connected with anthocaulus base portion tissue and organizes organic all-in-one-piece calyx with base portion, and ovary top is organically connected with male flower stamen, and ovary round base portion is organically connected with whole petal; Be exactly for important document with beggar room, the flower of organic connected pistil, petal, calyx, anthocaulus base portion tissue, the gynoecium end seat of flower is at the ovary center of flower, and to be that 93110506.4 patents of inventor and lot of documents quote the character that relevant entry word describes far different to Xiong Ningning.
3. described in claim 1, the harvesting of ovary flower is obtained is: colored gynoecium of gathering grows the flower being no more than 10 hours after not having the open flower of the alabastrum of Pollination Fertilization or gynoecium part Pollination Fertilization or gynoecium Pollination Fertilization, obtains by the dehydration technique of known flower.
4. product described in claim 1, JINHUA news of victory tablet half-finished drying time is within 2 hours, and granule half-finished drying time is within 1.5 hours, and flower serosity powdery half-finished drying time is within 58 minutes.
5. product described in claim 1, does Chinese crude drug food products or medicine, food, cosmetic material uses.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410623459.7A CN105560305A (en) | 2014-11-09 | 2014-11-09 | Abelmoschus manihot flower product |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410623459.7A CN105560305A (en) | 2014-11-09 | 2014-11-09 | Abelmoschus manihot flower product |
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| Publication Number | Publication Date |
|---|---|
| CN105560305A true CN105560305A (en) | 2016-05-11 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410623459.7A Pending CN105560305A (en) | 2014-11-09 | 2014-11-09 | Abelmoschus manihot flower product |
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| Country | Link |
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| CN (1) | CN105560305A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1088826A (en) * | 1993-01-01 | 1994-07-06 | 南京中医学院 | A kind of medicine for the treatment of primary glomerulopathy and chyluria and preparation method thereof |
| CN1131519A (en) * | 1995-03-21 | 1996-09-25 | 王凌 | Wild cottonrose hibiscus drink |
| CN1241408A (en) * | 1998-03-30 | 2000-01-19 | 王凌 | Medicine with wild cottonrose hibiscus |
| CN1524434A (en) * | 2003-02-26 | 2004-09-01 | 王 欣 | Extractive product of sunflower |
-
2014
- 2014-11-09 CN CN201410623459.7A patent/CN105560305A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1088826A (en) * | 1993-01-01 | 1994-07-06 | 南京中医学院 | A kind of medicine for the treatment of primary glomerulopathy and chyluria and preparation method thereof |
| CN1131519A (en) * | 1995-03-21 | 1996-09-25 | 王凌 | Wild cottonrose hibiscus drink |
| CN1241408A (en) * | 1998-03-30 | 2000-01-19 | 王凌 | Medicine with wild cottonrose hibiscus |
| CN1524434A (en) * | 2003-02-26 | 2004-09-01 | 王 欣 | Extractive product of sunflower |
Non-Patent Citations (1)
| Title |
|---|
| 莫明雅等: ""黄蜀葵茎段植株再生体系的建立和花各部愈伤组织总黄酮含量的测定比较"", 《四川大学学报（自然科学版）》 * |
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Application publication date: 20160511 |