CN105560086B - A kind of pure natural multiple-effect containing peony seed oil nourishes suncream and preparation method thereof - Google Patents
A kind of pure natural multiple-effect containing peony seed oil nourishes suncream and preparation method thereof Download PDFInfo
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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Abstract
The invention discloses a kind of all natural ingredients composition of sun-proof moisturizing anti aging effect, it is made up of peony seed oil, excellent olive emulsifying wax, Yilan hydrosol, rose, deionized water, trehalose, the solution of polymer hyaluronic acid sodium 1%, the solution of low-numerator sodium hyaluronate 1%, aloe gel stoste, red pomegranate extract, Silasoma MEA ultraviolet radiation absorptions inclusion enclave, fine particulate titanium dioxide dispersion liquid, Lycopene, pentanediol, 1,3 butanediols, the bark of official magnolia bark extract, antiseptic.The present invention not only can effectively keep out injury of the ultraviolet to face skin, prevention face skin is tanned and tans severely, simultaneously face skin can be nourished, facial skin cell is permeated while replenishing water and preserving moisture, easily absorbed by Skin Cell, and it can comprehensively provide the various nutrition required for face skin, damaged cell can be more repaired rapidly, recovers skin of face cytoactive, reduce wrinkle, recover elasticity of skin and pale, allow face to reappear brilliance at an early age.
Description
Technical field
The invention belongs to daily cosmetics preparing technical field, is related to a kind of uvioresistant, anti-skin oxidative aging and suppression
The composition that melanin processed is formed, more particularly to a kind of pure natural multiple-effect containing peony seed oil nourish suncream and its preparation side
Method.
Background technology
The sun also creates a large amount of ultraviolets while coming bright and warm to earth zone, purple according to the length of wavelength
Outside line can be divided into ultraviolet light,long wave (UVA, 320~400nm), UV-B (UVB, 280~320nm) and ultraviolet C (UVC, 200~
280nm) three kinds, UVA dominates sunlight aging, and UVB causes the chief-criminal arch-criminal of skin sunburn, and UVC then makes one highly carcinogenic, but
Fortunately, UVC is absorbed by atmosphere.Ultraviolet (UV) A and UVB can penetrate skin corium, and skin sunburn, tanned and generation is de-
Phenomenon after skin etc. shines, so as to cause skin to shift to an earlier date aging, carrys out some irremediable injuries, if for a long time by UVA to skin tape
With UVB influence, it is also possible to cause cutaneum carcinoma.
Sunshine is continuous electromagnetic radiation as waves, and with the high speed development of modern city, appearance of city is maked rapid progress, high building
Mansion, curtain wall stand in great numbers, and vehicle streams past in an endless flow, these cladding glass, the metope of skyscraper, automotive glazing and surface road
Will reflection ultraviolet, so as to increase the amount of ultraviolet irradiation of earth surface, therefore sun-proof be just particularly important.Correlative study
Show, the ultraviolet exposure rate on rainy day is the 21%-54% of fine day, and cloudy ultraviolet irradiation rate is the 81%- of fine day
95%, this explanation throughout the year all should be sun-proof.
Economic fast development, people's living standard is brought to improve constantly, skin care item maintain from a kind of skin care
Luxury goods be changed into necessity.Face is a people most intuitively external manifestation, and face skin is more fragile, be easiest to and
Most directly by ultraviolet injury position, in order to prevent skin by it is tanned and sunburn, with the addition of the suncream of sun-prevention component
Product arises at the historic moment, while as people endanger ultraviolet radiation the in-depth of understanding, sun-proof consciousness and after-sun maintenance meaning
Know constantly enhancing, sun care preparations is even more to occupy critical role as a kind of caused by cosmetics for special use.Presently commercially available sun-proof production
Product sun care preparations functional component is rich and varied, and it is (also referred to as inorganic that physical ultraviolet light screener can be divided into from mechanism of action
Sun-screening agent, this kind of material on skin for that can reflect, scatters ultraviolet) and chemically ultra-violet absorber (is also known as organic sunscreen
Agent, this kind of material can be with selective absorbing ultraviolets so as to play anti-sunlight function, such as p-aminobenzoic acid and its derivative, Chinese cassia tree
The plant extracts such as the compounds such as acid or natural materials such as aloe, there are some bioactive substances and antioxidant reductase etc.).Thing
Reason suncream is thick and heavy, and there is burden in summer to skin, easy fuel-displaced blocking pore, but not easily leads to skin sensitivity；Chemical sunscreen
Frost is frivolous, and cutaneous respiration is smooth, and quality oiliness easily absorbs, but sensitive skin does not adapt to.Meanwhile some manufacturers in order to
Increase white-skinned face function, do not stint and add heavy metal and the fluorescent whitening agents such as lead mercury, injury is brought to skin.And commercially available suncream work(
Can be relatively single, only focus on sun-proof function, it is few to have sun-proof and after-sun double effects suncreams concurrently and commercially sell
Sell, therefore there is certain gaps in market.And it is of note that can between existing sun-prevention component and after-sun composition
There can be certain relation that influences each other, i.e., when both are made an addition in identical product jointly, there may be certain counteracting to make
With, cause sun-proof function to weaken, while cause the system of suncream to become unstable, it is difficult to uniformly be applied on skin.
The content of the invention
The defects of in order to overcome prior art and deficiency, it is an object of the invention to provide one kind by physical sunscreen and chemistry
Sun-proof to be combined the ultraviolet that effectively resist each wave band, collection is sun-proof, moisturizing, moisturizing, whitening, anti-oxidant, prevention pigment sink
The composition of the sun-proof moisturizing anti aging effect of after-sun such as, a kind of pure day containing peony seed oil is especially provided
Right multiple-effect nourishes suncream and preparation method thereof.
In order to realize the purpose of the present invention, inventor is studied by lot of experiments, is finally obtained and is contained peony seeds as follows
The pure natural multiple-effect of oil nourishes the technical scheme of suncream：
A kind of all natural ingredients composition of sun-proof moisturizing anti aging effect, it is by peony seed oil, excellent olive emulsifying wax, Yilan
Hydrosol, rose, deionized water, trehalose, the solution of polymer hyaluronic acid sodium 1%, low-numerator sodium hyaluronate 1% are molten
Liquid, aloe gel stoste, red pomegranate extract, Silasoma MEA ultraviolet radiation absorptions inclusion enclave, fine particulate titanium dioxide dispersion liquid,
Lycopene, pentanediol, 1,3 butanediols, the bark of official magnolia bark extract, antiseptic composition.
Preferably, all natural ingredients composition of above-mentioned sun-proof moisturizing anti aging effect, wherein the component is by weight
The composition of number meter is：
It is further preferred that all natural ingredients composition of above-mentioned sun-proof moisturizing anti aging effect, wherein the component is pressed
The composition of parts by weight meter is：
Still further preferably, all natural ingredients composition of sun-proof moisturizing anti aging effect as described above, it is sun-proof
Frost, and described the bark of official magnolia bark extract is the bark of official magnolia bark extract 98 of German cosphatec productions.
In addition, the system of all natural ingredients composition suncream of above-mentioned sun-proof moisturizing anti aging effect provided by the present invention
Preparation Method, it is comprised the following steps：
(1) the bark of official magnolia bark extract, the red pomegranate extract of recipe quantity are weighed, is dissolved respectively with 1,3 butanediol, it is standby；
(2) A, B totally 2 beakers are taken, peony seed oil, the excellent olive emulsifying wax of recipe quantity are added in A beakers；
(3) Yilan hydrosol, rose, deionized water, trehalose and the Lycopene of recipe quantity are added in B beakers, is stirred
Mix to being completely dissolved；
(4) A beakers and B beakers are heated in a water bath, heated while stirring, until decorating film dissolves, temperature reaches 75
Stop heating after DEG C, the solution in B beakers is poured into A beakers according to a small amount of multiple mode and quickly stirred；
Etc. (5) when the temperature of mixed liquor drops to 40 DEG C, add according to this recipe quantity the solution of polymer hyaluronic acid sodium 1%,
The solution of low-numerator sodium hyaluronate 1%, aloe gel stoste, red pomegranate extract solution, Silasoma MEA ultraviolets parcel
Body, fine particulate titanium dioxide dispersion liquid, pentanediol, the bark of official magnolia bark extract solution, 1-3 minutes are stirred after often adding a kind of component；
(6) antiseptic of recipe quantity is eventually adding, stirs and both may be used.
Preferably, the preparation method of all natural ingredients composition suncream of sun-proof moisturizing anti aging effect as described above,
Red pomegranate extract therein is made as follows：Using granatum powder as raw material, the fourth using volume fraction as 50%-66%
For glycol solution as Extraction solvent, feed liquid adjusts pH=3.0 after mixing, normal temperature ultrasound extraction, extraction time 0.5-3h, filter,
Filter vacuum, which concentrates, to be produced.
It should be noted that the preparation of all natural ingredients composition suncream of sun-proof moisturizing anti aging effect as described above
Method, excellent olive emulsifying wax therein are the excellent olive liquid crystal olive emulsifying wax of the celestial graceful production of France, English name OLDERM CRYSTALM
O IST, INCI are sorbierite olive oleate, the hard ester group glucoside of spermaceti；Described Yilan hydrosol is that commercially available motor adds
This adds Yilan hydrosol, and Cananga odorata quintessence oil content is 0.025%；Described rose is pure for commercially available Bulgarian organic rose
Dew, Rosa Damascana content are 0.05%；The described solution (product code HA-TL) of polymer hyaluronic acid sodium 1% and low molecule
The solution (product code HA-TLLM) of Sodium Hyaluronate 1% is Bloomage Freda Biopharm Co., Ltd.'s product；Described reed
Luxuriant growth gel stoste be global healthy group of the U.S. good jade Lu Dema aloe gel stostes, purity ＞ 99%；Described Silasoma
MEA ultraviolet radiation absorptions inclusion enclave is that bag particulate capsule (give birth to by Nippon Kasei Chemical Company in commercially available organic uv absorbers
Production)；Described fine particulate titanium dioxide dispersion liquid is 60% particulate titanium dioxide aqueous phase of Nippon Kasei Chemical Company's production
Dispersion；Described the bark of official magnolia bark extract is high-purity (>=98%) the bark of official magnolia bark extract of German cosphatec productions
98, INCI entitled Magnolia Officinalis Bark Extract the bark of official magnolia bark extract.
Found according to antioxygenic property experimental study, simultaneously the sample 1 containing peony seed oil and red pomegranate extract
Inoxidizability be significantly higher than only addition a red pomegranate extract do not add the sample 2 of peony seed oil, and be significantly higher than only add
Peony seed oil does not add the sample 3 of red pomegranate extract, and this illustrates peony seed oil and red pomegranate extract according to a certain percentage
Be used in combination has the function that skin histology excessive free radicals are removed in collaboration in skin care item.Therefore, present invention also offers two
New opplication associated with kind specific components, i.e.,：Peony seed oil and red pomegranate extract are excessive free in removing skin histology is prepared
Application in the skin care item of base；Or peony seed oil and red pomegranate extract answering in skin inoxidizability skin care item are prepared
With.It is further preferred that described skin care item are suncream.
Compared with prior art, all natural ingredients composition of sun-proof moisturizing anti aging effect of the invention is (pure natural
Multiple-effect nourishes suncream) there is following beneficial technique effect：
(1) there is sun-proof, anti-oxidant, removing free radical, desalination color spot, whitening, anti-inflammation and keep face skin to hold
Moisten long and wait multi-efficiency, not only can effectively keep out injury of the ultraviolet to face skin, prevention face skin is tanned and shines
Wound, while can nourish face skin, permeate facial skin cell while replenishing water and preserving moisture, easily absorbed by Skin Cell,
And the various nutrition required for face skin can be comprehensively provided, damaged cell can be more repaired rapidly, recover skin of face cell
Activity, wrinkle is reduced, recover elasticity of skin and pale, allow face to reappear brilliance at an early age.
(2) in the state of summer face skin is by tanned or sunburn, as long as gently applying last layer contains tree peony
The pure natural multiple-effect of seed oil nourishes suncream, and is gently massaged, and just can intimately be merged with the skin that is hurt, infiltration is repaiied rapidly
Answer skin and diaphragm can be formed in skin surface, while absorbing and stopping ultraviolet, allow moisture veritably to stay in skin
On, allow nutrition to be really absorbed by the skin, occur away from reasons such as the stimulations because of sunlight and contact wind, dirt and color make-up residual
Coarse blackening and lost its bounce to puzzlement caused by skin, face skin is recovered elastic force, pale and delicate.
(3) composition retains active ingredient to greatest extent, and its major function is sun-proof and after-sun, can
Absorb and keep out ultraviolet, supplement the nutrient required for face skin, repair damaged cell, effectively suppress facial melanin shape
Into, remove free radical, replenishing water and preserving moisture, compact delicate and pale, accurately act on face skin cell, being capable of effective active cell
Metabolism, skin, desalination color spot are nourished, effect is persistently stablized.
(4) one layer of uvioresistant diaphragm can be formed on face skin surface and can fully penetrates into skin depths and assigned
Skin nutrition and vigor；It with the addition of with highly anti-ultraviolet peony seed oil, aloe gel stoste and fine particulate titanium dioxide point
Powder etc.；It with the addition of heigh antioxidation and alimentary red pomegranate extract and water-soluble Lycopene strong anti-oxidation elite
HYDROPOM；It with the addition of simultaneously with height moistness, humidity-preserving type and infiltrative trehalose, low-numerator sodium hyaluronate 1%
Solution and the solution of polymer hyaluronic acid sodium 1%；It also added with the rose for nourishing skin, activating cell and natural water lock effect
Rare hydrosol and Yilan hydrosol.
(5) after smearing face skin for a period of time, skin recovers elastic force and gloss.Because which are added Natural Antioxidants
Peony seed oil, American Red Punica granatum L. extract, ginseng extract and water-soluble Lycopene strong anti-oxidation elite HYDROPOM, Neng Gouyou
Effect removes free radical, so as to prevent cell senescence, anti-aging, and it is extremely strong with the affinity of skin, face skin can be played
Prolonged nourishes effect.
(6) composition uses pure natural antibacterial composition, reduces skin stimulation and mistake that addition artificial preservative is brought
Quick symptom, the pentanediol of addition are the natural moisture preserving agent of excellent performance and have anti-corrosion function, the bark of official magnolia bark extract of addition
With preferable antibacterial and anti-oxidation efficacy, the bright peptide antiseptic of addition is the filtrate of Carrot Roots tunning, is had very strong
Sterilization functions are sterilized, are all natural anticorrosion compositions, it is non-stimulated to skin.
(7) composition suncream forms for a variety of natural, greens, secure group branch compounding, the suncream tool prepared
Have good sun protection, can effectively resist the ultraviolet of each wave band, while there is good after-sun function, anti-oxidant,
The characteristics of tender skin moisturizing, Whitening, spot, nontoxic etc., the pure natural multiple-effect containing peony seed oil are nourished suncream and can be not only used for
Injury of the pre- antiultraviolet to skin, can repair and nourish again solarization after skin, including to facial scaly dry skin, pigment deposition,
Skin tanning, wrinkle deepen and colonization when following the string, and is alternatively arranged as preventing the anti-aging product of face skin aging,
The development trend of sunlight screening skin-protecting product will be turned into, there is wide market application foreground and economic value.
Embodiment
It is the specific embodiment of the present invention below, technical scheme is done and is further described, but it is of the invention
Protection domain be not limited to these embodiments.It is every to be included in this hair without departing substantially from the change of present inventive concept or equivalent substitute
Within bright protection domain.
It should be noted that excellent olive emulsifying wax is by French celestial graceful production, English name OLDERM in following examples
CRYSTALM O IST, INCI are sorbierite olive oleate, the hard ester group glucoside of spermaceti；Yilan hydrosol is commercially available motor
Jia Sijia Yilans hydrosol, Cananga odorata quintessence oil content are 0.025%；Rose is commercially available Bulgarian organic rose hydrosol, rose
Rare essential oil content is 0.05%；Trehalose is the Japanese woods original trehalose of Qingdao Abel Science and Technology Ltd. sale
Trehalose, purity ＞ 98%；The solution of polymer hyaluronic acid sodium 1% (HA-TL) and the solution of low-numerator sodium hyaluronate 1%
(HA-TLLM) it is Bloomage Freda Biopharm Co., Ltd.'s product；Aloe gel stoste is to use Global group of U.S. AGHG
Training technology -- the special dew fresh Aloe gel juice that SATT aloe process technologies produce, brand is good jade Lu Dema, purity
＞ 99%；Silasoma MEA ultraviolet radiation absorptions inclusion enclave is in the organic uv absorbers of Nippon Kasei Chemical Company's production
Bag particulate capsule；Fine particulate titanium dioxide dispersion liquid is 60% particulate titanium dioxide water of Nippon Kasei Chemical Company's production
Phase dispersion；Lycopene is commercially available water-soluble Lycopene strong anti-oxidation elite HYDROPOM, is produced by Italian Phenbiox；
The bark of official magnolia bark extract is natural organic the bark of official magnolia bark extract of German cosphatec high-purities (>=98%), and INCI is entitled
Magnolia Officinalis Bark Extract the bark of official magnolia bark extract；Antiseptic produces for U.S. Active Motif
Bright string coccus ＆ radish root tunning filtrate, production code member M15008.
The preparation of embodiment 1-3 suncreams
Formula is shown in Table 1：
The formula of the sunblock compositions of table 1
Above-mentioned formula preparing process is as follows：
(1) preparation of red pomegranate extract
Take Mengzi Yunnan fresh pomegranate → cleaning → 45 DEG C constant temperature drying → crushing → accurately weigh 10g powder → addition
200ml volume fractions are 60% butanediol solution (solid-liquid ratio 1:20, pH=3.0) → ultrasonic extraction 40min (extraction 3 times) →
Filtering vacuum concentration → red pomegranate extract finished product.
(2) solution is prepared
A, the bark of official magnolia bark extract solution is prepared
It is accurate to claim the bark of official magnolia bark extract 1g, dissolved with 1,3 butanediol, be configured to 1:20 butanediol solution is standby.
B, red pomegranate extract solution is prepared
Red pomegranate extract 1g accurately is weighed, is dissolved with 1,3 butanediol, is configured to 1:9 butanediol solution is standby.
(3) deionized water processing procedure：
1. filter impurities in water；
2. high pressure passes through reverse osmosis membrane；
3. ultraviolet-sterilization；
4. carry out ion exchange process maximum resistance rate 18,000,000.
(4) take 2 clean beakers of A, B stand-by, the peony seed oil of recipe quantity, excellent olive are added in A beakersTMLiquid crystal is protected
Wet emulsifying agent；
(5) Yilan hydrosol, rose, deionized water, trehalose and the water-soluble eggplant that recipe quantity is added in B beakers are red
Plain strong anti-oxidation elite HYDROPOM, stirring is to being completely dissolved；
(6) beaker A and beaker B are placed on constant temperature water proof on electromagnetic oven to heat, heated while stirring, until decorating film is molten
Solution, temperature immediately lift down beaker A, B after reaching 75 DEG C, and the aqua in B beakers is poured into burning according to a small amount of multiple method
Quickly stirred in cup A, approximate time 20 minutes or so；
(7) after stirring, when waiting the temperature of mixture to drop to 40 DEG C, the polymer hyaluronic acid of recipe quantity is added according to this
The solution of sodium 1%, the solution of low-numerator sodium hyaluronate 1%, good jade Lu Dema aloe gels stoste, American Red Punica granatum L. extract, ginseng
Extract, Silasoma MEA ultraviolets inclusion enclave, 60% particulate titanium oxide dispersion, pentanediol, Magnolia bark extraction
Thing, additive, which often adds a kind, needs stirring 2 minutes；
(8) antiseptic of recipe quantity is eventually adding, stirs and both may be used；
(9) preserved under the suncream sealing normal temperature that Packs sterilized installs, the term of validity 12 months.
The pure natural multiple-effect containing peony seed oil prepared using above-mentioned formula and technique, which nourishes suncream, has following work(
Effect：
(1) ultraviolet for effectively resisting each wave band injures to caused by skin, has excellent sun-proof performance；
(2) skin is nourished comprehensively, repairs damaged cell, effectively removes free radical, recovers skin of face cytoactive, is kept
The persistently pale colour of skin, the delicate water for allowing face to reappear at an early age moisten, and skin ageing after confrontation is shone, have good after-sun
Effect；
(3) diaphragm is formed in skin surface while permeating face skin rapidly, effectively stops ultraviolet and wind, dirt
Injured with color make-up to caused by skin, make face skin recovery elastic force, compact He Shuirun；
(4) effectively suppress the activity of Skin Cell tyrosinase, stop that melanin is formed, prevent pigementation；
(5) effectively activated cell activity, promotion cell metabolism regenerate, and reduce wrinkle, delaying skin aging.
Influence of the peony seed oil content of embodiment 4 to the sun-proof performance of sunblock compositions
Experiment set 5 samples, the sample 1-5 same embodiment of compound method, wherein peony seed oil content be followed successively by 1 part, 4
Part, 7 parts, 10 parts and 13 parts, other components content is the same as embodiment 1, then sample 4 is identical with embodiment 1, main measure
Product is sun protection under 6 wavelength of 280nm, 290nm, 300nm, 310nm, 320nm and 330nm.It is assumed that using quartz plate as cutin
The biomaterials such as layer, epidermis, in the sun-proof sample of coated thereon, their absorbance (printing opacity is determined using ultraviolet specrophotometer
Rate) value.According to the size of absorbance (light transmittance), the sun-proof performance of product is evaluated.Assay method is as follows:
(1) one layer of product of even application on quartz plate surface；
(2) and then outside is tied up with adhesive tape and be put into wherein；
(3) its light absorption value on each wavelength is surveyed on ultraviolet specrophotometer.Using be not added with the sample of peony seed oil as
Blank control.
According to Lambert-Beer laws, absorbance is determined as index using ultraviolet spectroscopy, initial reaction sun-proof result.To keep away
Random error when exempting to use single absorbance as index, ask for UVA, UVB wave band mean light absorbencySmoothly locate
Reason.The normal data of sun-proof result evaluation reference Diffey experiments gained erythema occurrence frequency and wavelength relationship, wavelength is in 290-
330nm UV has stronger erythemal effect, therefore selects 280,290,300,310,320 (UVB) and 330 (UVA) nm5 ripples
It is long, absorbance is determined, according to the size of absorbance, evaluates the sun-proof performance of product.Absorbance is bigger, and sun-proof result is better, examination
Test and the results are shown in Table 2.
The calculation formula of absorbance is：
A (UVB)=(A280+A290+A300+A310+A320)/5
A (UVA)=A330
The sun protection result of the test of sample is shown in Table 2.
The sun protection development test result of the sample of table 2
It is can be seen that from the test statistics result of table 2 in the range of wavelength is 280nm-330nm, each sample absorbance
Significant difference, and UVA is significantly greater than to UVB absorbance；With the increase of peony seed oil content in sample, absorbance gradually increases
Greatly, when peony seed oil content reaches 10 in sample, the absorbance of sample 4 (embodiment 1) shows as maximum in each wave band,
And it is notable to the absorbance difference of ultraviolet with other samples, but when peony seed oil content is 13, sample absorbance performance
To reduce, it may be possible to sun protection not to be further added by because suncream is thinning later more than 10 for peony seed oil content.Can from experimental result
To find out, sample 4 is embodiment 1, and stronger ultraviolet-absorbing is whether all shown to UVB or UVA.Therefore no matter
It is ultraviolet B radiation or long wave ultraviolet, suncream of the present invention can play the good function of resisting ultraviolet, be preferable
Sunlight screening skin-protecting product.
The performance of keeping humidity of embodiment 5 is tested
Respectively take 6 parts to be divided into 2 groups embodiment 1-3, glycerine, hyaluronic acid, each sample is mounted in a diameter of 4cm table respectively
On the ware of face, weigh.First group of sample is dared into hydroscopicity under high humidity to determine, that is, is put into the room temperature (25 DEG C) for filling silica gel
Lower relative humidity (RH) is to be precisely weighed after handling 24h in the drier of the 81% saturated ammonium sulfate aqueous solution.Equally by second
Group sample is used for hydroscopicity under low-moisture conditions and determined, that is, it is that 43%, vacuum is the true of -0.1MPa to be put into relative humidity (RH)
It is precisely weighed in empty drier after drying process 24h.By before and after moisture absorption sample it is of poor quality, hydroscopicity is obtained according to following formula：
Hydroscopicity=(Mn-M0)/M0× 100% formula (1)
In formula (1)：M0For quality before sample moisture absorption, Mn is quality after moisture absorption 24h.When the moisture of absorption, to reach saturation follow-up
It is continuous to place 24h, each sample mass is accurately weighed, by of poor quality before and after sample, moisturizing rate is obtained according to following formula：
Moisturizing rate=Hn/H0× 100% formula (2)
In formula (2)：HnContain water quality, H for sample0Contain water quality to place sample after 24h
Sample moisture-absorbing moisture-keeping type result of the test is shown in Table 3.
The sample moisture absorbability and moisture retentivity result of the test of table 3
The hydroscopicity of each sample and moisturizing rate difference under high humidity are can be seen that from the test statistics result of table 3 to show
Write, glycerine and hyaluronic acid show stronger hygroscopicity, and embodiment 1-3 hygroscopicity does not protrude, but moistening effect is obvious
Higher than glycerine and hyaluronic acid；The hydroscopicity of each sample and moisturizing rate significant difference under under low humidity conditions, embodiment 1-3 inhale
Wet, moisture retention is had outstanding performance, and especially embodiment 1 shows superior hygroscopicity and moisture retention, better than glycerine and hyalomitome
Acid, especially with good hygroscopicity, and moisture-absorbing moisture-keeping effect stability.Therefore after-sun replenishing water and preserving moisture, embodiment are directed to
Suncream can play good moistening effect.
The antioxygenic property of embodiment 6 is tested
Experiment sets 3 samples, and sample 1 is the suncream of embodiment 1, and sample 2 is to replace peony seed oil (other groups with glycerine
Point with embodiment 1), sample 3 be that American Red Punica granatum L. extract (other components are with embodiment 1) is replaced with deionized water, with 95%
Ethanol compound concentration be 0.04mg/ml DPPH solution.1ml sample solutions and 3mlDPPH solution are pipetted respectively in tool plug test tube
In, after fully mixing, lucifuge stands 30min after measure absorbance A under 517nm at room temperature1.Sample is replaced with 1ml ethanol
Solution makees blank determination absorbance A0, the absorbance A with 3ml ethanol instead of DPPH solution determination sample solution2.Count according to the following formula
Calculate the clearance rate of DPPH free radicals (experimental result is shown in Table 4)：
The clearance rate of DPPH free radicals=(1- (A1-A2)/A0) × 100%
Clearance rate of each sample of table 4 to DPPH free radicals
DPPH is a kind of free radical at very stable nitrogen center, resonance stabilized of its stability essentially from 3 phenyl ring
Effect and spatial obstacle, azygous electronics acts in pairs from playing its due electronics on the nitrogen-atoms for preventing to be clipped in the middle.
DPPH alcoholic solution is dark purple, due to DPPH free radicals centered on 517nm place there is strong absorption, when there is free radical
In the presence of scavenger, the lone pair electrons in DPPH on nitrogen are paired and so that solution colour shoal, and become colorless or light yellow, make
Absorbance is obtained to diminish, therefore absorbance is smaller, clearance rate is bigger, shows that the oxidation resistance of scavenger is stronger.Utilize this
One characteristic can intuitively detect clearance rate of the scavenger to DPPH.3 sample solutions are can be seen that from the result of the test of table 4
The clearance rate significant difference to DPPH free radicals, the clearance rate of sample 1 is up to 87.67%, shows stronger antioxygen
Change ability, next to that sample 2, clearance rate 45.06%, the clearance rate of sample 3 is most weak, is 38.63%.From the group of 3 samples
Divided by sample 1 contains peony seed oil and red pomegranate extract, and sample 2 is free of peony seed oil, and remaining component is the same as sample 1, sample
3 are free of red pomegranate extract, and remaining component is not difficult to find out from the clearance rate to DPPH free radicals with sample 1, contains tree peony simultaneously
The inoxidizability of the sample 1 of seed oil and red pomegranate extract is significantly higher than only addition red pomegranate extract and does not add peony seed oil
Sample 2 and an addition peony seed oil do not add the sample 3 of red pomegranate extract, and this illustrates peony seed oil and red pomegranate extract
Be used in combination according to a certain percentage has the function that skin histology excessive free radicals are removed in collaboration in skin care item.The experiment simultaneously
Show, the suncream of embodiment has compared with strong anti-oxidation, can effectively delay face skin aging, be that more satisfactory nourishing is prevented
Shine frost.
The sense organ physical and chemical index of embodiment 7 determines
Required to carry out conventional index inspection according to the standard indexs (being shown in Table 5) of China moisturizing cream industry QB/T 1857-2013
Suncream prepared by embodiment 1 is surveyed, the results are shown in Table 6.From result in table 6, the suncream indices prepared by the present invention
Meet relevant industries standard.
The sense organ of table 5, physical and chemical standards index
The embodiment sense organ of table 6, physical and chemical index measurement result
Claims (6)
1. a kind of sun-proof moisturizing anti aging effect composition, its by peony seed oil, excellent olive emulsifying wax, Yilan hydrosol, rose,
It is deionized water, trehalose, the solution of polymer hyaluronic acid sodium 1%, the solution of low-numerator sodium hyaluronate 1%, aloe gel stoste, red
Punica granatum L. extract, Silasoma MEA ultraviolet radiation absorptions inclusion enclave, fine particulate titanium dioxide dispersion liquid, Lycopene, pentanediol, 1,3-
Butanediol, the bark of official magnolia bark extract and antiseptic composition, the composition that each component is counted in parts by weight are：
Peony seed oil 9-11
Excellent olive emulsifying wax 3-5
Yilan hydrosol 20-40
Rose 15-35
Deionized water 10-20
Trehalose 4-6
The solution 2-4 of polymer hyaluronic acid sodium 1%
The solution 1-3 of low-numerator sodium hyaluronate 1%
Aloe gel stoste 1-3
Red pomegranate extract 0.44-0.67
Silasoma MEA ultraviolet radiation absorption inclusion enclaves 4-6
Fine particulate titanium dioxide dispersion liquid 11-13
Lycopene 1-3
1,3 butylene glycol 6-12
Pentanediol 1-3
The bark of official magnolia bark extract 0.025-0.075
Antiseptic 0.5-1.5.
2. sun-proof moisturizing anti aging effect composition according to claim 1, it is characterised in that each component is by weight
Counting the composition counted is：
Peony seed oil 10
Excellent olive emulsifying wax 4
Yilan hydrosol 30
Rose 25
Deionized water 15
Trehalose 5
The solution 3 of polymer hyaluronic acid sodium 1%
The solution 2 of low-numerator sodium hyaluronate 1%
Aloe gel stoste 2
Red pomegranate extract 0.56
Silasoma MEA ultraviolet radiation absorptions inclusion enclave 5
Fine particulate titanium dioxide dispersion liquid 12
Lycopene 2
1,3 butylene glycol 9
Pentanediol 2
The bark of official magnolia bark extract 0.05
Antiseptic 1.
3. sun-proof moisturizing anti aging effect composition according to claim 1 or claim 2, it is characterised in that described Magnolia bark
Extract is the bark of official magnolia bark extract 98 of German cosphatec productions.
4. sun-proof moisturizing anti aging effect composition according to claim 1 or claim 2, it is characterised in that described composition is
Suncream.
5. a kind of preparation method of moisturizing anti aging effect composition suncream sun-proof according to claim 4, its feature exist
In this method comprises the following steps：
（1）The bark of official magnolia bark extract, the red pomegranate extract of recipe quantity are weighed, is dissolved respectively with 1,3-BDO, it is standby；
（2）A, B totally 2 beakers are taken, peony seed oil, the excellent olive emulsifying wax of recipe quantity are added in A beakers；
（3）Yilan hydrosol, rose, deionized water, trehalose and the Lycopene of recipe quantity are added in B beakers, stirring is extremely
It is completely dissolved；
（4）A beakers and B beakers are heated in a water bath, heated while stirring, until decorating film dissolves, after temperature reaches 75 DEG C
Stop heating, the solution in B beakers is poured into A beakers according to a small amount of multiple mode and quickly stirred；
（5）When dropping to 40 DEG C Deng the temperature of mixed liquor, the solution of polymer hyaluronic acid sodium 1%, the low molecule of recipe quantity are sequentially added
The solution of Sodium Hyaluronate 1%, aloe gel stoste, step（1）Red pomegranate extract solution, the Silasoma MEA of preparation are ultraviolet
Line absorption inclusion enclave, fine particulate titanium dioxide dispersion liquid, pentanediol, step（1）The bark of official magnolia bark extract solution of preparation, is often added
1-3 minutes are stirred after a kind of component；
（6）The antiseptic of recipe quantity is eventually adding, is stirred.
6. the preparation method of sun-proof moisturizing anti aging effect composition suncream according to claim 5, it is characterised in that institute
The red pomegranate extract stated is made as follows：Using granatum powder as raw material, the butanediol using volume fraction as 50%-66%
Solution adjusts pH=3.0, normal temperature ultrasound extraction, extraction time 0.5-3h is filtered, and filtrate is true as Extraction solvent after feed liquid mixing
Sky, which concentrates, to be produced.
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| CN105078875A (en) * | 2015-09-06 | 2015-11-25 | 菏泽瑞璞牡丹产业科技发展有限公司 | Peony extract-containing cosmetic and preparation method thereof |
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| CN105078875A (en) * | 2015-09-06 | 2015-11-25 | 菏泽瑞璞牡丹产业科技发展有限公司 | Peony extract-containing cosmetic and preparation method thereof |
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