CN105558193A - Production method of composite tea made of folium ilicis hainanensis extract and eucommia ulmoides extract - Google Patents
Production method of composite tea made of folium ilicis hainanensis extract and eucommia ulmoides extract Download PDFInfo
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/34—Tea substitutes, e.g. matè; Extracts or infusions thereof
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Abstract
The invention discloses a production method of composite tea made of folium ilicis hainanensis extract and eucommia ulmoides extract and belongs to the technical field of tea. The production method includes: preprocessing before picking, preparing the folium ilicis hainanensis extract, preparing the eucommia ulmoides extract, and mixing and packaging to obtain the composite tea which is high in active ingredient content (especially high in flavonoid content). The production method has the advantages that the effect of the folium ilicis hainanensis extract and the effect of the eucommia ulmoides extract are sufficiently combined, the defect of single effect of tea is overcome, and the method is promising in development prospect.
Description
Technical field
The present invention relates to a kind of preparation method of hainan holly leaf eucommia ulmoides extracts compound tea, belong to tea technical field.
Background technology
Hainan holly leaf, also known as hainan holly leaf, it is cold in nature, bitter, through entering liver, spleen, lung, kidney, calms down liver, has clearing heat and detoxicating, swelling and pain relieving, blood circulation and channel invigorating effect.Can be used for hypotensive, reducing blood lipid, norcholesterol, coronary heart disease, hemiplegia caused by cerebrovas-cularaccident and anemopyretic cold, cough with lung heat, edema of throat, tonsillitis, dysentery.This is owing to containing flavonoids, triterpene acids, triterpene saponin in hainan holly leaf, the chemical composition such as Coumarins, chlorogenic acid, also containing certain trace element.Wherein, Flavonoid substances is the main active of hainan holly leaf, has the effect of reducing blood lipid, Suppress hyperplasia of prostate, anti-NASH etc.As Chinese patent CN101214269B discloses one " method of Extraction and enrichment total flavones of ilex hainanensis ", the method is achieved in that the alcohol reflux with weight concentration is 40-95% extracts, upper HPD-400 macroreticular resin after extract is concentrated, use sweat ethanol gradient elution, collect the part that concentration is 20-50% ethanol elution, it is after recycling design, dry.The method selectively deposition activity composition in leaching process, removes other compositions and impurity, obtains the general flavone content being greater than 50%.
The bark of eucommia, be Eucommiaceae bark of eucommia platymiscium, it is warm in nature, and taste is sweet, micro-pungent, has that anti-inflammatory is antibacterial, sedation-analgesia, diuresis, kidney tonifying step-down, strengthens the effect such as immunologic function and anticancer, strengthening the bones and muscles, strong waist knee, antifatigue, anti-ageing, fat-reducing.Why the bark of eucommia has these effects, mainly owing to containing various active composition in the bark of eucommia, as lignanoids, iridoids, Phenylpropanoid Glycosides class, polysaccharide, flavones etc.Along with socioeconomic fast development and people's living standard significantly improve, people are to health problem growing interest.Hypertension is a kind of common angiocardiopathy, usually can cause the complication of the internal organs such as the heart, brain, kidney, drastically influence people's quality of life.But the bark of eucommia is a kind of natural antihypertensive drugs of high-quality meeting modern.Therefore, the research and development of the bark of eucommia will have broad application prospects.At present, people carry out many-sided research to the bark of eucommia, and obtain certain achievement, as Chinese patent CN103773593B discloses one " a kind of method extracting bark of eucommia fruit oil from Eucommia seed "; CN103828983A discloses one " a kind of eucommia tea health "; CN104154719A discloses one " a kind of drying means of the bark of eucommia ".
Although the research of hainan holly leaf and the bark of eucommia has carried out the several years, through retrieval prior art, still not yet find the research report of the compound tea about their extracts composition so far.Consider that hainan holly leaf and the bark of eucommia have multiple efficacies, therefore, the preparation method studying a kind of hainan holly leaf eucommia ulmoides extracts compound tea is very important.
Summary of the invention
The technical problem to be solved in the present invention is to overcome the deficiencies in the prior art, the invention provides a kind of preparation method of hainan holly leaf eucommia ulmoides extracts compound tea.
The present invention for the taked technical scheme that solves the problem is:
The hainan holly leaf eucommia ulmoides extracts compound tea that the present invention relates to is that the Shanlu Tea extract for dropping of 50%:50% and eucommia ulmoides extracts form by mass percent.
The preparation method of the hainan holly leaf eucommia ulmoides extracts compound tea that the present invention relates to comprises following technique: pretreatment before plucking, the preparation of Shanlu Tea extract for dropping, the preparation of eucommia ulmoides extracts and hybrid packed.
(1) pretreatment before plucking:
S
1) growing the root 20cm place that the age is 3 years hainan holly leaf trees, digging the hole of long 10 ~ 15 ㎝, wide 10 ~ 15 ㎝, dark 10 ~ 15 ㎝, hainan holly leaf raw material being prepared fertilizer and is applied in hole, every strain consumption 120 ~ 150 grams, cover table soil, carried out once every 15 ~ 20 days, carry out 2 times continuously;
S
2) extraction of hainan holly leaf raw material is obtained extract dilution 180 ~ 200 times, with tree root, trunk, the leaf sprinkling hainan holly leaf extract of high-pressure sprayer to hainan holly leaf, carried out once every 15 ~ 20 days, carry out 2 times continuously, pluck after spraying latter 15 days;
(2) preparation of Shanlu Tea extract for dropping:
S
a) first by clean by 40 ~ 50 DEG C of hot water wash to hainan holly leaf tender leaf, the tender shoots of plucking, soak 10 ~ 15 minutes with 10% sodium chloride solution of 70 ~ 80 DEG C and then, then pull out after draining away the water, put into the drying baker of 60 ~ 80 DEG C, dry 50 ~ 60 minutes, be finally cooled to room temperature, be ground into powder, and cross 40 ~ 60 mesh sieves, obtain hainan holly leaf particle;
S
b) will be saccharomycete by weight ratio: lactic acid bacteria: acetic acid bacteria=(15 ~ 20): (25 ~ 35): the mixed bacteria stoste access step (S that (10 ~ 15) form
a) in hainan holly leaf particle, and 30 ~ 40 DEG C fermentation 160 ~ 180 hours, wherein, the weight ratio that mixed bacteria stoste accounts for hainan holly leaf particle is 1 ~ 3%;
S
c) hainan holly leaf after fermentation process is carried out drying and processing, first in the baking oven of 90 ~ 110 DEG C, dry 20 ~ 30 minutes, then regulate bake out temperature to be 60 ~ 80 DEG C, dry 60 ~ 70 minutes;
S
d) by step (S
c) in hainan holly leaf be 40 ~ 60kHz in supersonic frequency, extract twice at 40 ~ 50 DEG C, the distilled water that first time adds 7 times of weight, extracts 10 ~ 15 minutes, and second time adds the distilled water of 3 times of weight, extract 7 ~ 9 minutes, filter, merging filtrate, on centrifuge filtrate being placed in 4000 ~ 5000 turns centrifugal 10 ~ 15 minutes, again filter, concentrated, dry, obtain Shanlu Tea extract for dropping powder;
(3) preparation of eucommia ulmoides extracts:
The preparation of eucommia ulmoides extracts adopts above-mentioned method preparation, namely repeats step (1), (2) prepare eucommia ulmoides extracts powder;
(4) hybrid packed:
By Shanlu Tea extract for dropping powder and eucommia ulmoides extracts powder respectively spray-dried, pulverize and cross 400 ~ 500 mesh sieves; Then fully mix for 50%:50% by mass percentage, hainan holly leaf eucommia ulmoides extracts compound tea can be obtained.
It is be made up of each component of following weight that described hainan holly leaf raw material prepares fertilizer: 40 ~ 50 parts, hainan holly leaf waste material, hainan holly leaf extract 7 ~ 9 parts, rice straw 10 ~ 15 parts, powdered rice hulls 3 ~ 5 parts, chicken manure 15 ~ 20 parts, 0.4 ~ 0.8 part, chicken feather, cow dung 2 ~ 4 parts, 4 ~ 8 parts, weeds.
Preferably,
It is be made up of each component of following weight that described hainan holly leaf raw material prepares fertilizer: 45 parts, hainan holly leaf waste material, hainan holly leaf extract 8 parts, rice straw 12 parts, powdered rice hulls 4 parts, chicken manure 18 parts, 0.6 part, chicken feather, cow dung 3 parts, 6 parts, weeds.
Leftover bits and pieces after described hainan holly leaf waste material comprises non-compliant raw material in hainan holly leaf process, processing or hainan holly leaf extract a kind of in residue and/or more than one mixture.
Described hainan holly leaf raw material extracts and obtains extract, refer to and take standard compliant hainan holly leaf, boiling twice, add the distilled water of 8 times of weight for the first time, decoct 80 ~ 90 minutes in 110 DEG C, second time adds the distilled water of 6 times of weight, decoct 50 ~ 60 minutes in 120 DEG C, filter, merging filtrate, the hainan holly leaf extract obtained.
Adopt the preparation method identical with hainan holly leaf to prepare bark of eucommia raw material to prepare fertilizer and bark of eucommia raw material and extract and obtain extract.
Compared with prior art, tool of the present invention has the following advantages:
1, in hainan holly leaf, the bark of eucommia containing various active composition, just because of making compound tea containing these active components, there is heat-clearing, the effect such as hypotensive.The present invention prepares fertilizer and hainan holly leaf (bark of eucommia) raw material and extracts by applying hainan holly leaf (bark of eucommia) raw material to hainan holly leaf (bark of eucommia) before plucking and obtain extract, and in fertilizer, extract, include abundant hainan holly leaf (bark of eucommia) active component, active component not only slowly penetrates into blade from hainan holly leaf (bark of eucommia) leaf top layer, and slowly absorb blade from root, add the content of the active component of hainan holly leaf (bark of eucommia) leaf.
2, the leftover bits and pieces after the present invention takes full advantage of non-compliant raw material in hainan holly leaf (bark of eucommia) process, processing or hainan holly leaf (bark of eucommia) extract residue, and by hainan holly leaf (bark of eucommia) raw material is prepared fertilizer, extract obtain extract, be applied to the tree root of hainan holly leaf (bark of eucommia) before plucking, trunk and leaf, make it turn waste into wealth, reduce production cost, increase economic benefit.
3, adopt 10% sodium chloride solution to soak, form concentration difference with hainan holly leaf (bark of eucommia) blade, add cell membrane penetration, facilitate oxidizing ferment release, improve compound tea quality and effect; Also adopt fermented by mixed bacterium technology to produce compound tea simultaneously, not only overcome the defect of single culture, but also mouthfeel and effect of compound tea can be improved, thus make the range of application of compound tea more extensive, improve the market competitiveness.
Detailed description of the invention
Embodiment 1
A preparation method for hainan holly leaf eucommia ulmoides extracts compound tea, comprises the following steps:
(1) pretreatment before plucking:
S
1) growing the root 20cm place that the age is 3 years hainan holly leaf trees, digging the hole of long 10 ~ 15 ㎝, wide 10 ~ 15 ㎝, dark 10 ~ 15 ㎝, hainan holly leaf raw material being prepared fertilizer and is applied in hole, every strain consumption 140 grams, cover table soil, carried out once every 18 days, carry out 2 times continuously;
It is be made up of each component of following weight that described hainan holly leaf raw material prepares fertilizer: 45 parts, hainan holly leaf waste material, hainan holly leaf extract 8 parts, rice straw 12 parts, powdered rice hulls 4 parts, chicken manure 18 parts, 0.6 part, chicken feather, cow dung 3 parts, 6 parts, weeds;
Described hainan holly leaf waste material is non-compliant raw material in hainan holly leaf process;
Described hainan holly leaf raw material extracts and obtains extract, refer to and take standard compliant hainan holly leaf, boiling twice, add the distilled water of 8 times of weight for the first time, decoct 85 minutes in 110 DEG C, second time adds the distilled water of 6 times of weight, decoct 55 minutes in 120 DEG C, filter, merging filtrate, the hainan holly leaf extract obtained;
S
2) hainan holly leaf raw material extracted obtain extract and dilute 190 times, spray hainan holly leaf extract with high-pressure sprayer to the tree root of hainan holly leaf, trunk, leaf, carried out once every 18 days, carry out 2 times continuously, pluck after spraying latter 15 days;
(2) preparation of Shanlu Tea extract for dropping:
S
a) first by clean by 45 DEG C of hot water wash to hainan holly leaf tender leaf, the tender shoots of plucking, 12 minutes are soaked and then with 10% sodium chloride solution of 75 DEG C, then pull out after draining away the water, put into the drying baker of 70 DEG C, dry 55 minutes, be finally cooled to room temperature, be ground into powder, and cross 60 mesh sieves, obtain hainan holly leaf particle;
S
b) will be saccharomycete by weight ratio: lactic acid bacteria: the mixed bacteria stoste access step (S that acetic acid bacteria=17:30:12 forms
a) in hainan holly leaf particle, and 35 DEG C fermentation 170 hours, wherein, the weight ratio that mixed bacteria stoste accounts for hainan holly leaf particle is 2%;
S
c) hainan holly leaf after fermentation process is carried out drying and processing, first in the baking oven of 100 DEG C, dry 25 minutes, then regulate bake out temperature to be 70 DEG C, dry 65 minutes;
S
d) by step (S
c) in hainan holly leaf be 50kHz in supersonic frequency, extract twice at 45 DEG C, the distilled water that first time adds 7 times of weight, extracts 12 minutes, and second time adds the distilled water of 3 times of weight, extract 8 minutes, filter, merging filtrate, on centrifuge filtrate being placed in 4500 turns centrifugal 12 minutes, again filter, concentrated, dry, obtain Shanlu Tea extract for dropping powder;
(3) preparation of eucommia ulmoides extracts:
The preparation of eucommia ulmoides extracts adopts above-mentioned method preparation, namely repeats step (1), (2) prepare eucommia ulmoides extracts powder;
(4) hybrid packed:
By Shanlu Tea extract for dropping powder and eucommia ulmoides extracts powder respectively spray-dried, pulverize and cross 500 mesh sieves; Then fully mix for 50%:50% by mass percentage, hainan holly leaf eucommia ulmoides extracts compound tea can be obtained.
In hainan holly leaf eucommia ulmoides extracts compound tea, the mensuration of flavones content adopts HPLC method to detect, and after testing, flavones content is 36.46%.
Embodiment 2
A preparation method for hainan holly leaf eucommia ulmoides extracts compound tea, comprises the following steps:
(1) pretreatment before plucking:
S
1) growing the root 20cm place that the age is 3 years hainan holly leaf trees, digging the hole of long 10 ~ 15 ㎝, wide 10 ~ 15 ㎝, dark 10 ~ 15 ㎝, hainan holly leaf raw material being prepared fertilizer and is applied in hole, every strain consumption 120 grams, cover table soil, carried out once every 15 days, carry out 2 times continuously;
It is be made up of each component of following weight that described hainan holly leaf raw material prepares fertilizer: 40 parts, hainan holly leaf waste material, hainan holly leaf extract 7 parts, rice straw 10 parts, powdered rice hulls 3 parts, chicken manure 15 parts, 0.4 part, chicken feather, cow dung 2 parts, 4 parts, weeds;
Described hainan holly leaf waste material is the leftover bits and pieces after processing;
Described hainan holly leaf raw material extracts and obtains extract, refer to and take standard compliant hainan holly leaf, boiling twice, add the distilled water of 8 times of weight for the first time, decoct 80 minutes in 110 DEG C, second time adds the distilled water of 6 times of weight, decoct 50 minutes in 120 DEG C, filter, merging filtrate, the hainan holly leaf extract obtained;
S
2) hainan holly leaf raw material extracted obtain extract and dilute 180 times, spray hainan holly leaf extract with high-pressure sprayer to the tree root of hainan holly leaf, trunk, leaf, carried out once every 15 days, carry out 2 times continuously, pluck after spraying latter 15 days;
(2) preparation of Shanlu Tea extract for dropping:
S
a) first by clean by 40 DEG C of hot water wash to hainan holly leaf tender leaf, the tender shoots of plucking, 10 minutes are soaked and then with 10% sodium chloride solution of 70 DEG C, then pull out after draining away the water, put into the drying baker of 60 DEG C, dry 50 minutes, be finally cooled to room temperature, be ground into powder, and cross 40 mesh sieves, obtain hainan holly leaf particle;
S
b) will be saccharomycete by weight ratio: lactic acid bacteria: the mixed bacteria stoste access step (S that acetic acid bacteria=15:25:10 forms
a) in hainan holly leaf particle, and 30 DEG C fermentation 160 hours, wherein, the weight ratio that mixed bacteria stoste accounts for hainan holly leaf particle is 1%;
S
c) hainan holly leaf after fermentation process is carried out drying and processing, first in the baking oven of 90 DEG C, dry 20 minutes, then regulate bake out temperature to be 60 DEG C, dry 60 minutes;
S
d) by step (S
c) in hainan holly leaf be 40kHz in supersonic frequency, extract twice at 40 DEG C, the distilled water that first time adds 7 times of weight, extracts 10 minutes, and second time adds the distilled water of 3 times of weight, extract 7 minutes, filter, merging filtrate, on centrifuge filtrate being placed in 4000 turns centrifugal 10 minutes, again filter, concentrated, dry, obtain Shanlu Tea extract for dropping powder;
(3) preparation of eucommia ulmoides extracts:
The preparation of eucommia ulmoides extracts adopts above-mentioned method preparation, namely repeats step (1), (2) prepare eucommia ulmoides extracts powder;
(4) hybrid packed:
By Shanlu Tea extract for dropping powder and eucommia ulmoides extracts powder respectively spray-dried, pulverize and cross 400 mesh sieves; Then fully mix for 50%:50% by mass percentage, hainan holly leaf eucommia ulmoides extracts compound tea can be obtained.
In hainan holly leaf eucommia ulmoides extracts compound tea, the mensuration of flavones content adopts HPLC method to detect, and after testing, flavones content is 35.45%.
Embodiment 3
A preparation method for hainan holly leaf eucommia ulmoides extracts compound tea, comprises the following steps:
(1) pretreatment before plucking:
S
1) growing the root 20cm place that the age is 3 years hainan holly leaf trees, digging the hole of long 10 ~ 15 ㎝, wide 10 ~ 15 ㎝, dark 10 ~ 15 ㎝, hainan holly leaf raw material being prepared fertilizer and is applied in hole, every strain consumption 150 grams, cover table soil, carried out once every 20 days, carry out 2 times continuously;
It is be made up of each component of following weight that described hainan holly leaf raw material prepares fertilizer: 50 parts, hainan holly leaf waste material, hainan holly leaf extract 9 parts, rice straw 15 parts, powdered rice hulls 5 parts, chicken manure 20 parts, 0.8 part, chicken feather, cow dung 4 parts, 8 parts, weeds;
Described hainan holly leaf waste material is that hainan holly leaf extracts residue;
Described hainan holly leaf raw material extracts and obtains extract, refer to and take standard compliant hainan holly leaf, boiling twice, add the distilled water of 8 times of weight for the first time, decoct 90 minutes in 110 DEG C, second time adds the distilled water of 6 times of weight, decoct 60 minutes in 120 DEG C, filter, merging filtrate, the hainan holly leaf extract obtained;
S
2) hainan holly leaf raw material extracted obtain extract and dilute 200 times, spray hainan holly leaf extract with high-pressure sprayer to the tree root of hainan holly leaf, trunk, leaf, carried out once every 20 days, carry out 2 times continuously, pluck after spraying latter 15 days;
(2) preparation of Shanlu Tea extract for dropping:
S
a) first by clean by 50 DEG C of hot water wash to hainan holly leaf tender leaf, the tender shoots of plucking, 15 minutes are soaked and then with 10% sodium chloride solution of 80 DEG C, then pull out after draining away the water, put into the drying baker of 80 DEG C, dry 60 minutes, be finally cooled to room temperature, be ground into powder, and cross 60 mesh sieves, obtain hainan holly leaf particle;
S
b) will be saccharomycete by weight ratio: lactic acid bacteria: the mixed bacteria stoste access step (S that acetic acid bacteria=20:35:15 forms
a) in hainan holly leaf particle, and 40 DEG C fermentation 180 hours, wherein, the weight ratio that mixed bacteria stoste accounts for hainan holly leaf particle is 3%;
S
c) hainan holly leaf after fermentation process is carried out drying and processing, first in the baking oven of 110 DEG C, dry 30 minutes, then regulate bake out temperature to be 80 DEG C, dry 70 minutes;
S
d) by step (S
c) in hainan holly leaf be 60kHz in supersonic frequency, extract twice at 50 DEG C, the distilled water that first time adds 7 times of weight, extracts 15 minutes, and second time adds the distilled water of 3 times of weight, extract 9 minutes, filter, merging filtrate, on centrifuge filtrate being placed in 5000 turns centrifugal 15 minutes, again filter, concentrated, dry, obtain Shanlu Tea extract for dropping powder;
(3) preparation of eucommia ulmoides extracts:
The preparation of eucommia ulmoides extracts adopts above-mentioned method preparation, namely repeats step (1), (2) prepare eucommia ulmoides extracts powder;
(4) hybrid packed:
By Shanlu Tea extract for dropping powder and eucommia ulmoides extracts powder respectively spray-dried, pulverize and cross 500 mesh sieves; Then fully mix for 50%:50% by mass percentage, hainan holly leaf eucommia ulmoides extracts compound tea can be obtained.
In hainan holly leaf eucommia ulmoides extracts compound tea, the mensuration of flavones content adopts HPLC method to detect, and after testing, flavones content is 35.87%.
The applicant is to the compound tea research experiment of the embodiment of the present invention 1 ~ 3, and concrete test method is as follows:
1, by body weight 15 ~ 20g and clinical symptoms are the mouse 120 of cold cough, heating (body temperature 38 ~ 39 DEG C), be divided into A group, B group and C group at random, often organize 40;
2, A group is taken compound tea, B group prepared by embodiment 1 and is taken compound tea prepared by embodiment 2 and C group and take compound tea prepared by embodiment 3;
3, instructions of taking: a day three times, each 10mg, takes 7 days;
4, temperature taking is carried out to the mouse taken 7 days, and record data.
Find after tested, mouse temperature has 26 lower than 38 DEG C: A group; B group has 23; C group has 25.If with mouse temperature lower than 38 DEG C for standard, then efficient 57.5%, the C group efficient 62.5% of efficient 65.0%, the B group of A group.As can be seen here, compound tea of the present invention is adopted to have heat-clearing effect.
In addition, the applicant also studies as follows to the compound tea of the embodiment of the present invention 1:
1, by body weight 15 ~ 20g and clinical symptoms are the mouse 120 of hypertension (systolic pressure 130 ~ 140mmHg), be divided into A group, B group and C group at random, often organize 40;
2, A group take embodiment 1 prepare compound tea, B group takes Shanlu Tea extract for dropping tea and C group takes eucommia ulmoides extracts tea;
3, instructions of taking: a day three times, each 10mg, takes 30 days;
4, blood pressure test is carried out to the mouse taken 30 days, and record data.
Find after tested, Mouse Blood forces down has 32 in 125mmHg:A group; B group has 26; C group has 29.If force down in 125mmHg for standard with Mouse Blood, then efficient 65.0%, the C group efficient 72.5% of efficient 80.0%, the B group of A group.As can be seen here, compound tea of the present invention is adopted to have blood pressure reduction effect.
Certainly, just the preferred embodiments of the disclosure is described in detail above, not limits practical range of the present invention with this, and all equivalence changes done according to principle of the present invention, structure and structure, all should be covered by protection scope of the present invention.
Claims (3)
1. a preparation method for hainan holly leaf eucommia ulmoides extracts compound tea, is characterized in that: comprise the following steps:
(1) pretreatment before plucking:
S
1) growing the root 20cm place that the age is 3 years hainan holly leaf trees, digging the hole of long 10 ~ 15 ㎝, wide 10 ~ 15 ㎝, dark 10 ~ 15 ㎝, hainan holly leaf raw material being prepared fertilizer and is applied in hole, every strain consumption 120 ~ 150 grams, cover table soil, carried out once every 15 ~ 20 days, carry out 2 times continuously;
S
2) extraction of hainan holly leaf raw material is obtained extract dilution 180 ~ 200 times, with tree root, trunk, the leaf sprinkling hainan holly leaf extract of high-pressure sprayer to hainan holly leaf, carried out once every 15 ~ 20 days, carry out 2 times continuously, pluck after spraying latter 15 days;
(2) preparation of Shanlu Tea extract for dropping:
S
a) first by clean by 40 ~ 50 DEG C of hot water wash to hainan holly leaf tender leaf, the tender shoots of plucking, soak 10 ~ 15 minutes with 10% sodium chloride solution of 70 ~ 80 DEG C and then, then pull out after draining away the water, put into the drying baker of 60 ~ 80 DEG C, dry 50 ~ 60 minutes, be finally cooled to room temperature, be ground into powder, and cross 40 ~ 60 mesh sieves, obtain hainan holly leaf particle;
S
b) will be saccharomycete by weight ratio: lactic acid bacteria: acetic acid bacteria=(15 ~ 20): (25 ~ 35): the mixed bacteria stoste access step (S that (10 ~ 15) form
a) in hainan holly leaf particle, and 30 ~ 40 DEG C fermentation 160 ~ 180 hours, wherein, the weight ratio that mixed bacteria stoste accounts for hainan holly leaf particle is 1 ~ 3%;
S
c) hainan holly leaf after fermentation process is carried out drying and processing, first in the baking oven of 90 ~ 110 DEG C, dry 20 ~ 30 minutes, then regulate bake out temperature to be 60 ~ 80 DEG C, dry 60 ~ 70 minutes;
S
d) by step (S
c) in hainan holly leaf be 40 ~ 60kHz in supersonic frequency, extract twice at 40 ~ 50 DEG C, the distilled water that first time adds 7 times of weight, extracts 10 ~ 15 minutes, and second time adds the distilled water of 3 times of weight, extract 7 ~ 9 minutes, filter, merging filtrate, on centrifuge filtrate being placed in 4000 ~ 5000 turns centrifugal 10 ~ 15 minutes, again filter, concentrated, dry, obtain Shanlu Tea extract for dropping powder;
(3) preparation of eucommia ulmoides extracts:
The preparation of eucommia ulmoides extracts adopts above-mentioned method preparation, namely repeats step (1), (2) prepare eucommia ulmoides extracts powder;
(4) hybrid packed:
By Shanlu Tea extract for dropping powder and eucommia ulmoides extracts powder respectively spray-dried, pulverize and cross 400 ~ 500 mesh sieves; Then fully mix for 50%:50% by mass percentage, hainan holly leaf eucommia ulmoides extracts compound tea can be obtained.
2. the preparation method of hainan holly leaf eucommia ulmoides extracts compound tea according to claim 1, is characterized in that: it is be made up of each component of following weight that described hainan holly leaf raw material prepares fertilizer: 40 ~ 50 parts, hainan holly leaf waste material, hainan holly leaf extract 7 ~ 9 parts, rice straw 10 ~ 15 parts, powdered rice hulls 3 ~ 5 parts, chicken manure 15 ~ 20 parts, 0.4 ~ 0.8 part, chicken feather, cow dung 2 ~ 4 parts, 4 ~ 8 parts, weeds.
3. the preparation method of hainan holly leaf eucommia ulmoides extracts compound tea according to claim 1, it is characterized in that: described hainan holly leaf raw material extracts and obtains extract, refer to and take hainan holly leaf, boiling twice, add the distilled water of 8 times of weight for the first time, decoct 80 ~ 90 minutes in 110 DEG C, second time adds the distilled water of 6 times of weight, decocts 50 ~ 60 minutes in 120 DEG C, filters, merging filtrate, the hainan holly leaf extract obtained.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106538768A (en) * | 2016-10-29 | 2017-03-29 | 张家界甑山野岩茶业有限公司 | Bark of eucommia prophyll is combined brick tea and preparation method thereof with vine tea |
| CN110522883A (en) * | 2019-08-12 | 2019-12-03 | 山东佳硒雅生物有限公司 | One kind controlling tinea pedis selenium-rich Chinese medicine composition and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106538768A (en) * | 2016-10-29 | 2017-03-29 | 张家界甑山野岩茶业有限公司 | Bark of eucommia prophyll is combined brick tea and preparation method thereof with vine tea |
| CN110522883A (en) * | 2019-08-12 | 2019-12-03 | 山东佳硒雅生物有限公司 | One kind controlling tinea pedis selenium-rich Chinese medicine composition and preparation method thereof |
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