CN105476886B - A kind of after-sun composition and preparation method thereof - Google Patents
A kind of after-sun composition and preparation method thereof Download PDFInfo
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- CN105476886B CN105476886B CN201510868359.5A CN201510868359A CN105476886B CN 105476886 B CN105476886 B CN 105476886B CN 201510868359 A CN201510868359 A CN 201510868359A CN 105476886 B CN105476886 B CN 105476886B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/004—Aftersun preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
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- General Health & Medical Sciences (AREA)
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Abstract
The invention discloses a kind of after-sun compositions and preparation method thereof, the composition contains water-soluble eggshell membrane polypeptide 0.01-0.20%, Alps glacial water 0.50-4.00%, tocopherol acetate 0.50-2.00%, menthyl lactate 0.10-0.25%, beta glucan 1.00-4.00%, the compounding that after-sun component of the present invention passes through above several components, it suits the remedy to the case, repairs comprehensively by the impaired cell of ultraviolet light irradiation for the various problems of skin after solarization.It is glossy like wrapping one layer of very thin egg film to skin fragile after solarization, protecting impaired skin and it being made to restore water profit again by the compounding of several ingredients.Product of the present invention will not generate user allergic reaction, safe to use；Product of the present invention the after-sun the effect of on have remarkable result.
Description
【Technical field】
The present invention relates to a kind of after-sun compositions and preparation method thereof, belong to Cosmetic Manufacture technical field.
【Background technology】
Summer is scorching, even if can not avoid the injury of sunlight, burning blazing sun if carrying out strict sun-proof work completely
Always deep or shallow trace is left on the human skin.After skin is by ultraviolet irradiation, a large amount of oxonium ion will produce
Free radical leads to a series of photochemical reaction, causes skin water shortage, generates erythema, and barrier function is also damaged, and skin becomes
It obtains more sensitive.Fortunately, after being irradiated by ultraviolet light, it just must can send out celliferous change by the incubation period of 6-8h and occur
Symptom, 6-8h is also referred to as the gold after shining and repairs the phase after solarization, if can give the skin correctly side of maintenance within the gold reparation phase
Formula, in time eliminate skin in free radical simultaneously skin moisture is replenished in time, erythema index can be greatly reduced, avoid skin because
Solarization exsiccation blackening even aging.
Existing after-sun restorative product is most of only to focus on the moisturizing of skin, and has ignored and disappear to oxonium ion free radical
It removes, the reparation of skin after shining cannot be really achieved.And some products are biased to skin-whitening after shining, and add white-skinned face function in the product
Ingredient, and these functional components are easy to cause stimulation even allergy to sensitive skin after solarization, after could not only reaching solarization
The reparation of skin, in some instances it may even be possible to cause the further damage of skin.Lack one kind in the market and is carried out entirely for skin is damaged after shining
The skin care item that face is repaired.
【Invention content】
The purpose of the invention is to overcome the deficiencies in the prior art to provide one kind for the various situations of skin after solarization
More comprehensively, after-sun composition quickly, effective and safe.
The present invention to achieve the goals above, using following technical scheme：
A kind of after-sun composition, it is characterised in that the after-sun component A phases containing following weight percent：
The weight percent of the above components is using entire after-sun composition system total amount as radix.
Water-soluble eggshell membrane polypeptide：With magical repairing regenerating ability.Egg film, 0.07 millimeter of thin film, but can
21 days 1 cells of care meticulously of the divinity vouchsafed with the Nature become 10,000,000,000, and be finally born a fresh and alive life.Mainly
Ingredient is protein, close to the skin of the mankind and the ingredient of hair, is made of 18 kinds of amino acid.Because containing angle egg in egg shell membrane
In vain, the rigid albumen such as collagen is fibrous structure, not soluble in water, not by general protease hydrolyzed, it is difficult to straight by human body
Connect absorption.These insoluble macromolecular scleroproteins could be absorbed profit after being only hydrolyzed into small-molecule peptide and amino acid
With meeting the needs of each histoorgan, improve effective rate of utilization of the human body to nutriment.Egg shell membrane is hydrolyzed with special process
At micromolecule polypeptide, that is, eggshell membrane polypeptide of 8000 dalton or so.Eggshell membrane polypeptide is more by tropoelastin, desmosine, amino
Four kinds of sugar, transforming growth factor-β active constituent compositions, wherein tropoelastin, which has, maintains tissue, skin and blood vessel elasticity
Effect, desmosine is able to maintain that skin and blood vessel elasticity, glycosaminoglycan can promote cell repair to maintain tissue health, converts, raw
The long factor-β can promote cell proliferation and differentiation.By the collective effect of above several active constituents, for the cell note being damaged after solarization
Enter energy, assign the unlimited vigor of cell, the metabolism of skin, enhancing cycle is promoted to achieve the purpose that reparative regeneration.
Water-soluble eggshell membrane polypeptide in the present invention, accounts for 0.01-0.15% in total composition；It is water-soluble in the present invention
Property eggshell membrane polypeptide, accounts for 0.01-0.10% in total composition；Water-soluble eggshell membrane polypeptide in the present invention, in composition
0.01-0.05% is accounted in total amount；Water-soluble eggshell membrane polypeptide in the present invention, accounts for 0.05-0.20% in total composition；This
Water-soluble eggshell membrane polypeptide in invention, accounts for 0.10-0.20% in total composition, and the water-soluble eggshell membrane in the present invention is more
Peptide accounts for 0.15-0.20% in total composition.
Alps glacial water：It being capable of effective moisturizing.Alps is the maximum mountainous villas center in Europe.Often
One drop glacial water breeds hundreds of millions of years on stratum, undergoes Minerals And Rocks filtering in more than 50 years, continuous with fixed flow velocity and steady temperature
Gush out, mineral content ratio is very suitable for human body requirements, is the water that a suitable skin is drunk；It is numerous to human metabolism, cell
Spreading out, there play the role of to be positive, can open skin water circulation channel, and microelement-supplementing allows skin enjoying the same of pure pure and fresh environment
When, it carries back and obtains water replenishment by skin.
Tocopherol acetate：Free radical can strongly be removed.After skin is by ultraviolet irradiation, a large amount of oxygen will produce
Ion radical, excessive active oxygen radical just have destruction, lead to the damage of human normal cell and tissue, to
Cause a variety of diseases.As natural antioxidant with oxygen radical redox reaction can occur for tocopherol acetate, make
Oxygen radical is thoroughly removed.
Beta glucan, the immune function of repair cell.The Active Defending System Against of skin is with langerhans cells (abbreviation Lang Shi
Cell, langerhans cell are a kind of jejune dendron shapes, and Bai Beike is referred to as containing a large amount of columns or racket shape in endochylema
The particle of grain.When one piece of skin is infected, local langerhans cell will identify, capture and handle microbial antigen, then move
The T lymphocytes region of the cortex of draining lymph node is moved on to, and ripe as professional antigen presenting cells.If langerhans cell by
Damage, will influence the normal immunocompetence of skin.) based on the close reticular structure that is formed, once the antigen cell of intrusion, touches
Langerhans cell will be swallowed and partial digested by it.Simultaneously langerhans cell can also activating immune system, to by antigen it is thoroughly clear
It removes.Due to the irradiation of UVB, the network that langerhans cell is formed starts to start a leak, this so that antigen is able to penetrate skin, and skin
The ability for removing antigen is but damaged, and existing collagen, elastin laminin, proteoglycans is caused constantly to be destroyed.Make
Macrophage as langerhans cell can be activated with beta glucan, to enhance function of the human immune system.What is be activated is bright
Schwann Cells can secrete some factors, promote fibroblastic proliferation and skin histology mechanism (such as collagen, elastin laminin,
Proteoglycans and other components) synthesis, so that skin elasticity is increased, it is soft delicate.
Beta glucan in the present invention, accounts for 1.0-4.0% in total composition；Beta glucan in the present invention, in group
It closes in object total amount and accounts for 1.5-4.0%；Beta glucan in the present invention, accounts for 2.0-4.0% in total composition；In the present invention
Beta glucan accounts for 2.5-4.0% in total composition；Beta glucan in the present invention, accounts for 3.0- in total composition
4.0%；Beta glucan in the present invention, accounts for 3.5-4.0% in total composition；Beta glucan in the present invention is combining
0.5-3.5% is accounted in object total amount；Beta glucan in the present invention, accounts for 0.5-3.0% in total composition；β-in the present invention
Glucan accounts for 0.5-2.5% in total composition；Beta glucan in the present invention, accounts for 0.5- in total composition
2.0%；Beta glucan in the present invention, accounts for 0.5-1.5% in total composition；Beta glucan in the present invention is combining
0.5-1.0% is accounted in object total amount；Beta glucan in the present invention, accounts for 1.0-3.5% in total composition；β-in the present invention
Glucan accounts for 1.5-3.0% in total composition；Beta glucan in the present invention, accounts for 2.0- in total composition
3.5%.
Coolant of the menthyl lactate as skin, unique permanent cooling effect, can reduce solarization skin surface
Temperature 3-6 degree, effectively calmness skin, alleviate scorching erythralgia phenomenon at once.
After-sun component of the present invention by the compoundings of above several components, for skin after solarization various problems suit the medicine to the illness under
Medicine is repaired comprehensively by the impaired cell of ultraviolet light irradiation.Menthyl lactate can effective Lavender Extract, alleviate erythralgia at once；A Er
This inferior glacial water effectively lost moisture of supplement, opens skin water circulation channel；Tocopherol acetate strength removes free radical, prevents
Only skin light aging；Beta glucan can activate langerhans cell, to enhance function of the human immune system, promote fibroblast
Proliferation and skin histology mechanism (such as collagen, elastin laminin, proteoglycans and other components) synthesis, make skin again
Restore elasticity；Eggshell membrane polypeptide can be the cell Implantation Energy being damaged after shining, and so that Skin Cell is refilled vigor, get well
Gloss.It protects like wrapping one layer of very thin egg film to skin fragile after solarization by the compounding of several ingredients and is damaged skin simultaneously
It is set to restore water profit again glossy.
After-sun composition of the present invention further includes oil phase component 9.5-20%, adjuvant component 0.5%, triethanolamine adjusting
PH value to 5.0-7.0, water phase components surplus contains glycerine 6.0-8.0% wherein in water phase components.
Since tocopherol acetate is oil-soluble in the composition, therefore the composition is suitable for emulsification system, and uncomfortable
For transparent pure water agent system.Need to be added glycerine in formula for the breast in dispersing and dissolving after-sun composition of the present invention
Sour menthyl ester.
The weight percent of the above components is using entire after-sun composition system total amount as radix.
The preparation method of after-sun combination of the present invention, it is characterised in that include the following steps：
A, by after-sun component tocopherol acetate and oil phase component mix and be warming up to 80 DEG C, stirring and dissolving is complete
Entirely；
B, glycerine 2.00% is reserved, water phase remaining component mixing is warming up to 85 DEG C, keeps the temperature 20min, stirring and dissolving is complete；
C, water phase is first pumped into emulsification pot, then is pumped into oil phase, homogeneous 5min, insulated and stirred 5min vacuumize drop under stirring
Temperature is added triethanolamine and adjusts pH value, continue to cool down to 60 DEG C；
D, the menthyl lactate in after-sun component is mixed with the step b glycerine reserved, being heated to 45 DEG C keeps its molten
Solution is added when emulsifying the when of expecting that body is cooled to 45 DEG C in pot, stirs evenly；
E, adjuvant component and the beta glucan in after-sun component, Alps glacier is added when material body is cooled to 40 DEG C
Water, eggshell membrane polypeptide, stir evenly, you can.
Compared with prior art, the present invention having the advantage that：
The eggshell membrane polypeptide used in the present invention can be the cell Implantation Energy being damaged after shining, and assign the unlimited vigor of cell,
The metabolism of skin, enhancing cycle is promoted to have the function that reparative regeneration；Alps glacial water derives from natural ice
Chuan Shui can open skin water circulation channel, and microelement-supplementing allows skin while enjoying pure pure and fresh environment, and in advance one
Step allows skin to obtain water replenishment；As natural antioxidant with oxygen radical redox can occur for tocopherol acetate
Reaction, makes oxygen radical be thoroughly removed.Beta glucan can activate macrophage as langerhans cell, exempt to enhance human body
The function of epidemic disease system, the langerhans cell being activated can secrete some factors, promote fibroblastic proliferation and skin histology machine
The synthesis for making (such as collagen, elastin laminin, proteoglycans and other components), makes skin elasticity increase, soft delicate；Lactic acid
Menthyl ester can effective Lavender Extract, reduce skin surface temperature, alleviate scorching erythralgia phenomenon, pass through above several functional components
Compounding, reaches comprehensively and effectively after-sun.
Product of the present invention will not generate user allergic reaction, safe to use；Work(of the product of the present invention in after-sun
There is remarkable result in effect.
【Specific implementation mode】
A kind of after-sun composition, the after-sun component (A phases) containing following weight percent：
Also contain oil phase component (B phases) 9.5-20%, water phase components (C phases), triethanolamine (D phases), adjuvant component (E phases)
0.5%, adjuvant component is the mixture of essence and preservative.
The weight percent of the above components is using entire after-sun composition system total amount as radix, wherein in water phase
Water be surplus.
The present invention is further explained in the light of specific embodiments, and the percentage in following embodiment is weight
Percentage：
Embodiment 1：
A phases, after-sun component
B phases, oil phase components
C, water phase component
D, triethanolamine 0.45%
E, auxiliary agent component 0.5%.
The preparation method of embodiment 1 is：
A, by A phases tocopherol acetate and B mix and be warming up to 80 DEG C, stirring and dissolving is complete；
B, the glycerine 2.00% in C phases is reserved, remaining component mixing of C phases is warming up to 85 DEG C, keeps the temperature 20min, stirring is molten
Solution is complete；
C, C phases are first pumped into emulsification pot, then are pumped into B phases, homogeneous 5min, insulated and stirred 5min vacuumize cooling under stirring
To 60 DEG C, D phases are added and adjust pH value, continue to cool down；
D, the menthyl lactate in A phases is mixed with the step b glycerine reserved, is heated to 45 DEG C and makes it dissolve, works as emulsification
It is added, stirs evenly when material body is cooled to 45 DEG C in pot；
E, 40 DEG C when E phases and beta glucan, Alps glacial water, eggshell membrane polypeptide in A phases is added, stir evenly,
?.
Embodiment 2：
A phases, after-sun component
B phases, oil phase components
C, water phase component
D, triethanolamine 0.5%
E, auxiliary agent component 0.5%.
Embodiment 3：
A phases, after-sun component
B phases, oil phase components
C, water phase component
D, triethanolamine 0.20%
E, auxiliary agent component 0.5%.
Embodiment 4：
A phases, after-sun component
B phases, oil phase components
C, water phase component
D, triethanolamine 0.45%；
E, auxiliary agent component 0.5%.
Embodiment 5：
A phases, after-sun component
B phases, oil phase components
C, water phase component
D, triethanolamine 0.5%；
E, auxiliary agent component 0.5%.
Embodiment 6：
A phases, after-sun component
B phases, oil phase components
C, water phase component
D, triethanolamine 0.2%；
E, auxiliary agent component 0.5%.
That the preparation method is the same as that of Example 1 is identical by embodiment 2-6.
Some testing performance indexes are done to the after-sun composition of embodiment 1-6, test result is as follows：
1. appearance：Fine and smooth cream
2.pH values：5.0-7.0
3. viscosity：100000-150000 mpa.s
4. heat-resistant stability investigates (48 DEG C × 24H)：It is qualified
5. cold-resistant study on the stability (- 15 DEG C × 24H)：It is qualified.
In order to prove the performance of product of the present invention, experiment below has been carried out：
One, skin irritation test：
2.5~3kg healthy rabbits 70 are selected, every rabbit back is symmetrical to select 20 shaving 2.5cm2, right with itself
It is carried out according to test method(s), applies 0.5g embodiment of the present invention product or bare substrate every time, twice daily, left or right side is given at random
Medicine, observe and record for 24 hours, after 72h skin reacting phenomenon.
The result shows that：It applies product of the present invention and has no that the local stimulations such as rubefaction, dermexanthesis, water lump are reacted for 24 hours, after 72h, say
Bright after-sun modularization cosmetic of the present invention is to be perfectly safe, without any adverse reactions.
Two, product Curative effect of the present invention：
The effect of product of the present invention, counts：Trial volunteer 500, man 170, female 330, age reckling 17 years old,
The maximum 67 years old, average age 34.76 years old.Dry skin 410, neutral skin 60 and Oily 30.By it is all by
Examination person is divided into 6 groups, tries out 1-6 set products of the embodiment of the present invention, every group of 90 people of embodiment 1-2 groups, every group 80 of embodiment 4-6 respectively
People, each subject use after-sun modularization cosmetic of the present invention, outdoors movable a few hours, receive a degree of
After solarization, cleaning exposure and the skin under sunlight, and be respectively applied to skin with 1.00g or so invention products and gently rub, continuously
It uses one week (course for the treatment of).
Effect criterion：
It is excellent：Feel that comfortable, erythema completely disappears, elasticity of skin increases, soft delicate；
It is good：Feel general and objective sign (erythema) disappearance >=2/3；
Difference：It is substantially change using front and back have no.
As a result：In 500, effect judges the superior 480, accounts for 96%；Effect judges good person 20, accounts for 4%, total effective rate
It is 100%.There is adverse reaction without l in whole subjects.
Claims (3)
1. a kind of after-sun composition, it is characterised in that the after-sun component containing following weight percent：
The weight percent of the above components is using entire after-sun composition system total amount as radix.
2. a kind of after-sun composition according to claim 1, it is characterised in that further include oil phase component 9.5-20%,
Adjuvant component 0.5%, triethanolamine adjust pH value to 5.0-7.0, and water phase components surplus wherein contains glycerine in water phase components
6.0-8.0%；
The weight percent of the above components is using entire after-sun composition system total amount as radix.
3. a kind of preparation method of the after-sun composition described in claim 2, it is characterised in that include the following steps：
A, by after-sun component tocopherol acetate and oil phase component mix and be warming up to 80 DEG C, stirring and dissolving is complete；
B, glycerine 2.00% is reserved, water phase remaining component mixing is warming up to 85 DEG C, keeps the temperature 20min, stirring and dissolving is complete；
C, water phase is first pumped into emulsification pot, then is pumped into oil phase, homogeneous 5min, insulated and stirred 5min are vacuumized under stirring and be cooled to
60 DEG C, triethanolamine is added and adjusts pH value, continues to cool down；
D, the menthyl lactate in after-sun component is mixed with the step b glycerine reserved, is heated to 45 DEG C and makes it dissolve, when
It is added, stirs evenly when material body is cooled to 45 DEG C in emulsification pot；
E, be added when material body is cooled to 40 DEG C adjuvant component and beta glucan in after-sun component, Alps glacial water,
Eggshell membrane polypeptide stirs evenly, you can.
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| CN110731917A (en) * | 2018-07-20 | 2020-01-31 | 伽蓝（集团）股份有限公司 | preparation containing glacier water, and its preparation method and application |
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