CN105475942A - Freeze-dried bee product capsule - Google Patents
Freeze-dried bee product capsule Download PDFInfo
- Publication number
- CN105475942A CN105475942A CN201510949300.9A CN201510949300A CN105475942A CN 105475942 A CN105475942 A CN 105475942A CN 201510949300 A CN201510949300 A CN 201510949300A CN 105475942 A CN105475942 A CN 105475942A
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- Prior art keywords
- freeze
- drying
- bee product
- starch
- capsule
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- 239000002775 capsule Substances 0.000 title claims abstract description 49
- 238000004108 freeze drying Methods 0.000 claims abstract description 63
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 30
- 239000000843 powder Substances 0.000 claims abstract description 24
- 239000000203 mixture Substances 0.000 claims abstract description 23
- 238000000034 method Methods 0.000 claims abstract description 19
- 239000000463 material Substances 0.000 claims abstract description 13
- 239000007787 solid Substances 0.000 claims abstract description 11
- 238000002360 preparation method Methods 0.000 claims abstract description 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 32
- 235000012907 honey Nutrition 0.000 claims description 26
- 229920002472 Starch Polymers 0.000 claims description 18
- 239000008107 starch Substances 0.000 claims description 18
- 235000019698 starch Nutrition 0.000 claims description 18
- 238000003756 stirring Methods 0.000 claims description 18
- 235000011187 glycerol Nutrition 0.000 claims description 16
- 229920000881 Modified starch Polymers 0.000 claims description 15
- 241000206575 Chondrus crispus Species 0.000 claims description 14
- 241000241413 Propolis Species 0.000 claims description 9
- 229940069949 propolis Drugs 0.000 claims description 9
- 229940109850 royal jelly Drugs 0.000 claims description 9
- 229920002148 Gellan gum Polymers 0.000 claims description 6
- 235000013871 bee wax Nutrition 0.000 claims description 6
- 239000012166 beeswax Substances 0.000 claims description 6
- 239000000216 gellan gum Substances 0.000 claims description 6
- 235000010492 gellan gum Nutrition 0.000 claims description 6
- CYDQOEWLBCCFJZ-UHFFFAOYSA-N 4-(4-fluorophenyl)oxane-4-carboxylic acid Chemical compound C=1C=C(F)C=CC=1C1(C(=O)O)CCOCC1 CYDQOEWLBCCFJZ-UHFFFAOYSA-N 0.000 claims description 5
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims description 5
- 150000004676 glycans Chemical class 0.000 claims description 5
- 229920001282 polysaccharide Polymers 0.000 claims description 5
- 239000005017 polysaccharide Substances 0.000 claims description 5
- 239000001540 sodium lactate Substances 0.000 claims description 5
- 235000011088 sodium lactate Nutrition 0.000 claims description 5
- 229940005581 sodium lactate Drugs 0.000 claims description 5
- 235000009508 confectionery Nutrition 0.000 claims description 4
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 2
- 229930006000 Sucrose Natural products 0.000 claims description 2
- 239000011692 calcium ascorbate Substances 0.000 claims description 2
- 235000010376 calcium ascorbate Nutrition 0.000 claims description 2
- 229940047036 calcium ascorbate Drugs 0.000 claims description 2
- BLORRZQTHNGFTI-ZZMNMWMASA-L calcium-L-ascorbate Chemical compound [Ca+2].OC[C@H](O)[C@H]1OC(=O)C(O)=C1[O-].OC[C@H](O)[C@H]1OC(=O)C(O)=C1[O-] BLORRZQTHNGFTI-ZZMNMWMASA-L 0.000 claims description 2
- PHZLMBHDXVLRIX-UHFFFAOYSA-M potassium lactate Chemical compound [K+].CC(O)C([O-])=O PHZLMBHDXVLRIX-UHFFFAOYSA-M 0.000 claims description 2
- 239000001521 potassium lactate Substances 0.000 claims description 2
- 235000011085 potassium lactate Nutrition 0.000 claims description 2
- 229960001304 potassium lactate Drugs 0.000 claims description 2
- 239000005720 sucrose Substances 0.000 claims description 2
- 239000002994 raw material Substances 0.000 claims 2
- 229920001817 Agar Polymers 0.000 claims 1
- 108010010803 Gelatin Proteins 0.000 claims 1
- 235000010489 acacia gum Nutrition 0.000 claims 1
- 239000001785 acacia senegal l. willd gum Substances 0.000 claims 1
- 239000008272 agar Substances 0.000 claims 1
- 235000010443 alginic acid Nutrition 0.000 claims 1
- 229920000615 alginic acid Polymers 0.000 claims 1
- 239000001913 cellulose Substances 0.000 claims 1
- 229920002678 cellulose Polymers 0.000 claims 1
- 239000008273 gelatin Substances 0.000 claims 1
- 229920000159 gelatin Polymers 0.000 claims 1
- 235000019322 gelatine Nutrition 0.000 claims 1
- 235000011852 gelatine desserts Nutrition 0.000 claims 1
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 claims 1
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims 1
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims 1
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 claims 1
- 229920001285 xanthan gum Polymers 0.000 claims 1
- 238000001035 drying Methods 0.000 abstract description 4
- 239000011363 dried mixture Substances 0.000 abstract 1
- 238000007710 freezing Methods 0.000 abstract 1
- 230000008014 freezing Effects 0.000 abstract 1
- 241000256844 Apis mellifera Species 0.000 description 42
- 238000003860 storage Methods 0.000 description 7
- 238000012423 maintenance Methods 0.000 description 6
- 239000008213 purified water Substances 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 238000002372 labelling Methods 0.000 description 5
- 235000016709 nutrition Nutrition 0.000 description 5
- MKJXYGKVIBWPFZ-UHFFFAOYSA-L calcium lactate Chemical compound [Ca+2].CC(O)C([O-])=O.CC(O)C([O-])=O MKJXYGKVIBWPFZ-UHFFFAOYSA-L 0.000 description 3
- 239000001527 calcium lactate Substances 0.000 description 3
- 235000011086 calcium lactate Nutrition 0.000 description 3
- 229960002401 calcium lactate Drugs 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- BEFDCLMNVWHSGT-UHFFFAOYSA-N ethenylcyclopentane Chemical compound C=CC1CCCC1 BEFDCLMNVWHSGT-UHFFFAOYSA-N 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 235000015110 jellies Nutrition 0.000 description 3
- 239000008274 jelly Substances 0.000 description 3
- 230000028327 secretion Effects 0.000 description 3
- 235000010199 sorbic acid Nutrition 0.000 description 3
- 229940075582 sorbic acid Drugs 0.000 description 3
- 239000004334 sorbic acid Substances 0.000 description 3
- 238000009777 vacuum freeze-drying Methods 0.000 description 3
- 150000001413 amino acids Chemical class 0.000 description 2
- 230000003064 anti-oxidating effect Effects 0.000 description 2
- 230000002255 enzymatic effect Effects 0.000 description 2
- 230000003203 everyday effect Effects 0.000 description 2
- 210000004907 gland Anatomy 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 238000007711 solidification Methods 0.000 description 2
- 230000008023 solidification Effects 0.000 description 2
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 229930091371 Fructose Natural products 0.000 description 1
- 239000005715 Fructose Substances 0.000 description 1
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 1
- 241000726221 Gemma Species 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 241000218922 Magnoliophyta Species 0.000 description 1
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 description 1
- 241001122767 Theaceae Species 0.000 description 1
- OIPILFWXSMYKGL-UHFFFAOYSA-N acetylcholine Chemical compound CC(=O)OCC[N+](C)(C)C OIPILFWXSMYKGL-UHFFFAOYSA-N 0.000 description 1
- 229960004373 acetylcholine Drugs 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- GUBGYTABKSRVRQ-QUYVBRFLSA-N beta-maltose Chemical compound OC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O GUBGYTABKSRVRQ-QUYVBRFLSA-N 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 235000014633 carbohydrates Nutrition 0.000 description 1
- -1 casing play Substances 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 235000020151 honey milk drink Nutrition 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000002417 nutraceutical Substances 0.000 description 1
- 235000021436 nutraceutical agent Nutrition 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 210000003800 pharynx Anatomy 0.000 description 1
- 238000004080 punching Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000009747 swallowing Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000009966 trimming Methods 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Jellies, Jams, And Syrups (AREA)
Abstract
The invention discloses a freeze-dried bee product capsule, which is produced according to a preparation method: moderate water is added into bee products, and is uniformly stirred, a mixture is paved on a freezing disk, and is put into a freeze-dried machine, a vacuum pump is opened when the temperature of materials achieve below -35 DEG C and the temperature of cold traps achieves below -55 DEG C, a shelf is heated gradiently when the pressure is below 15Pa, the initial temperature of the shelf is -35 DEG C, the final temperature of the shelf is 10 DEG C, and the vacuum pressure of the whole freeze-drying process is controlled in 5-15 Pa to prepare a freeze-dried mixture. Solid matters which are obtained by freeze and drying are smashed, thereby preparing freeze-dried bee product powder. The freeze-dried bee product powder is filled into a special hollow capsule to prepare a finished freeze-dried bee product. The special hollow capsule comprises a waterproof layer, a skeleton layer and a water retention layer. The finished freeze-dried bee product is full of nutriments and convenient to carry and use.
Description
Technical field
The invention discloses a kind of freeze-drying bee product, belong to field of food.
Background technology
Bee product is the product of honeybee, and wherein the thing of gathering and processing of honeybee has honey, Bee Pollen, propolis etc., and the secretion of honeybee has royal jelly etc.Honey is a kind of sticky transparent or semitransparent colloidal liquid.In the main component of honey, water content is below 20%, and carbohydrate comprises glucose, fructose, sucrose and maltose etc., and total content is 75%-80%, in addition also containing various vitamin, mineral matter and amino acid; Bee Pollen is the male sex-cell in flowering plant stamen, and it not only carries the hereditary information of life, and contains the complete nutrients matter bred needed for new life, is described as " all-round nutraceutical ", " concentrated amino acid " etc.; Propolis is the resin that honeybee gathers from plant gemma or trunk, is mixed into the secretion of body of gland in honeybee mouthpart, then with a kind of colloid substance that pollen, beeswax are processed into, be described as " purple gold "; Royal jelly is the secretion of the young worker bee pharynx gland cultivating larva in honeycomb, is high protein, and containing Cobastab and acetylcholine etc.
At present, the method for honey solids mainly contains freeze drying, vacuum freeze drying, spraying dry and roller drying.Auxiliary material addition many (30%-70%) during owing to adopting cylinder drying processing solid bee honey, and temperature high (110 DEG C-200 DEG C), causes that honey solids powder color is very dark, purity is very poor, and enzymatic activity is destroyed substantially; Spray drying process auxiliary material is many, and auxiliary material accounts for more than 50%, and formula is complicated, and enzymatic activity is low; Tradition freeze-drying cost intensive; It not ideal solid method.
Chinese patent CN10269327B discloses a kind of health-care honey milk tea and preparation method thereof, it adopts vacuum freeze-drying method liquid towards honey to carry out solidification, remain the nutritional labeling of honey to a certain extent, but because royal jelly is high protein, high temperature can destroy its nutritional labeling, so there is the shortcoming of temperature drift (95-100 DEG C), narrow application range (be only applicable to honey, other bee products such as propolis, royal jelly can not be used for) in this method.
Because various bee product action effect is different, its proportioning is different, is applicable to the people of different demand.But the method for various bee product separate storage exists by tradition carries and uses inconvenient shortcoming, especially requires harsh royal jelly (requiring low tempertaure storage) to storage requirement.
The invention provides a kind of freeze-drying bee product, it is retaining under the prerequisite that various bee product main nutritional labeling do not scatter and disappear, according to the different demands of people, the bee product mixture of different action effect can be made, its each uniform composition, and be convenient to storage at normal temperature, have certain moistureproof antioxidation, can select to carry softgel shell number according to use amount every day, easy to use, especially be applicable to not liking sweet trencherman and person's use of often not going out, using method is: (1) directly send water to swallow; (2) drink after adding appropriate warm water or cold water impulsive motion.
Summary of the invention
The technical problem underlying that invention solves: a kind of freeze-drying bee product is provided, it is retaining under the prerequisite that various bee product main nutritional labeling do not scatter and disappear, can according to the different demands of people, make the bee product mixture of different action effect, its each uniform composition, and be convenient to storage at normal temperature, have certain moistureproof antioxidation, can select to carry softgel shell number according to use amount every day, easy to use, be especially applicable to not liking sweet trencherman and person's use of often not going out.
The technical method that technical solution problem adopts: a kind of freeze-drying bee product, produce according to following preparation method:
(1) get bee product and add appropriate water, stir;
(2) said mixture is laid on refrigerator tray, puts into freeze dryer, treat that temperature of charge reaches less than-35 DEG C, when condenser temperature reaches below-55 DEG C, open vavuum pump, start as below 15Pa shelf gradient-heated, arrange shelf initial temperature and be-35 DEG C, shelf final temperature is 10 DEG C; Controlling freeze-drying overall process vacuum pressure is 5 ~ 15Pa, obtains freeze-drying mixture;
(3) solid matter that above-mentioned freeze drying obtains is pulverized, obtain freeze-drying bee product powder;
(4) freeze-drying bee product powder is filled in special Capsules, obtains finished product freeze-drying bee product.
Described bee product powder, is characterized in that: bee product is selected from one or more the bee product in honey, Bee Pollen, propolis, royal jelly.
Described special Capsules, is characterized in that it is made up of interior, domestic and abroad three-decker, is respectively the watertight composition of internal layer, the casing play in middle level, outer field water conservation layer.
Described special Capsules, the watertight composition preferred material of internal layer is including but not limited to following one or more: starch, pregelatinized starch, glycerine, carragheen, beeswax, potassium lactate, wherein watertight composition preferably comprises following parts by weight ingredient: 100 parts of starch, 15 ~ 30 parts of pregelatinized starch, 0.5 ~ 1 part of glycerine, 0.5 ~ 1 part of carragheen, 0.1 ~ 0.5 part of sorbic acid.
Described special Capsules, the casing play preferred material in middle level is including but not limited to following one or more: starch, pregelatinized starch, glycerine, gellan gum, carragheen, D-sorbite, wherein casing play preferably comprises following parts by weight ingredient: 100 parts of starch, 10 ~ 20 parts of pregelatinized starch, 0.5 ~ 1 part of glycerine, 0.5 ~ 1 part of carragheen, 0.5 ~ 1 part of gellan gum, 0.1 ~ 0.5 part of calcium lactate, 0.1 ~ 0.5 part of D-sorbite.
Described special Capsules, outer field water conservation layer preferred material is including but not limited to following one or more: starch, pregelatinized starch, glycerine, pulullan polysaccharide, sodium lactate, Calcium Ascorbate, wherein water conservation layer preferably comprises following parts by weight ingredient: 100 parts of starch, 10 ~ 30 parts of pregelatinized starch, 0.5 ~ 1.5 part of glycerine, 0.5 ~ 1 part of carragheen, 0.1 ~ 0.5 part of sodium lactate.
Described special Capsules, is characterized in that preparation method comprises the steps:
1) 100 parts of starch, 15 ~ 30 parts of pregelatinized starch, 0.5 ~ 1 part of glycerine, 0.5 ~ 1 part of carragheen is taken, 0.1 ~ 0.5 part of sorbic acid joins in 350 parts of purified water and stirs, and be heated to 75 DEG C of maintenance stirring 1h, then vacuumize the most of bubble in removing colloidal sol, obtain watertight composition colloidal sol;
2) 100 parts of starch, 10 ~ 20 parts of pregelatinized starch, 0.5 ~ 1 part of glycerine, 0.5 ~ 1 part of carragheen is taken, 0.5 ~ 1 part of gellan gum, 0.1 ~ 0.5 part of calcium lactate, 0.1 ~ 0.5 part of D-sorbite join in 350 parts of purified water and stir, and be heated to 75 DEG C of maintenance stirring 1h, then vacuumize the most of bubble in removing colloidal sol, obtain casing play colloidal sol;
3) 100 parts of starch, 10 ~ 30 parts of pregelatinized starch, 0.5 ~ 1.5 part of glycerine, 0.5 ~ 1 part of carragheen is taken, 0.1 ~ 0.5 part of sodium lactate joins in 350 parts of purified water and stirs, and be heated to 75 DEG C of maintenance stirring 1h, then vacuumize the most of bubble in removing colloidal sol, obtain water conservation layer colloidal sol;
4) mould of selected capsule model is dipped in rapidly and wraps up in the beeswax melted, make the capsule drain pan of internal layer waterproof and oilproof;
5) then the mould wrapping beeswax is dipped in rapidly more successively in watertight composition colloidal sol, casing play colloidal sol, water conservation layer colloidal sol and wrap up in, all need at 25 ~ 35 DEG C after having dipped at every turn, dry cooling 5 ~ 60min in the environment of 35% ~ 55% humidity.
Beneficial effect: the present invention adopts vacuum freeze-drying method to carry out frozen drying to bee product, can retain the nutritional labeling of all kinds of bee product, is applicable to the solidification of all kinds of bee product and composition thereof, applied widely, workable.In the present invention, owing to having wrapped up the Capsules shell with three layers of effect of guaranteeing the quality outside freeze-drying bee product, have while protecting taste fresh-keeping effect and extend the shelf-life, suitable bee product can be selected directly to swallow according to individual demand in addition or eat appropriate capsule with water punching, remaining still can storage uses next time, avoid the storage of existing bee product and carry inconvenient shortcoming, the person that is especially applicable to often not going out uses, and adopts and be especially applicable to not liking sweet trencherman when sending the water method of swallowing to eat and use.
Accompanying drawing explanation
Fig. 1 freeze-drying bee product capsule structure schematic diagram.
Fig. 2 is 25 DEG C, the change of content of reducing sugar in the 0th, 1,2,3,5 day freeze-drying honey powder under the condition of 75% humidity; Wherein A is freeze-drying honey powder, and B is freeze-drying honey powder capsule.
Detailed description of the invention
Below by specific embodiment, the present invention is described in further detail.
Embodiment 1
Special Capsules is made by following steps:
1) 100kg starch, 20kg pregelatinized starch, 0.5kg glycerine, 0.5kg carragheen is taken, 0.1kg sorbic acid joins in 350kg purified water and stirs, and be heated to 75 DEG C of maintenance stirring 1h, then vacuumize the most of bubble in removing colloidal sol, obtain watertight composition colloidal sol;
2) 100kg starch, 10kg pregelatinized starch, 0.5kg glycerine, 0.5kg carragheen is taken, 0.3kg gellan gum, 0.1kg calcium lactate, 0.1kg D-sorbite join in 350kg purified water and stir, and be heated to 75 DEG C of maintenance stirring 1h, then vacuumize the most of bubble in removing colloidal sol, obtain casing play colloidal sol;
3) 100kg starch, 15kg pregelatinized starch, 20kg pulullan polysaccharide, 0.5kg glycerine, 0.5kg carragheen is taken, 0.1kg sodium lactate joins in 350kg purified water and stirs, and be heated to 75 DEG C of maintenance stirring 1h, then vacuumize the most of bubble in removing colloidal sol, obtain water conservation layer colloidal sol;
4) on mould, first wrap up in the thin beeswax of one deck, after cooling, wrap watertight composition, casing play, water conservation layer more successively, by trimming, screening, obtain special Capsules after fit after cooling.
Embodiment 2
1) get honey 20kg, add water 1.5kg, stirs;
2) said mixture is laid on refrigerator tray, puts into freeze dryer, treat that temperature of charge reaches less than-35 DEG C, when condenser temperature reaches below-55 DEG C, open vavuum pump, start as below 15Pa shelf gradient-heated, arrange shelf initial temperature and be-35 DEG C, shelf final temperature is 10 DEG C; Controlling freeze-drying overall process vacuum pressure is 5 ~ 15Pa, obtains freeze-drying honey;
3) solid matter that above-mentioned freeze drying obtains is pulverized, obtain freeze-drying honey powder;
4) freeze-drying bee product powder is filled in special Capsules, obtains finished product freeze-drying honey capsule.
Embodiment 3
1) get propolis 20kg, add water 3kg, stirs;
2) said mixture is laid on refrigerator tray, puts into freeze dryer, treat that temperature of charge reaches less than-35 DEG C, when condenser temperature reaches below-55 DEG C, open vavuum pump, start as below 15Pa shelf gradient-heated, arrange shelf initial temperature and be-35 DEG C, shelf final temperature is 10 DEG C; Controlling freeze-drying overall process vacuum pressure is 5 ~ 15Pa, obtains freeze-drying propolis;
3) solid matter that above-mentioned freeze drying obtains is pulverized, obtain Lyophylized Propolis end;
4) freeze-drying bee product powder is filled in special Capsules, obtains finished product freeze-drying bee glue capsule.
Embodiment 4
1) royal jelly extracting 20kg, add water 2kg, stirs;
2) said mixture is laid on refrigerator tray, puts into freeze dryer, treat that temperature of charge reaches less than-35 DEG C, when condenser temperature reaches below-55 DEG C, open vavuum pump, start as below 15Pa shelf gradient-heated, arrange shelf initial temperature and be-35 DEG C, shelf final temperature is 10 DEG C; Controlling freeze-drying overall process vacuum pressure is 5 ~ 15Pa, obtains frozen dry roral jelly;
3) solid matter that above-mentioned freeze drying obtains is pulverized, obtain frozen dry roral jelly powder;
4) freeze-drying bee product powder is filled in special Capsules, obtains finished product frozen dry roral jelly capsule.
Embodiment 5
1) get honey 5kg, Bee Pollen 7kg, propolis 4kg, royal jelly 4kg, add water 3.5kg, stirs;
2) said mixture is laid on refrigerator tray, puts into freeze dryer, treat that temperature of charge reaches less than-35 DEG C, when condenser temperature reaches below-55 DEG C, open vavuum pump, start as below 15Pa shelf gradient-heated, arrange shelf initial temperature and be-35 DEG C, shelf final temperature is 10 DEG C; Controlling freeze-drying overall process vacuum pressure is 5 ~ 15Pa, obtains freeze-drying bee product;
3) solid matter that above-mentioned freeze drying obtains is pulverized, obtain freeze-drying bee product powder;
4) freeze-drying bee product powder is filled in special Capsules, obtains finished product freeze-drying bee product capsule.
Test example 1
Freeze-drying honey powder obtained in embodiment 2 and freeze-drying honey capsule are placed in 25 DEG C, the climatic chamber of 75% humidity, at the 0th, 1,2,3,5 day, sampling was surveyed its Changes of Reducing Sugar Content and is also compared separately.
Interpretation of result
The content of reducing sugar of freeze-drying honey capsule and freeze-drying honey powder declines all to some extent as shown in Figure 2, but the content of reduced sugar have dropped about 14% in the freeze-drying honey powder directly exposed, and the freeze-drying Reducing Sugar in Honey content employing this special starch capsule packaging only have dropped about 5%.Which illustrate and adopt the freeze-drying honey product of this patent method process to have excellent ability of guaranteeing the quality.
Claims (9)
1. a freeze-drying bee product capsule, is characterized in that it loads Capsules by freeze-drying bee product powder and forms.
2. according to freeze-drying bee product capsule according to claim 1, it is characterized in that: described freeze-drying bee product powder is added water after freeze-drying is pulverized by bee product and obtains.
3. according to bee product capsule according to claim 2, it is characterized in that: bee product is selected from one or more the bee product in honey, Bee Pollen, propolis, royal jelly.
4. according to freeze-drying bee product capsule according to claim 1, it is characterized in that: Capsules adds by capsule raw material the capsule shells that auxiliary material and water makes, wherein said capsule raw material is one or more in starch, converted starch, gelatin, Hydroxypropyl methylcellulose, pulullan polysaccharide and algal polysaccharides; Described auxiliary material is one or more the auxiliary material in glycerine, cellulose family, carragheen, Arabic gum, algin class, xanthans, gellan gum, agar, albumen powder, sucrose, sorbierite and sweet mellow wine.
5., according to freeze-drying bee product capsule according to claim 4, it is characterized in that: described Capsules its be made up of interior, domestic and abroad three-decker, be respectively the watertight composition of internal layer, the casing play in middle level, outer field water conservation layer.
6. freeze-drying bee product capsule according to claim 5, is characterized in that the watertight composition preferred material of described Capsules internal layer is including but not limited to following one or more: starch, pregelatinized starch, glycerine, carragheen, beeswax, potassium lactate.
7. freeze-drying bee product capsule according to claim 5, is characterized in that the casing play preferred material in described Capsules middle level is including but not limited to following one or more: starch, pregelatinized starch, glycerine, gellan gum, carragheen, D-sorbite.
8. freeze-drying bee product capsule according to claim 5, is characterized in that described Capsules outer field water conservation layer preferred material is including but not limited to following one or more: starch, pregelatinized starch, glycerine, pulullan polysaccharide, sodium lactate, Calcium Ascorbate.
9., according to the preparation method of freeze-drying bee product capsule according to claim 1, comprising:
(1) get bee product and add appropriate water, stir;
(2) said mixture is laid on refrigerator tray, puts into freeze dryer, treat that temperature of charge reaches less than-35 DEG C, when condenser temperature reaches below-55 DEG C, open vavuum pump, start as below 15Pa shelf gradient-heated, arrange shelf initial temperature and be-35 DEG C, shelf final temperature is 10 DEG C; Controlling freeze-drying overall process vacuum pressure is 5 ~ 15Pa, obtains freeze-drying mixture;
(3) solid matter that above-mentioned freeze drying obtains is pulverized, obtain freeze-drying bee product powder;
(4) freeze-drying bee product powder is filled in Capsules, obtains finished product freeze-drying bee product.
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| CN201510949300.9A CN105475942A (en) | 2015-12-18 | 2015-12-18 | Freeze-dried bee product capsule |
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| CN108294269A (en) * | 2018-01-30 | 2018-07-20 | 叶水华 | A kind of strengthen immunity and health care capsule used for relieving physical fatigue production method |
| CN112641121A (en) * | 2020-10-10 | 2021-04-13 | 广州启键生物科技有限公司 | Preparation method of filling hollow capsules of hydroxypropyl methylcellulose and algal polysaccharide |
| CN115813878A (en) * | 2022-12-09 | 2023-03-21 | 浙江省食品药品检验研究院 | Water-proof coating solution and application for preparing water-proof capsule |
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