CN105342877B - A kind of amino acid cleansing paper and preparation method thereof - Google Patents
A kind of amino acid cleansing paper and preparation method thereof Download PDFInfo
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- CN105342877B CN105342877B CN201510823879.4A CN201510823879A CN105342877B CN 105342877 B CN105342877 B CN 105342877B CN 201510823879 A CN201510823879 A CN 201510823879A CN 105342877 B CN105342877 B CN 105342877B
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- paper
- slurry
- amino acid
- sodium
- gained
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- 150000001413 amino acids Chemical class 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 29
- 239000012528 membrane Substances 0.000 claims abstract description 11
- 239000000203 mixture Substances 0.000 claims description 31
- 229940024606 amino acid Drugs 0.000 claims description 26
- 229920001285 xanthan gum Polymers 0.000 claims description 24
- 240000003183 Manihot esculenta Species 0.000 claims description 23
- 235000016735 Manihot esculenta subsp esculenta Nutrition 0.000 claims description 23
- 239000002002 slurry Substances 0.000 claims description 23
- 235000010489 acacia gum Nutrition 0.000 claims description 20
- 239000001785 acacia senegal l. willd gum Substances 0.000 claims description 20
- 229920002472 Starch Polymers 0.000 claims description 18
- 229920001577 copolymer Polymers 0.000 claims description 18
- 235000019698 starch Nutrition 0.000 claims description 18
- 239000008107 starch Substances 0.000 claims description 18
- KSAVQLQVUXSOCR-UHFFFAOYSA-M sodium lauroyl sarcosinate Chemical compound [Na+].CCCCCCCCCCCC(=O)N(C)CC([O-])=O KSAVQLQVUXSOCR-UHFFFAOYSA-M 0.000 claims description 15
- TWJNQYPJQDRXPH-UHFFFAOYSA-N 2-cyanobenzohydrazide Chemical compound NNC(=O)C1=CC=CC=C1C#N TWJNQYPJQDRXPH-UHFFFAOYSA-N 0.000 claims description 14
- TUNFSRHWOTWDNC-UHFFFAOYSA-N Myristic acid Natural products CCCCCCCCCCCCCC(O)=O TUNFSRHWOTWDNC-UHFFFAOYSA-N 0.000 claims description 14
- 235000021360 Myristic acid Nutrition 0.000 claims description 14
- 229920002385 Sodium hyaluronate Polymers 0.000 claims description 12
- 229940010747 sodium hyaluronate Drugs 0.000 claims description 12
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims description 12
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 11
- 238000006243 chemical reaction Methods 0.000 claims description 11
- PXEDJBXQKAGXNJ-QTNFYWBSSA-L disodium L-glutamate Chemical compound [Na+].[Na+].[O-]C(=O)[C@@H](N)CCC([O-])=O PXEDJBXQKAGXNJ-QTNFYWBSSA-L 0.000 claims description 11
- 229930182478 glucoside Natural products 0.000 claims description 11
- 150000008131 glucosides Chemical class 0.000 claims description 11
- 235000013923 monosodium glutamate Nutrition 0.000 claims description 11
- 229960005323 phenoxyethanol Drugs 0.000 claims description 11
- 229940073490 sodium glutamate Drugs 0.000 claims description 11
- 229920001131 Pulp (paper) Polymers 0.000 claims description 9
- 238000004080 punching Methods 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 9
- 238000001704 evaporation Methods 0.000 claims description 8
- 230000008020 evaporation Effects 0.000 claims description 8
- RWDOCBHBDDFEQV-UQKRIMTDSA-M potassium;(4s)-4-amino-5-dodecanoyloxy-5-oxopentanoate Chemical compound [K+].CCCCCCCCCCCC(=O)OC(=O)[C@@H](N)CCC([O-])=O RWDOCBHBDDFEQV-UQKRIMTDSA-M 0.000 claims description 8
- 238000003825 pressing Methods 0.000 claims description 8
- 239000002562 thickening agent Substances 0.000 claims description 7
- 239000004094 surface-active agent Substances 0.000 claims description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
- 238000007493 shaping process Methods 0.000 claims description 2
- 239000011734 sodium Substances 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims 1
- QMHBZWNZCSNBGU-UHFFFAOYSA-N nonane-1,2,3-triol Chemical compound CCCCCCC(O)C(O)CO QMHBZWNZCSNBGU-UHFFFAOYSA-N 0.000 claims 1
- 239000007787 solid Substances 0.000 abstract description 7
- 239000000463 material Substances 0.000 abstract description 5
- 230000007613 environmental effect Effects 0.000 abstract description 4
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 abstract description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 abstract description 2
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 abstract description 2
- 239000011575 calcium Substances 0.000 abstract description 2
- 229910052791 calcium Inorganic materials 0.000 abstract description 2
- 238000004140 cleaning Methods 0.000 abstract description 2
- 150000002191 fatty alcohols Chemical class 0.000 abstract description 2
- 239000011777 magnesium Substances 0.000 abstract description 2
- 229910052749 magnesium Inorganic materials 0.000 abstract description 2
- 235000016709 nutrition Nutrition 0.000 abstract description 2
- 239000001103 potassium chloride Substances 0.000 abstract description 2
- 235000011164 potassium chloride Nutrition 0.000 abstract description 2
- 238000009472 formulation Methods 0.000 abstract 2
- 230000035764 nutrition Effects 0.000 abstract 1
- -1 Acyl potassium glutamate Chemical compound 0.000 description 7
- 235000013919 monopotassium glutamate Nutrition 0.000 description 7
- 230000000694 effects Effects 0.000 description 5
- 230000001815 facial effect Effects 0.000 description 4
- 239000003292 glue Substances 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 239000002775 capsule Substances 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 230000007935 neutral effect Effects 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000000344 soap Substances 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 230000008719 thickening Effects 0.000 description 2
- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 description 1
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 description 1
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 description 1
- 229920000945 Amylopectin Polymers 0.000 description 1
- 229920000856 Amylose Polymers 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 1
- 235000017491 Bambusa tulda Nutrition 0.000 description 1
- 239000001828 Gelatine Substances 0.000 description 1
- 239000004909 Moisturizer Substances 0.000 description 1
- 244000082204 Phyllostachys viridis Species 0.000 description 1
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- 239000004372 Polyvinyl alcohol Substances 0.000 description 1
- 241000220287 Sedum rubrotinctum Species 0.000 description 1
- 229920006243 acrylic copolymer Polymers 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 239000011425 bamboo Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000007767 bonding agent Substances 0.000 description 1
- 239000005018 casein Substances 0.000 description 1
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 description 1
- 235000021240 caseins Nutrition 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000003610 charcoal Substances 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000004925 denaturation Methods 0.000 description 1
- 230000036425 denaturation Effects 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 239000003974 emollient agent Substances 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 229920000159 gelatin Polymers 0.000 description 1
- 235000019322 gelatine Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000008236 heating water Substances 0.000 description 1
- 229920002674 hyaluronan Polymers 0.000 description 1
- 229960003160 hyaluronic acid Drugs 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000002480 mineral oil Substances 0.000 description 1
- 235000010446 mineral oil Nutrition 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000001333 moisturizer Effects 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000005022 packaging material Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 239000002861 polymer material Substances 0.000 description 1
- 229920002451 polyvinyl alcohol Polymers 0.000 description 1
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 1
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 1
- 239000001267 polyvinylpyrrolidone Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 235000010413 sodium alginate Nutrition 0.000 description 1
- 239000000661 sodium alginate Substances 0.000 description 1
- 229940005550 sodium alginate Drugs 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0208—Tissues; Wipes; Patches
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Emergency Medicine (AREA)
- Engineering & Computer Science (AREA)
- Biomedical Technology (AREA)
- Dermatology (AREA)
- Paper (AREA)
- Detergent Compositions (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Cosmetics (AREA)
Abstract
The preparation formula and preparation method of a kind of amino acid cleansing paper, are paper membrane piece film products due to making for cleaning face, floor space is very small by preparing the amino acid cleansing paper that formula and preparation method are made；Finished product is 0.1 0.3mm per a piece of thickness；Due to the small volume of finished product, and it is solid, it is portable；As long as can be to use using clear water dissolving, finished product energy 100% be biodegradable, and burden is not caused to environmental resource；The material of preparation is derived from natural safety, has amino acid, fatty alcohol calcium, magnesium and sylvite etc. after water dissolving, rich in nutrition and pure gentle non-stimulated to skin.
Description
Technical field
The invention belongs to daily-use chemical industry care product processing technique field, more particularly to a kind of amino acid cleansing paper and its
Preparation method.
Background technology
There are various skin care item, including soap, mildy wash, facial mask etc. currently on the market, but these skin care item
There are some inevitable shortcomings, be exactly to be inconvenient to carry.Also it is exactly that such as conventional soap is all block, contact mostly
Water unusual light, easily slides, and is used through excessive people transmission, also unhygienic.The canned shin moisturizer of conventional bottles, it is inconvenient to carry, even
In house, space-consuming is all compared in travelling to existing frequently-used mildy wash, and it is difficult reuse to be finished rear vacant packaging material, is caused greatly
The wasting of resources and environmental pressure.The equipment used in the process of these skin care item is manufactured also than larger, more spaces are taken.
The related document of access and market, also no one kind can be environmentally friendly so far, is convenient for carrying and practical skin care production
Product, although it is to compare bamboo charcoal face pack to have many facial masks in succession（Patent No. CN201210357562.2）With some facial mask liquids（Patent
Number be CN201210543465.2）Renewal, but currently on the market no one kind can water dissolving and free of contamination cleaning
The diaphragm of face.
Commercially, the skin care item into solid-state carrying are relatively more, but these skin care item, particularly facial skin care product, and
Do not turn into specific solid shape and water insoluble, it is on the living conditions and not convenient.Found in continuous research, script is belonged to
The solid-state of shaping is converted into the skin care item of liquid, from specific raw material and there must be appropriate ratio, it is no
Then easily easily fallen apart in wet environment or finished product.
The content of the invention
It is contemplated that invent a kind of amino acid cleansing paper and preparation method thereof, amino acid cleansing paper have be convenient for carrying,
The biodegradable complete, effect of function gently, preparation method is pollution-free.
The percentage that the present invention is referred to is to account for slurry component gross mass percentage.
In order to achieve the above object, the technical scheme is that：
A kind of amino acid cleansing paper, it is characterised in that：Its component and ratio are：Slurry：Starch 4:1, described slurry
Component is：
Surfactant：34-40%
Thickener：1.9-3.5%
NMF：0.2-0.4%
Fructus Hordei Germinatus oligose glucoside 8-12%；
Sodium glutamate 10%；
Phenoxyethanol 0.3-0.8%；
Water 34-45%.
Described starch is tapioca or its converted starch.
Described surfactant includes：It is any in sodium lauroyl sarcosine, lauroyl glutamate potassium and myristic acid
One kind, or matched according to following components：Sodium lauroyl sarcosine：28-32%, lauroyl glutamate potassium：4-5%, Pork and beans
Cool sour 2-3%；Or, sodium lauroyl sarcosine：29-33%, lauroyl glutamate potassium：5-7%；Or, sodium lauroyl sarcosine：
30-34%, myristic acid 4-6%；Or, lauroyl glutamate potassium：20-24%, myristic acid 14-16%.
Described thickener include Arabic gum, xanthans and acrylate copolymer in any one, or according to
Following components is matched：Arabic gum 0.3-0.8%, xanthans 0.1-0.2%, acrylate copolymer 1.5-2.5%；Or,
Arabic gum 1.8-3.3%, xanthans 0.1-0.2%；Or, xanthans 0.1-0.2%, acrylate copolymer 1.8-3.3%；Or
Person, Arabic gum 0.4-1.0%, acrylate copolymer 1.5-2.5%.
Described NMF includes any one of Sodium Hyaluronate, Sensiva SC50, or enters according to following components
Row proportioning：Sodium Hyaluronate：0.1-0.2%, Sensiva SC50：0.1-0.2%.
, can preferably following ratio in the application according to experimental data：
Sodium lauroyl sarcosine 28-32%；
Fructus Hordei Germinatus oligose glucoside 8-12%；
Sodium glutamate 10%；
Lauroyl glutamate potassium 4-5%；
Myristic acid 2-3%；
Acrylate copolymer 1.5-2.5%；
Phenoxyethanol 0.3-0.8%；
Arabic gum 0.3-0.8%；
Xanthans 0.1-0.2%；
Sodium Hyaluronate 0.1-0.2%；
Sensiva SC50 0.1-0.2%
Water 34-45%.
A kind of preparation method of amino acid cleansing paper, it is characterised in that at least comprise the following steps：
（1）By the water of described mass percent, sodium lauroyl sarcosine, Fructus Hordei Germinatus oligose glucoside, sodium glutamate, bay
Acyl potassium glutamate and myristic acid are heated to 80-85 °C of dissolving completely, stir；
（2）By the acrylate copolymer of described mass percent, Phenoxyethanol, Arabic gum, xanthans, hyalomitome
Sour sodium and Sensiva SC50 are added to step after being completely dissolved at normal temperatures（1）In the mixture of gained, slurry is made；
（3）Step is added to by the starch of described mass percent（2）In the slurry of gained, set with high-speed stirred is scattered
It is standby to stir into slurry；
（4）By step（3）The mixture of gained is put into paper web, while adjusting reaction temperature；
（5）Rotating paper web with 5r/s speed makes moisture evaporation completely, step（4）Gained paper pulp gradually becomes paper；
（6）Coil paper is carried out using wound membrane punching apparatus, then will be cut according to specification, recycles pressing equipment to carry out
Punch forming.
Step（2）In xanthans, the mass percent of hyaluronic acid and Sensiva SC50 be 1:1:1.
Step（4）Reaction temperature be 90 °C.
Step（1）With step（2）Separately it is able in suitable temperature（80-85°C）Dissolve above-mentioned steps（1）Interior
Dispensing.
The water solubility of described portable amino acid cleansing diaphragm is 10-25g/100g water；Described portable amino acid is clean
Face diaphragm thickness is 0.1-0.3mm.
Thickener on the market includes acrylamide, polyvinyl alcohol, polyvinylpyrrolidone, polyethylene glycol oxide, starch, bright
Glue, sodium alginate and casein etc., preferred Arabic gum, xanthans and acrylate copolymer in the application.
Arabic gum is a kind of solid crystalline object, when it is ducked in drink, meeting water absorption and swelling, finally glutinous as one kind
Shape colloid is molten to return to original solid state absorption on the space of a whole page.It, which is acted on, is that after glue drying, and being covered in the space of a whole page is in
Glued membrane is hardened, printing plate is come with air insulated, so that the purpose of anti-oxidation is reached, with fabulous weatherability film forming, shape
Into one layer of more preferable hydrophilic film, amino acid cleansing paper hydrophilicity is improved.
Xanthans is that collection is thickened, suspended, emulsifying, being stable at one, the biogum that best performance is got over.Xanthans is to insoluble
Solid and oil droplet have good suspension effect.Xanthans colloidal sol molecule can form the spiral EVA of superjunction crossed belt shape, constitute
The network structure of fragile similar glue, so the form of solid particle, drop and bubble can be supported, shows very strong emulsification
Stabilization and uphang i.Xanthans can quickly dissolve in water, there is good water solubility.Especially also can be molten in cold water
Solution, can save numerous and diverse process, easy to use.Also there is splendid thickening property ＆ pseudoplastic behavioies simultaneously, it is stable to hot-cool environment
Property and ph stability performance etc..
Acrylic copolymer when for personal cleansing product based on surfactant, can play suspension, stably,
The effect of thickening, and product can be improved into film outward appearance weather resistance etc..
Arabic gum, xanthans and acrylate copolymer.There are increase product stability, water to strengthening amino acid cleansing paper
Dissolubility, filming performance etc. has great help.
In this application, the bonding agent of the portable amino acid cleansing paper of water dissolving, preferably tapioca and its denaturation are prepared
Starch, the starch of special modification can be with moisturizing agent carrier be made, and usual this kind of emollient is mineral oil-based materials.Tapioca boiling
The paste formed afterwards is as clear as crystal, and tapioca can be used for the applying glue of high-grade paper, due to amylopectin in cassava ative starch
80 are up to the ratio of amylose:20, therefore with very high spike viscosity, cassava ative starch paste shows relatively low
It is Reversibility, thus can prevent moisture content from losing in freeze-thaw circulation.In addition, can also to make full starch thin for tapioca
Film capsule, the full starch capsule shells made by tapioca have stability height than traditional gelatine capsule shell, are difficult
The advantages of absorbing water, be difficult to crosslink reaction with medicinal powder, be difficult breed bacteria, is extensively praised highly, cassava ative starch in American-European countries
It can be mixed with converted starch with petroleum base or artificial synthesized high polymer material to improve the biodegradable of material, there is fabulous
Biodegradability.Therefore tapioca and its converted starch are to do amino acid cleansing scraps of paper optimal material, other raw materials without
Method is substituted.
Portable amino acid cleansing paper disclosed by the invention have be convenient for carrying, the effect of function gently.Arabic gum and Huang
Virgin rubber is natural origin composition, and acrylic acid is to belong to cosmetics to commonly use safe film forming ingredients, other constituents also non-stimulated skin
The effect of skin, so amino acid cleansing paper moderate performance, product safety.
Portable amino acid cleansing paper is sheet, has toughness, can stretch to a certain degree, and adding after water can be rapid molten after 3-7 seconds
Solution, can clean face after both hands friction foaming, and because composition is gentle, eyes and general skin not caused to stimulate shadow
Ring.Finished product is 0.1-0.3mm per a piece of thickness, very frivolous, can be cut into different shapes, meet the need of market fashion
Ask.
Compared with prior art, the beneficial effects of the present invention are：
1st, finished product is paper membrane piece film product due to making, and floor space is very small；Finished product is 0.1- per a piece of thickness
0.3mm；
2nd, due to the small volume of finished product, and it is solid, is not take up excessive bottle Bottle ＆ Can tank, it is portable；
As long as the 3rd, can be to use using clear water dissolving, finished product energy 100% be biodegradable, and burden is not caused to environmental resource；
4th, the material prepared is derived from natural safety, has amino acid, fatty alcohol calcium, magnesium and sylvite etc. after water dissolving, rich in battalion
Support and pure gentle non-stimulated to skin；（Accompanying drawing 2 and embodiment 8）
5th, equipment and tradition are inconsistent used in preparing, and floor space is small, and safety operation performance is good.Preparation process is used
Machine there is electric-heating water bath to configure film forming agent solution pot, normal temperature mixed amino acid solution pot is cold with the mixing of the no consumption energy
Drying roller is dried in pot, electrical heating environmental protection.
Figure of description
Fig. 1 is step（4）The paper pulp yield of middle differential responses temperature；
Fig. 2 is the nutritional ingredient figure after amino acid cleansing paper water dissolves.
Embodiment
Below in conjunction with the embodiment of the present invention, the present invention is described in further detail.
Embodiment 1：
（1）By 38.9% water, 30% sodium lauroyl sarcosine, 10% Fructus Hordei Germinatus oligose glucoside, 10% sodium glutamate, 5% bay
Acyl potassium glutamate and 3% myristic acid are heated to 82 °C of degree dissolvings completely, stir；（2）By 2% acrylate copolymer,
0.5% Phenoxyethanol, 0.3% Arabic gum, 0.1% xanthans, 0.1% Sodium Hyaluronate and 0.1% Sensiva SC50 are at normal temperatures
Step is added to after being completely dissolved（1）In the mixture of gained；（3）Tapioca and step again（2）The mixture 1 of gained:4
Tapioca, is added to step by ratio（2）In the mixture of gained, slurry is stirred into high-speed stirred dispersing apparatus；（4）Will step
Suddenly（3）The mixture of gained is put into paper web, while adjusting to 90 °C of reaction temperatures；（5）It is slow to rotate paper web, make step（4）
Gained paper pulp gradually becomes paper, until moisture evaporation is complete；（6）Coil paper is carried out using wound membrane punching apparatus, then will be according to
Specification is cut, and recycles pressing equipment to carry out punch forming.
Embodiment 2：
（1）By 44.6% water, 28% sodium lauroyl sarcosine, 8% Fructus Hordei Germinatus oligose glucoside, 10% sodium glutamate, 4% bay
Acyl potassium glutamate and 2% myristic acid are heated to 85 °C of degree dissolvings completely, stir；（2）By 1.5% acrylate copolymer,
0.8% Phenoxyethanol, 0.8% Arabic gum, 0.1% xanthans, 0.1% Sodium Hyaluronate and 0.1% Sensiva SC50 are at normal temperatures
Step is added to after being completely dissolved（1）In the mixture of gained；（3）Tapioca and step again（2）The mixture 1 of gained:4
Tapioca, is added to step by ratio（2）In the mixture of gained, slurry is stirred into high-speed stirred dispersing apparatus；（4）Will step
Suddenly（3）The mixture of gained is put into paper web, while adjusting to 90 °C of reaction temperatures；（5）It is slow to rotate paper web, make step（4）
Gained paper pulp gradually becomes paper, until moisture evaporation is complete；（6）Coil paper is carried out using wound membrane punching apparatus, then will be according to
Specification is cut, and recycles pressing equipment to carry out punch forming.
Embodiment 3：
（1）By 34.7% water, 32% sodium lauroyl sarcosine, 12% Fructus Hordei Germinatus oligose glucoside, 10% sodium glutamate, 5% bay
Acyl potassium glutamate and 3% myristic acid are heated to 82 °C of degree dissolvings completely, stir；（2）By 2% acrylate copolymer,
0.5% Phenoxyethanol, 0.5% Arabic gum, 0.1% xanthans, 0.1% Sodium Hyaluronate and 0.1% Sensiva SC50 are at normal temperatures
Step is added to after being completely dissolved（1）In the mixture of gained；（3）Tapioca and step again（2）The mixture 1 of gained:4
Tapioca, is added to step by ratio（2）In the mixture of gained, slurry is stirred into high-speed stirred dispersing apparatus；（4）Will step
Suddenly（3）The mixture of gained is put into paper web, while adjusting to 90 °C of reaction temperatures；（5）It is slow to rotate paper web, make step（4）
Gained paper pulp gradually becomes paper, until moisture evaporation is complete；（6）Coil paper is carried out using wound membrane punching apparatus, then will be according to
Specification is cut, and recycles pressing equipment to carry out punch forming.
Embodiment 4：
（1）By 39.6% water, 30% sodium lauroyl sarcosine, 10% Fructus Hordei Germinatus oligose glucoside, 10% sodium glutamate, 4% bay
Acyl potassium glutamate and 3% myristic acid are heated to 85 °C of degree dissolvings completely, stir；（2）By 2% acrylate copolymer,
0.4% Phenoxyethanol, 0.4% Arabic gum, 0.2% xanthans, 0.2% Sodium Hyaluronate and 0.2% Sensiva SC50 are at normal temperatures
Step is added to after being completely dissolved（1）In the mixture of gained；（3）Tapioca and step again（2）The mixture 1 of gained:4
Tapioca, is added to step by ratio（2）In the mixture of gained, slurry is stirred into high-speed stirred dispersing apparatus；（4）Will step
Suddenly（3）The mixture of gained is put into paper web, while adjusting to 90 °C of reaction temperatures；（5）It is slow to rotate paper web, make step（4）
Gained paper pulp gradually becomes paper, until moisture evaporation is complete；（6）Coil paper is carried out using wound membrane punching apparatus, then will be according to
Specification is cut, and recycles pressing equipment to carry out punch forming.
Embodiment 5：
（1）By 41.3% water, 28% sodium lauroyl sarcosine, 12% Fructus Hordei Germinatus oligose glucoside, 10% sodium glutamate, 4% bay
Acyl potassium glutamate and 2% myristic acid are heated to 82 °C of degree dissolvings completely, stir；（2）By 1.5% acrylate copolymer,
0.3% Phenoxyethanol, 0.3% Arabic gum, 0.2% xanthans, 0.2% Sodium Hyaluronate and 0.2% Sensiva SC50 are at normal temperatures
Step is added to after being completely dissolved（1）In the mixture of gained；（3）Tapioca and step again（2）The mixture 1 of gained:4
Tapioca, is added to step by ratio（2）In the mixture of gained, slurry is stirred into high-speed stirred dispersing apparatus；（4）Will step
Suddenly（3）The mixture of gained is put into paper web, while adjusting to 90 °C of reaction temperatures；（5）It is slow to rotate paper web, make step（4）
Gained paper pulp gradually becomes paper, until moisture evaporation is complete；（6）Coil paper is carried out using wound membrane punching apparatus, then will be according to
Specification is cut, and recycles pressing equipment to carry out punch forming.
Embodiment 6：
（1）By 41.8% water, 32% sodium lauroyl sarcosine, 9% Fructus Hordei Germinatus oligose glucoside, 10% sodium glutamate, 4% bay
Acyl potassium glutamate and 2% myristic acid are heated to 85 °C of degree dissolvings completely, stir；（2）By 2% acrylate copolymer,
0.8% Phenoxyethanol, 0.3% Arabic gum, 0.1% xanthans, 0.1% Sodium Hyaluronate and 0.1% Sensiva SC50 are at normal temperatures
Step is added to after being completely dissolved（1）In the mixture of gained；（3）Tapioca and step again（2）The mixture 1 of gained:4
Tapioca, is added to step by ratio（2）In the mixture of gained, slurry is stirred into high-speed stirred dispersing apparatus；（4）Will step
Suddenly（3）The mixture of gained is put into paper web, while adjusting to 90 °C of reaction temperatures；（5）It is slow to rotate paper web, make step（4）
Gained paper pulp gradually becomes paper, until moisture evaporation is complete；（6）Coil paper is carried out using wound membrane punching apparatus, then will be according to
Specification is cut, and recycles pressing equipment to carry out punch forming.
Select 20-30 Sui to choose the 20 people men and women with neutral skin in general population to be tested.Experiment is divided to two groups, the
One group：10 people, 4 male 6 female, use amino acid cleansing paper useless；Second group：10 people, 5 male 5 female, sooner or later using amino acid cleansing
Paper；After one month, the skin of second group of crowd of amino acid cleansing paper has been used to be had clear improvement than first group.
The people of selection 15 of 20-30 Sui is selected to be tested in general population.Three groups, first group of experiment point：Dry people
Group；Second group：Neutral skin crowd；3rd group, Oily crowd；Three groups use amino acid cleansing paper sooner or later, after one month
Three groups of crowds are using amino acid cleansing paper without significant discomfort.
The present invention is not limited to above-mentioned preferred forms, and anyone should learn that the dosage made under present invention enlightenment
Or formula, and be that those skilled in the art obviously change, it is every that there is same or similar composition with of the invention
Technical scheme, belong to protection scope of the present invention.
Claims (5)
1. a kind of amino acid cleansing paper, it is characterised in that：Its component and mass ratio are：Slurry：Starch 4:1, described slurry group
It is divided into：
Surfactant：34-40%；
Thickener：1.9-3.5%；
NMF：0.2-0.4%；
Fructus Hordei Germinatus oligose glucoside：8-12%；
Sodium glutamate：10%；
Phenoxyethanol：0.3-0.8%；
Water：34-45%,
The slurry component percentages are to account for slurry component gross mass percentage；
Described starch is tapioca or its converted starch；
Described surfactant is matched according to following components：
Sodium lauroyl sarcosine：28-32%, lauroyl glutamate potassium：4-5%, myristic acid：2-3%；
Or, sodium lauroyl sarcosine：29-33%, lauroyl glutamate potassium：5-7%；
Or, sodium lauroyl sarcosine：30-34%, myristic acid：4-6%；
Or, lauroyl glutamate potassium：20-24%, myristic acid：14-16%,
The component percentages are to account for slurry component gross mass percentage；
Described thickener is matched according to following components：
Arabic gum 0.3-0.8%, xanthans 0.1-0.2%, acrylate copolymer 1.5-2.5%；
Or, Arabic gum 1.8-3.3%, xanthans 0.1-0.2%；
Or, xanthans 0.1-0.2%, acrylate copolymer 1.8-3.3%；
Or, Arabic gum 0.4-1.0%, acrylate copolymer 1.5-2.5%,
The component percentages are to account for slurry component gross mass percentage.
2. amino acid cleansing paper according to claim 1, it is characterised in that：Described NMF includes Sodium Hyaluronate, ethyl
Any one of hexyl glycerine, or matched according to following components：
Sodium Hyaluronate：0.1-0.2%, Sensiva SC50：0.1-0.2%,
The component percentages are to account for slurry component gross mass percentage.
3. a kind of prepare such as the preparation method of any one amino acid cleansing paper of claim 1-2, it is characterised in that at least includes
Following steps：
（1）Water, surfactant, Fructus Hordei Germinatus oligose glucoside and sodium glutamate are heated to 80-85 DEG C of dissolving completely, stirring is equal
It is even；
（2）Step is added to after thickener, Phenoxyethanol and NMF are completely dissolved at normal temperatures（1）The mixture of gained
In, slurry is made；
（3）Starch is added to step（2）In the slurry of gained, slurry is stirred into high-speed stirred dispersing apparatus；
（4）By step（3）The mixture of gained is put into paper web, while adjusting reaction temperature；
（5）Rotating paper web with 5r/s speed makes moisture evaporation completely, step（4）Gained paper pulp gradually becomes paper；
（6）Coil paper is carried out using wound membrane punching apparatus, then will be cut according to specification, recycles pressing equipment to carry out punching press
Shaping.
4. a kind of preparation method as claimed in claim 3, it is characterised in that：Step（2）Described in thickener match somebody with somebody by following components
Than：Arabic gum 0.3-0.8%, xanthans 0.1-0.2%, acrylate copolymer 1.5-2.5%；Described NMF is transparent
Matter acid sodium 0.1-0.2% and Sensiva SC50 0.1-0.2%, wherein xanthans, Sodium Hyaluronate and Sensiva SC50 matter
It is 1 to measure percentage:1:1, the component percentages are to account for slurry component gross mass percentage.
5. a kind of preparation method as claimed in claim 3, it is characterised in that：Step（4）Reaction temperature be 90 DEG C.
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| CN106580729A (en) * | 2016-11-13 | 2017-04-26 | 何志德 | Preparation formula for novel amino acid face cleaning slice and preparation method thereof |
| CN106667795B (en) * | 2017-02-06 | 2018-05-08 | 邹伟权 | A kind of soluble cleaning tissue with deep layer cleaning and preparation method thereof |
| CN106726637B (en) * | 2017-03-28 | 2018-06-19 | 广州同康生物科技有限公司 | A kind of soluble cleaning tissue of moist moisturizing and preparation method thereof |
| CN106798665A (en) * | 2017-03-29 | 2017-06-06 | 广州洁明洗涤制品有限公司 | A kind of face cleaning piece and preparation method thereof |
| CN106974861B (en) * | 2017-04-07 | 2020-01-31 | 深圳微伴生物有限公司 | amino acid soluble facial cleaning paper and preparation method thereof |
| CN107080704A (en) * | 2017-04-27 | 2017-08-22 | 缪来耿 | Soluble cleaning tissue of a kind of skin whitening, moisturizing and preparation method thereof |
| CN107028772B (en) * | 2017-04-28 | 2019-11-01 | 安徽清荷纸业有限公司 | A kind of mild non-stimulated soluble cleaning tissue and preparation method thereof |
| TWI647357B (en) * | 2017-06-08 | 2019-01-11 | 十藝生技股份有限公司 | Cleansing paper formula with natural plant source and preparation method thereof |
| CN112972351A (en) * | 2021-02-22 | 2021-06-18 | 广州妍瑟化妆品有限公司 | Clean sheet for attaching amino acid foaming agent to cotton sheet |
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| CN1420140A (en) * | 2001-11-16 | 2003-05-28 | 国家淀粉及化学投资控股公司 | Thin film contg. starch |
| CN101185613A (en) * | 2007-12-18 | 2008-05-28 | 美晨集团股份有限公司 | Gargle tablet and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1420140A (en) * | 2001-11-16 | 2003-05-28 | 国家淀粉及化学投资控股公司 | Thin film contg. starch |
| CN101185613A (en) * | 2007-12-18 | 2008-05-28 | 美晨集团股份有限公司 | Gargle tablet and preparation method thereof |
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