CN1053260A - Color flame candles and preparation technology thereof - Google Patents

Color flame candles and preparation technology thereof Download PDF

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Publication number
CN1053260A
CN1053260A CN 91106031 CN91106031A CN1053260A CN 1053260 A CN1053260 A CN 1053260A CN 91106031 CN91106031 CN 91106031 CN 91106031 A CN91106031 A CN 91106031A CN 1053260 A CN1053260 A CN 1053260A
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CN
China
Prior art keywords
preparation
candle
color
oxidation promotor
oxidation
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Pending
Application number
CN 91106031
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Chinese (zh)
Inventor
陈�光
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SHENYANG PRATICAL INDUSTRIAL AND AGRICULTURAL TECHNOLOGY INST
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SHENYANG PRATICAL INDUSTRIAL AND AGRICULTURAL TECHNOLOGY INST
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Priority to CN 91106031 priority Critical patent/CN1053260A/en
Publication of CN1053260A publication Critical patent/CN1053260A/en
Pending legal-status Critical Current

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Abstract

Can send the color flame candles and the preparation technology thereof of required color flame when the invention provides a kind of lighting, it be by separate configurations through the burning core of oxidation promotor aqueous dispersions dip treating and the candle wick that constitutes through the color development core that chromogenic reagent-oxidation promotor solution impregnation is handled, with the candle body that adopts urethane or oxalic acid ester, fusing point to mix, cooperate with the system wax method of routine and to make color flame candles at the stearic acid more than 38 ℃ and synthetic resins.This technology simply, the candle kindling operating easily, make is good, pure, bright-coloured, the no gold zone of the flame color after lighting.

Description

Color flame candles and preparation technology thereof
The present invention relates to the decorative candle that a kind of daily life is used, can send the color flame candles of required color flame during particularly a kind of lighting.
Color flame candles comes out and has the years of development history so far.Flame color is pure, bright-coloured, nothing " gold zone " phenomenon but still can't reach after its point burns, and promptly lights the back flame core and still is the common yellowish-orange flame light of common candle.Although all being devoted to overcome above-mentioned shortcoming, taked some technical measures both at home and abroad,, all do not reach gratifying degree as U.S. Pat 4386904, the clear 50-34043 of Japanese Patent Laid, Chinese patent 86105053 etc.
The purpose of this invention is to provide that a kind of technology is simple, the preparation technology of maneuverable color flame candles, the candle kindling that it makes is good, pure, bright-coloured, the no gold zone of the flame color after lighting.
The object of the present invention is achieved like this: this color flame candles is constituting through the burning core of oxidation promotor aqueous dispersions dip treating and the chromogenic reagent of handling through chromogenic reagent-oxidation promotor solution impregnation by separate configurations; Candle body employing urethane or oxalic acid fat, fusing point mix at stearic acid more than 38 ℃ and synthetic resins.Its preparation technology operates according to the following steps:
A, preparation candle body: take by weighing urethane or oxalic acid fat 85-90 by weight percentage, fusing point is at the stearic acid 8-12 more than 38 ℃, synthetic resins 0.5-1.5, and the heating mixing is standby;
B, preparation color development core: twist thread or bunch dipping chromogenic reagent-oxidation promotor solution drying treatment with combustible;
Core is burnt in c, preparation: twist thread or bunch oxide impregnation promotor aqueous dispersions drying treatment with combustible;
D, the color development core of above-mentioned preparation, burning core are adopted side by side or the way of twining, fit together independently and make candle wick, system wax method routinely cooperates with the candle body and to make color flame candles.
Because the present invention adopts urethane or oxalic acid fat to make main fuel, it is bordering on colourless when burning, but its bad adhesion must be added an amount of fusing point in stearic acid more than 38 ℃ or stearyl alcohol, strengthens the formability and the model keeping character of candle.Yet only make the wax body with above-mentioned two kinds of raw materials, be difficult for lighting, therefore, the present invention adds an amount of synthetic resins and makes ignition dope, and the preferred vinyl acetate between to for plastic commonly used and the multipolymer of MALEIC ANHYDRIDE can obviously overcome and light difficult shortcoming in the prior art.The existing color flame candles of making relies on the inorganic salt that add metallic element in the candle body merely, or with this inorganic salt solution dipping candle wick, to reach the effect of coloured flame.But experimental results show that aforesaid method still can not eliminate the phenomenon of " do branch ", " gold zone ", color instability, impure, not bright-coloured when lighting fully.And the present invention puts forth effort on the structure of improving candle wick when improving candle body combustionproperty.Candle wick is designed to the burning core and the color development core of separate configurations, lays particular emphasis on the dip treating of burning core and color development core especially.Be " the doing branch ", the difficult problem of " gold zone " that overcome simple impregnating metal inorganic salt solution, it is oxidation promotor that the burning core adopts platinum catalyst powder, makes it sufficient combustion, and flame is bright, avoids the appearance of yellowish-orange.The color development core adopts the toner solutions that is added with oxidation promotor, can make the burning of color development core more abundant, and color development is more bright-coloured, stable, gorgeous.
The invention will be further described below in conjunction with embodiment.
Embodiment: the preparation of scarlet flame candle
A, preparation candle body: take by weighing 89 parts of urethane or oxalic acid esters, 10 parts of stearic acid, vinyl acetate between to for plastic-MALEIC ANHYDRIDE (weight ratio 1: 1) copolymer 1 part by weight, heating mixes.
B, preparation color development core: earlier with lithium chloride, polyvinyl alcohol, water by 12: 0.1: 87.9 ratio state heat to 80-85 ℃, make it to dissolve, be made into the chromogenic reagent lithium chloride solution; Produce oxidation promotor platinum catalyst powder-take by weighing 0.1 part of Platinic chloride by weight, 5 parts in micro mist aluminum oxide, 0.2 part of hydrazine again, 0.1 part in sodium hydroxide, 2200 parts in water mixes, place more than 24 hours, filter, isolate micro mist aluminum oxide and water, get 0.1 part in platinum catalyst powder.Then with platinum catalyst powder dispersing and mixing in lithium chloride solution, weight ratio is 0.1: 100, produces chromogenic reagent-oxidation promotor solution.Twist thread with 20 yarn cotton thread 20-30 roots at last or bunch floods in chromogenic reagent-oxidation promotor solution, in 120 ℃ dry down, promptly make the color development core.
C, preparation burning core: the oxidation promotor platinum catalyst powder dispersing and mixing that will make as stated above earlier is in water, its weight ratio is 1: 5000, make the oxidation promotor aqueous dispersions, twist thread or bunch oxide impregnation promotor aqueous dispersions with 20 yarn cotton thread 20-30 roots then, dry under 120 ℃, promptly make the burning core.
D, with the pitch of color development core with 25 millimeter one week, be wound in burning and make candle wick on the core, system wax method routinely cooperates with the candle body and to make color flame candles.
Utilization has the metal-salt of certain wavelength characteristic, as strontium nitrate, SODIUMNITRATE, barium oxide (or chromic oxide), cupric chloride, iron nitrate, nitrocalcite, magnesium nitrate (or antimony oxychloride) etc. as chromogenic reagent, or with arranging in pairs or groups more than two kinds, make chromogenic reagent-oxidation promotor solution impregnation color development core, can be made into the color flame candles that sends red, green, blue, brown, powder, pure, gorgeous color such as white when lighting.For making the easier differentiation of various color flame candles, can add common pigments and make the consistent colour candle of color that sends when lighting.

Claims (6)

1, a kind of by candle wick and the color flame candles formed of candle body, it is characterized in that candle wick by separate configurations through the burning core of oxidation promotor aqueous dispersions dip treating with through chromogenic reagent--the chromogenic reagent formation that the oxidation promotor solution impregnation is handled; Candle body employing urethane or oxalic acid fat, fusing point mix at stearic acid more than 38 ℃ and synthetic resins.
2, candle according to claim 1 is characterized in that described stearic acid can replace with the mixture of stearyl alcohol or stearic acid and stearyl alcohol.
3, a kind of preparation technology of color flame candles is characterized in that operating according to the following steps:
A, preparation candle body: take by weighing urethane or oxalic acid fat 85-90 by weight percentage, fusing point is at the stearic acid 8-12 more than 38 ℃, synthetic resins 0.5-1.5, and the heating mixing is standby;
B, preparation color development core: twist thread or bunch dipping chromogenic reagent-oxidation promotor solution drying treatment with combustible;
C, preparation burning core: twist thread or bunch oxide impregnation promotor aqueous dispersions drying treatment with combustible;
D, the color development core of above-mentioned preparation, burning core are adopted side by side or the way of twining, fit together independently and make candle wick, system wax method routinely cooperates with the candle body and to make color flame candles.
4, preparation technology according to claim 3 is characterized in that the preparation method of chromogenic reagent-oxidation promotor solution is as follows:
The preparation of a, toner solutions: choose lithium, strontium, barium, chromium, copper, iron, calcium, antimony, the oxymuriate of magnesium metal, nitrate, with one or two or more kinds combination wherein, by 12% and 87.9% water of its weight and 0.1% polyvinyl alcohol, be heated to 80-85 ℃, make it dissolving and promptly get toner solutions;
The preparation of b, oxidation promotor: with following raw material is Platinic chloride 0.1, micro mist aluminum oxide 5, hydrazine 0.2, sodium hydroxide 0.1, water 2200 mixings by weight, precipitate after 24 hours, filter, sedimentary micro mist aluminum oxide is gone out with water sepn, get 0.1 part in oxidation promotor platinum catalyst powder;
C, with above-mentioned oxidation promotor platinum catalyst powder dispersing and mixing in toner solutions, its weight percent is 0.1: 100, mixing promptly gets chromogenic reagent-oxidation promotor solution.
5, preparation technology according to claim 3 is characterized in that the oxidation promotor aqueous dispersions is made of in water oxidation promotor platinum catalyst powder dispersing and mixing, and its weight ratio is 1: 5000.
6, preparation technology according to claim 3 is characterized in that synthetic resins is that weight ratio is 1: 1 the vinyl acetate between to for plastic and the multipolymer of MALEIC ANHYDRIDE.
CN 91106031 1991-02-09 1991-02-09 Color flame candles and preparation technology thereof Pending CN1053260A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 91106031 CN1053260A (en) 1991-02-09 1991-02-09 Color flame candles and preparation technology thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 91106031 CN1053260A (en) 1991-02-09 1991-02-09 Color flame candles and preparation technology thereof

Publications (1)

Publication Number Publication Date
CN1053260A true CN1053260A (en) 1991-07-24

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Application Number Title Priority Date Filing Date
CN 91106031 Pending CN1053260A (en) 1991-02-09 1991-02-09 Color flame candles and preparation technology thereof

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CN (1) CN1053260A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103497846A (en) * 2013-09-30 2014-01-08 昆山市巴城镇顺拓工程机械配件厂 Color-flame candle
CN107523425A (en) * 2017-09-15 2017-12-29 李淑存 A kind of method for production of colorful flame candle

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103497846A (en) * 2013-09-30 2014-01-08 昆山市巴城镇顺拓工程机械配件厂 Color-flame candle
CN107523425A (en) * 2017-09-15 2017-12-29 李淑存 A kind of method for production of colorful flame candle

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