CN1095099A - Preparation method of multicolor flame candle - Google Patents
Preparation method of multicolor flame candle Download PDFInfo
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- CN1095099A CN1095099A CN 94102000 CN94102000A CN1095099A CN 1095099 A CN1095099 A CN 1095099A CN 94102000 CN94102000 CN 94102000 CN 94102000 A CN94102000 A CN 94102000A CN 1095099 A CN1095099 A CN 1095099A
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- heart yearn
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Abstract
The invention provides a kind of preparation method of multicolor flame candle.It forms main fuel by urethane, stearic acid, vinyl acetate-ethylene, the common resin of EVA etc.The heart yearn that combustion parts adopts the plant cotton to make, with plant ash, paper ash, each portion of coal ash, add water and soaked at normal temperatures 48 hours, add water by Platinic chloride, caustic soda, micro mist aluminum oxide, hydrazine hydrate again the cotton heart yearn was soaked 48 hours, make the burning heart yearn after drying.Color development partly adopts the burning heart yearn immersion corrosion of different metal oxides to making, and makes color development heart yearns such as red, green, white respectively.The core rope that two kinds of heart yearns are made ties up on worker's mould at last, injects the main fuel of heating, and Lian worker's mould constitutes color flame candle together after cooling.The present invention has that manufacture craft is simple, cost is low, flameholding, the yellow core of nothing, one's eyes drop millstones etc., and is safe and reliable, environmentally safe.
Description
The present invention relates to colour candle, particularly a kind of preparation method of multicolor flame candle.
The technology of preparing of color flame candles was early reported at home and abroad the patent documentation several years ago.Employing paraffin that has in these technology or paraffin wax type incendiary material are main fuel, add some kinds of metal chlorides as chromogenic reagent.As the patent No. is such technology of report in [USP4,386,904, the clear 611-16996 of Japanese Patent], because its paraffin is long carbochain hydro carbons, the temperature of luminous flame district and air contact part is lower during burning, and the oxidation rate of carbon granules is slow and can not fully burn.And the small grain of unoxidized heat makes flame produce very dark gold zone when stopping in flame, and the color that causes chromogenic reagent to produce is difficult to cover gold zone, has a strong impact on color effect.In addition, also be prone to prosperous cigarette during the burning of this color flame candle, do branch, quality problems such as shed tears.For addressing these problems, there are many people to develop in recent years with non-paraffin wax type incendiary material.As the patent No. is in the patent documentation of CN86105053A and CN8910615.6, and successively disclosing a kind of is the preparation method of the flame candle of main fuel with the urethane.Though this method can solve the sort of gold zone of traditional candle, smolders, do branch, phenomenon such as shed tears, but in the preparation owing to do not grasp the solvent temperature of urethane well, do not adopt an effective measure yet and continue its solubleness, therefore, when the temperature on average of weather reaches 30 degree when above, this product one dispatches from the factory will moistening profit, thereby has influenced the appearance of product.In addition, because its burning heart yearn is dealt with improperly, cause combustionvelocity too slow, can not maintain an equal level with the same heart yearn combustionvelocity of urethane upper surface, face rings the practicality of product.Defective such as its complex manufacturing technology, cost height causes this patented technology still to can not get effective enforcement so far in addition.
The objective of the invention is to overcome above-mentioned deficiency, provide a kind of manufacture craft simple, have attractive appearance, can effectively slow down the urethane combustionvelocity, the preparation method of the color flame candle that the burning of guaranteeing heart yearn and urethane combustionvelocity are fair.
Technical solution of the present invention is: based on urethane, be mixed with several raw materials composition main fuels such as senior stearic acid, form the color development part with multiple metal chloride, form oxygenant by multiple mixing raw material, wherein main fuel is by urethane 93%, stearic acid 3%, vinyl acetate-ethylene, dehydration apple oxalic anhydride copolymerization 2%, EVA copolymer resins 2% constitutes.Combustion parts is after adopting the plant cotton to be processed into heart yearn, again with 1 part of natural grass wood ash, and 1 part in paper ash, 1 part of coal ash, adds water and soaked 48 hours for 3 liters, as the oxidation contact first time of heart yearn by totally 5 kilograms.Adopt Platinic chloride 0.1 gram, caustic soda 13 grams, micro mist aluminum oxide 40 grams, 30 milliliters of hydrazine hydrates, 3000 milliliters in water carries out the oxidation second time to the cotton heart yearn and soaks, and treats to dry after 48 hours, and making the cotton rope promptly becomes the burning heart yearn.Color development partly is the burning heart yearn that will make, adopt different metal chlorides that it is corroded, after making multicolour such as red, green, white respectively, the cotton rope is surrounded burning core as acknowledgment copy by left and right directions with the color development core with hand rib machine, worker's mould of gypsum manufacturing is fastened the core rope again main fuel heating 60 degree are injected worker's mould, Lian worker's mould constitutes a broken colour candle together after cooling.
The burning heart yearn of color development part of the present invention, comprise multicolour such as red, green, white, wherein by lithium chloride 3.5 grams, Preparation of Metallic Strontium 2 grams, polyvinyl alcohol 1.2 grams, platinum matchmaker powder 0.005 gram, red the color producing species of 100 milliliters of compositions of water, wherein platinum melts matchmaker's powder: be made up of platinum chloride 0.0005 gram, caustic soda 5 grams, 30 milliliters of hydrazine hydrates, micro mist aluminum oxide 30 grams.By cupric chloride 60 grams, 100 milliliters in water, platinum melt matchmaker's powder 0.001 gram, and the combustion of three chloroethenes is formed green the color producing species for 85 milliliters.Form white the color producing species for 50 milliliters by antimony oxychloride 40 grams, vanadium chloride 15 grams, pyroxylin (e) cement 5 grams, acetic acid formicester.Form the cotton of different color by three assembly sides respectively and restrict, carried out immersion corrosion at normal temperatures 2 hours, then the cotton rope of handling well is dried, promptly become the burning heart yearn that can send different color.
The invention has the advantages that: in main fuel, increase the lipid acid of certain proportioning, protect shape EVA copolymer resins and strengthen its molten point.Adopt vinyl acetate-ethylene to make the present invention not only inflammable but also plasticity arranged.Have characteristics such as manufacture craft is simple, cost is low, flameholding, the yellow core of nothing, one's eyes drop millstones, the dried branch of nothing.The present invention measures through environmental administration, meets the environmentally-friendly sanitary standard.Safe and reliable, can not pollute environment.
Embodiment:
The preparation of main fuel: by urethane 93%, stearic acid 3%, vinyl acetate-ethylene, dehydration apple oxalic anhydride copolymerization 2%, it is standby that EVA copolymer resins 2% mixes the back.
Combustion parts is after adopting the plant cotton to be processed into heart yearn, again with 1 part of natural grass wood ash, and 1 part in paper ash, 1 part of coal ash, adds 3 liters in water and soaks the each oxidation contact as heart yearn in 48 hours by totally 5 kilograms, adopt Platinic chloride 0.1 gram, caustic soda 13 grams, micro mist aluminum oxide 40 grams, 30 milliliters of hydrazine hydrates, 3000 milliliters in water, the cotton heart yearn is carried out the oxidation second time soak, treat to dry after 48 hours, making the cotton rope promptly becomes the burning heart yearn.
The preparation of color development part: (with red example)
With the burning heart yearn that makes, employing is by lithium chloride 3.5 grams, Preparation of Metallic Strontium 2 grams, polyvinyl alcohol 1.2 grams, platinum matchmaker powder 0.005 gram, the metal chloride of 100 milliliters of compositions of water corrodes it, wherein platinum melts matchmaker's powder by platinum chloride 0.0005 gram, caustic soda 5 gram, 30 milliliters of hydrazine hydrates, micro mist aluminum oxide 30 are restrained.
Green the color producing species, by cupric chloride 60 grams, 100 milliliters in water, platinum melt matchmaker's powder 0.001 gram, and 85 milliliters of three chloroethenes combustions need not add thermal etching and dry the cotton rope after 2 hours.
White the color producing species: form for 50 milliliters by antimony oxychloride 40 gram, vanadium chloride 15 grams, pyroxylin (e) cement 5 grams, acetic acid formicester, with above-mentioned identical preparation method to its immersion corrosion.
After above work finished, the color development core is surrounded burn heart yearn standby with hand rib machine by left and right directions in the cotton rope for preparing.To the core rope be fastened with worker's mould of gypsum manufacturing at last, and again main fuel heating 60 degree be injected plaster mould, Lian worker's mould and candle constitute product together after cooling.
Claims (2)
1, a kind of preparation method of colorful flame candle, based on urethane, be mixed with several raw materials composition main fuels such as senior stearic acid, form the color development part with multiple metal chloride, form oxygenant by multiple mixing raw material, it is characterized in that: main fuel is by urethane 93%, stearic acid 3%, vinyl acetate-ethylene, dehydration apple oxalic anhydride copolymerization 2%, EVA copolymer resins 2%, combustion parts is after adopting the plant cotton to be processed into heart yearn, again with 1 part of natural grass wood ash, 1 part in paper ash, 1 part of coal ash, totally 5 kilograms, adding water soaked 48 hours for 3 liters, the oxidation contact first time as heart yearn, adopt Platinic chloride 0.1 gram, caustic soda 13 grams, micro mist aluminum oxide 40 grams, 30 milliliters of hydrazine hydrates, 3000 milliliters in water carries out the oxidation second time to the cotton heart yearn and soaks, and treats to dry after 48 hours, make the cotton rope and promptly become the burning heart yearn, color development partly is the burning heart yearn that will make, and adopts different metal chlorides that it is corroded, and makes red respectively, green, after the multicolour such as white, the cotton rope is surrounded burning core as acknowledgment copy by left and right directions with the color development core with hand rib machine, worker's mould of gypsum manufacturing is fastened the core rope again, main fuel heating 60 degree are injected worker's mould, Lian worker's mould constitutes a broken colour candle together after cooling.
2, preparation method of multicolor flame candle according to claim 1, it is characterized in that: the burning heart yearn of said color development part, comprise red, green, multicolour such as white, wherein by lithium chloride 3.5 grams, Preparation of Metallic Strontium 2 grams, polyvinyl alcohol 1.2 grams, platinum matchmaker powder 0.005 gram, red the color producing species of 100 milliliters of compositions of water, by cupric chloride 60 grams, 100 milliliters in water, platinum melt matchmaker's powder 0.001 gram, the combustion of three chloroethenes is formed green the color producing species for 85 milliliters, by antimony oxychloride 40 grams, vanadium chloride 15 grams, pyroxylin (e) cement 5 grams, 50 milliliters of acetic acid formicesters are formed white the color producing species, and the cotton rope with three kinds of different colors making carried out immersion corrosion 2 hours at normal temperatures, then the cotton rope of handling well is dried, promptly become the burning heart yearn that can send different color.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 94102000 CN1095099A (en) | 1994-03-15 | 1994-03-15 | Preparation method of multicolor flame candle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 94102000 CN1095099A (en) | 1994-03-15 | 1994-03-15 | Preparation method of multicolor flame candle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1095099A true CN1095099A (en) | 1994-11-16 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 94102000 Pending CN1095099A (en) | 1994-03-15 | 1994-03-15 | Preparation method of multicolor flame candle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1095099A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2002099022A1 (en) * | 2001-06-04 | 2002-12-12 | Novaflame Pty Ltd | Candles with coloured flames |
| US6712865B2 (en) | 2002-07-12 | 2004-03-30 | Xin Lu | Colored flame candle and manufacture thereof |
-
1994
- 1994-03-15 CN CN 94102000 patent/CN1095099A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2002099022A1 (en) * | 2001-06-04 | 2002-12-12 | Novaflame Pty Ltd | Candles with coloured flames |
| AU2002257373B2 (en) * | 2001-06-04 | 2005-05-12 | Novaflame Pty Ltd | Candles with coloured flames |
| US6712865B2 (en) | 2002-07-12 | 2004-03-30 | Xin Lu | Colored flame candle and manufacture thereof |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C01 | Deemed withdrawal of patent application (patent law 1993) | ||
| WD01 | Invention patent application deemed withdrawn after publication |