CN105310936B - A kind of freckle removing and whitening face cream and preparation method thereof - Google Patents
A kind of freckle removing and whitening face cream and preparation method thereof Download PDFInfo
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Abstract
The invention belongs to cosmetic technical fields, and in particular to a kind of freckle removing and whitening face cream and preparation method thereof.The freckle removing and whitening face cream includes propylene glycol, C20-22 alcohol phosphate, glycerine, hyaluronic acid, isononanoic acid ethylhexyl, dimethyl silicone polymer, acrylic acid（Ester）Class/acrylamide copolymer, Butyrospermum parkii fruit fat, mulberry-leaf extract, ginkgo biloba p.e, Rhizoma Gastrodiae extract, Herba Paederiae extract etc..Freckle removing and whitening face cream good penetrability provided by the invention easily absorbs, effective replenishing water and preserving moisture, reduces pigmentation, lightens the stain, whitening.
Description
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of freckle removing and whitening face cream and preparation method thereof.
Background technology
All the time, whitening spot-removing is all the topic that people earnestly pay close attention to.Color spot is always the puzzlement mankind for a long time
One big problem of skin, in particular with the growth at age, the probability that color spot occurs in skin also obviously increases.The original that color spot is formed
Because mainly since the distribution of human epidermal lower layer is there are many chromatophore, catalysis oxidation of the chromatophore through internal tyrosinase and
Form melanin, in skin melanin increase and uneven aggregation and form color spot.In addition the reason of different color spot type formation
Also it is different, if freckle is the reason of heredity mostly, chloasma and cyasma are because Endocrine and metabolism disorder is made mostly
At, sunburn is then the influence due to ultraviolet light, senile plaque be due to skin and internal metabolism of pigment slowly and caused by.To
Achieve the purpose that whitening, nti-freckle, following two main paths can be passed through：One is the generations for preventing pigment；It is another then be promote
The chromocrinia of generation is set to go out in vitro.The skin-color that needs to inhibit to generate or excrete is known as melanin, lipofuscin and Ye Hong
Element.Melanin and phylloerythrin (also known as carrot element) are physiologic agents, there is certain physiological function, harmless；And fat is brown
It is plain then be harmful substance.According to the pigmented influence degree of human skin, inhibition is beautiful with melanin is excluded
In vain, the main method that cosmetics use.
World cosmetics expert has been devoted to develop various whitening spot-removing class cosmetics, it is current market sales of such
Nearly thousand kinds of cosmetics solve the problems, such as skin splash to a certain extent, but due to the limitation of scientific and technological level, many whitenings are dispelled
The safety of spot agent only could be determined gradually by long-term use, therefore whitening and freckle-removing product is while bringing people U.S.
Also many hidden dangers are brought.For example, whitening and freckle-removing product on the market contain more vitamin C, tartaric acid, ursin etc. at
Point, there is also certain disadvantages while generating whitening spot-removing effect, Vitamin C Stability is poor, and preparation process is easy to lose work
Property, it is therefore desirable to carry out specially treated；Fruit acid concentration is excessively high to cause red swelling of the skin, allergy even to fester；Ursin has height
The photosensitivity of degree needs to add a large amount of sun-screening agents in the product, aggravates skin burden, accelerates skin aging.With life water
Flat raising, people for skin care item it is diversified require it is higher and higher, it is also higher and higher to the quality requirements of skin care item, need
Safe, mild, effective new product of more high-quality is provided.
Invention content
For overcome the deficiencies in the prior art, the purpose of the present invention is to provide a kind of freckle removing and whitening face cream, permeability
It is good, it easily absorbs, whitening composition is effectively sent to skin deep layer, pigment is inhibited to generate, promote pigment to decompose, lighten the stain, it is beautiful
In vain, keep skin glosser moving.To achieve the goals above, technical scheme is as follows：
A kind of freckle removing and whitening face cream includes the component of following weight percent meter：Propylene glycol 2~4%, C20-22 alcohol phosphoric acid
Ester 1~2%, glycerine 4~8%, hyaluronic acid 4~8%, isononanoic acid ethylhexyl 1~2%, dimethyl silicone polymer 1~2%,
Acrylic acid (ester) class/acrylamide copolymer 0.08~1%, Butyrospermum parkii fruit fat 2~4%, mulberry-leaf extract 4~8%, ginkgo
Leaf extract 4~8%, Rhizoma Gastrodiae extract 2~6%, Millettia extract 2~6%, natrium adetate 0.08~1%, oxybenzene first
Ester 0.04~1%, ethyl hydroxy benzoate 0.02~1%, triethanolamine 1~4%, essence 0.008~0.2% and water 45~65%.
In the technical solution of the present invention, the humectant properties and human body for the unsaturated fatty acid that the Butyrospermum parkii fruit fat contains
The sebaceous glands of skin is very much like, is natural emollient, has extraordinary penetration, can quickly be penetrated into after contact skin
To skin bottom, skin water loss can be prevented, increases skin defence capability and compliance.
The mulberry-leaf extract can be removed effectively rich in flavonoid substances, ecdysterone, rutin sophorin, the ingredients such as alkaloid
Free radical prevents oxidative damage, improves the activity of internal superoxide dismutase, prevents the generation of internal harmful substance, inhibits junket ammonia
The activity of sour enzyme inhibits the formation of pigment, to reduce pigmentation, generates freckle removing and whitening, the effect of anti-aging.
The ginkgo biloba p.e is rich in brass glycoside, terpene lactones, organic acid, separating Ginkgo phenolic acids, alkyl phenol, alkyl phenol
The ingredients such as acid, inoxidizability is strong, improves microcirculation, so as to improve the texture, color and luster and brightness of skin.
The Rhizoma Gastrodiae extract is rich in Gastrodin, vitamin A, sterols, vanillyl alcohol, vanillin, gastrodia elata polysaccharide etc.
There is calmness, hypnosis, the effect of anti-aging there is apparent skin to support, crease-resistant and color spot of dispelling for ingredient, Central nervous system
Effect.
The Millettia extract is rich in the ingredients such as milletol, irony, terpene, campesterol, stigmasterol, sitosterol,
With increasing hemoglobin, reducing blood viscosity, the effect of microcirculation, blood-enriching face-nourishing is promoted to keep skin ruddy, it is glossy.
Freckle removing and whitening face cream of the present invention contains Butyrospermum parkii fruit fat, mulberry-leaf extract, ginkgo biloba p.e, Rhizoma Gastrodiae extraction
A variety of natural plant compositions such as object, Millettia extract, in conjunction with propylene glycol of the present invention, C20-22 alcohol phosphate, glycerine, transparent
The basic materials such as matter acid, dimethyl silicone polymer, acrylic acid (ester) class/acrylamide copolymer, each component collaboration so that this hair
Bright freckle removing and whitening face cream good penetrability easily absorbs, deep water supplement moisturizing, nourishes maintenance skin, enhances skin elastic and improves dry
Dry, relaxation repairs impaired or innutritive cell；Nti-freckle ingredient is effectively sent to skin deep layer simultaneously, inhibits color
Element generates, and promotes pigment to decompose, lightens the stain, whitening, keep skin glosser moving.
The present invention also provides the preparation methods of above-mentioned freckle removing and whitening face cream, specifically include following steps：
S1, by C20-22 alcohol phosphate, isononanoic acid ethylhexyl, dimethyl silicone polymer, Butyrospermum parkii fruit fat, oxybenzene first
Ester, ethyl hydroxy benzoate are placed in oil phase pot, are heated to 80~85 DEG C, and material A is obtained after stirring and dissolving is complete, and heat preservation is spare；
S2, Jiang Shui, propylene glycol, glycerine, hyaluronic acid, natrium adetate be added water phase pot in, be heated to 80~90 DEG C it is molten
Solution is complete, is then pumped into warmed-up emulsifying pot, opens stirring, then material A is slowly pumped into emulsification pot, homogeneous 10
Cool down after~20min；
S3,60 DEG C are down to, acrylic acid (ester) class/acrylamide copolymer and triethanolamine, 5~10min of homogeneous is added；
S4, continue to be cooled to 45 DEG C, mulberry-leaf extract, ginkgo biloba p.e, Rhizoma Gastrodiae extract, Millettia extract is added
It is stirred until homogeneous, sampling Detection, discharges after qualified up to freckle removing and whitening face cream with essence.
Further, the rotating speed of the homogeneous is 2500~3500rpm.
Further, the mixing speed of the stirring is 45~55r/min.
Further, the preparation method of the mulberry-leaf extract is：It is crushed after taking mulberry leaf cleaning, drying, crosses 90-100 mesh
Sieve is added 6-10 times of its weight and measures the ethyl alcohol that volume fraction is 70-85%, impregnates 3-6 hours, ultrasonic at a temperature of 45-65 DEG C
Twice, 30-60 minutes each, supersonic frequency 25-35kHz is filtered, merging filtrate, when filtrate decompression is concentrated into 60 DEG C for extraction
Relative density be 1.05-1.25 medicinal extract to get.
Further, the preparation method of the ginkgo biloba p.e is：Ginkgo leaf is taken, impurity, crushed after being dried, mistake are washed away
60-80 mesh sieves, and obtains coarse powder；Coarse powder is placed in supercritical carbon dioxide extraction apparatus, coarse powder total amount 30-45% volumes point are added
Number is the ethyl alcohol of 70-85%, and regulation and control carbon dioxide flow is 15~20L/h, and extracting pressure is 15~20MPa, and extraction temperature is
40~60 DEG C, extraction time be 1.5~2h, decompression separation to get.
Further, the preparation method of the Rhizoma Gastrodiae extract is：Rhizoma Gastrodiae is taken, impurity is washed away, crushed after being dried crosses 60-
80 mesh sieve, and 6-8 times of Rhizoma Gastrodiae total weight is added and measures the ethyl alcohol that volume fraction is 60-80%, Microwave Extraction 8-15 minutes, microwave power
For 240-300W, Extracting temperature is 45-65 DEG C, filtering, and it is 1.20-1.25's that filtrate decompression, which is concentrated at 60 DEG C and surveys relative density,
Medicinal extract to get.
Further, the preparation method of the Millettia extract is：Caulis Spatholobi is taken, impurity, crushed after being dried, mistake are washed away
80-100 mesh sieves, and 8-10 times of medicinal material total weight is added and measures the ethyl alcohol that volume fraction is 60-80%, adds Caulis Spatholobi total amount 0.8-
1.2% cellulase, extracts 1-2 hours at 38-45 DEG C, then in 85-95 DEG C of refluxing extraction 1-2 hours, filtering, filtrate
Be concentrated under reduced pressure into the medicinal extract that relative density at 60 DEG C is 1.10-1.25 to get.
Therefore, compared with prior art, advantage of the invention is that：
(1) freckle removing and whitening face cream of the present invention contains Butyrospermum parkii fruit fat, mulberry-leaf extract, ginkgo biloba p.e, Rhizoma Gastrodiae and carries
It takes a variety of natural plant active components such as object, Millettia extract, deep water supplement moisturizing to nourish maintenance skin, it is dry to improve skin
Dry, relaxation, while nti-freckle ingredient is effectively sent to skin deep layer, inhibit pigment to generate, pigment is promoted to decompose, desalinates color
Spot, whitening keep skin glosser moving, high resilience, and it is slight to promote skin year.
(2) freckle removing and whitening face cream safety and stability of the present invention, good penetrability easily absorb, clearly not sticky using rear skin；And
The preparation method of freckle removing and whitening face cream of the present invention is simple, and condition is controllable, process stabilizing, can be applicable.
Specific implementation mode
The present invention is further described below by way of specific implementation mode, but the present invention is not limited only to following embodiment.?
It in the scope of the present invention or is not departing from present disclosure, in spirit and scope, crease-resistant face cream of the present invention is being carried out
It is suitably modified, replaces the identical component of effect, it will become apparent to those skilled in the art that they are considered as wrapping
It includes within the scope of the present invention.
The information such as the producer of part material and article No. are as follows in freckle removing and whitening face cream described in the embodiment of the present invention：
The raw material and proportioning (by weight percentage) of 1~2 freckle removing and whitening face cream of the embodiment of the present invention 2,3 and comparative example are such as
Under：
The embodiment of the present invention 2, the preparation method of 3 freckle removing and whitening face creams are as follows：
S1, by C20-22 alcohol phosphate, isononanoic acid ethylhexyl, dimethyl silicone polymer, Butyrospermum parkii fruit fat, oxybenzene first
Ester, ethyl hydroxy benzoate are placed in oil phase pot, are heated to 80 DEG C, and material A is obtained after stirring and dissolving is complete, and heat preservation is spare；
S2, Jiang Shui, propylene glycol, glycerine, hyaluronic acid, natrium adetate are added in water phase pot, are heated to 80 DEG C and have dissolved
Entirely, it is then pumped into warmed-up emulsifying pot, opens stirring, then material A is slowly pumped into emulsification pot, homogeneous 20min
After cool down；
S3,60 DEG C are down to, acrylic acid (ester) class/acrylamide copolymer and triethanolamine, homogeneous 10min is added；
S4, continue to be cooled to 45 DEG C, mulberry-leaf extract, ginkgo biloba p.e, Rhizoma Gastrodiae extract, Millettia extract is added
It is stirred until homogeneous, sampling Detection, discharges after qualified up to freckle removing and whitening face cream with essence.
Wherein, the rotating speed of the homogeneous is 2500rpm；The mixing speed of the stirring is 45r/min；
The preparation method of the mulberry-leaf extract is：It is crushed after taking mulberry leaf cleaning, drying, crosses 90 mesh sieve, its weight 8 is added
Times amount volume fraction be 75% ethyl alcohol, impregnate 4 hours, at a temperature of 45 DEG C ultrasonic extraction twice, 30 minutes every time, supersonic frequency
Rate is 30kHz, filtering, merging filtrate, when filtrate decompression is concentrated into 60 DEG C relative density be 1.05 medicinal extract to get；
The preparation method of the ginkgo biloba p.e is：Ginkgo leaf is taken, impurity is washed away, crushed after being dried is crossed 60 mesh sieve, obtained
Coarse powder；Coarse powder is placed in supercritical carbon dioxide extraction apparatus, the ethyl alcohol that 45% volume fraction of coarse powder total amount is 75% is added,
Regulation and control carbon dioxide flow is 15L/h, and extracting pressure 15MPa, extraction temperature is 45 DEG C, extraction time 2h, decompression separation,
To obtain the final product；
The preparation method of the Rhizoma Gastrodiae extract is：Rhizoma Gastrodiae is taken, impurity is washed away, crushed after being dried crosses 60 mesh sieve, day is added
The ethyl alcohol that 6 times of amount volume fractions of numb total weight are 75%, Microwave Extraction 10 minutes, microwave power 240W, Extracting temperature 45
DEG C, filtering, filtrate decompression be concentrated at 60 DEG C survey relative density be 1.20 medicinal extract to get；
The preparation method of the Millettia extract is：Caulis Spatholobi is taken, impurity is washed away, crushed after being dried is crossed 80 mesh sieve, added
Enter the ethyl alcohol that 8 times of amount volume fractions of medicinal material total weight are 75%, the cellulase of Caulis Spatholobi total amount 1% is added, at 45 DEG C
Extraction 2 hours, then in 85 DEG C of refluxing extractions 2 hours, filtering, filtrate decompression is concentrated into the leaching that relative density is 1.10 at 60 DEG C
Cream to get.
The preparation method of comparative example 1~2 refers to the preparation method of the embodiment of the present invention.
Through examining 2~3 product of embodiment to meet the pertinent regulations requirement of QB/T1857-2013, sense index (color and luster, perfume (or spice)
Gas, structure) meet industry regulation, physical and chemical index (pH, heat-resisting, cold-resistant, active matter) meets industry regulation.
Test example one, product effect assessment
First part：
One, trial target：Freckle removing and whitening face cream prepared by embodiment 2 and comparative example 1~2
Two, tested crowd's data and grouping：90 skin healths, the tested volunteer of women of no skin disease allergies, 35
~55 years old, average age 40 years old was randomly divided into 3 groups, every group of 30 people.
Three, test method：The freckle removing and whitening face cream prepared by embodiment 2 and comparative example 1~2, observation and sense are used respectively
By using effect.Application method：After subject cleans face, suitable face cream is applied to face skin in the palm of the hand, uniformly point, gently
Massage is each using once, adhering to using one month daily morning and evening up to fully absorbing, and at least checks weekly once with understanding
Whether there is or not whole body and local adverse reactions, and record result in detail.
Four, test assessment result is as follows：
(one month) on probation feedback conclusive table of 1 embodiment of table, 2 freckle removing and whitening face cream
(one month) on probation feedback conclusive table of 2 comparative example of table, 1 freckle removing and whitening face cream
(one month) on probation feedback conclusive table of 3 comparative example of table, 2 freckle removing and whitening face cream
By upper table 1~3 it is found that the freckle removing and whitening face cream of the embodiment of the present invention 2 liking and approving by subject, tested
Person indicates freckle removing and whitening face cream good penetrability of the present invention, easily absorbs, moisturizing, moistening effect clearly not sticky using rear face
Good, nti-freckle, whitening promotes skin metabolism, makes skin smooth, flexible.And comparative example 1,2 face creams lack the present invention and dispel
Speckles, beautification and white face cream formula in certain components, permeability, freckle removing and whitening, moisturizing, moisturizing effect be not so good as embodiment 2, say
Bright inventive formulation ingredient mutually cooperates with, and plays better effect.Simultaneously whole subjects do not occur pruitus, shouting pain,
The allergic phenomenas such as redness, therefore, freckle removing and whitening face cream of the present invention are mildly safe, can be used for a long time.
The above-described embodiments merely illustrate the principles and effects of the present invention, and is not intended to limit the present invention.It is any ripe
The personage for knowing this technology can all carry out modifications and changes to above-described embodiment without violating the spirit and scope of the present invention.Cause
This, institute is complete without departing from the spirit and technical ideas disclosed in the present invention by those of ordinary skill in the art such as
At all equivalent modifications or change, should by the present invention claim be covered.
Claims (1)
1. a kind of freckle removing and whitening face cream, which is characterized in that be grouped as by the group of following weight percent meter：Propylene glycol 2%, C20-
22 alcohol phosphates 1%, glycerine 4%, hyaluronic acid 4%, isononanoic acid ethylhexyl 2%, dimethyl silicone polymer 2%, acrylic acid
(ester) class/acrylamide copolymer 1%, Butyrospermum parkii fruit fat 4%, mulberry-leaf extract 4%, ginkgo biloba p.e 4%, Rhizoma Gastrodiae carry
Take object 4%, Millettia extract 2%, natrium adetate 0.6%, methyl hydroxybenzoate 0.4%, ethyl hydroxy benzoate 0.4%, triethanolamine
2%, essence 0.06%, surplus are water；
The preparation method of the freckle removing and whitening face cream is as follows：
S1, by C20-22 alcohol phosphate, isononanoic acid ethylhexyl, dimethyl silicone polymer, Butyrospermum parkii fruit fat, methyl hydroxybenzoate,
Ethyl hydroxy benzoate is placed in oil phase pot, is heated to 80 DEG C, and material A is obtained after stirring and dissolving is complete under 45r/min speed, and heat preservation is standby
With；
S2, Jiang Shui, propylene glycol, glycerine, hyaluronic acid, natrium adetate are added in water phase pot, are heated to 80 DEG C of dissolvings completely, so
It is pumped into afterwards in warmed-up emulsifying pot, opens stirring, then material A is slowly pumped into emulsification pot, under 2500rpm rotating speeds
Cool down after matter 20min；
S3,60 DEG C are down to, is added acrylic acid (ester) class/acrylamide copolymer and triethanolamine, homogeneous under 2500rpm rotating speeds
10min；
S4, continue to be cooled to 45 DEG C, mulberry-leaf extract, ginkgo biloba p.e, Rhizoma Gastrodiae extract, Millettia extract and perfume (or spice) is added
Essence is stirred until homogeneous under 45r/min speed, sampling Detection, is discharged after qualified up to freckle removing and whitening face cream；
The preparation method of the mulberry-leaf extract is：It is crushed after taking mulberry leaf cleaning, drying, crosses 90 mesh sieve, 8 times of amounts of its weight are added
The ethyl alcohol that volume fraction is 75% impregnates 4 hours, and twice, 30 minutes every time, supersonic frequency was ultrasonic extraction at a temperature of 45 DEG C
30kHz, filtering, merging filtrate, when filtrate decompression is concentrated into 60 DEG C relative density be 1.05 medicinal extract to get；
The preparation method of the ginkgo biloba p.e is：Ginkgo leaf is taken, impurity is washed away, crushed after being dried is crossed 60 mesh sieve, obtained slightly
Powder；Coarse powder is placed in supercritical carbon dioxide extraction apparatus, the ethyl alcohol that 45% volume fraction of coarse powder total amount is 75% is added, adjusts
Control carbon dioxide flow is 15L/h, and extracting pressure 15MPa, extraction temperature is 45 DEG C, extraction time 2h, decompression separation, i.e.,
?；
The preparation method of the Rhizoma Gastrodiae extract is：Rhizoma Gastrodiae is taken, impurity is washed away, crushed after being dried crosses 60 mesh sieve, it is total that Rhizoma Gastrodiae is added
The ethyl alcohol that 6 times of amount volume fractions of weight are 75%, Microwave Extraction 10 minutes, microwave power 240W, Extracting temperature is 45 DEG C, mistake
Filter, filtrate decompression be concentrated at 60 DEG C survey relative density be 1.20 medicinal extract to get；
The preparation method of the Millettia extract is：Caulis Spatholobi is taken, impurity is washed away, crushed after being dried crosses 80 mesh sieve, medicine is added
The ethyl alcohol that 8 times of amount volume fractions of material total weight are 75%, adds the cellulase of Caulis Spatholobi total amount 1%, 2 is extracted at 45 DEG C
Hour, then in 85 DEG C of refluxing extractions 2 hours, filtering, filtrate decompression is concentrated into the medicinal extract that relative density is 1.10 at 60 DEG C, i.e.,
?.
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| CN103393568A (en) * | 2013-07-28 | 2013-11-20 | 娇时化妆品（杭州）有限公司 | Whitening and freckle-removing cream |
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| CN103393568A (en) * | 2013-07-28 | 2013-11-20 | 娇时化妆品（杭州）有限公司 | Whitening and freckle-removing cream |
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| "天麻多糖面霜的制备及临床应用观察";杜江等;《贵阳中医学院学报》;19951231;第17卷(第1期);第62页左栏倒数第2行至右栏第11行和第63页左栏第1-16行 * |
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