CN105296177B - A kind of multifunctional meter surface cleaning agent and preparation method thereof - Google Patents

A kind of multifunctional meter surface cleaning agent and preparation method thereof Download PDF

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Publication number
CN105296177B
CN105296177B CN201510650059.XA CN201510650059A CN105296177B CN 105296177 B CN105296177 B CN 105296177B CN 201510650059 A CN201510650059 A CN 201510650059A CN 105296177 B CN105296177 B CN 105296177B
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cleaning agent
multifunctional meter
reaction kettle
ether
dissolving
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CN105296177A (en
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张京
夏泉
温霖
李燕杰
李永强
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Guozhen Health Science and Technology (Beijing) Co., Ltd.
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Guozhen Health Science And Technology (beijing) Co Ltd
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Abstract

A kind of multifunctional meter surface cleaning agent and preparation method thereof, the composition of the surface cleaner are:Surfactant, 1~30 parts by weight;D limonenes, 0.1~4 parts by weight;Protease, 0.1~2 parts by weight;Bamboo-leaves flavones, 0.0055~0.022 parts by weight;Auxiliary agent, 0.1~10 parts by weight;Water, 10~90 parts by weight.The multifunctional meter surface cleaning agent is the product that conventional multifunction detergent and kitchen heavy oil pollution cleanser integrate, using surfactant, organic solvent, enzyme preparation reasonable compounding, reaching reduces alkalinity, synergistic clean effect.

Description

A kind of multifunctional meter surface cleaning agent and preparation method thereof
Technical field
The present invention relates to a kind of detergent, and in particular to a kind of hard surface multifunctional detergent.
Background technology
The multifunction detergent and kitchen greasy dirt that domestic and international market has occurred at present are net, and majority is with anion, nonionic table Face activating agent, alkali additive, based on organic solvent, it is impossible to have both that heavy oil is dirty and floor, furniture, the cleaning work(of automobile interior exterior decorations etc. Energy.Heavy oil pollution cleanser is strong basicity, human body, environment is harmful to, corrosivity only for the cleaning of weight greasy surfaces in kitchen It is extremely strong.And general multifunction detergent is only the simple superposition of a variety of surfactants, is suitable for the general clear of household hard surface Clean dose, counterweight greasy dirt effect is very poor.
Invention content
The present invention provides the product that a kind of multifunction detergent and kitchen heavy oil pollution cleanser integrate, and is lived using surface Property agent, organic solvent, enzyme preparation reasonable compounding, reaching reduces alkalinity, synergistic clean effect.
To achieve the above object, the present invention provides following technical solution:
A kind of multifunctional meter surface cleaning agent is into being grouped as by following proportioning:
A kind of multifunctional meter surface cleaning agent is into being grouped as by following proportioning:
Multifunctional meter surface cleaning agent as described above, it is preferable that the organic solvent is propylene glycol monomethyl ether, dipropylene glycol first Ether, propylene-glycol ethyl ether, butyl glycol ether, butyl and/or 3-Methoxy-3-methyl-1-butanol.
Multifunctional meter surface cleaning agent as described above, it is preferable that the surfactant is nonionic surfactant, the moon Ionic surface active agent, cationic surfactant and/or zwitterionic surfactant.
Multifunctional meter surface cleaning agent as described above, it is preferable that the nonionic surfactant is triethanolamine, fat Alcohol polyoxyethylene ether, alkyl glycosides, nonylphenol polyoxyethylene ether and/or isomery fatty alcohol polyoxyethylene ether;
Anion surfactant for sulfonic acid, fatty alcohol polyoxyethylene ether sulfate sodium salt, fatty acid methyl ester sulfonate, Alkenyl sulfonate, lauryl sodium sulfate and/or aliphatic acid polyethenoxy ether phosphate;
Cationic surfactant is dodecyl benzyl dimethyl ammonium chloride and/or benzalkonium bromide;
Zwitterionic surfactant is dodecyldimethylammonium hydroxide inner salt, Cocoamidopropyl betaine and/or oxidation Amine.
Multifunctional meter surface cleaning agent as described above, it is preferable that the auxiliary agent is preservative or essence;The light quick-drying Agent is carboxylic acid salt copolymer.
Multifunctional meter surface cleaning agent as described above, it is preferable that the multifunctional meter surface cleaning agent is by following proportioning Into being grouped as:
Multifunctional meter surface cleaning agent as described above, it is preferable that the multifunctional meter surface cleaning agent is by following proportioning Into being grouped as:
On the other hand, the present invention provides the preparation method of multifunctional meter surface cleaning agent as described above, and this method is included such as Lower step:
A. deionized water is put into reaction kettle, is warming up to 35-40 DEG C;
B. citric acid, potassium pyrophosphate are poured into reaction kettle to stir 10~20 minutes;
C. by CQ100, alkyl glycosides, triethanolamine, aliphatic alcohol polyethenoxy (9) ether, aliphatic alcohol polyethenoxy (7) ether, Isomery fatty alcohol polyoxyethylene ether is poured into reaction kettle and is stirred 15~25 minutes;
D. by butyl, butyl glycol ether, bamboo-leaves flavones pour into stirring in reaction kettle and extremely dissolve;
E. D- limonenes are poured into stirring in reaction kettle extremely to dissolve;
F. by benzoisothiazolinone, acrylic copolymer, protease, which is poured into reaction kettle, to be stirred to dissolving;
G. essence is eventually adding to stir to dissolving.
Another aspect, the present invention provide a kind of multifunctional meter surface cleaning agent, are prepared using method as described above.
This product is the natural material that D- limonenes derive from sweet orange, fine to the effect for removing heavy oil dirt, in the market very Multi-product, by using for reference other products, is added to D- limonenes, we are multiple simultaneously using it as addition during product development With biological enzyme, play the role of.
The present invention adds biological enzyme formulation, life in the product using biological enzyme technology and organic solvent synergistic function Object enzyme decomposes greasy dirt, greasy dirt macromolecular is resolved into small-molecule substance, so as to achieve the purpose that degreasing.Using this technology come Surface multifunction detergent is developed, overcomes the problem of heavy oil pollution cleanser alkalinity is strong in the prior art.Specifically:
CQ 100 has the double action of surfactant and organic solvent, has to dirt Wetting, dissolving, the effect of emulsification.General additive amount is 0.5-4%, and additive amount can excessively generate not pleasant smell.It is comprehensive Valency ratio is considerably beyond single surfactant role.
Alkyl glycosides APG raw materials are natural origin, substantially reduce other surfaces activating agent and the stimulation of other organic solvents Property, it is detected by national correlation department, APG natural due to being added to, mild, multifunction detergent belongs to non-stimulated product. Irritation is well below the detergent product of commercially available removal heavy oil dirt.
Organic solvent butyl glycol ether and butyl are compounded, and play synergistic function.
Individually any raw material will not all play the role of good degreasing by AEO-9, AEO-7, XL-70, AEO-9, AEO-7, which carries out compounding, synergistic function, and XL-70 belongs to isomery alcohol ether, has osmosis, and three acts synergistically, infiltration, Dissolving, wetting greasy dirt are indispensable.
D- limonenes belong to oil-soluble organic solvent, very high for greasy dirt dissolubility.Protease decomposes greasy dirt macromolecular It is easy to clean into small molecule.Two different raw materials of the mechanism of action are compounded, and play synergistic function.
Quick-drying brightener makes the hard surface quick-drying after cleaning bright, is not easy to be stained with dirt, is easy to secondary cleaning.
The advantageous effect of the multifunctional meter surface cleaning agent is that formula is using plant origin active matter, in alkalescent, to ring Border is friendly, mild to skin, does not stimulate.Mainly for the dirt of kitchen heavy oil, furniture, ground, floor and other hard surfaces are taken into account Cleaning.It deoils far superior to commercially available heavy oil pollution cleanser by test.
Specific embodiment
Embodiment 1 prepares multifunctional meter surface cleaning agent (one)
(1) raw material is weighed according to the composition and proportioning of table 1.
Table 1
Serial number Raw material Content (%)
1 Bamboo-leaves flavones 0.002
2 Goldschmidt chemical corporation CQ100 3
3 Triethanolamine 4
4 Alkyl glycosides APG-CH100 4
5 Aliphatic alcohol polyethenoxy (9) ether (AEO-9) 5
6 Aliphatic alcohol polyethenoxy (7) ether (AEO-7) 5
7 Isomery fatty alcohol polyoxyethylene ether XL70 4
8 Butyl glycol ether 5
9 Butyl 14
10 D- limonenes 2
11 Acrylic copolymer 149 0.2
12 Benzoisothiazolinone (CMG) 0.2
13 The superpower protease of 16XL 0.05
14 Essence MK95159 0.3
15 Potassium pyrophosphate 3H2O 1.5
16 Citric acid 0.47
17 Deionized water Surplus
(2) multifunctional meter surface cleaning agent is prepared
1st, load weighted deionized water is put into reaction kettle, is warming up to 35-40 DEG C.
2nd, by load weighted citric acid, potassium pyrophosphate 3H2O pours into stirring and dissolves for 10 minutes.
3rd, by load weighted CQ100, APG-CH100, triethanolamine, AEO-9, AEO-7, XL70 pours into reaction kettle and stirs It dissolves within 20 minutes.
4th, by load weighted butyl, butyl glycol ether, bamboo-leaves flavones (Zhejiang Sheng Shi biotechnologies company) are Enter stirring and dissolving.
5th, load weighted D- limonenes are poured into stirring and dissolving.
6th, load weighted CMG is poured into stirring and dissolving.
7th, essence stirring and dissolving is eventually adding, obtains multifunctional meter surface cleaning agent sample one.
8th, sampling detection.Inspection content is appearance, smell, pH value, solid content.
Specific targets are:PH (25 DEG C, stoste):8.5-9.5;Appearance:It is colourless to light yellow clear liquid;Solid content:≥ 26%.
Embodiment 2 prepares multifunctional meter surface cleaning agent (two)
(1) raw material is weighed according to the composition and proportioning of table 2.
Table 2
Serial number Raw material Content (%)
1 Bamboo-leaves flavones 0.002
2 CQ100 3
3 Triethanolamine 4
4 APG-CH100 4
5 Aliphatic alcohol polyoxyvinethene phosphate salt 5
6 AEO-7 5
7 XL70 4
8 Butyl glycol ether 5
9 Butyl 14
10 D- limonenes 2
11 149 0.2
12 CMG 0.2
13 The superpower protease of 16XL 0.05
14 MK95159 0.3
15 Potassium pyrophosphate 3H2O 1.5
16 Citric acid 0.47
17 Deionized water Surplus
(2) multifunctional meter surface cleaning agent is prepared
1st, load weighted deionized water is put into reaction kettle, is warming up to 35-40 DEG C.
2nd, by load weighted citric acid, potassium pyrophosphate 3H2O pours into stirring and dissolves for 15 minutes.
3rd, by load weighted CQ100, APG-CH100, triethanolamine, aliphatic alcohol polyoxyvinethene phosphate salt, AEO-7, XL70, which pours into reaction kettle to stir 20 minutes, to be dissolved.
4th, by load weighted butyl, butyl glycol ether, bamboo-leaves flavones (Zhejiang Sheng Shi biotechnologies company) are Enter stirring and dissolving.
5th, load weighted D- limonenes are poured into stirring and dissolving.
6th, by load weighted CMG, acrylic copolymer, superpower protease 16XL pours into stirring and dissolving.
7th, essence stirring and dissolving is eventually adding, obtains multifunctional meter surface cleaning agent sample two.
8th, sampling detection.Inspection content is appearance, smell, pH value, solid content.
Specific targets are:PH (25 DEG C, stoste):8.5-9.5;Appearance:It is colourless to light yellow clear liquid;Solid content:≥ 26%.
Embodiment 3 prepares multifunctional meter surface cleaning agent (three)
(1) raw material is weighed according to the composition and proportioning of table 3.
Table 3
Serial number Raw material Content (%)
1 Bamboo-leaves flavones 0.002
2 CQ100 3
3 Triethanolamine 4
4 APG-CH100 4
5 AEO-9 2
6 AEO-7 8
7 XL70 4
8 Butyl glycol ether 10
9 Butyl 10
10 D- limonenes 1
11 149 0.2
12 CMG 0.2
13 The superpower protease of 16XL 0.2
14 MK95159 0.3
15 Potassium pyrophosphate 3H2O 1.5
16 Citric acid 0.47
17 Deionized water Surplus
(2) multifunctional meter surface cleaning agent is prepared
1st, load weighted deionized water is put into reaction kettle, is warming up to 35-40 DEG C.
2nd, by load weighted citric acid, potassium pyrophosphate 3H2O pours into stirring and dissolves for 10 minutes.
3rd, by load weighted CQ100, APG-CH100, triethanolamine, AEO-9, AEO-7, XL70 pours into reaction kettle and stirs It dissolves within 20 minutes.
4th, by load weighted butyl, butyl glycol ether, bamboo-leaves flavones (Zhejiang Sheng Shi biotechnologies company) plus Enter stirring and dissolving.
5th, load weighted D- limonenes are poured into stirring and dissolving.
6th, by load weighted CMG, acrylic copolymer, superpower protease 16XL pours into stirring and dissolving.
7th, essence stirring and dissolving is eventually adding, obtains multifunctional meter surface cleaning agent sample three.
8th, sampling detection.Inspection content is appearance, smell, pH value, solid content.
Specific targets are:PH (25 DEG C, stoste):8.5-9.5;Appearance:It is colourless to light yellow clear liquid;Solid content:≥ 26%
Embodiment 4 prepares multifunctional meter surface cleaning agent (four)
(1) raw material is weighed according to the composition and proportioning of table 4.
Table 4
Serial number Raw material Content (%)
1 Bamboo-leaves flavones 0.002
2 CQ100 2
3 Triethanolamine 4
4 APG-CH100 4
5 AEO-9 5
6 AEO-7 5
7 XL70 4
8 Butyl glycol ether 5
9 Butyl 14
10 D- limonenes 2
11 149 0.2
12 CMG 0.2
13 The superpower protease of 16XL 0.05
14 MK95159 0.3
15 Potassium pyrophosphate 3H2O 2
16 Citric acid 0.4
17 Dodecyldimethylammonium hydroxide inner salt 3
18 Deionized water Surplus
(2) multifunctional meter surface cleaning agent is prepared
1st, load weighted deionized water is put into reaction kettle, is warming up to 35-40 DEG C.
2nd, by load weighted citric acid, potassium pyrophosphate 3H2O pours into stirring minute dissolving.
3rd, by load weighted CQ100, APG-CH100, triethanolamine, dodecyldimethylammonium hydroxide inner salt, AEO-9, AEO- 7, XL70 pour into reaction kettle stir 20 minutes dissolve.
4th, by load weighted butyl, butyl glycol ether, bamboo-leaves flavones (Zhejiang Sheng Shi biotechnologies company) are Enter stirring and dissolving.
5th, load weighted D- limonenes are poured into stirring and dissolving.
6th, by load weighted CMG, acrylic copolymer, superpower protease 16XL pours into stirring and dissolving.
7th, essence stirring and dissolving is eventually adding, obtains multifunctional meter surface cleaning agent sample four.
8th, sampling detection.Inspection content is appearance, smell, pH value, solid content.
Specific targets are:PH (25 DEG C, stoste):8.5-9.5;Appearance:It is colourless to light yellow clear liquid;Solid content:≥ 26%.
Comparative example 1 prepares multifunctional meter surface cleaning agent (five)
(1) raw material is weighed according to the composition and proportioning of table 5.
Table 5
Serial number Raw material Content (%)
1 Bamboo-leaves flavones 0.002
2 CQ100 3
3 Triethanolamine 4
4 APG-CH100 4
5 AEO-9 5
6 AEO-7 5
7 XL70 4
8 Butyl glycol ether 5
9 Butyl 14
10 D- limonenes 2
11 149 0.2
12 CMG 0.2
13 MK95159 0.3
14 Potassium pyrophosphate 3H2O 1.5
15 Citric acid 0.47
16 Deionized water Surplus
(2) multifunctional meter surface cleaning agent is prepared
Raw material is as shown in table 5, using method same as Example 1, does not add protease only.Obtain multifunction surface Detergent sample five.
Comparative example 2 prepares multifunctional meter surface cleaning agent (six)
(1) raw material is weighed according to the composition and proportioning of table 6.
Table 6
Serial number Raw material Content (%)
1 Bamboo-leaves flavones 0.002
2 CQ100 3
3 Triethanolamine 4
4 APG-CH100 4
5 AEO-9 5
6 AEO-7 5
7 XL70 4
8 Butyl glycol ether 5
9 Butyl 14
11 149 0.2
12 CMG 0.2
13 The superpower protease of 16XL 0.05
14 MK95159 0.3
15 Potassium pyrophosphate 3H2O 1.5
16 Citric acid 0.47
17 Deionized water Surplus
(2) multifunctional meter surface cleaning agent is prepared
Raw material is as shown in table 6, using method same as Example 1, does not add D- limonenes only.Obtain multifunctional meter Surface cleaning agent sample six.
1 properties of sample of experimental example detects
Sample detection is carried out according to QB/T4348-2012 standards, as a result as follows:
(1) sample one
Table 7
(2) sample two:
Table 8
(3) sample three:
Table 9
(4) sample four:
Table 10
(5) sample five
Table 11
(6) sample six
Table 12

Claims (4)

1. a kind of multifunctional meter surface cleaning agent, which is characterized in that it is into being grouped as by following proportioning:
2. multifunctional meter surface cleaning agent as described in claim 1, which is characterized in that the multifunctional meter surface cleaning agent be by with Lower proportioning into being grouped as:
3. the preparation method of multifunctional meter surface cleaning agent as claimed in claim 1 or 2, which is characterized in that this method is included such as Lower step:
A. deionized water is put into reaction kettle, is warming up to 35-40 DEG C;
B. citric acid, potassium pyrophosphate are poured into reaction kettle to stir 10~20 minutes;
C. by CQ100, alkyl glycosides, triethanolamine, aliphatic alcohol polyethenoxy (9) ether, aliphatic alcohol polyethenoxy (7) ether, isomery Fatty alcohol polyoxyethylene ether is poured into reaction kettle and is stirred 15~25 minutes;
D. by butyl, butyl glycol ether, bamboo-leaves flavones pour into stirring in reaction kettle and extremely dissolve;
E. D- limonenes are poured into stirring in reaction kettle extremely to dissolve;
F. by benzoisothiazolinone, acrylic copolymer, protease, which is poured into reaction kettle, to be stirred to dissolving;
G. essence is eventually adding to stir to dissolving.
4. a kind of multifunctional meter surface cleaning agent, which is characterized in that it is prepared using claim 3 the method.
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