CN105295606B - A kind of lacquer that can be constructed under the conditions of low temperature and high relative humidity and preparation method thereof - Google Patents
A kind of lacquer that can be constructed under the conditions of low temperature and high relative humidity and preparation method thereof Download PDFInfo
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Abstract
The present invention provides a kind of lacquer that can be constructed under the conditions of low temperature and high relative humidity and preparation method thereof, the component and the mass content of component that the lacquer includes are：Lotion 18 22%, natural colour sand 70 75%, fungicide 0.2 0.4%, coalescents 0.5 1.1%, surfactant AS 81 1.5%, antifreezing agent 0.4 0.6%, thickener 0.2 0.4%, water 2 8%.Lacquer provided by the invention, because adding a kind of surfactant AS 8 in lacquer mixed emulsion, coating modification can be carried out to emulsion particle, cause to form hydrophobic group on the surface of emulsion particle, the rate of drying of emulsion paint is improved with this, the defects of so as to make lacquer energy fast filming under the conditions of low temperature and high relative humidity, overcome existing lacquer.The preparation method that the present invention provides can produce the lacquer of the present invention that can be constructed under the conditions of low temperature and high relative humidity.
Description
Technical field
The present invention relates to building material field, more specifically, be related to it is a kind of can construct under the conditions of low temperature and high relative humidity it is true
Mineral varnish and preparation method thereof.
Background technology
Lacquer is the coating that a kind of decorative effect exactly likes marble, granite.The main natural stone for using a variety of colors
Powder is formulated, applied to the imitative stone effect of building wall, also known as liquid stone.Building after lacquer finishing, has day
Right true natural colour, gives graceful, harmonious, serious aesthetic feeling, is suitable for the indoor and outdoor decoration of all kinds of buildings.Especially
It is to be decorated on curved-surface building object, it is vivid, there is a kind of effect of back to nature.There is lacquer easy construction, Yi Gan to save
When, it is easy for construction the advantages that so that lacquer product is the main product of stone-like coating currently on the market.
But since China region is wide, north-south climate differs greatly, particularly in northern area and coastal area in the winter
In season, temperature is relatively low, air humidity is big, and the duration of construction now is again relatively tight, is often required under conditions of low temperature and high relative humidity
Rapid construction, it is bad to be susceptible to film formation at low temp, meet rainwater there is rainprint, floating phenomenon of whitening, influence lacquer product decoration
Effect and its intrinsic defencive function.Therefore, there is an urgent need for develop can construct under the conditions of low temperature and high relative humidity and filming performance it is good,
It is not in the lacquer of floating phenomenon of whitening to meet after rainwater, to adapt to needed for market.
Invention content
To solve the above-mentioned problems, the present invention is obtained by adding in a kind of special surfactant in traditional lacquer
Can construct under high temperature low humidity conditions and with being not in the true stone of floating phenomenon of whitening after good filming performance, chance rainwater
Paint and preparation method thereof.
Specifically, an aspect of of the present present invention provides a kind of lacquer that can be constructed under the conditions of low temperature and high relative humidity, including
Component and the mass content of component be：
Wherein, the molecular formula of the surfactant AS -8 is：
The acrylic emulsion that conventional lacquer uses currently on the market is obtained using radical polymerization,
And acrylic monomers is divided into oleophylic and hydrophilic, usually the monomer of oleophylic likes reaction inside micella, hydrophilic list
Body likes reaction outside micella, exactly because hydrophilic monomer reaction is then constructed under hot and humid environment and is led outside micella
Cause is not easy drying, and it is bad to be susceptible to film formation at low temp, meet rainwater there is rainprint, floating phenomenon of whitening.True stone provided by the invention
Paint because adding a kind of surfactant AS -8 in lacquer mixed emulsion, can carry out coating modification to emulsion particle, thus
The surface of emulsion particle forms hydrophobic group, and the rate of drying of emulsion paint is improved with this, makes lacquer in low temperature and high relative humidity item
Under part can fast filming, the defects of overcoming existing lacquer.
Specifically the present invention, which can solve the mechanism of existing issue, is：It can be in polyphosphazene polymer during emulsion polymerization
It closes object surface and forms double-deck surfactant, first layer surfactant is the emulsifier in lotion building-up process, the emulsification
The hydrophobic side of agent and high molecular polymer are combined, and its water-wet side is outside, so as to make high molecular polymer in the packet of emulsifier
Cover lower formation emulsion particle.Second layer surfactant is AS-8, according to the similar principle that mixes, the water-wet side of AS-8 and emulsifier
Water-wet side forms double-deck micella, and the hydrophobic side of AS-8 is outside, so as to form hydrophobic group on the surface of emulsion particle.Due to double
The effect of layer surface activating agent can improve the space steric effect of emulsion particle, so as to which emulsion particle is made to be distributed to polarity well
In solvent.Therefore, lacquer of the invention not only good dispersion, can construct under the conditions of low temperature and high relative humidity, can rapid draing, quick
Film forming, chance rainwater does not occur rainprint, floating phenomenon of whitening.
According to one embodiment of the lacquer of the present invention that can be constructed under the conditions of low temperature and high relative humidity, it is preferable that described
The mesh number and its mass content of natural colour sand be：
120-180 mesh 5%
80-120 mesh 70%
40-80 mesh 25%.
According to another embodiment of the lacquer of the present invention that can be constructed under the conditions of low temperature and high relative humidity, it is preferable that institute
The mesh number and its mass content for stating natural colour sand be：
80-120 mesh 55%
40-80 mesh 30%
20-40 mesh 15%.
According to the further embodiment of the lacquer of the present invention that can be constructed under the conditions of low temperature and high relative humidity, it is preferable that institute
The mesh number and its mass content for stating natural colour sand be：
Each natural colour sand has different mesh numbers, in the market general mesh number be 10-20 mesh, 20-40 mesh, 40-80 mesh,
80-120 mesh, 120-180 mesh, and different mesh numbers plays different effects in lacquer：120-180 mesh and 80-120 mesh are
Lacquer provides covering power and color, 80-120 mesh and 40-80 mesh provide covering power and texture for lacquer；20-40 mesh and 10-
20 mesh provide texture for lacquer.
According to a still further embodiment of the lacquer of the present invention that can be constructed under the conditions of low temperature and high relative humidity, it is preferable that institute
Coalescents are stated as alcohol ester coalescents (trade name coalescents CS water).CS water can be effectively reduced film-forming temperature, improve
Paint film scrub resistance improves pigment uniformity, has good color developing, improves the adhesive force of paint film, reduces alligatoring, stripping
From and it is not hydrolyzed in general alkaline medium, has good storage stability, relatively low in temperature, larger severe of humidity
Under the conditions of, still there is preferable filming performance.
Another aspect provides the preparation method for the lacquer that can be constructed under the conditions of low temperature and high relative humidity, including with
Lower step：
Step 101, the lotion of 18-22% is put into the first Scattered Kettle, is added with stirring in the speed of 300-500rpm
Surfactant AS -8 of 1-1.5%, stirring are for use after twenty minutes；
Step 102, fungicide, the 0.4- of 0.2-0.4% is sequentially added after the water of addition 2-8% in the second Scattered Kettle
0.6% antifreezing agent is stirred 3 minutes using the speed of 300-500rpm, adds the breast handled through above-mentioned steps 101
Liquid；
Step 103, the coalescents of 0.5-1.1%, the thickener of 0.2-0.4% are added in into second reaction kettle,
It is stirred 5 minutes using the speed of 300-500rpm；
Step 104, the natural colour sand of 70-75% then into second reaction kettle is sequentially added, is uniformly dispersed, examines packet
The lacquer is made in dress；
Wherein, the molecular formula of the surfactant AS -8 is：
The above-mentioned preparation method that the present invention provides, can produce the lacquer that can be constructed under the conditions of low temperature and high relative humidity, this is true
Mineral varnish can carry out coating modification because adding a kind of surfactant AS -8 in lacquer mixed emulsion to emulsion particle, so as to
Hydrophobic group is formed on the surface of emulsion particle, the rate of drying of emulsion paint is improved with this, so as to make the lacquer low
Energy fast filming, overcomes existing lacquer to construct under conditions of low temperature and high relative humidity and is susceptible to film formation at low temp not under warm super-humid conditions
The defects of there is rainprint in good, chance rainwater, floating phenomenon of whitening.
According to one embodiment of preparation method of the lacquer of the present invention that can be constructed under the conditions of low temperature and high relative humidity, preferably
Ground, the mesh number and its mass content of the natural colour sand are：
120-180 mesh 5%
80-120 mesh 70%
40-80 mesh 25%
Wherein, sand mesh number feeding sequence is：120-180 mesh, 80-120 mesh, 40-80 mesh, feeding intake for different color sand are suitable
Sequence is：White sand, light sand, dark sand.
According to another embodiment of preparation method of the lacquer of the present invention that can be constructed under the conditions of low temperature and high relative humidity, preferably
Ground, the mesh number and its mass content of the natural colour sand are：
80-120 mesh 55%
40-80 mesh 30%
20-40 mesh 15%
Wherein, sand mesh number feeding sequence is：80-120 mesh, 40-80 mesh, 20-40 mesh, the feeding sequence of different color sand
For：White sand, light sand, dark sand.
According to the preparation method another embodiment of the lacquer of the present invention that can be constructed under the conditions of low temperature and high relative humidity, preferably
Ground, the mesh number and its mass content of the natural colour sand are：
Wherein, sand mesh number feeding sequence is：120-180 mesh, 80-120 mesh, 40-80 mesh, 20-40 mesh, 10-20 mesh, no
The feeding sequence of homochromy color sand is：White sand, light sand, dark sand.
Each natural colour sand has different mesh numbers, in the market general mesh number be 10-20 mesh, 20-40 mesh, 40-80 mesh,
80-120 mesh and 120-180 mesh, and different mesh numbers plays different effects in lacquer：120-180 mesh and 80-120 mesh
Covering power and color are provided for lacquer, 80-120 mesh and 40-80 mesh provide covering power and texture for lacquer；20-40 mesh and
10-20 mesh provides texture for lacquer.
According to the preparation method a further embodiment of the lacquer of the present invention that can be constructed under the conditions of low temperature and high relative humidity, preferably
Ground, the coalescents are alcohol ester coalescents (trade name coalescents CS water).CS water can be effectively reduced film-forming temperature,
Paint film scrub resistance is improved, improves pigment uniformity, there is good color developing, improves the adhesive force of paint film, reduces paint film tortoise
It splits, remove, and it is not hydrolyzed in general alkaline medium, there is good storage stability, temperature is relatively low, humidity is larger
Under mal-condition, still there is preferable filming performance.
Additional aspect and advantage according to the present invention will become apparent or by the present invention in following description section
Practice is recognized.
Description of the drawings
Fig. 1 is the preparation method flow diagram of the lacquer of the present invention that can be constructed under the conditions of low temperature and high relative humidity.
Specific embodiment
To better understand the objects, features and advantages of the present invention, illustrate basis below in conjunction with the accompanying drawings
The specific embodiment of the present invention.It should be noted that in the absence of conflict, in embodiments herein and embodiment
Feature can be combined with each other.
Many details are elaborated in the following description to facilitate a thorough understanding of the present invention, still, the present invention may be used also
To be implemented using other different from other modes described here, therefore, protection scope of the present invention is not by described below
Specific embodiment limitation.
Some embodiments of the present invention provide a kind of lacquer that can be constructed under the conditions of low temperature and high relative humidity, including component
Mass content with component is：
Wherein, the molecular formula of the surfactant AS -8 is：
The acrylic emulsion that conventional lacquer uses currently on the market is obtained using radical polymerization,
And acrylic monomers is divided into oleophylic and hydrophilic, usually the monomer of oleophylic likes reaction inside micella, hydrophilic list
Body likes reaction outside micella, really because hydrophilic monomer reaction is then constructed under hot and humid environment and led outside micella
Cause is not easy drying, and it is bad to be susceptible to film formation at low temp, be susceptible to meet rainwater there is rainprint, floating phenomenon of whitening.The present invention carries
The lacquer of confession because adding a kind of surfactant AS -8 in lacquer mixed emulsion, can carry out emulsion particle cladding and change
Property, so as to form hydrophobic group on the surface of emulsion particle, the rate of drying of emulsion paint is improved with this, so as to make the lacquer
Under the conditions of low temperature and high relative humidity can fast filming, the defects of overcoming existing lacquer.
According to some embodiments of the lacquer of the present invention that can be constructed under the conditions of low temperature and high relative humidity, it is preferable that described
The mesh number and its mass content of natural colour sand be：
120-180 mesh 5%
80-120 mesh 70%
40-80 mesh 25%.
According to other embodiments of the lacquer of the present invention that can be constructed under the conditions of low temperature and high relative humidity, it is preferable that institute
The mesh number and its mass content for stating natural colour sand be：
80-120 mesh 55%
40-80 mesh 30%
20-40 mesh 15%.
According to the still other embodiments of the lacquer of the present invention that can be constructed under the conditions of low temperature and high relative humidity, it is preferable that institute
The mesh number and its mass content for stating natural colour sand be：
Each natural colour sand has different mesh numbers, in the market general mesh number be 10-20 mesh, 20-40 mesh, 40-80 mesh,
80-120 mesh, 120-180 mesh, and different mesh numbers plays different effects in lacquer：120-180 mesh and 80-120 mesh are
Lacquer provides covering power and color, 80-120 mesh and 40-80 mesh provide covering power and texture for lacquer；20-40 mesh and 10-
20 mesh provide texture for lacquer.
According to also some embodiments of the lacquer of the present invention that can be constructed under the conditions of low temperature and high relative humidity, it is preferable that institute
Coalescents are stated as alcohol ester coalescents (trade name coalescents CS water).CS water can be effectively reduced film-forming temperature, improve
Paint film scrub resistance improves pigment uniformity, has good color developing, improves the adhesive force of paint film, reduces alligatoring, stripping
From and it is not hydrolyzed in general alkaline medium, has good storage stability, that temperature is relatively low, humidity is larger is severe
Under the conditions of, still there is preferable filming performance.
The lacquer that can be constructed under the conditions of low temperature and high relative humidity that the above embodiment of the present invention provides, because adding the table of feature
Face activating agent AS-8 so that the lacquer can construct in the environment of low temperature and high relative humidity, and can rapid draing, so as to good film-forming property,
Meet rainwater do not occur rainprint, floating phenomenon of whitening, the defects of overcoming the prior art can realize the invention mesh of the present invention well
's.
It is the specific embodiment of the lacquer of the present invention that can be constructed under the conditions of low temperature and high relative humidity below：
Embodiment one
The component of lacquer one embodiment that can be constructed under the conditions of low temperature and high relative humidity and the quality of component of the present invention
Content is：
Embodiment two
The component of lacquer another embodiment of the present invention that can be constructed under the conditions of low temperature and high relative humidity and the matter of component
Measuring content is：
Embodiment three
The component of lacquer further embodiment that can be constructed under the conditions of low temperature and high relative humidity and the matter of component of the present invention
Measuring content is：
The lacquer that can be constructed under the conditions of low temperature and high relative humidity that above-mentioned three embodiment provides after testing, meets claimed below：
Therefore, the lacquer that above-mentioned three embodiment provides, can construct in the environment of low temperature and high relative humidity, and can soon rapid-curing cutback it is miscellaneous,
So as to good film-forming property, meet rainwater do not occur rainprint, floating phenomenon of whitening, the defects of overcoming the prior art, can realize well
The goal of the invention of the present invention.
As shown in Figure 1, another aspect provides the above-mentioned lacquers available for constructing under the conditions of low temperature and high relative humidity
Preparation method,
Include the following steps：
Step 101, the lotion of 18-22% is put into the first Scattered Kettle, is added with stirring in the speed of 300-500rpm
Surfactant AS -8 of 1-1.5%, stirring are for use after twenty minutes；
Step 102, fungicide, the 0.4- of 0.2-0.4% is sequentially added after the water of addition 2-8% in the second Scattered Kettle
0.6% antifreezing agent is stirred 3 minutes using the speed of 300-500rpm, adds the breast handled through above-mentioned steps 101
Liquid；
Step 103, the coalescents of 0.5-1.1%, the thickener of 0.2-0.4% are added in into second reaction kettle,
It is stirred 5 minutes using the speed of 300-500rpm；
Step 104, the natural colour sand of 70-75% then into second reaction kettle is added in, is uniformly dispersed, test package,
The lacquer is made；
Wherein, the molecular formula of the surfactant AS -8 is：
The above-mentioned preparation method that the present invention provides, can produce the lacquer that can be constructed under the conditions of low temperature and high relative humidity, this is true
Mineral varnish can carry out coating modification because adding a kind of surfactant AS -8 in lacquer mixed emulsion to emulsion particle, so as to
Hydrophobic group is formed on the surface of emulsion particle, the rate of drying of emulsion paint is improved with this, so as to make the lacquer low
Energy fast filming, overcomes existing lacquer to construct under conditions of low temperature and high relative humidity and is susceptible to film formation at low temp not under warm super-humid conditions
The defects of there is rainprint in good, chance rainwater, floating phenomenon of whitening.
According to some embodiments of the preparation method of the lacquer of the present invention that can be constructed under the conditions of low temperature and high relative humidity, preferably
Ground, the mesh number and its mass content of the natural colour sand are：
120-180 mesh 5%
80-120 mesh 70%
40-80 mesh 25%
Wherein, sand mesh number feeding sequence is：120-180 mesh, 80-120 mesh, 40-80 mesh, feeding intake for different color sand are suitable
Sequence is：White sand, light sand, dark sand.
It is excellent according to other embodiments of the preparation method of the lacquer of the present invention that can be constructed under the conditions of low temperature and high relative humidity
Selection of land, the mesh number and its mass content of the natural colour sand are：
80-120 mesh 55%
40-80 mesh 30%
20-40 mesh 15%
Wherein, sand mesh number feeding sequence is：80-120 mesh, 40-80 mesh, 20-40 mesh, the feeding sequence of different color sand
For：White sand, light sand, dark sand.
It is excellent according to the preparation method still other embodiments of the lacquer of the present invention that can be constructed under the conditions of low temperature and high relative humidity
Selection of land, the mesh number and its mass content of the natural colour sand are：
Wherein, sand mesh number feeding sequence：120-180 mesh, 80-120 mesh, 40-80 mesh, 20-40 mesh, 10-20 mesh, it is different
The feeding sequence of color sand：White sand, light sand, dark sand.
Each natural colour sand has different mesh numbers, in the market general mesh number be 10-20 mesh, 20-40 mesh, 40-80 mesh,
80-120 mesh, 120-180 mesh, and different mesh numbers plays different effects in lacquer：120-180 mesh and 80-120 mesh are
Lacquer provides covering power and color, 80-120 mesh and 40-80 mesh provide covering power and texture for lacquer；20-40 mesh and 10-
20 mesh provide texture for lacquer.
It is excellent according to the preparation method of the lacquer of the present invention that can be constructed under the conditions of low temperature and high relative humidity also some embodiments
Selection of land, the coalescents are alcohol ester coalescents (trade name coalescents CS water).CS water can be effectively reduced film forming temperature
Degree improves paint film scrub resistance, improves pigment uniformity, has good color developing, improves the adhesive force of paint film, reduces paint film
Cracking, stripping, and it is not hydrolyzed in general alkaline medium, has good storage stability, temperature is relatively low, humidity is larger
Mal-condition under, still have preferable filming performance.
In the description of this specification, the description of term " one embodiment ", " some embodiments ", " specific embodiment " etc.
Mean that combining the particular features, structures, materials, or characteristics that the embodiment or example describe is contained at least the one of the utility model
In a embodiment or example.In the present specification, schematic expression of the above terms are not necessarily referring to identical embodiment
Or example.Moreover, the particular features, structures, materials, or characteristics of description can be in any one or more embodiments or example
In combine in an appropriate manner.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, for the skill of this field
For art personnel, the invention may be variously modified and varied.All within the spirits and principles of the present invention, that is made any repaiies
Change, equivalent replacement, improvement etc., should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of lacquer that can be constructed under the conditions of low temperature and high relative humidity, which is characterized in that it is composed of the following components, and each component
Mass content is：
Wherein, the molecular formula of the surfactant AS -8 is：
2. the lacquer according to claim 1 that can be constructed under the conditions of low temperature and high relative humidity, which is characterized in that the natural color
The mesh number and its mass content of sand be：
120-180 mesh 5%
80-120 mesh 70%
40-80 mesh 25%.
3. the lacquer according to claim 1 that can be constructed under the conditions of low temperature and high relative humidity, which is characterized in that the natural color
The mesh number and its mass content of sand be：
80-120 mesh 55%
40-80 mesh 30%
20-40 mesh 15%.
4. the lacquer according to claim 1 that can be constructed under the conditions of low temperature and high relative humidity, which is characterized in that the natural color
The mesh number and its mass content of sand be：
5. the lacquer that can be constructed under the conditions of low temperature and high relative humidity according to any one of claim 1-4, which is characterized in that
The coalescents are alcohol ester coalescents.
6. the preparation method of the lacquer described in claim 1 that can be constructed under the conditions of low temperature and high relative humidity, which is characterized in that including
Following steps：
Step 101, the lotion of 18-22% is put into the first Scattered Kettle, 1- is added with stirring in the speed of 300-500rpm
1.5% surfactant AS -8, stirring are for use after twenty minutes；
Step 102, fungicide, the 0.4-0.6% of 0.2-0.4% is sequentially added after the water of addition 2-8% in the second Scattered Kettle
Antifreezing agent, using 300-500rpm speed stir 3 minutes, add the lotion handled through above-mentioned steps 101；
Step 103, the coalescents of 0.5-1.1%, the thickener of 0.2-0.4% are added in into second reaction kettle, is used
The speed of 300-500rpm stirs 5 minutes；
Step 104, the natural colour sand of 70-75% then into second reaction kettle is added in, is uniformly dispersed, test package is made
The lacquer；
Wherein, the molecular formula of the surfactant AS -8 is：
7. the preparation method of the lacquer according to claim 6 that can be constructed under the conditions of low temperature and high relative humidity, which is characterized in that
The mesh number and its mass content of the natural colour sand be：
120-180 mesh 5%
80-120 mesh 70%
40-80 mesh 25%
Wherein, sand mesh number feeding sequence is：120-180 mesh, 80-120 mesh, 40-80 mesh, the feeding sequence of different color sand
For：White sand, light sand, dark sand.
8. the preparation method of the lacquer according to claim 6 that can be constructed under the conditions of low temperature and high relative humidity, which is characterized in that
The mesh number and its mass content of the natural colour sand be：
80-120 mesh 55%
40-80 mesh 30%
20-40 mesh 15%
Wherein, sand mesh number feeding sequence is：80-120 mesh, 40-80 mesh, 20-40 mesh, the feeding sequence of different color sand are：
White sand, light sand, dark sand.
9. the preparation method of the lacquer according to claim 6 that can be constructed under the conditions of low temperature and high relative humidity, which is characterized in that
The mesh number and its mass content of the natural colour sand be：
Wherein, sand mesh number feeding sequence is：120-180 mesh, 80-120 mesh, 40-80 mesh, 20-40 mesh, 10-20 mesh, it is not homochromy
The feeding sequence of color sand is：White sand, light sand, dark sand.
10. the preparation method of the lacquer that can be constructed under the conditions of low temperature and high relative humidity according to any one of claim 6-9,
It is characterized in that, the coalescents are alcohol ester coalescents.
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| CN201510829658.8A CN105295606B (en) | 2015-11-25 | 2015-11-25 | A kind of lacquer that can be constructed under the conditions of low temperature and high relative humidity and preparation method thereof |
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| CN103627272B (en) * | 2013-11-07 | 2015-07-15 | 湖北启利新材料科技有限公司 | Liquid rock particles of artificial granite sand textured coating |
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