CN105294361A - Humic acid type organic water-retaining agent using vinegar factory liquid waste and preparation method thereof - Google Patents
Humic acid type organic water-retaining agent using vinegar factory liquid waste and preparation method thereof Download PDFInfo
- Publication number
- CN105294361A CN105294361A CN201510702699.0A CN201510702699A CN105294361A CN 105294361 A CN105294361 A CN 105294361A CN 201510702699 A CN201510702699 A CN 201510702699A CN 105294361 A CN105294361 A CN 105294361A
- Authority
- CN
- China
- Prior art keywords
- humic acid
- organic water
- acid type
- holding agent
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Abstract
The invention discloses a humic acid type organic water-retaining agent using vinegar factory liquid waste and a preparation method thereof, and belongs to the technical field of water-retaining agent preparation. The humic acid type organic water-retaining agent is prepared from, by weight, 35-45 parts of organic water-retaining agent, 30-40 parts of humic acid, 8-10 parts of distilled water, 0.06-0.09 part of mildew preventive and 0.06-0.09 part of insecticide composition. The humic acid type organic water-retaining agent is prepared through the steps of humic acid preparation, insecticide composition preparation, mixing, pelleting, drying and the like. According to the humic acid type organic water-retaining agent, diseases and insect pests can be effectively prevented, the lodging resistance of crops can be enhanced, and the yield is increased. The humic acid type organic water-retaining agent is low in preparation cost, good in application effect and beneficial to application and popularization.
Description
[technical field]
The invention belongs to water-holding agent preparing technical field, be specifically related to a kind of organic water-holding agent of humic acid type utilizing vinegar factory waste liquid and preparation method thereof.
[background technology]
Containing a large amount of organic matters and beneficial element in vinegar factory waste liquid, China discharges this waste liquid more than 1,000,000 tons at present every year, has caused serious problem of environmental pollution.The main Land use systems of current this waste liquid remains direct irrigation, and on the one hand, the method for application of this extensive style is unfavorable for effective utilization of nutrition; On the other hand, due to the restriction of the aspects such as transport, this method of application is only limitted to factory's periphery; Moreover the waste liquid of directly discharge is in acid, and life-time service can cause soil compaction.
Farm crop, at Growing season, if there is weather of blowing, are easy to lodge, and farm crop are once lodging, greatly will reduce output.
Facts have proved, conventional organic water-holding agent is functional single, is used alone and easily causes soil compaction, and therefore, a kind of multi-functional novel organic water-holding agent of research becomes developing direction.
[summary of the invention]
The invention provides a kind of organic water-holding agent of humic acid type utilizing vinegar factory waste liquid and preparation method thereof, to solve the functional problem such as single of conventional organic water-holding agent, the organic water-holding agent of humic acid type of the present invention can not only preventing disease and pest effectively, and the lodging resistance of farm crop can be strengthened, improve output; Corruption of the present invention is implanted with that machine water-holding agent preparation cost is low, effect good, is conducive to applying.
For solving above technical problem, the present invention by the following technical solutions:
Utilize the organic water-holding agent of humic acid type of vinegar factory waste liquid, in units of weight part, comprise following raw material: organic water-holding agent 35-45 part, humic acids 30-40 part, distilled water 8-10 part, mould inhibitor 0.06-0.09 part, insect-killing composition 0.06-0.09 part.
Preferably, described organic water-holding agent comprises one or more in polyacrylamide, sodium polyacrylate, polyacrylic acid potassium, ammonium polyacrylate, starch graft acrylic acid sodium.
Preferably, described humic acids is made up of vinegar factory waste liquid.
Preferably, described mould inhibitor comprises one or both in quinoxyfen, triazolone.
Preferably, described insect-killing composition is extracted made by China tree, pyrethrum, the root of large-flowered skullcap, capsicum, tobacco, Herba Patriniae, tarragon, Herba Sophorae alopecuroidis.
The present invention also provides a kind of preparation method utilizing the organic water-holding agent of humic acid type of vinegar factory waste liquid, comprises the following steps:
S1: vinegar factory waste liquid is left standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 70-80 DEG C and carries out evaporation concentration, being concentrated into pH value is 2.5-3.5, stops heating, left at room temperature activation 13-15h, then add volatile salt adjust ph to 6.3-7.5, obtain humic acid solution, humic acid solution is dried to water content≤6% at 90-100 DEG C, 100-300 mesh sieve is crossed, obtained humic acids after pulverizing;
S2: by China tree, pyrethrum, the root of large-flowered skullcap, capsicum, tobacco, Herba Patriniae, tarragon, Herba Sophorae alopecuroidis co-grinding, liquid is extracted under ultrasonic assistant ethanol extraction method, gained medical filtration, to be concentrated into after water content≤20% to obtain mixture A, gained mixture A is dried to water content≤6% at 90-100 DEG C, 100-300 mesh sieve is crossed, obtained insect-killing composition after pulverizing;
S3: take humic acids that step S1 obtains, step S2 obtained insect-killing composition, organic water-holding agent, mould inhibitor and distilled water respectively in described ratio, mix to obtain mixture B, described mixture B is carried out making 1.5-2.5mm particle and be dried to water content≤6% at 90-100 DEG C, the obtained organic water-holding agent of humic acid type.
Preferably, the condition of the ethanol extraction method of ultrasonic assistant described in step S2 extraction liquid is: solid-liquid ratio is 1:8-16, and ultrasonic power is 140-180W, and alcohol concn is 50%-80%, and Extracting temperature is 50-70 DEG C, and extraction time is 60-90min.
The humic acids utilizing vinegar factory waste liquid to make contains a large amount of organic matters and beneficial element, is conducive to growing up healthy and sound of farm crop, shortens growth cycle.
Mould inhibitor, refers to and can prevent microorganism from causing mouldy medicament, has very strong suppression, killing action to bacterium, fungi.
China tree famous paradise tree, it contains toxin, can as sterilant, wormer and growth inhibitor.
Pyrethrum containing 4 kinds of insecticidal constituents, pyrethrin (pyrethrin) I, II and cinerin (cinerin) I, II, pyrethrum to various insects as mosquito, fly, bedbug and cockroach etc. have toxic action.
The root of large-flowered skullcap has the effects such as heat-clearing and damp-drying drug, eliminating fire and detoxication, antiabortive, cooling blood for hemostasis, step-down, calmness, antimicrobial, antibacterial, antiviral, desinsection.
Capsicum can alleviate chest abdomen crymodynia, prevents dysentery, kills and presses down stomach abdomen entozoa, controls heart trouble and coronary sclerosis, the function such as have sterilization, anticorrosion, seasoning, nutrition, dispel cold.
Tobacco has the effects such as promoting the circulation of QI to relieve pain, eliminating dampness, detumescence, removing toxic substances desinsection.
Herba Patriniae, with root stock and root, all herbal medicine, belongs to antipyretic and antidotal type medicine in Chinese medicine, cool in nature, taste is pungent, bitter.Return liver, stomach, large intestine channel, have effect that is clearing heat and detoxicating, removing blood stasis and expelling pus.Modern pharmacy is thought, it is containing volatile oil, Patrinia scaniosaefolia saponin and β-sterol glucose formula, have anti-inflammatory, antibacterial, calm, protect the liver the effect with cardiac stimulant diuresis.Herba Patriniae has suppression or killing action to streptococcus aureus, dysentery bacterium, Corynebacterium diphtheriae, Pseudomonas aeruginosa.
Tarragon has strong antibacterial and anti-inflammation functions, all has suppression and killing action to multiple coccus, bacillus, fungi and virus etc., is the one that in the natural phant found at present, anti-microbial effect is extremely strong.
The total alkaloid of sophora alopecuroide extracted in Herba Sophorae alopecuroidis has anti-inflammatory, anticancer, anti-allergic, anti-heart disorder, antiulcer agent, leukocyte increasing, relievings asthma, antipyretic, desinsection, calmness, analgesia, the effect such as antiviral; The external application of Herba Sophorae alopecuroidis powder has suppression or killing action to staphylococcus, intestinal bacteria, suis, fungi, bacterium protein of Gardnerella vaginalis and trichomonad; The killing ability of Herba Sophorae alopecuroidis plant is between neonicotine (Anadasine) and lupin alkaloid (Lupinine), and Tocosamine is Biocidal agriculture the effective elements of the medicine.
The present invention has following beneficial effect:
(1) the organic water-holding agent of humic acid type of the present invention can obviously promote that farm crop take root, and increases the rhizome ratio of farm crop, strengthens lodging resistance;
(2) the present invention is by combinations such as organic water-holding agent, humic acids, mould inhibitor, insect-killing compositions, adds the function of organic water-holding agent;
(3) the present invention utilizes vinegar factory waste liquid to prepare humic acids, is conducive to the resource utilization of waste, reduces cost of the present invention;
(4) the organic water-holding agent of humic acid type of the present invention can not only preventing disease and pest effectively, and can improve edatope;
(5) humic acid type of the present invention organic water-holding agent composition degradable, can not bring environmental pollution;
(6) the organic water-holding agent effect of humic acid type of the present invention is good, is conducive to applying.
[embodiment]
Be specifically described below in conjunction with specific embodiment.
Embodiment 1
Utilize the organic water-holding agent of humic acid type of vinegar factory waste liquid, in units of weight part, comprise following raw material: polyacrylamide 35 parts, humic acids 30 parts, distilled water 8 parts, quinoxyfen 0.06 part, insect-killing composition 0.06 part.
The described preparation method utilizing the organic water-holding agent of humic acid type of vinegar factory waste liquid, comprises the following steps:
S1: vinegar factory waste liquid is left standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 70 DEG C and carries out evaporation concentration, being concentrated into pH value is 3.5, stops heating, left at room temperature activation 13h, then add volatile salt adjust ph to 6.3, obtain humic acid solution, humic acid solution being dried at 100 DEG C water content is 6%, 100 mesh sieve are crossed, obtained humic acids after pulverizing;
S2: by China tree, pyrethrum, the root of large-flowered skullcap, capsicum, tobacco, Herba Patriniae, tarragon, Herba Sophorae alopecuroidis co-grinding, liquid is extracted under ultrasonic assistant ethanol extraction method, condition is: solid-liquid ratio is 1:8, and ultrasonic power is 140W, and alcohol concn is 50%, Extracting temperature is 50 DEG C, extraction time is 90min, gained medical filtration, be concentrated into water content be after 20% mixture A, it is 6% that gained mixture A is dried to water content at 90 DEG C, 100 mesh sieve are crossed, obtained insect-killing composition after pulverizing;
S3: take humic acids that step S1 obtains, step S2 obtained insect-killing composition, organic water-holding agent, mould inhibitor and distilled water respectively in described ratio, mix to obtain mixture B, being carried out making 1.5-2.5mm particle and at 90 DEG C, be dried to water content by described mixture B is 6%, the obtained organic water-holding agent of humic acid type.
Embodiment 2
Utilize the organic water-holding agent of humic acid type of vinegar factory waste liquid, in units of weight part, comprise following raw material: ammonium polyacrylate 45 parts, humic acids 40 parts, distilled water 10 parts, quinoxyfen 0.09 part, insect-killing composition 0.09 part.
The described preparation method utilizing the organic water-holding agent of humic acid type of vinegar factory waste liquid, comprises the following steps:
S1: vinegar factory waste liquid is left standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 80 DEG C and carries out evaporation concentration, being concentrated into pH value is 2.5, stops heating, left at room temperature activation 15h, then add volatile salt adjust ph to 7.5, obtain humic acid solution, humic acid solution being dried at 100 DEG C water content is 5%, 300 mesh sieve are crossed, obtained humic acids after pulverizing;
S2: by China tree, pyrethrum, the root of large-flowered skullcap, capsicum, tobacco, Herba Patriniae, tarragon, Herba Sophorae alopecuroidis co-grinding, liquid is extracted under ultrasonic assistant ethanol extraction method, condition is: solid-liquid ratio is 1:16, ultrasonic power is 180W, alcohol concn is 80%, Extracting temperature is 70 DEG C, extraction time is 60min, gained medical filtration, be concentrated into water content be after 16% mixture A, it is 5% that gained mixture A is dried to water content at 100 DEG C, 300 mesh sieve are crossed, obtained insect-killing composition after pulverizing;
S3: take humic acids that step S1 obtains, step S2 obtained insect-killing composition, organic water-holding agent, mould inhibitor and distilled water respectively in described ratio, mix to obtain mixture B, being carried out making 1.5-2.5mm particle and at 100 DEG C, be dried to water content by described mixture B is 5%, the obtained organic water-holding agent of humic acid type.
Embodiment 3
Utilize the organic water-holding agent of humic acid type of vinegar factory waste liquid, in units of weight part, comprise following raw material: ammonium polyacrylate 40 parts, humic acids 35 parts, distilled water 9 parts, quinoxyfen 0.08 part, insect-killing composition 0.08 part.
The described preparation method utilizing the organic water-holding agent of humic acid type of vinegar factory waste liquid, comprises the following steps:
S1: vinegar factory waste liquid is left standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 75 DEG C and carries out evaporation concentration, being concentrated into pH value is 3, stops heating, left at room temperature activation 14h, then add volatile salt adjust ph to 7, obtain humic acid solution, humic acid solution being dried at 95 DEG C water content is 4%, 200 mesh sieve are crossed, obtained humic acids after pulverizing;
S2: by China tree, pyrethrum, the root of large-flowered skullcap, capsicum, tobacco, Herba Patriniae, tarragon, Herba Sophorae alopecuroidis co-grinding, liquid is extracted under ultrasonic assistant ethanol extraction method, condition is: solid-liquid ratio is 1:12, and ultrasonic power is 160W, and alcohol concn is 65%, Extracting temperature is 60 DEG C, extraction time is 75min, gained medical filtration, be concentrated into water content be after 16% mixture A, it is 4% that gained mixture A is dried to water content at 95 DEG C, 200 mesh sieve are crossed, obtained insect-killing composition after pulverizing;
S3: take humic acids that step S1 obtains, step S2 obtained insect-killing composition, organic water-holding agent, mould inhibitor and distilled water respectively in described ratio, mix to obtain mixture B, being carried out making 1.5-2.5mm particle and at 95 DEG C, be dried to water content by described mixture B is 4%, the obtained organic water-holding agent of humic acid type.
Embodiment 4
A kind of organic water-holding agent of humic acid type utilizing vinegar factory waste liquid, in units of weight part, comprise following raw material: sodium polyacrylate 10 parts, polyacrylic acid potassium 10 parts, ammonium polyacrylate 10 parts, 8 parts, starch graft acrylic acid sodium, humic acids 32 parts, distilled water 8 parts, quinoxyfen 0.07 part, insect-killing composition 0.07 part.
The described preparation method utilizing the organic water-holding agent of humic acid type of vinegar factory waste liquid, comprises the following steps:
S1: vinegar factory waste liquid is left standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 80 DEG C and carries out evaporation concentration, being concentrated into pH value is 2.8, stops heating, left at room temperature activation 15h, then add volatile salt adjust ph to 6.8, obtain humic acid solution, humic acid solution being dried at 100 DEG C water content is 6%, 200 mesh sieve are crossed, obtained humic acids after pulverizing;
S2: by China tree, pyrethrum, the root of large-flowered skullcap, capsicum, tobacco, Herba Patriniae, tarragon, Herba Sophorae alopecuroidis co-grinding, liquid is extracted under ultrasonic assistant ethanol extraction method, condition is: solid-liquid ratio is 1:10, ultrasonic power is 150W, alcohol concn is 60%, Extracting temperature is 70 DEG C, extraction time is 80min, gained medical filtration, be concentrated into water content be after 20% mixture A, it is 6% that gained mixture A is dried to water content at 100 DEG C, 200 mesh sieve are crossed, obtained insect-killing composition after pulverizing;
S3: take humic acids that step S1 obtains, step S2 obtained insect-killing composition, organic water-holding agent, mould inhibitor and distilled water respectively in described ratio, mix to obtain mixture B, being carried out making 1.5-2.5mm particle and at 100 DEG C, be dried to water content by described mixture B is 6%, the obtained organic water-holding agent of humic acid type.
Embodiment 5
A kind of organic water-holding agent of humic acid type utilizing vinegar factory waste liquid, in units of weight part, comprise following raw material: 42 parts, starch graft acrylic acid sodium, humic acids 38 parts, distilled water 10 parts, quinoxyfen 0.04 part, triazolone 0.04 part, insect-killing composition 0.08 part.
The described preparation method utilizing the organic water-holding agent of humic acid type of vinegar factory waste liquid, comprises the following steps:
S1: vinegar factory waste liquid is left standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 75 DEG C and carries out evaporation concentration, being concentrated into pH value is 3.5, stops heating, left at room temperature activation 13h, then add volatile salt adjust ph to 7.2, obtain humic acid solution, humic acid solution being dried at 95 DEG C water content is 5%, 300 mesh sieve are crossed, obtained humic acids after pulverizing;
S2: by China tree, pyrethrum, the root of large-flowered skullcap, capsicum, tobacco, Herba Patriniae, tarragon, Herba Sophorae alopecuroidis co-grinding, liquid is extracted under ultrasonic assistant ethanol extraction method, condition is: solid-liquid ratio is 1:14, and ultrasonic power is 170W, and alcohol concn is 70%, Extracting temperature is 70 DEG C, extraction time is 70min, gained medical filtration, be concentrated into water content be after 18% mixture A, it is 5% that gained mixture A is dried to water content at 95 DEG C, 300 mesh sieve are crossed, obtained insect-killing composition after pulverizing;
S3: take humic acids that step S1 obtains, step S2 obtained insect-killing composition, organic water-holding agent, mould inhibitor and distilled water respectively in described ratio, mix to obtain mixture B, being carried out making 1.5-2.5mm particle and at 95 DEG C, be dried to water content by described mixture B is 5%, the obtained organic water-holding agent of humic acid type.
For the organic water-holding agent of checking humic acid type of the present invention is to the effect of farm crop, for corn, by following experimental verification.
(1) rhizome compares effect experimental
Choose one piece of smooth plot, divide block coldest days of the year end region, every region area about 0.6 mu, respectively to the material of each region Yield-increasing Baallus In Maize following table as base manure, it is 7.5kg/ mu that its amount of application amounts to into mu consumption, and other planting conditions is basically identical.
| Sequence number | Application of substances | Consumption (kg) |
| 1 | The embodiment of the present invention 1 product | 4.5 |
| 2 | The embodiment of the present invention 2 product | 4.5 |
| 3 | The embodiment of the present invention 3 product | 4.5 |
| 4 | Ammonium polyacrylate | 4.5 |
| 5 | The humic acids of embodiment 1 | 4.5 |
| 6 | Quinoxyfen | 4.5 |
| 7 | The insect-killing composition of embodiment 1 | 4.5 |
| 8 | Distilled water | 4.5 |
| 9 | Blank (not using any material) | 4.5 |
Wherein when maize seedling grew to about 6 leaf phases, each process is sampled (five point sampling methods, every point sampling 3) respectively, gather the maize seedling of the 6 leaf phases that were in.Afterwards maize seedling being placed in clear water to clean, over-ground part and underground part scissors are cut off, carrying out rhizome than measuring.
Concrete measuring method is: respectively over-ground part and underground part are placed in 65 DEG C of baking ovens and dry to constant weight, calculates rhizome ratio (ratio of underground part dry weight and over-ground part dry weight), as shown in the table.
| Sequence number | Application of substances | Rhizome ratio |
| 1 | The embodiment of the present invention 1 product | 0.8 |
| 2 | The embodiment of the present invention 2 product | 0.8 |
| 3 | The embodiment of the present invention 3 product | 0.82 |
| 4 | Ammonium polyacrylate | 0.53 |
| 5 | The humic acids of embodiment 1 | 0.56 |
| 6 | Quinoxyfen | 0.55 |
| 7 | The insect-killing composition of embodiment 1 | 0.57 |
| 8 | Distilled water | 0.51 |
| 9 | Blank (not using any material) | 0.51 |
As can be seen from upper table data, the organic water-holding agent of humic acid type of the present invention, relative to using separately ammonium polyacrylate, humic acids, mould inhibitor, insect-killing composition, distilled water and blank, all significantly increase the rhizome ratio of Maize Seedling, describe and use the organic water-holding agent of humic acid type of the present invention, be conducive to the lodging resistance strengthening corn.
(2) product preventing disease and pest effect experimental of the present invention
Choose the corn field that six block specifications are basically identical, be set to corn field a, corn field b, corn field c, corn field d, corn field e, corn field f, corn is planted on six pieces of ground, wherein corn field a, corn field b, corn field c use organic water-holding agent ammonium polyacrylate, corn field d, corn field e, corn field f use the organic water-holding agent of humic acid type of embodiment 1,2,3 respectively, execute 7.5kg with every mu to calculate, observe the corn growth situation of six plots of corn fields.Result shows: corn gloss difference, plant that corn field a, corn field b, corn field c kind are planted are unhealthy, and the speed of growth is slow, and plant is little, yields poorly, and has volt to fall phenomenon; And the corn good luster that corn field d, corn field e, corn field f kind are planted, plant is healthy, leaf dark green is plump, output is high, without volt phenomenon, compared with not using the corn field of product of the present invention, every mu of volume increase 212.4-220.5kg, and use the disease and pest in the corn field of product of the present invention substantially not have, the organic water-holding agent of visible humic acid type of the present invention can not only preventing disease and pest effectively, and can lodging resistance be strengthened, improve corn yield.
Above content can not assert that the present invention specifically implements to be confined to these explanations; for general technical staff of the technical field of the invention; do not departing under concept thereof of the present invention; some simple deduction or replace can also be made, all should be considered as belonging to the scope of patent protection that the present invention is determined by submitted to claims.
Claims (7)
1. one kind utilizes the organic water-holding agent of humic acid type of vinegar factory waste liquid, it is characterized in that, in units of weight part, comprise following raw material: organic water-holding agent 35-45 part, humic acids 30-40 part, distilled water 8-10 part, mould inhibitor 0.06-0.09 part, insect-killing composition 0.06-0.09 part.
2. the organic water-holding agent of humic acid type utilizing vinegar factory waste liquid according to claim 1, it is characterized in that, described organic water-holding agent comprise in polyacrylamide, sodium polyacrylate, polyacrylic acid potassium, ammonium polyacrylate, starch graft acrylic acid sodium one or more.
3. the organic water-holding agent of humic acid type utilizing vinegar factory waste liquid according to claim 1, it is characterized in that, described humic acids is made up of vinegar factory waste liquid.
4. the organic water-holding agent of humic acid type utilizing vinegar factory waste liquid according to claim 1, is characterized in that, described mould inhibitor comprise in quinoxyfen, triazolone one or both.
5. the organic water-holding agent of humic acid type utilizing vinegar factory waste liquid according to claim 1, is characterized in that, described insect-killing composition is extracted made by China tree, pyrethrum, the root of large-flowered skullcap, capsicum, tobacco, Herba Patriniae, tarragon, Herba Sophorae alopecuroidis.
6. the preparation method utilizing the organic water-holding agent of humic acid type of vinegar factory waste liquid according to any one of claim 1-5, is characterized in that, comprise the following steps:
S1: vinegar factory waste liquid is left standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 70-80 DEG C and carries out evaporation concentration, being concentrated into pH value is 2.5-3.5, stops heating, left at room temperature activation 13-15h, then add volatile salt adjust ph to 6.3-7.5, obtain humic acid solution, humic acid solution is dried to water content≤6% at 90-100 DEG C, 100-300 mesh sieve is crossed, obtained humic acids after pulverizing;
S2: by China tree, pyrethrum, the root of large-flowered skullcap, capsicum, tobacco, Herba Patriniae, tarragon, Herba Sophorae alopecuroidis co-grinding, liquid is extracted under ultrasonic assistant ethanol extraction method, gained medical filtration, to be concentrated into after water content≤20% to obtain mixture A, gained mixture A is dried to water content≤6% at 90-100 DEG C, 100-300 mesh sieve is crossed, obtained insect-killing composition after pulverizing;
S3: take humic acids that step S1 obtains, step S2 obtained insect-killing composition, organic water-holding agent, mould inhibitor and distilled water respectively in described ratio, mix to obtain mixture B, described mixture B is carried out making 1.5-2.5mm particle and be dried to water content≤6% at 90-100 DEG C, the obtained organic water-holding agent of humic acid type.
7. the preparation method utilizing the organic water-holding agent of humic acid type of vinegar factory waste liquid according to claim 6, it is characterized in that, the condition that the ethanol extraction method of ultrasonic assistant described in step S2 extracts liquid is: solid-liquid ratio is 1:8-16, ultrasonic power is 140-180W, alcohol concn is 50%-80%, Extracting temperature is 50-70 DEG C, and extraction time is 60-90min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510702699.0A CN105294361A (en) | 2015-10-26 | 2015-10-26 | Humic acid type organic water-retaining agent using vinegar factory liquid waste and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510702699.0A CN105294361A (en) | 2015-10-26 | 2015-10-26 | Humic acid type organic water-retaining agent using vinegar factory liquid waste and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105294361A true CN105294361A (en) | 2016-02-03 |
Family
ID=55192296
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510702699.0A Pending CN105294361A (en) | 2015-10-26 | 2015-10-26 | Humic acid type organic water-retaining agent using vinegar factory liquid waste and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105294361A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105948402A (en) * | 2016-06-25 | 2016-09-21 | 张莘蔓 | Preparation method of oily sewage biofermentation treating agent |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20120099873A (en) * | 2011-03-02 | 2012-09-12 | 김정환 | Eco-friendly custom crop rhizodegradation enzyme complexes |
| CN103664384A (en) * | 2013-12-13 | 2014-03-26 | 叶长东 | Humid acid type organic water-retaining agent containing wastes in sugar refinery and alcohol plant |
| CN103664383A (en) * | 2013-12-13 | 2014-03-26 | 叶长东 | Humid acid type organic-inorganic water-retaining agent containing wastes in sugar refinery and alcohol plant |
-
2015
- 2015-10-26 CN CN201510702699.0A patent/CN105294361A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20120099873A (en) * | 2011-03-02 | 2012-09-12 | 김정환 | Eco-friendly custom crop rhizodegradation enzyme complexes |
| CN103664384A (en) * | 2013-12-13 | 2014-03-26 | 叶长东 | Humid acid type organic water-retaining agent containing wastes in sugar refinery and alcohol plant |
| CN103664383A (en) * | 2013-12-13 | 2014-03-26 | 叶长东 | Humid acid type organic-inorganic water-retaining agent containing wastes in sugar refinery and alcohol plant |
Non-Patent Citations (3)
| Title |
|---|
| 中华人民共和国科学技术部农村与社会发展司等编: "《中国节水农业发展战略研究与实践》", 31 March 2006 * |
| 李瑞波等: "《生物腐植酸肥料生产与应用》", 30 November 2011 * |
| 黄亚东等: "《发酵调味品生产技术》", 30 June 2014 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105948402A (en) * | 2016-06-25 | 2016-09-21 | 张莘蔓 | Preparation method of oily sewage biofermentation treating agent |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105542777A (en) | Humic acid type water-retaining agent by using edible vinegar factory waste liquid and preparation method thereof | |
| CN105394111A (en) | Organic conditioner utilizing starch industrial production wastewater and preparation method thereof | |
| CN105295934A (en) | Novel water-retaining agent using vinegar factory liquid waste and preparation method thereof | |
| CN102775238A (en) | Organic plant pesticide fertilizer with pesticidal and bactericidal effects and production technique thereof | |
| CN102217661B (en) | Botanical bactericide and preparation method and application thereof | |
| CN105237138A (en) | Release-controlled fertilizer for Chinese yam and preparation method thereof | |
| CN105198602A (en) | Fertilizer with natural insecticidal effect and preparation method thereof | |
| CN105272527A (en) | Sweet potato controlled release fertilizer and preparation method thereof | |
| CN105732214A (en) | Special mothproof fertilizer for Wogan planting and preparation method thereof | |
| CN105542778A (en) | Humic acid type organic water-retaining agent and preparation method thereof | |
| CN105272539A (en) | Organic plant medicinal fertilizer with desinsection and sterilization efficacy, and preparation method thereof | |
| CN105419813A (en) | Novel conditioning agent utilizing starch industry production wastewater and preparation method of novel conditioning agent | |
| CN105272630A (en) | Method for preparing fertilizer capable of controlling soil crop pests | |
| CN105503385A (en) | Conditioner using production wastewater in starch industry and preparation method of conditioner | |
| CN108093730B (en) | Method for returning residual cucumber plants to field in sunlight greenhouse and application thereof | |
| CN105315071A (en) | Humic acid type water-retaining agent utilizing vinegar factory waste liquid, and preparation method for humic acid type water-retaining agent | |
| CN105542780A (en) | Novel water-retaining agent by using edible vinegar factory waste liquid and preparation method thereof | |
| CN105272606A (en) | Controlled release fertilizer for tomatoes and preparation method of controlled release fertilizer | |
| CN107372653A (en) | Medicament and the application of snail are prevented and treated in officinal dendrobium stem plantation production | |
| CN105567243A (en) | Humic acid-type inorganic-organic water-retaining agent utilizing waste liquid of vinegar factory and preparation method for humic acid-type inorganic-organic water-retaining agent | |
| CN110786344A (en) | Method for preventing and treating downy mildew of fruits and vegetables by utilizing baeckea frutescens branch and leaf extracting solution | |
| CN105565977A (en) | Controlled-release fertilizer for oranges and preparation method of controlled-release fertilizer | |
| CN105542783A (en) | Humic acid type inorganic water-retaining agent by using edible vinegar factory waste liquid and preparation method thereof | |
| CN105272529A (en) | Pumpkin controlled release fertilizer and preparation method thereof | |
| CN106034605B (en) | A kind of prevention and control processing method of pseudo-ginseng leaf jaundice |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160203 |
|
| RJ01 | Rejection of invention patent application after publication |