CN105287471A - Quick-dissolving branched chain amino acid product - Google Patents
Quick-dissolving branched chain amino acid product Download PDFInfo
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- CN105287471A CN105287471A CN201510707301.2A CN201510707301A CN105287471A CN 105287471 A CN105287471 A CN 105287471A CN 201510707301 A CN201510707301 A CN 201510707301A CN 105287471 A CN105287471 A CN 105287471A
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Abstract
The invention discloses a quick-dissolving branched chain amino acid product, and belongs to the technical field of preparations. The quick-dissolving branched chain amino acid is prepared by taking sunflower seed phospholipid and food-grade phospholipase A2 as auxiliaries and taking a 50% ethanol water solution as mixed solvent through a drying method of combining hot-air drying with catalytic infrared radiation. The quick-dissolving branched chain amino acid product is good in quick-dissolving effect, good in stability and long in shelf life.
Description
Technical field
The present invention relates to a kind of instant branched-amino acid product, belong to preparation technique field.
Background technology
Branched-chain amino acid (BCAA:BranchedChainAminoAcids) refers to a group aminoacid containing side chain in structure, includes leucine, isoleucine, valine.This three seed amino acid belongs to essential amino acids, has inseparable relation, require no body metabolism with synthetic protein, just directly can supply energy to human body and use.In human body, the muscle protein of about 33% is become by BCAA Group, accounts for essential amino acids about about 35%.The lowering of concentration of catabolism, fatigue and Testosterone (testosterone) that the motion (such as: heavily instruct, extreme sport, body-building) of middle intensity can cause the content of BCAA to decline fast causing muscle.BCAA is the pith of muscle protein, and when the BCAA in blood of human body is inadequate, just the BCCA that can decompose in muscle makes the energy, produce power, carbon dioxide and water.During training, in skeletal muscle, the consumption of BCAA quickly, supplements the muscle that branched-chain amino acid can improve motor capacity, delay fatigue, the reparation loss because of motion before motion or in motion.Other amino acid whose absorption is contributed to canteen BCAA at once or after motion after motion.
The main function of BCAA has: recover moisture and the electrolyte of health, recover glycogen deposit rapidly, strengthen muscular endurance, rebuild intramuscular protein.Generally speaking, the function of BCAA is used to the synthesis and the metabolism that promote rest period protein, the decomposition of muscular tissue can also be reduced except accelerating muscle synthesis, and BCAA has good anti-decomposability, can be used for preventing the loss of muscle and protein, can also insulin be stimulated simultaneously, promote that muscle is to other amino acid whose absorptions.
At present, commercially available amino acid products existence is dissolved slowly, the problem of bad dispersibility, can not meet the Market Demand dissolved rapidly.
Summary of the invention
In order to overcome the problems referred to above, the invention provides a kind of instant branched-amino acid product, described instant branched-amino acid product take branched-chain amino acid as raw material, the mixture of sunflower seed phospholipid and food stage phospholipase A 2 is auxiliary agent, wherein the mass ratio of branched-chain amino acid and sunflower seed phospholipid is 100:2.5-100:1, and is added with the food stage phospholipase A 2 of 10-20U by every g sunflower seed phospholipid.
The present invention also provides a kind of preparation method of described instant branched-amino acid product, described method is take branched-chain amino acid as raw material, the mixture of sunflower seed phospholipid and food stage phospholipase A 2 is auxiliary agent, the ethanol water being 40-55% with volume fraction of ethanol mixes, stir 30min, after hot air drying and the process of catalysis type infrared radiation, pulverize and sieve, obtain instant branched-amino acid product.
Described branched-chain amino acid in one embodiment of the invention, can be any one or the two or more mixing in leucine, isoleucine, valine.
Described method, in one embodiment of the invention, according to the mass fraction, sunflower seed phosphatidase 1-2.5 parts, ethanol water 15-25 part in every 100 parts of raw materials, add the food stage phospholipase A 2 of 10-20U by every g sunflower seed phospholipid.Preferably, sunflower seed phosphatidase 1 .5 part, ethanol water 20 parts, food stage phospholipase A 2 15U/g sunflower seed phospholipid.
Described method in one embodiment of the invention, is first at 60-70 DEG C of hot air drying 1-2h, then catalysis type infrared radiation process 1-3min.
Described catalysis type infrared radiation, in one embodiment of the invention, the distance between the infrared emission plate of its datatron and bed of material surface is 30 ~ 40cm, thickness of feed layer 4 ~ 10mm, the gaseous-pressure 1 ~ 2kPa of the infrared datatron of catalysis type; Infrared emitting panel surface temperature 150 ~ 400 DEG C.
Described method, in one embodiment of the invention, preferably 65 DEG C of hot air drying 1h, catalysis type infrared radiation process 2min, thickness of feed layer 4mm.
Describedly sieving, in one embodiment of the invention, was 120-150 mesh sieve.
Described method, in one embodiment of the invention, specifically:
(1) every 100g branched-chain amino acid, adds 1.5g sunflower seed phospholipid, 22.5U food stage phospholipase A 2, then adds the ethanol water 20 parts of 50%, mix and blend 30min in mixer;
(2) material previous step mixed is at 65 DEG C of hot air drying 1h, and then catalysis type infrared radiation process 2min, thickness of feed layer 4mm, regulates the distance between infrared emission plate and bed of material surface to be 40cm;
(3) material handled well is put into pulverizer to pulverize, then cross 120-150 mesh sieve, obtain instant branched-amino acid product.
Beneficial effect of the present invention: (1) instant branched-amino acid product of the present invention, adopt sunflower seed phospholipid and food stage phospholipase A 2 as auxiliary agent, by controlling the ratio of sunflower seed phospholipid and phospholipase, hydrophilic group in sunflower seed phospholipid is effectively discharged, both play synergism, improve the dissolubility of amino acid products, dispersibility, the 2g product jitter time dropped in water is 10s, dissolving settling time is 3min28s; (2) adopt the ethanol water of 50% as mixed solvent, accelerate dry carrying out, can also be cost-saving relative to high concentration ethanol; (3) adopt hot air drying in conjunction with the method for catalysis type infra-red radiation, accelerate rate of drying, early stage, hot air drying can promote the volatilization of ethanol, later stage adopts catalysis type infrared radiation short time treatment, not only accelerate drying, and simultaneously the high-temperature process deactivation phospholipase of infrared radiation, the amino acid whose stability of effective guarantee, can not product quality be affected; About 1h can complete drying simultaneously, effectively reduces production cost and expenditure of time, effectively reduces the dust problem that material dry blending causes, improve working environment; (4) simple by the inventive method technique, be easy to suitability for industrialized production; The instant branched-amino acid product obtained, uniform particle diameter, instant effective, good stability, shelf life are long.
Detailed description of the invention
Dispersibility assay method in water: refer to the speed that combination of amino acids composition granule disperses in water is also the speed of wetting of particulates " sinking ".Assay method: get 150ml beaker, and the 25 DEG C of water adding 100ml wherein, leave standstill bubble-free in 15 ~ 45s to water, the water surface be tranquil.Sample thief 2g (being accurate to 0.01g) is poured into water rapidly from beaker overcentre 50mm, and the time of the whole moistening of timing sample also at the bottom of " sinking " to cup, record required time T1, s, i.e. jitter time in water.
Settling time is dissolved: refer to that combination of amino acids composition granule is under the condition stirred or vibrate, and is dissolved to the time of finding of naked eye clear in water in water.Assay method: sample thief 2g (being accurate to 0.01g) adds to and is equipped with in the 150ml beaker of 25 DEG C of 100ml water, at the uniform velocity stir with 140-160r/min, (completely water-solublely solution clear is characterized by sample is completely water-soluble, without precipitation and floating particle), and record required time T2, min.
Solution turbidity in water: be used for express amino acid composition solution clarity feature.Assay method: sample thief 2g (being accurate to 0.01g) adds 25 DEG C to and is equipped with in the 150ml beaker of 100ml water, at the uniform velocity stirs with 140-160r/min, completely water-soluble to sample.Completely water-solublely be characterized by solution clear, without precipitation and floating particle; Transmissometer is used to measure solution turbidity, and record.
Embodiment 1:
Prepare instant amino acid product by the following method:
(1) branched-chain amino acid 100kg (wherein the mass ratio of leucine, isoleucine, valine is 2:1:1) is got, add the food stage phospholipase A 2 (200U/mg of sunflower seed phospholipid (purchased from Hubei Ju Sheng Science and Technology Ltd.) 1.5kg and 22500U, Jinan Chang Nuo Bioisystech Co., Ltd), add the ethanol water 20kg of 50% again, mix and blend 30min in mixer;
(2) material previous step mixed is at 65 DEG C of hot air drying 1h, and then catalysis type infrared radiation process 2min, thickness of feed layer 4mm, regulates the distance between infrared emission plate and bed of material surface to be 40cm; The wherein gaseous-pressure 1 ~ 2kPa of the infrared datatron of catalysis type; Infrared emitting panel surface temperature 150 ~ 400 DEG C.
(3) material handled well is put into pulverizer to pulverize, then cross 120 mesh sieves, obtain instant branched-amino acid product.
2g product drops in water, and jitter time is 10s, and dissolving settling time in water is 3min28s (if use 1g product, then 1min30s can dissolve completely, and speed is very fast).Simultaneously aqueous solution clear, without precipitation, without floating, non-foam, in water, solution turbidity is 10NTU.After pulverizing, 120 order sieving rates reach 98%, and size is homogeneous, and particle diameter accounts for 92% at 100-120um.
After the packing of product, be placed in 45 DEG C, 75% humidity climatic chamber accelerated test 3 months, the dispersibility, dissolubility, turbidity etc. of product all do not change; In less than 25 DEG C, shady and cool place's storage 2 years, product does not lump, and dispersibility, dissolubility, turbidity etc. all do not change.Product stability of the present invention is good, shelf life is long.
Embodiment 2: auxiliary agent mixing ratio is on the impact of product
Prepare instant amino acid product by the following method:
(1) get branched-chain amino acid 100kg, add the food stage phospholipase A 2 of sunflower seed phosphatidase 2 .5kg, 50000U, then add the ethanol water 25kg of 45%, mix and blend 30min in mixer;
(2) material previous step mixed is at 70 DEG C of hot air drying 2h, and then catalysis type infrared radiation process 3min, thickness of feed layer 6mm, regulates the distance between infrared emission plate and bed of material surface to be 30cm; The wherein gaseous-pressure 1 ~ 2kPa of the infrared datatron of catalysis type; Infrared emitting panel surface temperature 150 ~ 400 DEG C.
(3) material handled well is put into pulverizer to pulverize, then cross 120 mesh sieves, obtain instant branched-amino acid product.
2g product drops in water, and jitter time is 12s, and dissolving settling time in water is 4min.Simultaneously aqueous solution clear, without precipitation, without floating, non-foam, in water, solution turbidity is 12NTU.After pulverizing, 120 order sieving rates reach 92%, and size is homogeneous, and particle diameter accounts for 88% at 100-120um.In less than 25 DEG C, shady and cool place's storage 2 years, product does not lump, and dispersibility, dissolubility, turbidity etc. all do not change.Product stability of the present invention is good, shelf life is long.
The present invention also finds, when other conditions are identical, when food stage phospholipase A 2 addition excessive (being greater than 30U/g sunflower seed phospholipid) or addition very few (being less than 6U/g sunflower seed phospholipid), product solubility property significantly reduces, and dissolution time is respectively 5min20s, 4min30s.Illustrate that phosphide enzyme and sunflower seed content of phospholipid control within the scope of certain proportion, the hydrophilic group in sunflower seed phospholipid just can be made effectively to discharge, just can significantly improve the instant performance of product.
Embodiment 3: auxiliary agent kind is on the impact of product
Prepare instant amino acid product by the following method:
(1) get branched-chain amino acid 100kg, add sunflower seed phosphatidase 1 kg, 10000U food stage phospholipase A 2, then add the ethanol water 15kg of 55%, mix and blend 30min in mixer;
(2) material previous step mixed is at 60 DEG C of hot air drying 1.5h, and then catalysis type infrared radiation process 1min, thickness of feed layer 10mm, regulates the distance between infrared emission plate and bed of material surface to be 35cm;
(3) material handled well is put into pulverizer to pulverize, then cross 120 mesh sieves, obtain instant branched-amino acid product.
2g product drops in water, and jitter time is 12s, and dissolving settling time in water is 4min8s.Simultaneously aqueous solution clear, without precipitation, without floating, non-foam, in water, solution turbidity is 13NTU.After pulverizing, 120 order sieving rates reach 90%, and size is homogeneous, and particle diameter accounts for 89% at 100-120um.In less than 25 DEG C, shady and cool place's storage 2 years, product does not lump, and dispersibility, dissolubility, turbidity etc. all do not change.Product stability of the present invention is good, shelf life is long.
The present invention also finds, when concentration of alcohol too low (lower than 40%), drying time significantly increases, and hot-wind-drying time is that 3h just can reach above-mentioned effect.And concentration of alcohol high (such as 60%), not only increase cost, and the instant performance of product is not also significantly improved.In addition, other conditions are identical with embodiment, and when using common fats enzyme or Phospholipase C to replace phospholipase A 2,2g product drops in water, and jitter time is respectively 16s, 14s, and dissolving settling time in water is 5min22s, 6min43s.
Embodiment 4: auxiliary agent kind is on the impact of product
Prepare instant amino acid product by the following method:
(1) get branched-chain amino acid 100kg, add the food stage phospholipase A 2 of soybean phospholipid 1.5kg and 22500U, then add the ethanol water 20kg of 50%, mix and blend 30min in mixer;
(2) material previous step mixed is at 65 DEG C of hot air drying 1h, and then catalysis type infrared radiation process 2min, thickness of feed layer 4mm, regulates the distance between infrared emission plate and bed of material surface to be 40cm;
(3) material handled well is put into pulverizer to pulverize, then cross 120 mesh sieves, obtain instant branched-amino acid product.
2g product drops in water, and jitter time is 15s, and dissolving settling time in water is 5min48s.Aqueous solution clear, nothing precipitation, on a small quantity floating, a small amount of foam simultaneously, in water, solution turbidity is 18NTU.After pulverizing, 120 order sieving rates reach 89%, and size is homogeneous, and particle diameter accounts for 90% at 100-120um.Be placed in 45 DEG C, 75% humidity climatic chamber accelerated test 3 months, the dispersibility of product is constant, but dissolves that settling time is increased to 7min30s, turbidity solution turbidity is 23NTU.In less than 25 DEG C, shady and cool place's storage 1 year, just there is caking phenomenon in product.
Embodiment 5: auxiliary agent kind is on the impact of product
Prepare instant amino acid product by the following method:
(1) get branched-chain amino acid 100kg, add sunflower seed phosphatidase 1 .5kg, then add the ethanol water 20kg of 50%, mix and blend 30min in mixer;
(2) material previous step mixed is at 65 DEG C of hot air drying 1h, and then catalysis type infrared radiation process 2min, thickness of feed layer 4mm, regulates the distance between infrared emission plate and bed of material surface to be 40cm;
(3) material handled well is put into pulverizer to pulverize, then cross 120 mesh sieves, obtain instant branched-amino acid product.
Dropped in water by the branched-amino acid product 2g obtained, jitter time is 15s, and dissolving settling time in water is 6min43s.After pulverizing, 120 order sieving rates reach 92%, and size is homogeneous, and particle diameter accounts for 90% at 100-120um.
Under similarity condition, use food stage phospholipase A 2 to replace sunflower seed phospholipid, the product 2g obtained drops in water, and jitter time is 30s, and dissolving settling time in water is 15min, cannot reach instant at all.
Embodiment 6: drying condition is on the impact of product
Prepare instant amino acid product by the following method: (1) gets branched-chain amino acid 100kg, add the food stage phospholipase A 2 of sunflower seed phosphatidase 1 .5kg and 22500U, then add the ethanol water 20kg of 50%, mix and blend 30min in mixer; (2) material previous step mixed is at 70 DEG C of hot air drying 2h, and then catalysis type infrared radiation process 2min, thickness of feed layer 4mm, regulates the distance between infrared emission plate and bed of material surface to be 40cm; (3) material handled well is put into pulverizer to pulverize, then cross 120 mesh sieves, obtain instant branched-amino acid product.Dropped in water by the 2g product obtained, jitter time is 12s, and dissolving settling time in water is 4min18s (if use 1g product, then 112s can dissolve completely, and speed is very fast).Simultaneously aqueous solution clear, without precipitation, without floating, non-foam, in water, solution turbidity is 11NTU.Compared with embodiment 1, embodiment 1 is aided with infrared radiation technology, significantly can shorten drying time, the instant better effects if of the product obtained.
Embodiment 7: drying condition is on the impact of product
Prepare instant amino acid product by the following method:
(1) get branched-chain amino acid 100kg, add the food stage phospholipase A 2 of sunflower seed phosphatidase 1 .5kg and 22500U, then add the ethanol water 20kg of 50%, mix and blend 30min in mixer; (2) material catalysis type infrared radiation process 20min previous step mixed, thickness of feed layer 4mm, regulate the distance between infrared emission plate and bed of material surface to be 40cm; (3) material handled well is put into pulverizer to pulverize, then cross 120 mesh sieves, obtain instant branched-amino acid product.
Dropped in water by the 2g product obtained, jitter time is 11s, and dissolving settling time in water is 4min (if use 1g product, then 102s can dissolve completely, and speed is very fast), and in water, solution turbidity is 13NTU.But the catalysis type infrared radiation time is long, aminoacid quality can be affected, simultaneously catalysis type infrared radiation machine long-play, can cause certain infringement by equipment itself.
Although the present invention with preferred embodiment openly as above; but it is also not used to limit the present invention, any person skilled in the art, without departing from the spirit and scope of the present invention; all can do various changes and modification, what therefore protection scope of the present invention should define with claims is as the criterion.
Claims (6)
1. an instant branched-amino acid product, it is characterized in that, described instant amino acid product take branched-chain amino acid as the mixture of raw material, sunflower seed phospholipid and food stage phospholipase A 2 is auxiliary agent, wherein the mass ratio of branched-chain amino acid and sunflower seed phospholipid is 100:2.5-100:1, and is added with the food stage phospholipase A 2 of 10-20U by every g sunflower seed phospholipid.
2. instant branched-amino acid product according to claim 1, it is characterized in that, described product prepares by the following method: being take branched-chain amino acid as raw material, the mixture of sunflower seed phospholipid and food stage phospholipase A 2 is auxiliary agent, with the ethanol water mix and blend 30min that volume fraction of ethanol is 40-55%, after hot air drying and the process of catalysis type infrared radiation, pulverize and sieve, obtain branched-amino granulates; According to the mass fraction, sunflower seed phosphatidase 1-2.5 parts, ethanol water 15-25 part in every 100 parts of raw materials; In described auxiliary agent, add the food stage phospholipase A 2 of 10-20U by every g sunflower seed phospholipid.
3. instant branched-amino acid product according to claim 2, is characterized in that, described is first at 60-70 DEG C of hot air drying 1-2h in conjunction with hot air drying and catalysis type infrared radiation, then catalysis type infrared radiation process 1-3min; Distance between the infrared emission plate of the datatron of described catalysis type infrared radiation and bed of material surface is 30 ~ 40cm, thickness of feed layer 4 ~ 10mm, the gaseous-pressure 1 ~ 2kPa of the infrared datatron of catalysis type; Infrared emitting panel surface temperature 150 ~ 400 DEG C.
4. instant branched-amino acid product according to claim 2, is characterized in that, described in sieve be 120-150 mesh sieve.
5. instant branched-amino acid product according to claim 2, is characterized in that, described method specifically:
(1) every 100g branched-chain amino acid, adds 1.5g sunflower seed phospholipid, 22.5U food stage phospholipase A 2, then adds the ethanol water 20 parts of 50%, and in mixer, mix homogeneously stirs 30min;
(2) then by the material that mixes at 65 DEG C of hot air drying 1h, then catalysis type infrared radiation process 2min, thickness of feed layer 4mm, regulates the distance between infrared emission plate and bed of material surface to be 40cm;
(3) material handled well is put into pulverizer to pulverize, then cross 120-150 mesh sieve, obtain instant branched-amino acid product.
6. instant branched-amino acid product according to claim 1, is characterized in that, described branched-chain amino acid is following any one or two or more mixing: leucine, isoleucine, valine.
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| WO2013109863A1 (en) * | 2012-01-20 | 2013-07-25 | Milk Specialties Company | Method of instantizing amino acids |
| CN102908337A (en) * | 2012-10-12 | 2013-02-06 | 大连医诺生物有限公司 | Microencapsulated amino-acid composition and preparation method of microencapsulated amino-acid composition |
| CN103536585A (en) * | 2013-10-24 | 2014-01-29 | 江苏神华药业有限公司 | Method for preparing instant branched chain amino acid by extrusion method |
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