CN108217776A - It is a kind of to be used to handle medicament at water source of chemical contamination and preparation method thereof - Google Patents
It is a kind of to be used to handle medicament at water source of chemical contamination and preparation method thereof Download PDFInfo
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- CN108217776A CN108217776A CN201810124808.9A CN201810124808A CN108217776A CN 108217776 A CN108217776 A CN 108217776A CN 201810124808 A CN201810124808 A CN 201810124808A CN 108217776 A CN108217776 A CN 108217776A
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
- C02F2101/20—Heavy metals or heavy metal compounds
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- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Separation Of Suspended Particles By Flocculating Agents (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of for handling medicament at water source of chemical contamination and preparation method thereof, includes the raw material of following parts by weight：25 38 parts of 12 16 parts of stalk, 24 30 parts of sodium bentonite, 48 parts of cinnamic acid, 10 13 parts of ion exchange resin, 68 parts of polyacrylamide, 1.2 2.5 parts of casein, 8 15 parts of zeolite powder, 2.5 4 parts of sodium cellulose glycolate, 35 parts of vaseline, 15 18 parts of ethylene glycol, 8 12 parts of slag, 6 10 parts of citric acid and cyanobacteria.This product raw material sources are extensive, and various raw materials play synergistic effect under corresponding preparation process, and the finished product of preparation has the COD in water and heavy metal ion very high removal rate, and using effect is good, can meet the use demand of people.
Description
Technical field
The present invention relates to chemical contamination process field, the medicament at specifically a kind of water source for being used to handle chemical contamination.
Background technology
The inorganic matter that water is made of two kinds of hydrogen, oxygen elements is nontoxic.It is the transparent liquid of colorless and odorless at normal temperatures and pressures
Body is referred to as the source of human life.Water, including natural water（River, lake, atmospheric water, seawater, underground water etc.）, distilled water
It is pure water, artificial water processed（Hydrogen-oxygen atom is made to combine obtained water by chemical reaction）.Water is most common substance on the earth
One of, it is the valuable source of all life existence and the most important composition portion of organism including inorganic chemical, the mankind
Point, water plays important function in Life Evolution.
With the increase of chemical agent usage amount and the quickening of process of industrialization in people's rural activity, produce a large amount of
Rural sewage and trade effluent, people understand direct emission mostly when handling rural sewage and trade effluent, this will be to water source
It pollutes, hidden danger is brought to environmental ecology and health.People must be handled the chemical contamination in water source, dirty
Water treatment agent is most common treatment of pharmaceutical products, but existing sewage-treating agent treatment effect is not thorough, this just makes for people
With bringing inconvenience.
Invention content
The purpose of the present invention is to provide a kind of for handling the medicament at the water source of chemical contamination, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the present invention provides following technical solution：
A kind of medicament at the water source for being used to handle chemical contamination includes the raw material of following parts by weight：12-16 parts of stalk, sodium base are swollen
Moisten 24-30 parts of soil, 4-8 parts of cinnamic acid, 10-13 parts of ion exchange resin, 6-8 parts of polyacrylamide, 1.2-2.5 parts of casein, boiling
8-15 parts of mountain flour, 2.5-4 parts of sodium cellulose glycolate, 3-5 parts of vaseline, 15-18 parts of ethylene glycol, 8-12 parts of slag, citric acid
6-10 parts and 25-38 parts of cyanobacteria.
As further embodiment of the present invention：Stalk include wheat stalk, maize straw, sugarcane stalk, soybean stalk and
One or several kinds of mixtures in broomcorn straw, ion exchange resin use cation exchange resin.
As further embodiment of the present invention：The grain size of slag is 1.56-3.86mm, and the grain size of sodium cellulose glycolate is
0.34-0.73mm。
The preparation method of the medicament at the water source for being used to handle chemical contamination, is as follows：
Cyanobacteria is cleaned up and freezes 2-4 hours in subzero 25 environment to subzero 20 degrees Celsius, then powder by step 1
Broken and mistake 100-120 mesh sieves, the enzyme of water and its weight 1-2% for adding 3-5 times of its weight are put in reaction kettle, add in nothing
Machine acid adjusts pH value as 4.6-5.8 and is stirred 80-100 minutes under 36-44 degrees Celsius, then high temperature bath enzyme deactivation, centrifuges
Filtering can obtain cyanobacteria enzymolysis liquid；
Stalk, vaseline, zeolite powder and slag are milled to 200-240 by step 2 with the rotating speed of 30-45rpm in the ball mill
Mesh obtains the first mixture；
Step 3 mixes cinnamic acid, sodium bentonite, polyacrylamide and ethylene glycol and supersonic oscillations 20-30 minutes,
Obtain the second mixture；
Ion exchange resin and casein are immersed in cyanobacteria enzymolysis liquid and supersonic oscillations 15-20 minutes, then by step 4
It adds in citric acid and stirs evenly, obtain third mixture；
Step 5 stirs evenly the first mixture, the second mixture, third mixture and sodium cellulose glycolate and in 3-
8 degrees Celsius are kept for 4-6 hours, are then dried under 50-66 degrees Celsius and are crossed 160-240 mesh sieve, you can obtain finished product.
As further embodiment of the present invention：In step 4 before citric acid is added in electric field strength is 25-40KV
It is kept for 10-15 minutes.
The application method of the medicament at the water source for being used to handle chemical contamination：By finished product and sewage according to mass ratio 1:
100-140 is mixed, and is stirred evenly.
Compared with prior art, the beneficial effects of the invention are as follows：This product raw material sources are extensive, and various raw materials are corresponding
Synergistic effect is played under preparation process, the finished product of preparation has the COD in water and heavy metal ion very high removal rate, makes
It is good with effect, the use demand of people can be met.
Specific embodiment
The technical solution of this patent is described in more detail With reference to embodiment.
Embodiment 1
A kind of medicament at the water source for being used to handle chemical contamination includes the raw material of following parts by weight：12 parts of stalk, sodium bentonite
24 parts, 4 parts of cinnamic acid, 10 parts of ion exchange resin, 6 parts of polyacrylamide, 1.2 parts of casein, 8 parts of zeolite powder, hydroxylmethyl cellulose
25 parts of plain 2.5 parts of sodium, 3 parts of vaseline, 15 parts of ethylene glycol, 8 parts of slag, 6 parts of citric acid and cyanobacteria.Stalk include wheat stalk,
The mixture of sugarcane stalk and soybean stalk, ion exchange resin use cation exchange resin.
The preparation method of the medicament at the water source for being used to handle chemical contamination, is as follows：
Cyanobacteria is cleaned up and freezes 3 hours in subzero 24 degrees Celsius of environment by step 1, is then crushed and mistake
100 mesh sieve, and add the water of 4 times of its weight and the enzyme of its weight 1% is put in reaction kettle, and it is 4.8 to add in inorganic acid and adjust pH value
And it is stirred 90 minutes under 40 degrees Celsius, then high temperature bath enzyme deactivation, centrifugal filtration can obtain cyanobacteria enzymolysis liquid；
Stalk, vaseline, zeolite powder and slag are milled to 240 mesh with the rotating speed of 30rpm in the ball mill, obtained by step 2
First mixture；
Cinnamic acid, sodium bentonite, polyacrylamide and ethylene glycol are mixed and supersonic oscillations 25 minutes, obtained by step 3
To the second mixture；
Ion exchange resin and casein are immersed in cyanobacteria enzymolysis liquid and supersonic oscillations 18 minutes, Ran Houjia by step 4
Enter citric acid and stir evenly, obtain third mixture；
Step 5 stirs evenly the first mixture, the second mixture, third mixture and sodium cellulose glycolate and 6
It degree Celsius is kept for 4 hours, it is then dry under 56 degrees Celsius and cross 180 mesh sieve, you can to obtain finished product.
The application method of the medicament at the water source for being used to handle chemical contamination：By finished product and sewage according to mass ratio 1:
120 mixing, stir evenly.
The sewage after chemical contamination is handled using the product of embodiment 1, the removal rate of COD is in water after processing
98.1%, the removal rate of heavy metal is 89.4%
Embodiment 2
A kind of medicament at the water source for being used to handle chemical contamination includes the raw material of following parts by weight：13.5 parts of stalk, Na-bentonite
27 parts of soil, 5.5 parts of cinnamic acid, 11 parts of ion exchange resin, 6.6 parts of polyacrylamide, 1.6 parts of casein, 11 parts of zeolite powder, hydroxyl first
32 parts of 3 parts of base sodium cellulosate, 3.8 parts of vaseline, 16.5 parts of ethylene glycol, 10 parts of slag, 7.5 parts of citric acid and cyanobacteria.Slag
Grain size is 1.93mm, and the grain size of sodium cellulose glycolate is 0.56mm.
The preparation method of the medicament at the water source for being used to handle chemical contamination, is as follows：
Cyanobacteria is cleaned up and freezes 3 hours in subzero 20 degrees Celsius of environment by step 1, is then crushed and mistake
120 mesh sieve, and add the water of 5 times of its weight and the enzyme of its weight 2% is put in reaction kettle, and it is 5.3 to add in inorganic acid and adjust pH value
And it is stirred 90 minutes under 42 degrees Celsius, then high temperature bath enzyme deactivation, centrifugal filtration can obtain cyanobacteria enzymolysis liquid；
Stalk, vaseline, zeolite powder and slag are milled to 200 mesh with the rotating speed of 45rpm in the ball mill, obtained by step 2
First mixture；
Cinnamic acid, sodium bentonite, polyacrylamide and ethylene glycol are mixed and supersonic oscillations 25 minutes, obtained by step 3
To the second mixture；
Ion exchange resin and casein are immersed in cyanobacteria enzymolysis liquid and supersonic oscillations 18 minutes, Ran Houjia by step 4
Enter citric acid and stir evenly, obtain third mixture；
Step 5 stirs evenly the first mixture, the second mixture, third mixture and sodium cellulose glycolate and 4
It degree Celsius is kept for 4 hours, it is then dry at 62 c and cross 210 mesh sieve, you can to obtain finished product.
The application method of the medicament at the water source for being used to handle chemical contamination：By finished product and sewage according to mass ratio 1:
130 mixing, stir evenly
The sewage after chemical contamination is handled using the product of embodiment 2, the removal rate of COD is 93.5% in water after processing,
The removal rate of heavy metal is 94.1%
Embodiment 3
A kind of medicament at the water source for being used to handle chemical contamination includes the raw material of following parts by weight：15 parts of stalk, sodium bentonite
28 parts, 6 parts of cinnamic acid, 12 parts of ion exchange resin, 7.5 parts of polyacrylamide, 2.2 parts of casein, 14 parts of zeolite powder, methylol it is fine
36 parts of plain 3.8 parts of the sodium of dimension, 4.6 parts of vaseline, 17 parts of ethylene glycol, 11 parts of slag, 9 parts of citric acid and cyanobacteria.The grain size of slag is
2.64mm, the grain size of sodium cellulose glycolate is 0.66mm.
The preparation method of the medicament at the water source for being used to handle chemical contamination, is as follows：
Cyanobacteria is cleaned up and is freezed 4 hours in subzero 25 environment to subzero 20 degrees Celsius, then crushed by step 1
And 120 mesh sieve is crossed, the water of 4 times of its weight is added and the enzyme of its weight 1% is put in reaction kettle, inorganic acid is added in and adjusts PH
It is worth 5.4 and to be stirred 96 minutes under 42 degrees Celsius, then high temperature bath enzyme deactivation, centrifugal filtration can obtain cyanobacteria enzymolysis
Liquid；
Stalk, vaseline, zeolite powder and slag are milled to 220 mesh with the rotating speed of 30rpm in the ball mill, obtained by step 2
First mixture；
Cinnamic acid, sodium bentonite, polyacrylamide and ethylene glycol are mixed and supersonic oscillations 25 minutes, obtained by step 3
To the second mixture；
Ion exchange resin and casein are immersed in cyanobacteria enzymolysis liquid and supersonic oscillations 18 minutes, in electric field by step 4
Then the middle holding that intensity is 33KV 13 minutes adds in citric acid and stirs evenly, obtains third mixture；
Step 5 stirs evenly the first mixture, the second mixture, third mixture and sodium cellulose glycolate and 8
It degree Celsius is kept for 5 hours, it is then dry under 64 degrees Celsius and cross 220 mesh sieve, you can to obtain finished product.
The application method of the medicament at the water source for being used to handle chemical contamination：By finished product and sewage according to mass ratio 1:
120 mixing, stir evenly
The sewage after chemical contamination is handled using the product of embodiment 3, the removal rate of COD is 98.2% in water after processing,
The removal rate of heavy metal is 94.7%
Embodiment 4
A kind of medicament at the water source for being used to handle chemical contamination includes the raw material of following parts by weight：16 parts of stalk, sodium bentonite
30 parts, 8 parts of cinnamic acid, 13 parts of ion exchange resin, 8 parts of polyacrylamide, 2.5 parts of casein, 15 parts of zeolite powder, hydroxylmethyl cellulose
38 parts of plain 4 parts of sodium, 5 parts of vaseline, 18 parts of ethylene glycol, 12 parts of slag, 10 parts of citric acid and cyanobacteria.Stalk include wheat stalk,
Maize straw, sugarcane stalk, soybean stalk and broomcorn straw mixture, ion exchange resin uses cation exchange resin.
The grain size of slag is 2.63mm, and the grain size of sodium cellulose glycolate is 0.66mm.
The preparation method of the medicament at the water source for being used to handle chemical contamination, is as follows：
Cyanobacteria is cleaned up and freezes 1.6 hours in subzero 20 degrees Celsius of environment by step 1, is then crushed and mistake
120 mesh sieve, and add the water of 4 times of its weight and the enzyme of its weight 2% is put in reaction kettle, and it is 5.8 to add in inorganic acid and adjust pH value
And it is stirred 100 minutes under 44 degrees Celsius, then high temperature bath enzyme deactivation, centrifugal filtration can obtain cyanobacteria enzymolysis liquid；
Stalk, vaseline, zeolite powder and slag are milled to 220 mesh with the rotating speed of 30rpm in the ball mill, obtained by step 2
First mixture；
Cinnamic acid, sodium bentonite, polyacrylamide and ethylene glycol are mixed and supersonic oscillations 30 minutes, obtained by step 3
To the second mixture；
Ion exchange resin and casein are immersed in cyanobacteria enzymolysis liquid and supersonic oscillations 20 minutes, in electric field by step 4
Then the middle holding that intensity is 36KV 15 minutes adds in citric acid and stirs evenly, obtains third mixture；
Step 5 stirs evenly the first mixture, the second mixture, third mixture and sodium cellulose glycolate and 8
It degree Celsius is kept for 5 hours, it is then dry under 65 degrees Celsius and cross 220 mesh sieve, you can to obtain finished product.
The application method of the medicament at the water source for being used to handle chemical contamination：By finished product and sewage according to mass ratio 1:
140 mixing, stir evenly.
The sewage after chemical contamination is handled using the product of embodiment 4, the removal rate of COD is in water after processing
96.8%, the removal rate of heavy metal is 92.4%.
It is obvious to a person skilled in the art that the present invention is not limited to the details of above-mentioned exemplary embodiment, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requirement rather than above description limit, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in each embodiment can also be properly combined, forms those skilled in the art
The other embodiment being appreciated that.
Claims (6)
1. a kind of medicament at the water source for being used to handle chemical contamination, which is characterized in that include the raw material of following parts by weight：Stalk
12-16 parts, 24-30 parts of sodium bentonite, 4-8 parts of cinnamic acid, 10-13 parts of ion exchange resin, 6-8 parts of polyacrylamide, junket
1.2-2.5 parts plain, 8-15 parts of zeolite powder, 2.5-4 parts of sodium cellulose glycolate, 3-5 parts of vaseline, 15-18 parts of ethylene glycol, slag
25-38 parts of 8-12 parts, 6-10 parts of citric acid and cyanobacteria.
2. the medicament at the water source according to claim 1 for being used to handle chemical contamination, which is characterized in that the stalk includes
One or several kinds of mixtures in wheat stalk, maize straw, sugarcane stalk, soybean stalk and broomcorn straw, ion are handed over
Resin is changed using cation exchange resin.
3. the medicament at the water source according to claim 1 for being used to handle chemical contamination, which is characterized in that the grain of the slag
Diameter is 1.56-3.86mm, and the grain size of sodium cellulose glycolate is 0.34-0.73mm.
4. it is a kind of as described in any one of claims 1-3 for handling the preparation method of the medicament at the water source of chemical contamination, it is special
Sign is, is as follows：
Cyanobacteria is cleaned up and freezes 2-4 hours in subzero 25 environment to subzero 20 degrees Celsius, then powder by step 1
Broken and mistake 100-120 mesh sieves, the enzyme of water and its weight 1-2% for adding 3-5 times of its weight are put in reaction kettle, add in nothing
Machine acid adjusts pH value as 4.6-5.8 and is stirred 80-100 minutes under 36-44 degrees Celsius, then high temperature bath enzyme deactivation, centrifuges
Filtering can obtain cyanobacteria enzymolysis liquid；
Stalk, vaseline, zeolite powder and slag are milled to 200-240 by step 2 with the rotating speed of 30-45rpm in the ball mill
Mesh obtains the first mixture；
Step 3 mixes cinnamic acid, sodium bentonite, polyacrylamide and ethylene glycol and supersonic oscillations 20-30 minutes,
Obtain the second mixture；
Ion exchange resin and casein are immersed in cyanobacteria enzymolysis liquid and supersonic oscillations 15-20 minutes, then by step 4
It adds in citric acid and stirs evenly, obtain third mixture；
Step 5 stirs evenly the first mixture, the second mixture, third mixture and sodium cellulose glycolate and in 3-
8 degrees Celsius are kept for 4-6 hours, are then dried under 50-66 degrees Celsius and are crossed 160-240 mesh sieve, you can obtain finished product.
5. the preparation method of the medicament at the water source according to claim 4 for being used to handle chemical contamination, which is characterized in that institute
It states in step 4 before citric acid is added in middle holding 10-15 minutes that electric field strength is 25-40KV.
6. it is a kind of as described in any one of claims 1-3 for handling the application method of the medicament at the water source of chemical contamination, it is special
Sign is, is as follows：By finished product and sewage according to mass ratio 1:100-140 is mixed, and is stirred evenly.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810124808.9A CN108217776A (en) | 2018-02-08 | 2018-02-08 | It is a kind of to be used to handle medicament at water source of chemical contamination and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810124808.9A CN108217776A (en) | 2018-02-08 | 2018-02-08 | It is a kind of to be used to handle medicament at water source of chemical contamination and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109621892A (en) * | 2019-01-23 | 2019-04-16 | 云南天朗再生资源有限责任公司 | A kind of AMD fast purification inorganic agent and the preparation method and application thereof |
| CN110316867A (en) * | 2019-07-17 | 2019-10-11 | 广州隆盛景观建设有限公司 | Sewage water treatment method based on ultrafiltration membrane technique |
| CN110482785A (en) * | 2019-08-12 | 2019-11-22 | 广东长海建设工程有限公司 | Lake water processing method |
| CN110526369A (en) * | 2019-08-20 | 2019-12-03 | 广州鸿粤园林环保有限公司 | The processing method of city domestic sewage |
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| CN104030308A (en) * | 2014-06-05 | 2014-09-10 | 河海大学 | Method for preparing salt-resistant stain-resistant bentonite with adsorption function |
| CN105198021A (en) * | 2015-10-19 | 2015-12-30 | 晋城职业技术学院 | Chemical wastewater treatment agent and preparation method thereof |
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| CN104030308A (en) * | 2014-06-05 | 2014-09-10 | 河海大学 | Method for preparing salt-resistant stain-resistant bentonite with adsorption function |
| CN105198021A (en) * | 2015-10-19 | 2015-12-30 | 晋城职业技术学院 | Chemical wastewater treatment agent and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109621892A (en) * | 2019-01-23 | 2019-04-16 | 云南天朗再生资源有限责任公司 | A kind of AMD fast purification inorganic agent and the preparation method and application thereof |
| CN110316867A (en) * | 2019-07-17 | 2019-10-11 | 广州隆盛景观建设有限公司 | Sewage water treatment method based on ultrafiltration membrane technique |
| CN110482785A (en) * | 2019-08-12 | 2019-11-22 | 广东长海建设工程有限公司 | Lake water processing method |
| CN110526369A (en) * | 2019-08-20 | 2019-12-03 | 广州鸿粤园林环保有限公司 | The processing method of city domestic sewage |
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Application publication date: 20180629 |