CN105265356B - A kind of pearl nucleus for shortening the producing nucleated pearls phase - Google Patents
A kind of pearl nucleus for shortening the producing nucleated pearls phase Download PDFInfo
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- CN105265356B CN105265356B CN201510641050.2A CN201510641050A CN105265356B CN 105265356 B CN105265356 B CN 105265356B CN 201510641050 A CN201510641050 A CN 201510641050A CN 105265356 B CN105265356 B CN 105265356B
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- 239000011049 pearl Substances 0.000 title claims abstract description 309
- 238000004904 shortening Methods 0.000 title claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 89
- 241001518148 Euphorbia soongarica Species 0.000 claims abstract description 53
- 238000000034 method Methods 0.000 claims abstract description 9
- 241001080798 Polygala tenuifolia Species 0.000 claims description 61
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 60
- 239000003795 chemical substances by application Substances 0.000 claims description 29
- 239000012141 concentrate Substances 0.000 claims description 21
- 239000007788 liquid Substances 0.000 claims description 20
- 239000000463 material Substances 0.000 claims description 15
- 238000001816 cooling Methods 0.000 claims description 14
- 238000005245 sintering Methods 0.000 claims description 14
- 239000003153 chemical reaction reagent Substances 0.000 claims 1
- 238000001354 calcination Methods 0.000 abstract description 10
- 238000002360 preparation method Methods 0.000 abstract description 7
- 241000208966 Polygala Species 0.000 abstract description 3
- 238000002474 experimental method Methods 0.000 description 37
- 238000003306 harvesting Methods 0.000 description 24
- 241000196324 Embryophyta Species 0.000 description 15
- 239000010984 cultured pearl Substances 0.000 description 14
- 239000003643 water by type Substances 0.000 description 13
- 230000003698 anagen phase Effects 0.000 description 12
- 239000013505 freshwater Substances 0.000 description 10
- 102000001999 Transcription Factor Pit-1 Human genes 0.000 description 7
- 108010040742 Transcription Factor Pit-1 Proteins 0.000 description 7
- 230000006837 decompression Effects 0.000 description 6
- 235000015170 shellfish Nutrition 0.000 description 6
- 241000237536 Mytilus edulis Species 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 235000020638 mussel Nutrition 0.000 description 5
- 241000208368 Euonymus alatus Species 0.000 description 3
- 241000221079 Euphorbia <genus> Species 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 210000000515 tooth Anatomy 0.000 description 3
- 241000237519 Bivalvia Species 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 235000007466 Corylus avellana Nutrition 0.000 description 1
- 240000003211 Corylus maxima Species 0.000 description 1
- 241000208367 Euonymus Species 0.000 description 1
- 241000382840 Hyriopsis cumingii Species 0.000 description 1
- 241000208977 Polygalaceae Species 0.000 description 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- 241000217379 Unionidae Species 0.000 description 1
- 239000011324 bead Substances 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 238000012258 culturing Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 210000004907 gland Anatomy 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 230000001902 propagating effect Effects 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 238000009966 trimming Methods 0.000 description 1
- 230000009278 visceral effect Effects 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/80—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in fisheries management
- Y02A40/81—Aquaculture, e.g. of fish
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- Farming Of Fish And Shellfish (AREA)
Abstract
The invention belongs to cultural technique field, it is related to a kind of pearl nucleus for shortening the producing nucleated pearls phase, in order to solve to cultivate the problem of pearl is small, the cycle is long in the prior art, the invention provides a kind of pearl nucleus for shortening the producing nucleated pearls phase, including：Pearl nucleus and the pearl nucleus soak stayed on pearl nucleus, the pearl nucleus surface are uniformly distributed pit, and pit aperture area is less than base area；The preparation method of the pearl nucleus soak includes：A. fresh spindleberry, the petal of E. Soongarica Boiss, the blade of polygala are chosen and is placed on calcination 4h in Muffle furnace；B. take out and cool down, then add water and decoct 2h with small fire, obtain spindleberry decoction liquor, E. Soongarica Boiss petal decoction liquor, Folium Polygalae decoction liquor；C. decoction liquor obtained above is concentrated under reduced pressure respectively with Rotary Evaporators, then dissolved with water, be well mixed, obtain pearl nucleus soak.
Description
Technical field
The invention belongs to cultural technique field, it is related to a kind of pearl nucleus for shortening the producing nucleated pearls phase.
Background technology
China's freshwater resources enrich, and freshwater shellfish, which is grown cultured pearls, to have a extensive future.At present, China fresh water pearl annual production kiloton with
On, but high-quality, high-grade pearl, less than hundred tons, a diameter of more than 8mm pearl is difficult to meet international market in a short time
It is required that.The size of pearl particles determines the economic benefit of pearl production in many degree.It is precious for freshwater shellfish bulky grain
It is still a problem that pearl, which is cultivated in production,.Pearl nucleus are the use being implanted into when propagating nucleated pearl artificially in mother pearl shellfish outer embrane
The circular granular that shell or other materials are made, a female shellfish, can insert how many bead cores, should by operation shellfish size and pearl core
The specification of diameter is determined.In general, operation shellfish is big, then the pearl core inserted is more；Conversely, then few.Pearl nuclear diameter is big, then inserts
Grain number it is few；Pearl nuclear diameter is small, then the grain number inserted is more.Pearl nuclear diameter is more than 9-10 millimeters, and general 1 nacre only inserts 1
Grain core.But, in the prior art bulky grain pearl core insert educated after core the problem of pearl particles are little, the cycle is long it is still outstanding and not
Certainly, in the urgent need to carrying out technological innovation in production technology, to solve the above problems.
The content of the invention
It is small, cycle length that technical problem underlying to be solved by this invention is that existing visceral mass cultivates nucleated pearl particle
Problem, and provide a kind of method for cultivating the short cycle nucleated pearl of bulky grain for the problem, it may also be said to it is that one kind can be cultivated
The pearl nucleus of the short cycle nucleated pearl of bulky grain, it may also be said to be a kind of pearl nucleus leaching for cultivating the short cycle nucleated pearl of bulky grain
Steep liquid.
The technical solution adopted in the present invention is：A diameter of 8mm of pearl nucleus.
The surface of pearl nucleus 1 is uniformly distributed pit 2, and the aperture area of pit 2 is less than base area.
The surface of pearl nucleus 1 is uniformly distributed the groove 3 around the axis of pearl nucleus 1.
Redistribution grooves 3 in the surface largest circumference of pearl nucleus 1.
Pearl nucleus 1 soak 3 days in pearl nucleus soak, the preparation method of the soak, including：
(1) fresh spindleberry 32-40 parts by weight are chosen, preferred scope is 35-37 parts by weight, is placed on less than 1000 DEG C
Muffle furnace is after 500 ± 25 DEG C of high temperature sintering 4h, and taking-up is cooled to room temperature, standby；
(2) the petal 11-20 parts by weight of fresh E. Soongarica Boiss are chosen, preferred scope is 14-15 parts by weight, is placed on
Less than 1000 DEG C Muffle furnaces are after 500 ± 25 DEG C of high temperature sintering 4h, and taking-up is cooled to room temperature, standby；
(3) fresh Leaves In Polygala Tenuifolia 50-60 parts by weight are chosen, preferred scope is 57-60 parts by weight, be placed on 1000 DEG C with
Lower Muffle furnace is after 500 ± 25 DEG C of high temperature sintering 4h, and taking-up is cooled to room temperature, standby；
(4) the water small fire that three kinds of materials after cooling are separately added into 200 parts by weight decocts 2h, respectively obtains spindleberry and decocts
Boil liquid, E. Soongarica Boiss petal decoction liquor, Leaves In Polygala Tenuifolia decoction liquor, it is standby；
(5) spindleberry decoction liquor is concentrated under reduced pressure with Rotary Evaporators, agents useful for same is water, obtains spindleberry concentration
Thing, adds the water of 100 parts by weight, fully dissolving obtains spindleberry juice, standby；E. Soongarica Boiss is spent with Rotary Evaporators
Valve decoction liquor is concentrated under reduced pressure, and agents useful for same is water, obtains E. Soongarica Boiss petal concentrate, adds the water of 100 parts by weight,
Fully dissolving, obtains E. Soongarica Boiss petal juice, standby；Decompression is carried out to Leaves In Polygala Tenuifolia decoction liquor with Rotary Evaporators dense
Contracting, agents useful for same is water, obtains Leaves In Polygala Tenuifolia concentrate, adds the water of 100 parts by weight, and fully dissolving obtains Leaves In Polygala Tenuifolia juice
Liquid, it is standby；
(6) spindleberry juice obtained above, E. Soongarica Boiss petal juice, Leaves In Polygala Tenuifolia juice are sufficiently mixed
It is even, that is, obtain pearl nucleus soak；
The pearl nucleus for selecting a diameter of 8mm soak 3 days in obtained pearl nucleus soak, choose a length of 160- of body
200mm adult hydriopsis cumingii, inserts pearl nucleus on its outer embrane, and each hydriopsis cumingii inserts a pearl nucleus, then entered
Row artificial pearl culture, Cultivated water is special cultured pearl waters, plants pearl operating technology and artificial pearl culture technology is belonged to now
There is technology.
The pearl culturing clam used in the present invention be hydriopsis cumingii, Classification system be Hyriopsis cumingii, be commonly called as freshwater mussel,
Pearl freshwater mussel, fresh water pearl freshwater mussel, triangle freshwater mussel, Non-marine Bivalvess mollusk, category lamellibranchiata, Unionidae, sail freshwater mussel category.It is distributed widely in lake
South, Hubei, Anhui, Jiangsu, Zhejiang, Jiangxi etc. are saved, especially more with China's Dongting Lake and the distribution of medium-sized lake.Such a shell is big
And it is flat-sided, have upward triangle sail rear wing, profile is slightly triangular in shape.Shell is most greatly enhanced up to 240 millimeters.Shell surface is in Huang
Brown, the thick rib of diagonal that back ridge is made up of several tubercle projection.Hinge is flourishing, and left and right shell respectively has 2 pieces of pseudocardinal tooths, left housing
There are 2 pieces of side teeth, right shell has 1 piece of side tooth.Pearl thickness, it is glossy.
The present invention relates to a kind of pearl nucleus soak, using three kinds of plant materials is respectively：Winged euonymus, Classification system is
Euonymus alatus (Thunb.) Sieb., is Celastraceae Euonymus shrub, originates in China northeast, North China, northwest to the Changjiang river
Basin various regions；Japan, Korea are also distributed, strong adaptability, resist cold, resistance to shade, resistance to trimming is drought-resistant, barren.Capsule palm fibre purple,
Drastic crack, into 4 slivers, is sometimes 1-3 slivers, and what is used in the present invention is the fruit of winged euonymus；E. Soongarica Boiss, Classification system is
Euphorbia soongarica Boiss., are the plant of Euphorbiaceae Euphorbia.Be distributed in Mongolia, West Siberia, the Central Asia with
And the ground such as Gansu, Xinjiang of China's Mainland, it is grown on height above sea level 500 meters to 2,000 meter of area is grown on desert river valley, low more
More universal by mountain hillside, saline meadow and field wing, at present by artificial introducing and planting, inflorescence list is born in branch top, always
Luxuriant mitriform, is about 2.5 millimeters, 2-2.5 millimeters of diameter, and tip 5 splits, and sliver is semicircle to oval, edge and inner side tool echinid,
Body of gland 5, semicircle, filbert, what is used in the present invention is the petal of E. Soongarica Boiss；Polygala, Classification system is
Polygala tenuifolia Willd, are Polygalaceae rogation flower perennial herbs, production northeast, North China, northwest and Central China and
Sichuan, is born in grassland, patana, shrubbery and under shaw, 200-2300 meters of height above sea level, leaf alternate, narrow linear or wire
Lanceolar, long 1-4 centimetres, wide 1-3 millimeters, tip is tapering, and base portion is tapered, full edge, stockless or nearly stockless, is used in the present invention
The as blade of polygala.
The instruments such as less than the 1000 DEG C Muffle furnaces, Rotary Evaporators, the spiral micrometer that are related in the present invention are existing
Technology, calcination process, cooling procedure, decocting method, the method for being concentrated under reduced pressure fall within prior art.
Brief description of the drawings
Fig. 1 is the structural representation of prior art.
Fig. 2 is the schematic diagram of the pit 2 of the present invention.
Fig. 3 is the structural representation for being uniformly distributed the groove 3 around axis of the invention.
Fig. 4 is less than the structural representation of base area for the aperture area of pit 2 of the present invention.
Fig. 5 is the structural representation of redistribution grooves 3 in the largest circumference of the present invention.
Referring to Fig. 1-5,1-pearl nucleus, 2-pit, 3-groove
Embodiment
In order that those skilled in the art are well understood by the particular technique feature of the present invention, in favor of the reality of the present invention
Apply, existing the present invention will be further explained.
Referring to Fig. 1-5, the surface of pearl nucleus 1 design pit 2 and groove 3 be in order to be able to remain more pearl nucleus soaks,
So that the effect of the present invention becomes apparent from.
Referring to Fig. 4, the effect that the aperture area of pit 2 is less than base area is to be more than or equal to bottom surface face compared to aperture area
Long-pending pit 2 can store more pearl nucleus soaks.
Embodiment 1
The surface of pearl nucleus 1 is wrapped in pearl nucleus soak, the preparation method of the soak, including：
(1) the fresh parts by weight of spindleberry 32 are chosen, less than 1000 DEG C Muffle furnaces is placed on and is burnt by 500 ± 25 DEG C of high temperature
Burn after 4h, taking-up is cooled to room temperature, standby；
(2) parts by weight of petal 20 of fresh E. Soongarica Boiss are chosen, be placed on less than 1000 DEG C Muffle furnaces by 500 ±
After 25 DEG C of high temperature sintering 4h, taking-up is cooled to room temperature, standby；
(3) the fresh parts by weight of Leaves In Polygala Tenuifolia 55 are chosen, less than 1000 DEG C Muffle furnaces are placed on by 500 ± 25 DEG C of high temperature
After calcination 4h, taking-up is cooled to room temperature, standby；
(4) the water small fire that three kinds of materials after cooling are separately added into 200 parts by weight decocts 2h, respectively obtains spindleberry and decocts
Boil liquid, E. Soongarica Boiss petal decoction liquor, Leaves In Polygala Tenuifolia decoction liquor, it is standby；
(5) spindleberry decoction liquor is concentrated under reduced pressure with Rotary Evaporators, agents useful for same is water, obtains spindleberry concentration
Thing, adds the water of 100 parts by weight, fully dissolving obtains spindleberry juice, standby；E. Soongarica Boiss is spent with Rotary Evaporators
Valve decoction liquor is concentrated under reduced pressure, and agents useful for same is water, obtains E. Soongarica Boiss petal concentrate, adds the water of 100 parts by weight,
Fully dissolving, obtains E. Soongarica Boiss petal juice, standby；Decompression is carried out to Leaves In Polygala Tenuifolia decoction liquor with Rotary Evaporators dense
Contracting, agents useful for same is water, obtains Leaves In Polygala Tenuifolia concentrate, adds the water of 100 parts by weight, and fully dissolving obtains Leaves In Polygala Tenuifolia juice
Liquid, it is standby；
(6) spindleberry juice obtained above, E. Soongarica Boiss petal juice, Leaves In Polygala Tenuifolia juice are sufficiently mixed
It is even, that is, obtain pearl nucleus soak；
In April, 2011, the pearl nucleus for selecting a diameter of 8mm soak 3 days in obtained pearl nucleus soak, choose body long
For 160-200mm adult hydriopsis cumingii, pearl nucleus are inserted on its outer embrane, each hydriopsis cumingii inserts three pearl nucleus,
Then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plants pearl operating technology and artificial pearl culture technology is equal
Belong to prior art, the experiment totally 300 hydriopsis cumingiis cultivate 300 pearls, are divided into three groups of progress altogether, i.e., often repeatedly 100
100 pearls of hydriopsis cumingii, the record harvest pearl time, measure the diameter and record of every pearl, calculate every group and repeat to test
Pearl diameter average value, survey tool be spiral micrometer, accuracy is 0.01mm.
Result of the test is as follows：
It in October, 2011-November, i.e. pearl growth phase is 7 months or so that the harvest pearl time, which is,；
The pearl totally 100 that battery of tests is cultivated, average diameter is 15.28mm；
The pearl totally 100 that second group of experiment is cultivated, average diameter is 15.47mm；
The pearl totally 100 that 3rd group of experiment is cultivated, average diameter is 16.02mm；
300 pearl diameter average values are 15.59mm.
Embodiment 2
The surface of pearl nucleus 1 is wrapped in pearl nucleus soak, the preparation method of the soak, including：
(1) the fresh parts by weight of spindleberry 40 are chosen, less than 1000 DEG C Muffle furnaces is placed on and is burnt by 500 ± 25 DEG C of high temperature
Burn after 4h, taking-up is cooled to room temperature, standby；
(2) parts by weight of petal 17 of fresh E. Soongarica Boiss are chosen, be placed on less than 1000 DEG C Muffle furnaces by 500 ±
After 25 DEG C of high temperature sintering 4h, taking-up is cooled to room temperature, standby；
(3) the fresh parts by weight of Leaves In Polygala Tenuifolia 52 are chosen, less than 1000 DEG C Muffle furnaces are placed on by 500 ± 25 DEG C of high temperature
After calcination 4h, taking-up is cooled to room temperature, standby；
(4) the water small fire that three kinds of materials after cooling are separately added into 200 parts by weight decocts 2h, respectively obtains spindleberry and decocts
Boil liquid, E. Soongarica Boiss petal decoction liquor, Leaves In Polygala Tenuifolia decoction liquor, it is standby；
(5) spindleberry decoction liquor is concentrated under reduced pressure with Rotary Evaporators, agents useful for same is water, obtains spindleberry concentration
Thing, adds the water of 100 parts by weight, fully dissolving obtains spindleberry juice, standby；E. Soongarica Boiss is spent with Rotary Evaporators
Valve decoction liquor is concentrated under reduced pressure, and agents useful for same is water, obtains E. Soongarica Boiss petal concentrate, adds the water of 100 parts by weight,
Fully dissolving, obtains E. Soongarica Boiss petal juice, standby；Decompression is carried out to Leaves In Polygala Tenuifolia decoction liquor with Rotary Evaporators dense
Contracting, agents useful for same is water, obtains Leaves In Polygala Tenuifolia concentrate, adds the water of 100 parts by weight, and fully dissolving obtains Leaves In Polygala Tenuifolia juice
Liquid, it is standby；
(6) spindleberry juice obtained above, E. Soongarica Boiss petal juice, Leaves In Polygala Tenuifolia juice are sufficiently mixed
It is even, that is, obtain pearl nucleus soak；
In April, 2011, the pearl nucleus for selecting a diameter of 8mm soak 3 days in obtained pearl nucleus soak, choose body long
For 160-200mm adult hydriopsis cumingii, pearl nucleus are inserted on its outer embrane, each hydriopsis cumingii inserts three pearl nucleus,
Then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plants pearl operating technology and artificial pearl culture technology is equal
Belong to prior art, the experiment totally 300 hydriopsis cumingiis cultivate 300 pearls, are divided into three groups of progress altogether, i.e., often repeatedly 100
100 pearls of hydriopsis cumingii, the record harvest pearl time, measure the diameter and record of every pearl, calculate every group and repeat to test
Pearl diameter average value, survey tool be spiral micrometer, accuracy is 0.01mm.
Result of the test is as follows：
It in October, 2011-November, i.e. pearl growth phase is 7 months or so that the harvest pearl time, which is,；
The pearl totally 100 that battery of tests is cultivated, average diameter is 15.66mm；
The pearl totally 100 that second group of experiment is cultivated, average diameter is 15.83mm；
The pearl totally 100 that 3rd group of experiment is cultivated, average diameter is 15.32mm；
300 pearl diameter average values are 15.60mm.
Embodiment 3
The surface of pearl nucleus 1 is wrapped in pearl nucleus soak, the preparation method of the soak, including：
(1) the fresh parts by weight of spindleberry 38 are chosen, less than 1000 DEG C Muffle furnaces is placed on and is burnt by 500 ± 25 DEG C of high temperature
Burn after 4h, taking-up is cooled to room temperature, standby；
(2) parts by weight of petal 11 of fresh E. Soongarica Boiss are chosen, be placed on less than 1000 DEG C Muffle furnaces by 500 ±
After 25 DEG C of high temperature sintering 4h, taking-up is cooled to room temperature, standby；
(3) the fresh parts by weight of Leaves In Polygala Tenuifolia 50 are chosen, less than 1000 DEG C Muffle furnaces are placed on by 500 ± 25 DEG C of high temperature
After calcination 4h, taking-up is cooled to room temperature, standby；
(4) the water small fire that three kinds of materials after cooling are separately added into 200 parts by weight decocts 2h, respectively obtains spindleberry and decocts
Boil liquid, E. Soongarica Boiss petal decoction liquor, Leaves In Polygala Tenuifolia decoction liquor, it is standby；
(5) spindleberry decoction liquor is concentrated under reduced pressure with Rotary Evaporators, agents useful for same is water, obtains spindleberry concentration
Thing, adds the water of 100 parts by weight, fully dissolving obtains spindleberry juice, standby；E. Soongarica Boiss is spent with Rotary Evaporators
Valve decoction liquor is concentrated under reduced pressure, and agents useful for same is water, obtains E. Soongarica Boiss petal concentrate, adds the water of 100 parts by weight,
Fully dissolving, obtains E. Soongarica Boiss petal juice, standby；Decompression is carried out to Leaves In Polygala Tenuifolia decoction liquor with Rotary Evaporators dense
Contracting, agents useful for same is water, obtains Leaves In Polygala Tenuifolia concentrate, adds the water of 100 parts by weight, and fully dissolving obtains Leaves In Polygala Tenuifolia juice
Liquid, it is standby；
(6) spindleberry juice obtained above, E. Soongarica Boiss petal juice, Leaves In Polygala Tenuifolia juice are sufficiently mixed
It is even, that is, obtain pearl nucleus soak；
In April, 2011, the pearl nucleus for selecting a diameter of 8mm soak 3 days in obtained pearl nucleus soak, choose body long
For 160-200mm adult hydriopsis cumingii, pearl nucleus are inserted on its outer embrane, each hydriopsis cumingii inserts three pearl nucleus,
Then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plants pearl operating technology and artificial pearl culture technology is equal
Belong to prior art, the experiment totally 300 hydriopsis cumingiis cultivate 300 pearls, are divided into three groups of progress altogether, i.e., often repeatedly 100
100 pearls of hydriopsis cumingii, the record harvest pearl time, measure the diameter and record of every pearl, calculate every group and repeat to test
Pearl diameter average value, survey tool be spiral micrometer, accuracy is 0.01mm.
Result of the test is as follows：
It in October, 2011-November, i.e. pearl growth phase is 7 months or so that the harvest pearl time, which is,；
The pearl totally 100 that battery of tests is cultivated, average diameter is 16.12mm；
The pearl totally 100 that second group of experiment is cultivated, average diameter is 15.87mm；
The pearl totally 100 that 3rd group of experiment is cultivated, average diameter is 15.32mm；
300 pearl diameter average values are 15.77mm.
Embodiment 4
The surface of pearl nucleus 1 is wrapped in pearl nucleus soak, the preparation method of the soak, including：
(1) the fresh parts by weight of spindleberry 35 are chosen, less than 1000 DEG C Muffle furnaces is placed on and is burnt by 500 ± 25 DEG C of high temperature
Burn after 4h, taking-up is cooled to room temperature, standby；
(2) parts by weight of petal 14 of fresh E. Soongarica Boiss are chosen, be placed on less than 1000 DEG C Muffle furnaces by 500 ±
After 25 DEG C of high temperature sintering 4h, taking-up is cooled to room temperature, standby；
(3) the fresh parts by weight of Leaves In Polygala Tenuifolia 57 are chosen, less than 1000 DEG C Muffle furnaces are placed on by 500 ± 25 DEG C of high temperature
After calcination 4h, taking-up is cooled to room temperature, standby；
(4) the water small fire that three kinds of materials after cooling are separately added into 200 parts by weight decocts 2h, respectively obtains spindleberry and decocts
Boil liquid, E. Soongarica Boiss petal decoction liquor, Leaves In Polygala Tenuifolia decoction liquor, it is standby；
(5) spindleberry decoction liquor is concentrated under reduced pressure with Rotary Evaporators, agents useful for same is water, obtains spindleberry concentration
Thing, adds the water of 100 parts by weight, fully dissolving obtains spindleberry juice, standby；E. Soongarica Boiss is spent with Rotary Evaporators
Valve decoction liquor is concentrated under reduced pressure, and agents useful for same is water, obtains E. Soongarica Boiss petal concentrate, adds the water of 100 parts by weight,
Fully dissolving, obtains E. Soongarica Boiss petal juice, standby；Decompression is carried out to Leaves In Polygala Tenuifolia decoction liquor with Rotary Evaporators dense
Contracting, agents useful for same is water, obtains Leaves In Polygala Tenuifolia concentrate, adds the water of 100 parts by weight, and fully dissolving obtains Leaves In Polygala Tenuifolia juice
Liquid, it is standby；
(6) spindleberry juice obtained above, E. Soongarica Boiss petal juice, Leaves In Polygala Tenuifolia juice are sufficiently mixed
It is even, that is, obtain pearl nucleus soak；
In April, 2011, the pearl nucleus for selecting a diameter of 8mm soak 3 days in obtained pearl nucleus soak, choose body long
For 160-200mm adult hydriopsis cumingii, pearl nucleus are inserted on its outer embrane, each hydriopsis cumingii inserts a pearl nucleus,
Then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plants pearl operating technology and artificial pearl culture technology is equal
Belong to prior art, the experiment totally 300 hydriopsis cumingiis cultivate 300 pearls, are divided into three groups of progress altogether, i.e., often repeatedly 100
100 pearls of hydriopsis cumingii, the record harvest pearl time, measure the diameter and record of every pearl, calculate every group and repeat to test
Pearl diameter average value, survey tool be spiral micrometer, accuracy is 0.01mm.
Result of the test is as follows：
It in October, 2011-November, i.e. pearl growth phase is 7 months or so that the harvest pearl time, which is,；
The pearl totally 100 that battery of tests is cultivated, average diameter is 16.34mm；
The pearl totally 100 that second group of experiment is cultivated, average diameter is 16.51mm；
The pearl totally 100 that 3rd group of experiment is cultivated, average diameter is 16.09mm；
300 pearl diameter average values are 16.31mm.
Embodiment 5
The surface of pearl nucleus 1 is wrapped in pearl nucleus soak, the preparation method of the soak, including：
(1) the fresh parts by weight of spindleberry 37 are chosen, less than 1000 DEG C Muffle furnaces is placed on and is burnt by 500 ± 25 DEG C of high temperature
Burn after 4h, taking-up is cooled to room temperature, standby；
(2) parts by weight of petal 15 of fresh E. Soongarica Boiss are chosen, be placed on less than 1000 DEG C Muffle furnaces by 500 ±
After 25 DEG C of high temperature sintering 4h, taking-up is cooled to room temperature, standby；
(3) the fresh parts by weight of Leaves In Polygala Tenuifolia 60 are chosen, less than 1000 DEG C Muffle furnaces are placed on by 500 ± 25 DEG C of high temperature
After calcination 4h, taking-up is cooled to room temperature, standby；
(4) the water small fire that three kinds of materials after cooling are separately added into 200 parts by weight decocts 2h, respectively obtains spindleberry and decocts
Boil liquid, E. Soongarica Boiss petal decoction liquor, Leaves In Polygala Tenuifolia decoction liquor, it is standby；
(5) spindleberry decoction liquor is concentrated under reduced pressure with Rotary Evaporators, agents useful for same is water, obtains spindleberry concentration
Thing, adds the water of 100 parts by weight, fully dissolving obtains spindleberry juice, standby；E. Soongarica Boiss is spent with Rotary Evaporators
Valve decoction liquor is concentrated under reduced pressure, and agents useful for same is water, obtains E. Soongarica Boiss petal concentrate, adds the water of 100 parts by weight,
Fully dissolving, obtains E. Soongarica Boiss petal juice, standby；Decompression is carried out to Leaves In Polygala Tenuifolia decoction liquor with Rotary Evaporators dense
Contracting, agents useful for same is water, obtains Leaves In Polygala Tenuifolia concentrate, adds the water of 100 parts by weight, and fully dissolving obtains Leaves In Polygala Tenuifolia juice
Liquid, it is standby；
(6) spindleberry juice obtained above, E. Soongarica Boiss petal juice, Leaves In Polygala Tenuifolia juice are sufficiently mixed
It is even, that is, obtain pearl nucleus soak；
In April, 2011, the pearl nucleus for selecting a diameter of 8mm soak 3 days in obtained pearl nucleus soak, choose body long
For 160-200mm adult hydriopsis cumingii, pearl nucleus are inserted on its outer embrane, each hydriopsis cumingii inserts a pearl nucleus,
Then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plants pearl operating technology and artificial pearl culture technology is equal
Belong to prior art, the experiment totally 300 hydriopsis cumingiis cultivate 300 pearls, are divided into three groups of progress altogether, i.e., often repeatedly 100
100 pearls of hydriopsis cumingii, the record harvest pearl time, measure the diameter and record of every pearl, calculate every group and repeat to test
Pearl diameter average value, survey tool be spiral micrometer, accuracy is 0.01mm.
Result of the test is as follows：
It in October, 2011-November, i.e. pearl growth phase is 7 months or so that the harvest pearl time, which is,；
The pearl totally 100 that battery of tests is cultivated, average diameter is 16.42mm；
The pearl totally 100 that second group of experiment is cultivated, average diameter is 16.55mm；
The pearl totally 100 that 3rd group of experiment is cultivated, average diameter is 16.59mm；
300 pearl diameter average values are 16.52mm.
Embodiment 6
(1) the fresh parts by weight of spindleberry 37 are chosen, less than 1000 DEG C Muffle furnaces is placed on and is burnt by 500 ± 25 DEG C of high temperature
Burn after 4h, taking-up is cooled to room temperature, standby；
(2) the water small fire that the material after cooling is added into 200 parts by weight decocts 2h, obtains spindleberry decoction liquor, standby；
(3) spindleberry decoction liquor is concentrated under reduced pressure with Rotary Evaporators, agents useful for same is water, obtains spindleberry concentration
Thing, adds the water of 100 parts by weight, fully dissolving obtains spindleberry juice, standby；
(4) spindleberry juice obtained above is sufficiently mixed uniformly, that is, obtains pearl nucleus soak；
In April, 2011, the pearl nucleus for selecting a diameter of 8mm soak 3 days in obtained pearl nucleus soak, choose body long
For 160-200mm adult hydriopsis cumingii, pearl nucleus are inserted on its outer embrane, each hydriopsis cumingii inserts three pearl nucleus,
Then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plants pearl operating technology and artificial pearl culture technology is equal
Belong to prior art, the experiment totally 300 hydriopsis cumingiis cultivate 300 pearls, are divided into three groups of progress altogether, i.e., often repeatedly 100
100 pearls of hydriopsis cumingii, the record harvest pearl time, measure the diameter and record of every pearl, calculate every group and repeat to test
Pearl diameter average value, survey tool be spiral micrometer, accuracy is 0.01mm.
Result of the test is as follows：
It in January, -2013 in December, 2012, i.e. pearl growth phase is 9 months or so 1 year that the harvest pearl time, which is,；
The pearl totally 100 that battery of tests is cultivated, average diameter is 10.02mm；
The pearl totally 100 that second group of experiment is cultivated, average diameter is 9.89mm；
The pearl totally 100 that 3rd group of experiment is cultivated, average diameter is 10.11mm；
300 pearl diameter average values are 10.01mm.
Embodiment 7
(1) parts by weight of petal 15 of fresh E. Soongarica Boiss are chosen, be placed on less than 1000 DEG C Muffle furnaces by 500 ±
After 25 DEG C of high temperature sintering 4h, taking-up is cooled to room temperature, standby；
(2) the water small fire that the material after cooling is added into 200 parts by weight decocts 2h, obtains the decoction of E. Soongarica Boiss petal
Liquid, it is standby；
(3) E. Soongarica Boiss petal decoction liquor is concentrated under reduced pressure with Rotary Evaporators, agents useful for same is water, obtains standard
Ge Er roots of Beijing euphorbia petal concentrate, adds the water of 100 parts by weight, fully dissolving obtains E. Soongarica Boiss petal juice, standby；
(4) E. Soongarica Boiss petal juice obtained above is sufficiently mixed uniformly, that is, obtains pearl nucleus soak；
In April, 2011, the pearl nucleus for selecting a diameter of 8mm soak 3 days in obtained pearl nucleus soak, choose body long
For 160-200mm adult hydriopsis cumingii, pearl nucleus are inserted on its outer embrane, each hydriopsis cumingii inserts a pearl nucleus,
Then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plants pearl operating technology and artificial pearl culture technology is equal
Belong to prior art, the experiment totally 300 hydriopsis cumingiis cultivate 300 pearls, are divided into three groups of progress altogether, i.e., often repeatedly 100
100 pearls of hydriopsis cumingii, the record harvest pearl time, measure the diameter and record of every pearl, calculate every group and repeat to test
Pearl diameter average value, survey tool be spiral micrometer, accuracy is 0.01mm.
Result of the test is as follows：
It in January, -2013 in December, 2012, i.e. pearl growth phase is 9 months or so 1 year that the harvest pearl time, which is,；
The pearl totally 100 that battery of tests is cultivated, average diameter is 10.31mm；
The pearl totally 100 that second group of experiment is cultivated, average diameter is 10.12mm；
The pearl totally 100 that 3rd group of experiment is cultivated, average diameter is 10.33mm；
300 pearl diameter average values are 10.25mm.
Embodiment 8
(1) the fresh parts by weight of Leaves In Polygala Tenuifolia 60 are chosen, less than 1000 DEG C Muffle furnaces are placed on by 500 ± 25 DEG C of high temperature
After calcination 4h, taking-up is cooled to room temperature, standby；
(2) the water small fire that the material after cooling is added into 200 parts by weight decocts 2h, obtains Leaves In Polygala Tenuifolia decoction liquor, standby；
(3) Leaves In Polygala Tenuifolia decoction liquor is concentrated under reduced pressure with Rotary Evaporators, agents useful for same is water, obtains Leaves In Polygala Tenuifolia
Concentrate, adds the water of 100 parts by weight, fully dissolving obtains Leaves In Polygala Tenuifolia juice, standby；
(4) Leaves In Polygala Tenuifolia juice obtained above is sufficiently mixed uniformly, that is, obtains pearl nucleus soak；
In April, 2011, the pearl nucleus for selecting a diameter of 8mm soak 3 days in obtained pearl nucleus soak, choose body long
For 160-200mm adult hydriopsis cumingii, pearl nucleus are inserted on its outer embrane, each hydriopsis cumingii inserts a pearl nucleus,
Then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plants pearl operating technology and artificial pearl culture technology is equal
Belong to prior art, the experiment totally 300 hydriopsis cumingiis cultivate 300 pearls, are divided into three groups of progress altogether, i.e., often repeatedly 100
100 pearls of hydriopsis cumingii, the record harvest pearl time, measure the diameter and record of every pearl, calculate every group and repeat to test
Pearl diameter average value, survey tool be spiral micrometer, accuracy is 0.01mm.
Result of the test is as follows：
It in January, -2013 in December, 2012, i.e. pearl growth phase is 9 months or so 1 year that the harvest pearl time, which is,；
The pearl totally 100 that battery of tests is cultivated, average diameter is 9.92mm；
The pearl totally 100 that second group of experiment is cultivated, average diameter is 10.13mm；
The pearl totally 100 that 3rd group of experiment is cultivated, average diameter is 10.01mm；
300 pearl diameter average values are 10.02mm.
Embodiment 9
(1) the fresh parts by weight of spindleberry 37 are chosen, less than 1000 DEG C Muffle furnaces is placed on and is burnt by 500 ± 25 DEG C of high temperature
Burn after 4h, taking-up is cooled to room temperature, standby；
(2) parts by weight of petal 15 of fresh E. Soongarica Boiss are chosen, be placed on less than 1000 DEG C Muffle furnaces by 500 ±
After 25 DEG C of high temperature sintering 4h, taking-up is cooled to room temperature, standby；
(3) the water small fire that two kinds of materials after cooling are separately added into 200 parts by weight decocts 2h, respectively obtains spindleberry and decocts
Boil liquid, E. Soongarica Boiss petal decoction liquor, it is standby；
(4) spindleberry decoction liquor is concentrated under reduced pressure with Rotary Evaporators, agents useful for same is water, obtains spindleberry concentration
Thing, adds the water of 100 parts by weight, fully dissolving obtains spindleberry juice, standby；E. Soongarica Boiss is spent with Rotary Evaporators
Valve decoction liquor is concentrated under reduced pressure, and agents useful for same is water, obtains E. Soongarica Boiss petal concentrate, adds the water of 100 parts by weight,
Fully dissolving, obtains E. Soongarica Boiss petal juice, standby；
(5) spindleberry juice obtained above, E. Soongarica Boiss petal juice are sufficiently mixed uniformly, that is, obtain pearl nucleus
Soak；
In April, 2011, the pearl nucleus for selecting a diameter of 8mm soak 3 days in obtained pearl nucleus soak, choose body long
For 160-200mm adult hydriopsis cumingii, pearl nucleus are inserted on its outer embrane, each hydriopsis cumingii inserts a pearl nucleus,
Then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plants pearl operating technology and artificial pearl culture technology is equal
Belong to prior art, the experiment totally 300 hydriopsis cumingiis cultivate 300 pearls, are divided into three groups of progress altogether, i.e., often repeatedly 100
100 pearls of hydriopsis cumingii, the record harvest pearl time, measure the diameter and record of every pearl, calculate every group and repeat to test
Pearl diameter average value, survey tool be spiral micrometer, accuracy is 0.01mm.
Result of the test is as follows：
It in November, 2012-December, i.e. pearl growth phase is 7 months or so 1 year that the harvest pearl time, which is,；
The pearl totally 100 that battery of tests is cultivated, average diameter is 12.33mm；
The pearl totally 100 that second group of experiment is cultivated, average diameter is 12.47mm；
The pearl totally 100 that 3rd group of experiment is cultivated, average diameter is 12.56mm；
300 pearl diameter average values are 12.45mm.
Embodiment 10
(1) the fresh parts by weight of spindleberry 37 are chosen, less than 1000 DEG C Muffle furnaces is placed on and is burnt by 500 ± 25 DEG C of high temperature
Burn after 4h, taking-up is cooled to room temperature, standby；
(2) the fresh parts by weight of Leaves In Polygala Tenuifolia 60 are chosen, less than 1000 DEG C Muffle furnaces are placed on by 500 ± 25 DEG C of high temperature
After calcination 4h, taking-up is cooled to room temperature, standby；
(3) the water small fire that two kinds of materials after cooling are separately added into 200 parts by weight decocts 2h, respectively obtains spindleberry and decocts
Boil liquid, Leaves In Polygala Tenuifolia decoction liquor, it is standby；
(4) spindleberry decoction liquor is concentrated under reduced pressure with Rotary Evaporators, agents useful for same is water, obtains spindleberry concentration
Thing, adds the water of 100 parts by weight, fully dissolving obtains spindleberry juice, standby；Leaves In Polygala Tenuifolia is decocted with Rotary Evaporators
Liquid is concentrated under reduced pressure, and agents useful for same is water, obtains Leaves In Polygala Tenuifolia concentrate, adds the water of 100 parts by weight, and fully dissolving is obtained
It is standby to Leaves In Polygala Tenuifolia juice；
(5) spindleberry juice obtained above, Leaves In Polygala Tenuifolia juice are sufficiently mixed uniformly, that is, obtain pearl nucleus immersion
Liquid；
In April, 2011, the pearl nucleus for selecting a diameter of 8mm soak 3 days in obtained pearl nucleus soak, choose body long
For 160-200mm adult hydriopsis cumingii, pearl nucleus are inserted on its outer embrane, each hydriopsis cumingii inserts a pearl nucleus,
Then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plants pearl operating technology and artificial pearl culture technology is equal
Belong to prior art, the experiment totally 300 hydriopsis cumingiis cultivate 300 pearls, are divided into three groups of progress altogether, i.e., often repeatedly 100
100 pearls of hydriopsis cumingii, the record harvest pearl time, measure the diameter and record of every pearl, calculate every group and repeat to test
Pearl diameter average value, survey tool be spiral micrometer, accuracy is 0.01mm.
Result of the test is as follows：
It in November, 2012, i.e. pearl growth phase is 7 months or so 1 year that the harvest pearl time, which is,；
The pearl totally 100 that battery of tests is cultivated, average diameter is 12.39mm；
The pearl totally 100 that second group of experiment is cultivated, average diameter is 13.05mm；
The pearl totally 100 that 3rd group of experiment is cultivated, average diameter is 12.62mm；
300 pearl diameter average values are 12.69mm.
Embodiment 11
(1) parts by weight of petal 15 of fresh E. Soongarica Boiss are chosen, be placed on less than 1000 DEG C Muffle furnaces by 500 ±
After 25 DEG C of high temperature sintering 4h, taking-up is cooled to room temperature, standby；
(2) the fresh parts by weight of Leaves In Polygala Tenuifolia 60 are chosen, less than 1000 DEG C Muffle furnaces are placed on by 500 ± 25 DEG C of high temperature
After calcination 4h, taking-up is cooled to room temperature, standby；
(3) the water small fire that two kinds of materials after cooling are separately added into 200 parts by weight decocts 2h, respectively obtains quasi- Ge Er big
Halberd petal decoction liquor, Leaves In Polygala Tenuifolia decoction liquor, it is standby；
(4) E. Soongarica Boiss petal decoction liquor is concentrated under reduced pressure with Rotary Evaporators, agents useful for same is water, obtains standard
Ge Er roots of Beijing euphorbia petal concentrate, adds the water of 100 parts by weight, fully dissolving obtains E. Soongarica Boiss petal juice, standby；With
Rotary Evaporators are concentrated under reduced pressure to Leaves In Polygala Tenuifolia decoction liquor, and agents useful for same is water, obtain Leaves In Polygala Tenuifolia concentrate, add
The water of 100 parts by weight, fully dissolving, obtain Leaves In Polygala Tenuifolia juice, standby；
(5) E. Soongarica Boiss petal juice obtained above, Leaves In Polygala Tenuifolia juice are sufficiently mixed uniformly, that is, obtain pearl
Core soak；
In April, 2011, the pearl nucleus for selecting a diameter of 8mm soak 3 days in obtained pearl nucleus soak, choose body long
For 160-200mm adult hydriopsis cumingii, pearl nucleus are inserted on its outer embrane, each hydriopsis cumingii inserts a pearl nucleus,
Then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plants pearl operating technology and artificial pearl culture technology is equal
Belong to prior art, the experiment totally 300 hydriopsis cumingiis cultivate 300 pearls, are divided into three groups of progress altogether, i.e., often repeatedly 100
100 pearls of hydriopsis cumingii, the record harvest pearl time, measure the diameter and record of every pearl, calculate every group and repeat to test
Pearl diameter average value, survey tool be spiral micrometer, accuracy is 0.01mm.
Result of the test is as follows：
It in November, 2012, i.e. pearl growth phase is 7 months or so 1 year that the harvest pearl time, which is,；
The pearl totally 100 that battery of tests is cultivated, average diameter is 12.53mm；
The pearl totally 100 that second group of experiment is cultivated, average diameter is 12.28mm；
The pearl totally 100 that 3rd group of experiment is cultivated, average diameter is 12.34mm；
300 pearl diameter average values are 12.38mm.
Embodiment 12
The embodiment is check experiment
In April, 2011, the pearl nucleus for selecting a diameter of 8mm soak 3 days in clear water, choose a length of 160-200mm's of body
Grown up hydriopsis cumingii, and pearl nucleus are inserted on its outer embrane, and each hydriopsis cumingii inserts a pearl nucleus, then manually educated
Pearl, Cultivated water is special cultured pearl waters, plants pearl operating technology and artificial pearl culture technology belongs to prior art, should
Totally 300 hydriopsis cumingiis are tested, 300 pearls are cultivated altogether, are divided into three groups of progress, i.e., often repeat 100 hydriopsis cumingiis, 100 treasure
Pearl, the record harvest pearl time, measures the diameter and record of every pearl, calculates every group of pearl diameter for repeating experiment and is averaged
Value, survey tool is spiral micrometer, and accuracy is 0.01mm.
Result of the test is as follows：
It -2 months in January, 2013, i.e. pearl growth phase is 10 months or so 1 year that the harvest pearl time, which is,；
The pearl totally 100 that battery of tests is cultivated, average diameter is 9.31mm；
The pearl totally 100 that second group of experiment is cultivated, average diameter is 9.22mm；
The pearl totally 100 that 3rd group of experiment is cultivated, average diameter is 9.06mm；
300 pearl diameter average values are 9.20mm.
Claims (1)
1. a kind of pearl nucleus for shortening the producing nucleated pearls phase, it is characterized in that, including pearl nucleus (1), pit (2), pearl nucleus
A diameter of 8mm, pearl nucleus (1) surface is uniformly distributed pit (2), and pit (2) aperture area is less than base area；Pearl nucleus (1)
Redistribution grooves (3) in the largest circumference of surface；Pearl nucleus (1) soak 3 days, the making of pearl nucleus soak in pearl nucleus soak
Method, including：
(1) the fresh parts by weight of spindleberry 32 are chosen, less than 1000 DEG C Muffle furnaces are placed on by 500 ± 25 DEG C of high temperature sintering 4h
Afterwards, take out and be cooled to room temperature, it is standby；
(2) parts by weight of petal 20 of fresh E. Soongarica Boiss are chosen, less than 1000 DEG C Muffle furnaces are placed on by 500 ± 25 DEG C
After high temperature sintering 4h, taking-up is cooled to room temperature, standby；
(3) the fresh parts by weight of Leaves In Polygala Tenuifolia 55 are chosen, less than 1000 DEG C Muffle furnaces are placed on by 500 ± 25 DEG C of high temperature sinterings
After 4h, taking-up is cooled to room temperature, standby；
(4) the water small fire that three kinds of materials after cooling are separately added into 200 parts by weight decocts 2h, respectively obtains spindleberry decoction
Liquid, E. Soongarica Boiss petal decoction liquor, Leaves In Polygala Tenuifolia decoction liquor, it is standby；
(5) spindleberry decoction liquor is concentrated under reduced pressure with Rotary Evaporators, agents useful for same is water, obtains spindleberry concentrate,
The water of 100 parts by weight is added, fully dissolving, obtain spindleberry juice, it is standby；E. Soongarica Boiss petal is decocted with Rotary Evaporators
Boil liquid is concentrated under reduced pressure, and agents useful for same is water, obtains E. Soongarica Boiss petal concentrate, adds the water of 100 parts by weight, fully
Dissolving, obtains E. Soongarica Boiss petal juice, standby；Leaves In Polygala Tenuifolia decoction liquor is concentrated under reduced pressure with Rotary Evaporators, institute
It is water with reagent, obtains Leaves In Polygala Tenuifolia concentrate, adds the water of 100 parts by weight, fully dissolving obtains Leaves In Polygala Tenuifolia juice, standby
With；
(6) uniformly, i.e., spindleberry juice obtained above, E. Soongarica Boiss petal juice, Leaves In Polygala Tenuifolia juice are sufficiently mixed
Obtain pearl nucleus soak.
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