CN105265356A - Pearl nucleus capable of shortening nucleated pearl cultivation period - Google Patents
Pearl nucleus capable of shortening nucleated pearl cultivation period Download PDFInfo
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- CN105265356A CN105265356A CN201510641050.2A CN201510641050A CN105265356A CN 105265356 A CN105265356 A CN 105265356A CN 201510641050 A CN201510641050 A CN 201510641050A CN 105265356 A CN105265356 A CN 105265356A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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Abstract
The invention belongs to the technical field of cultivation, and particularly relates to a pearl nucleus capable of shortening a nucleated pearl cultivation period, so as to solve the problems that the cultivated pearl is small, and the period is long in the prior art. The pearl nucleus capable of shortening the nucleated pearl cultivation period comprises a pearl nucleus and a pearl nucleus soaking solution left on the pearl nucleus, wherein the surface of the pearl nucleus is uniformly distributed with pits, and the opening area of each pit is smaller than the bottom surface area. The preparation method for the pearl nucleus soaking solution comprises steps: a, fresh euonymus fruits, petals of euphorbia soongarica boiss and leaves of polygala tenuifolia are selected to be put to a muffle furnace for burning for 4 hours; b, the mixture in the above step is taken out and cooled, water is then added for boiling for 2 hours by using soft fire, and a euonymus fruit boiling liquid, a euphorbia soongarica boiss petal boiling liquid and a polygala tenuifolia leaf boiling liquid are obtained; and c, a rotary evaporator is used for carrying out decompressing concentration on the above boiling liquids, water is then used for dissolution, uniform mixing is carried out, and the pearl nucleus soaking solution is obtained.
Description
Technical field
The invention belongs to cultural technique field, relate to a kind of pearl nucleus cultivating short period nucleated pearl.
Background technology
China's freshwater resources enrich, and freshwater shellfish is grown cultured pearls and had a extensive future.At present, more than China's fresh water pearl annual production kiloton, but the pearl of high-quality, top grade is less than hundred tons, and diameter is the requirement that the pearl of more than 8mm is difficult to meet international market in a short time.The size of pearl particles determines the economic benefit of pearl production in a lot of degree.In production, a difficult problem is still for freshwater shellfish bulky grain pearl cultivating.Pearl nucleus are the circular granulars made with shell or other materials implanted when propagating nucleated pearl artificially in mother pearl shellfish outer embrane, and a female shellfish, can insert how many pearl cores, should be decided by the operation size of shellfish and the specification of pearl nuclear diameter.In general, operation shellfish is large, then the pearl core inserted is many; Otherwise, then few.Pearl nuclear diameter is large, then the grain number inserted is few; Pearl nuclear diameter is little, then the grain number inserted is many.Pearl nuclear diameter is more than 9-10 millimeter, and general 1 nacre only inserts 1 core.But, after in prior art, bulky grain pearl core inserts core educate that pearl particles is little, problem that the cycle is long is still undecided, in the urgent need to carrying out technological innovation in production technology, to solve the problem.
Summary of the invention
Technical problem underlying to be solved by this invention is that existing visceral mass cultivates the problem that nucleated pearl particle is little, the cycle is long, and provide a kind of method of cultivating bulky grain short period nucleated pearl for this problem, being alternatively a kind of pearl nucleus cultivating bulky grain short period nucleated pearl, is alternatively a kind of pearl nucleus soak cultivating bulky grain short period nucleated pearl.
The technical solution adopted in the present invention is: the diameter of pearl nucleus is 8mm.
Pearl nucleus 1 surface uniform distribution pit 2, pit 2 aperture area is less than base area.
The groove 3 of pearl nucleus 1 surface uniform distribution rings around the axis of pearl nucleus 1.
Redistribution grooves 3 in the surperficial largest circumference of pearl nucleus 1.
Pearl nucleus 1 soak 3 days in pearl nucleus soak, and the preparation method of this soak, comprising:
(1) choose fresh spindleberry 32-40 weight portion, preferable range is 35-37 weight portion, is placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, takes out and is cooled to room temperature, for subsequent use;
(2) choose the petal 11-20 weight portion of fresh E. Soongarica Boiss, preferable range is 14-15 weight portion, is placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, takes out and is cooled to room temperature, for subsequent use;
(3) choose fresh Leaves In Polygala Tenuifolia 50-60 weight portion, preferable range is 57-60 weight portion, is placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, takes out and is cooled to room temperature, for subsequent use;
(4) the little fire of the water cooled three kinds of materials being added 200 weight portions respectively decocts 2h, obtains spindleberry decoction liquor, E. Soongarica Boiss petal decoction liquor, Leaves In Polygala Tenuifolia decoction liquor respectively, for subsequent use;
(5) carry out reduced pressure concentration with Rotary Evaporators to spindleberry decoction liquor, agents useful for same is water, obtains spindleberry concentrate, adds the water of 100 weight portions, fully dissolves, and obtains spindleberry juice, for subsequent use; Carry out reduced pressure concentration with Rotary Evaporators to E. Soongarica Boiss petal decoction liquor, agents useful for same is water, obtains E. Soongarica Boiss petal concentrate, adds the water of 100 weight portions, fully dissolve, and obtains E. Soongarica Boiss petal juice, for subsequent use; Carry out reduced pressure concentration with Rotary Evaporators to Leaves In Polygala Tenuifolia decoction liquor, agents useful for same is water, obtains Leaves In Polygala Tenuifolia concentrate, adds the water of 100 weight portions, fully dissolves, and obtains Leaves In Polygala Tenuifolia juice, for subsequent use;
(6) spindleberry juice obtained above, E. Soongarica Boiss petal juice, Leaves In Polygala Tenuifolia juice are fully mixed, namely obtain pearl nucleus soak;
Selecting diameter is that the pearl nucleus of 8mm soak 3 days in obtained pearl nucleus soak, choose the long adult hydriopsis cumingii for 160-200mm of body, its outer embrane inserts pearl nucleus, each hydriopsis cumingii inserts pearl nucleus, then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plants pearl operating technology and artificial pearl culture technology all belongs to prior art.
The pearl culturing clam used in the present invention is hydriopsis cumingii, and Classification system is Hyriopsiscumingii, is commonly called as freshwater mussel, pearl freshwater mussel, fresh water pearl freshwater mussel, triangle freshwater mussel, Non-marine Bivalves mollusk, belongs to lamellibranchiata, Unionidae, sail freshwater mussel genus.Be distributed widely in the provinces such as Hunan, Hubei, Anhui, Jiangsu, Zhejiang, Jiangxi, especially distribute more with China's Dongting Lake and medium-sized lake.This kind of shell is large and flat-sided, and tool triangle sail rear wing upwardly, profile is slightly triangular in shape.Shell greatly enhances and can reach 240 millimeters most.Shell face is yellowish-brown, the thick rib of the diagonal that back ridge is made up of tubercle projection several.Hinge is flourishing, and left and right shell respectively has 2 pieces of pseudocardinal tooths, and left shell has 2 pieces of side teeth, and right shell has 1 piece of side tooth.Pearl thickness, glossy.
The present invention relates to a kind of pearl nucleus soak, use three Plants raw materials to be respectively: winged euonymus, Classification system is Euonymusalatus (Thunb.) Sieb., is Celastraceae Euonymus shrub, originates in China northeast, North China, northwest to various places, the Yangtze river basin; Also there are distribution in Japan, Korea, strong adaptability, cold-resistant, resistance to shade, and resistance to pruning is drought-resistant, barren.Capsule palm fibre purple, drastic crack becomes 4 slivers, is 1-3 slivers sometimes, the fruit being winged euonymus used in the present invention; E. Soongarica Boiss, Classification system is EuphorbiasoongaricaBoiss., is the plant of Euphorbiaceae Euphorbia.Be distributed in the ground such as Gansu, Xinjiang of Mongolia, West Siberia, the Central Asia and China's Mainland, be grown on height above sea level 500 meters to 2, the area of 000 meter, be grown on desert river valley, hillside, low mountain, saline meadow and field wing other comparatively general more, at present by artificial introducing and planting, branch top is born in by inflorescence list, involucre mitriform, is about 2.5 millimeters, diameter 2-2.5 millimeter, tip 5 splits, and sliver is semicircle to oval, edge and inner side tool echinid, body of gland 5, semicircle, filbert, the petal being E. Soongarica Boiss used in the present invention; Polygala root, Classification system is PolygalatenuifoliaWilld, is Polygalaceae rogation flower perennial herb, produce northeast, North China, northwest and Central China and Sichuan, be born in grassland, patana, shrubbery and under shaw, height above sea level 200-2300 rice, leaf alternate, narrow linear or wire lanceolar, long 1-4 centimetre, wide 1-3 millimeter, tip is gradually sharp, and base portion is gradually narrow, Quan Yuan, stockless or nearly stockless, the blade being polygala root used in the present invention.
The instrument such as less than 1000 DEG C Muffle furnaces, Rotary Evaporators, spiral micrometer related in the present invention is prior art, and calcination process, cooling procedure, decocting method, reduced pressure concentration method also belong to prior art.
Accompanying drawing explanation
Fig. 1 is the structural representation of prior art.
Fig. 2 is the schematic diagram of pit 2 of the present invention.
Fig. 3 is the structural representation being uniformly distributed groove 3 around axis of the present invention.
Fig. 4 is the structural representation that pit 2 aperture area of the present invention is less than base area.
Fig. 5 is the structural representation of redistribution grooves 3 in largest circumference of the present invention.
See Fig. 1-5,1-pearl nucleus, 2-pit, 3-groove
Embodiment
In order to make those skilled in the art well understand concrete technical characteristic of the present invention, be beneficial to enforcement of the present invention, existing the present invention will be further explained.
See Fig. 1-5, pearl nucleus 1 surface design pit 2 and groove 3 are to remain more pearl nucleus soak, make effect of the present invention more obvious.
See Fig. 4, the effect that pit 2 aperture area is less than base area compares the pit 2 that aperture area is more than or equal to base area can store more pearl nucleus soak.
Embodiment 1
Pearl nucleus 1 surface is wrapped in pearl nucleus soak, and the preparation method of this soak, comprising:
(1) choose fresh spindleberry 32 weight portion, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(2) choose petal 20 weight portion of fresh E. Soongarica Boiss, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(3) choose fresh Leaves In Polygala Tenuifolia 55 weight portion, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(4) the little fire of the water cooled three kinds of materials being added 200 weight portions respectively decocts 2h, obtains spindleberry decoction liquor, E. Soongarica Boiss petal decoction liquor, Leaves In Polygala Tenuifolia decoction liquor respectively, for subsequent use;
(5) carry out reduced pressure concentration with Rotary Evaporators to spindleberry decoction liquor, agents useful for same is water, obtains spindleberry concentrate, adds the water of 100 weight portions, fully dissolves, and obtains spindleberry juice, for subsequent use; Carry out reduced pressure concentration with Rotary Evaporators to E. Soongarica Boiss petal decoction liquor, agents useful for same is water, obtains E. Soongarica Boiss petal concentrate, adds the water of 100 weight portions, fully dissolve, and obtains E. Soongarica Boiss petal juice, for subsequent use; Carry out reduced pressure concentration with Rotary Evaporators to Leaves In Polygala Tenuifolia decoction liquor, agents useful for same is water, obtains Leaves In Polygala Tenuifolia concentrate, adds the water of 100 weight portions, fully dissolves, and obtains Leaves In Polygala Tenuifolia juice, for subsequent use;
(6) spindleberry juice obtained above, E. Soongarica Boiss petal juice, Leaves In Polygala Tenuifolia juice are fully mixed, namely obtain pearl nucleus soak;
In April, 2011, selecting diameter is that the pearl nucleus of 8mm soak 3 days in obtained pearl nucleus soak, choose the long adult hydriopsis cumingii for 160-200mm of body, its outer embrane inserts pearl nucleus, each hydriopsis cumingii inserts three pearl nucleus, then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plant pearl operating technology and artificial pearl culture technology all belongs to prior art, this test is totally 300 hydriopsis cumingiis, cultivate 300 pearls altogether, be divided into three groups to carry out, namely often 100 hydriopsis cumingiis, 100 pearls are repeated, the record results pearl time, measure the diameter of every pearl and record, calculate the pearl diameter mean value often organizing repeated test, survey tool is spiral micrometer (accuracy is 0.01mm).
Result of the test is as follows:
The results pearl time is in October, 2011-November, and namely the pearl growth phase is about 7 months;
The pearl totally 100 that battery of tests is cultivated, average diameter is 15.28mm;
The pearl totally 100 that second group of test is cultivated, average diameter is 15.47mm;
The pearl totally 100 that 3rd group of test is cultivated, average diameter is 16.02mm;
300 pearl diameter mean values are 15.59mm.
Embodiment 2
Pearl nucleus 1 surface is wrapped in pearl nucleus soak, and the preparation method of this soak, comprising:
(1) choose fresh spindleberry 40 weight portion, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(2) choose petal 17 weight portion of fresh E. Soongarica Boiss, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(3) choose fresh Leaves In Polygala Tenuifolia 52 weight portion, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(4) the little fire of the water cooled three kinds of materials being added 200 weight portions respectively decocts 2h, obtains spindleberry decoction liquor, E. Soongarica Boiss petal decoction liquor, Leaves In Polygala Tenuifolia decoction liquor respectively, for subsequent use;
(5) carry out reduced pressure concentration with Rotary Evaporators to spindleberry decoction liquor, agents useful for same is water, obtains spindleberry concentrate, adds the water of 100 weight portions, fully dissolves, and obtains spindleberry juice, for subsequent use; Carry out reduced pressure concentration with Rotary Evaporators to E. Soongarica Boiss petal decoction liquor, agents useful for same is water, obtains E. Soongarica Boiss petal concentrate, adds the water of 100 weight portions, fully dissolve, and obtains E. Soongarica Boiss petal juice, for subsequent use; Carry out reduced pressure concentration with Rotary Evaporators to Leaves In Polygala Tenuifolia decoction liquor, agents useful for same is water, obtains Leaves In Polygala Tenuifolia concentrate, adds the water of 100 weight portions, fully dissolves, and obtains Leaves In Polygala Tenuifolia juice, for subsequent use;
(6) spindleberry juice obtained above, E. Soongarica Boiss petal juice, Leaves In Polygala Tenuifolia juice are fully mixed, namely obtain pearl nucleus soak;
In April, 2011, selecting diameter is that the pearl nucleus of 8mm soak 3 days in obtained pearl nucleus soak, choose the long adult hydriopsis cumingii for 160-200mm of body, its outer embrane inserts pearl nucleus, each hydriopsis cumingii inserts three pearl nucleus, then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plant pearl operating technology and artificial pearl culture technology all belongs to prior art, this test is totally 300 hydriopsis cumingiis, cultivate 300 pearls altogether, be divided into three groups to carry out, namely often 100 hydriopsis cumingiis, 100 pearls are repeated, the record results pearl time, measure the diameter of every pearl and record, calculate the pearl diameter mean value often organizing repeated test, survey tool is spiral micrometer (accuracy is 0.01mm).
Result of the test is as follows:
The results pearl time is in October, 2011-November, and namely the pearl growth phase is about 7 months;
The pearl totally 100 that battery of tests is cultivated, average diameter is 15.66mm;
The pearl totally 100 that second group of test is cultivated, average diameter is 15.83mm;
The pearl totally 100 that 3rd group of test is cultivated, average diameter is 15.32mm;
300 pearl diameter mean values are 15.60mm.
Embodiment 3
Pearl nucleus 1 surface is wrapped in pearl nucleus soak, and the preparation method of this soak, comprising:
(1) choose fresh spindleberry 38 weight portion, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(2) choose petal 11 weight portion of fresh E. Soongarica Boiss, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(3) choose fresh Leaves In Polygala Tenuifolia 50 weight portion, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(4) the little fire of the water cooled three kinds of materials being added 200 weight portions respectively decocts 2h, obtains spindleberry decoction liquor, E. Soongarica Boiss petal decoction liquor, Leaves In Polygala Tenuifolia decoction liquor respectively, for subsequent use;
(5) carry out reduced pressure concentration with Rotary Evaporators to spindleberry decoction liquor, agents useful for same is water, obtains spindleberry concentrate, adds the water of 100 weight portions, fully dissolves, and obtains spindleberry juice, for subsequent use; Carry out reduced pressure concentration with Rotary Evaporators to E. Soongarica Boiss petal decoction liquor, agents useful for same is water, obtains E. Soongarica Boiss petal concentrate, adds the water of 100 weight portions, fully dissolve, and obtains E. Soongarica Boiss petal juice, for subsequent use; Carry out reduced pressure concentration with Rotary Evaporators to Leaves In Polygala Tenuifolia decoction liquor, agents useful for same is water, obtains Leaves In Polygala Tenuifolia concentrate, adds the water of 100 weight portions, fully dissolves, and obtains Leaves In Polygala Tenuifolia juice, for subsequent use;
(6) spindleberry juice obtained above, E. Soongarica Boiss petal juice, Leaves In Polygala Tenuifolia juice are fully mixed, namely obtain pearl nucleus soak;
In April, 2011, selecting diameter is that the pearl nucleus of 8mm soak 3 days in obtained pearl nucleus soak, choose the long adult hydriopsis cumingii for 160-200mm of body, its outer embrane inserts pearl nucleus, each hydriopsis cumingii inserts three pearl nucleus, then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plant pearl operating technology and artificial pearl culture technology all belongs to prior art, this test is totally 300 hydriopsis cumingiis, cultivate 300 pearls altogether, be divided into three groups to carry out, namely often 100 hydriopsis cumingiis, 100 pearls are repeated, the record results pearl time, measure the diameter of every pearl and record, calculate the pearl diameter mean value often organizing repeated test, survey tool is spiral micrometer (accuracy is 0.01mm).
Result of the test is as follows:
The results pearl time is in October, 2011-November, and namely the pearl growth phase is about 7 months;
The pearl totally 100 that battery of tests is cultivated, average diameter is 16.12mm;
The pearl totally 100 that second group of test is cultivated, average diameter is 15.87mm;
The pearl totally 100 that 3rd group of test is cultivated, average diameter is 15.32mm;
300 pearl diameter mean values are 15.77mm.
Embodiment 4
Pearl nucleus 1 surface is wrapped in pearl nucleus soak, and the preparation method of this soak, comprising:
(1) choose fresh spindleberry 35 weight portion, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(2) choose petal 14 weight portion of fresh E. Soongarica Boiss, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(3) choose fresh Leaves In Polygala Tenuifolia 57 weight portion, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(4) the little fire of the water cooled three kinds of materials being added 200 weight portions respectively decocts 2h, obtains spindleberry decoction liquor, E. Soongarica Boiss petal decoction liquor, Leaves In Polygala Tenuifolia decoction liquor respectively, for subsequent use;
(5) carry out reduced pressure concentration with Rotary Evaporators to spindleberry decoction liquor, agents useful for same is water, obtains spindleberry concentrate, adds the water of 100 weight portions, fully dissolves, and obtains spindleberry juice, for subsequent use; Carry out reduced pressure concentration with Rotary Evaporators to E. Soongarica Boiss petal decoction liquor, agents useful for same is water, obtains E. Soongarica Boiss petal concentrate, adds the water of 100 weight portions, fully dissolve, and obtains E. Soongarica Boiss petal juice, for subsequent use; Carry out reduced pressure concentration with Rotary Evaporators to Leaves In Polygala Tenuifolia decoction liquor, agents useful for same is water, obtains Leaves In Polygala Tenuifolia concentrate, adds the water of 100 weight portions, fully dissolves, and obtains Leaves In Polygala Tenuifolia juice, for subsequent use;
(6) spindleberry juice obtained above, E. Soongarica Boiss petal juice, Leaves In Polygala Tenuifolia juice are fully mixed, namely obtain pearl nucleus soak;
In April, 2011, selecting diameter is that the pearl nucleus of 8mm soak 3 days in obtained pearl nucleus soak, choose the long adult hydriopsis cumingii for 160-200mm of body, its outer embrane inserts pearl nucleus, each hydriopsis cumingii inserts pearl nucleus, then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plant pearl operating technology and artificial pearl culture technology all belongs to prior art, this test is totally 300 hydriopsis cumingiis, cultivate 300 pearls altogether, be divided into three groups to carry out, namely often 100 hydriopsis cumingiis, 100 pearls are repeated, the record results pearl time, measure the diameter of every pearl and record, calculate the pearl diameter mean value often organizing repeated test, survey tool is spiral micrometer (accuracy is 0.01mm).
Result of the test is as follows:
The results pearl time is in October, 2011-November, and namely the pearl growth phase is about 7 months;
The pearl totally 100 that battery of tests is cultivated, average diameter is 16.34mm;
The pearl totally 100 that second group of test is cultivated, average diameter is 16.51mm;
The pearl totally 100 that 3rd group of test is cultivated, average diameter is 16.09mm;
300 pearl diameter mean values are 16.31mm.
Embodiment 5
Pearl nucleus 1 surface is wrapped in pearl nucleus soak, and the preparation method of this soak, comprising:
(1) choose fresh spindleberry 37 weight portion, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(2) choose petal 15 weight portion of fresh E. Soongarica Boiss, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(3) choose fresh Leaves In Polygala Tenuifolia 60 weight portion, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(4) the little fire of the water cooled three kinds of materials being added 200 weight portions respectively decocts 2h, obtains spindleberry decoction liquor, E. Soongarica Boiss petal decoction liquor, Leaves In Polygala Tenuifolia decoction liquor respectively, for subsequent use;
(5) carry out reduced pressure concentration with Rotary Evaporators to spindleberry decoction liquor, agents useful for same is water, obtains spindleberry concentrate, adds the water of 100 weight portions, fully dissolves, and obtains spindleberry juice, for subsequent use; Carry out reduced pressure concentration with Rotary Evaporators to E. Soongarica Boiss petal decoction liquor, agents useful for same is water, obtains E. Soongarica Boiss petal concentrate, adds the water of 100 weight portions, fully dissolve, and obtains E. Soongarica Boiss petal juice, for subsequent use; Carry out reduced pressure concentration with Rotary Evaporators to Leaves In Polygala Tenuifolia decoction liquor, agents useful for same is water, obtains Leaves In Polygala Tenuifolia concentrate, adds the water of 100 weight portions, fully dissolves, and obtains Leaves In Polygala Tenuifolia juice, for subsequent use;
(6) spindleberry juice obtained above, E. Soongarica Boiss petal juice, Leaves In Polygala Tenuifolia juice are fully mixed, namely obtain pearl nucleus soak;
In April, 2011, selecting diameter is that the pearl nucleus of 8mm soak 3 days in obtained pearl nucleus soak, choose the long adult hydriopsis cumingii for 160-200mm of body, its outer embrane inserts pearl nucleus, each hydriopsis cumingii inserts pearl nucleus, then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plant pearl operating technology and artificial pearl culture technology all belongs to prior art, this test is totally 300 hydriopsis cumingiis, cultivate 300 pearls altogether, be divided into three groups to carry out, namely often 100 hydriopsis cumingiis, 100 pearls are repeated, the record results pearl time, measure the diameter of every pearl and record, calculate the pearl diameter mean value often organizing repeated test, survey tool is spiral micrometer (accuracy is 0.01mm).
Result of the test is as follows:
The results pearl time is in October, 2011-November, and namely the pearl growth phase is about 7 months;
The pearl totally 100 that battery of tests is cultivated, average diameter is 16.42mm;
The pearl totally 100 that second group of test is cultivated, average diameter is 16.55mm;
The pearl totally 100 that 3rd group of test is cultivated, average diameter is 16.59mm;
300 pearl diameter mean values are 16.52mm.
Embodiment 6
(1) choose fresh spindleberry 37 weight portion, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(2) the little fire of water cooled material being added 200 weight portions decocts 2h, obtains spindleberry decoction liquor, for subsequent use;
(3) carry out reduced pressure concentration with Rotary Evaporators to spindleberry decoction liquor, agents useful for same is water, obtains spindleberry concentrate, adds the water of 100 weight portions, fully dissolves, and obtains spindleberry juice, for subsequent use;
(4) spindleberry juice obtained above is fully mixed, namely obtain pearl nucleus soak;
In April, 2011, selecting diameter is that the pearl nucleus of 8mm soak 3 days in obtained pearl nucleus soak, choose the long adult hydriopsis cumingii for 160-200mm of body, its outer embrane inserts pearl nucleus, each hydriopsis cumingii inserts three pearl nucleus, then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plant pearl operating technology and artificial pearl culture technology all belongs to prior art, this test is totally 300 hydriopsis cumingiis, cultivate 300 pearls altogether, be divided into three groups to carry out, namely often 100 hydriopsis cumingiis, 100 pearls are repeated, the record results pearl time, measure the diameter of every pearl and record, calculate the pearl diameter mean value often organizing repeated test, survey tool is spiral micrometer (accuracy is 0.01mm).
Result of the test is as follows:
The results pearl time is in January ,-2013 in December, 2012, and namely the pearl growth phase is 1 year about 9 months;
The pearl totally 100 that battery of tests is cultivated, average diameter is 10.02mm;
The pearl totally 100 that second group of test is cultivated, average diameter is 9.89mm;
The pearl totally 100 that 3rd group of test is cultivated, average diameter is 10.11mm;
300 pearl diameter mean values are 10.01mm.
Embodiment 7
(1) choose petal 15 weight portion of fresh E. Soongarica Boiss, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(2) the little fire of water cooled material being added 200 weight portions decocts 2h, obtains E. Soongarica Boiss petal decoction liquor, for subsequent use;
(3) carry out reduced pressure concentration with Rotary Evaporators to E. Soongarica Boiss petal decoction liquor, agents useful for same is water, obtains E. Soongarica Boiss petal concentrate, adds the water of 100 weight portions, fully dissolve, and obtains E. Soongarica Boiss petal juice, for subsequent use;
(4) E. Soongarica Boiss petal juice obtained above is fully mixed, namely obtain pearl nucleus soak;
In April, 2011, selecting diameter is that the pearl nucleus of 8mm soak 3 days in obtained pearl nucleus soak, choose the long adult hydriopsis cumingii for 160-200mm of body, its outer embrane inserts pearl nucleus, each hydriopsis cumingii inserts pearl nucleus, then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plant pearl operating technology and artificial pearl culture technology all belongs to prior art, this test is totally 300 hydriopsis cumingiis, cultivate 300 pearls altogether, be divided into three groups to carry out, namely often 100 hydriopsis cumingiis, 100 pearls are repeated, the record results pearl time, measure the diameter of every pearl and record, calculate the pearl diameter mean value often organizing repeated test, survey tool is spiral micrometer (accuracy is 0.01mm).
Result of the test is as follows:
The results pearl time is in January ,-2013 in December, 2012, and namely the pearl growth phase is 1 year about 9 months;
The pearl totally 100 that battery of tests is cultivated, average diameter is 10.31mm;
The pearl totally 100 that second group of test is cultivated, average diameter is 10.12mm;
The pearl totally 100 that 3rd group of test is cultivated, average diameter is 10.33mm;
300 pearl diameter mean values are 10.25mm.
Embodiment 8
(1) choose fresh Leaves In Polygala Tenuifolia 60 weight portion, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(2) the little fire of water cooled material being added 200 weight portions decocts 2h, obtains Leaves In Polygala Tenuifolia decoction liquor, for subsequent use;
(3) carry out reduced pressure concentration with Rotary Evaporators to Leaves In Polygala Tenuifolia decoction liquor, agents useful for same is water, obtains Leaves In Polygala Tenuifolia concentrate, adds the water of 100 weight portions, fully dissolves, and obtains Leaves In Polygala Tenuifolia juice, for subsequent use;
(4) Leaves In Polygala Tenuifolia juice obtained above is fully mixed, namely obtain pearl nucleus soak;
In April, 2011, selecting diameter is that the pearl nucleus of 8mm soak 3 days in obtained pearl nucleus soak, choose the long adult hydriopsis cumingii for 160-200mm of body, its outer embrane inserts pearl nucleus, each hydriopsis cumingii inserts pearl nucleus, then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plant pearl operating technology and artificial pearl culture technology all belongs to prior art, this test is totally 300 hydriopsis cumingiis, cultivate 300 pearls altogether, be divided into three groups to carry out, namely often 100 hydriopsis cumingiis, 100 pearls are repeated, the record results pearl time, measure the diameter of every pearl and record, calculate the pearl diameter mean value often organizing repeated test, survey tool is spiral micrometer (accuracy is 0.01mm).
Result of the test is as follows:
The results pearl time is in January ,-2013 in December, 2012, and namely the pearl growth phase is 1 year about 9 months;
The pearl totally 100 that battery of tests is cultivated, average diameter is 9.92mm;
The pearl totally 100 that second group of test is cultivated, average diameter is 10.13mm;
The pearl totally 100 that 3rd group of test is cultivated, average diameter is 10.01mm;
300 pearl diameter mean values are 10.02mm.
Embodiment 9
(1) choose fresh spindleberry 37 weight portion, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(2) choose petal 15 weight portion of fresh E. Soongarica Boiss, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(3) the little fire of the water cooled two kinds of materials being added 200 weight portions respectively decocts 2h, obtains spindleberry decoction liquor, E. Soongarica Boiss petal decoction liquor respectively, for subsequent use;
(4) carry out reduced pressure concentration with Rotary Evaporators to spindleberry decoction liquor, agents useful for same is water, obtains spindleberry concentrate, adds the water of 100 weight portions, fully dissolves, and obtains spindleberry juice, for subsequent use; Carry out reduced pressure concentration with Rotary Evaporators to E. Soongarica Boiss petal decoction liquor, agents useful for same is water, obtains E. Soongarica Boiss petal concentrate, adds the water of 100 weight portions, fully dissolve, and obtains E. Soongarica Boiss petal juice, for subsequent use;
(5) spindleberry juice obtained above, E. Soongarica Boiss petal juice are fully mixed, namely obtain pearl nucleus soak;
In April, 2011, selecting diameter is that the pearl nucleus of 8mm soak 3 days in obtained pearl nucleus soak, choose the long adult hydriopsis cumingii for 160-200mm of body, its outer embrane inserts pearl nucleus, each hydriopsis cumingii inserts pearl nucleus, then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plant pearl operating technology and artificial pearl culture technology all belongs to prior art, this test is totally 300 hydriopsis cumingiis, cultivate 300 pearls altogether, be divided into three groups to carry out, namely often 100 hydriopsis cumingiis, 100 pearls are repeated, the record results pearl time, measure the diameter of every pearl and record, calculate the pearl diameter mean value often organizing repeated test, survey tool is spiral micrometer (accuracy is 0.01mm).
Result of the test is as follows:
The results pearl time is in November, 2012-December, and namely the pearl growth phase is 1 year about 7 months;
The pearl totally 100 that battery of tests is cultivated, average diameter is 12.33mm;
The pearl totally 100 that second group of test is cultivated, average diameter is 12.47mm;
The pearl totally 100 that 3rd group of test is cultivated, average diameter is 12.56mm;
300 pearl diameter mean values are 12.45mm.
Embodiment 10
(1) choose fresh spindleberry 37 weight portion, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(2) choose fresh Leaves In Polygala Tenuifolia 60 weight portion, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(3) the little fire of the water cooled two kinds of materials being added 200 weight portions respectively decocts 2h, obtains spindleberry decoction liquor, Leaves In Polygala Tenuifolia decoction liquor respectively, for subsequent use;
(4) carry out reduced pressure concentration with Rotary Evaporators to spindleberry decoction liquor, agents useful for same is water, obtains spindleberry concentrate, adds the water of 100 weight portions, fully dissolves, and obtains spindleberry juice, for subsequent use; Carry out reduced pressure concentration with Rotary Evaporators to Leaves In Polygala Tenuifolia decoction liquor, agents useful for same is water, obtains Leaves In Polygala Tenuifolia concentrate, adds the water of 100 weight portions, fully dissolves, and obtains Leaves In Polygala Tenuifolia juice, for subsequent use;
(5) spindleberry juice obtained above, Leaves In Polygala Tenuifolia juice are fully mixed, namely obtain pearl nucleus soak;
In April, 2011, selecting diameter is that the pearl nucleus of 8mm soak 3 days in obtained pearl nucleus soak, choose the long adult hydriopsis cumingii for 160-200mm of body, its outer embrane inserts pearl nucleus, each hydriopsis cumingii inserts pearl nucleus, then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plant pearl operating technology and artificial pearl culture technology all belongs to prior art, this test is totally 300 hydriopsis cumingiis, cultivate 300 pearls altogether, be divided into three groups to carry out, namely often 100 hydriopsis cumingiis, 100 pearls are repeated, the record results pearl time, measure the diameter of every pearl and record, calculate the pearl diameter mean value often organizing repeated test, survey tool is spiral micrometer (accuracy is 0.01mm).
Result of the test is as follows:
The results pearl time is in November, 2012, and namely the pearl growth phase is 1 year about 7 months;
The pearl totally 100 that battery of tests is cultivated, average diameter is 12.39mm;
The pearl totally 100 that second group of test is cultivated, average diameter is 13.05mm;
The pearl totally 100 that 3rd group of test is cultivated, average diameter is 12.62mm;
300 pearl diameter mean values are 12.69mm.
Embodiment 11
(1) choose petal 15 weight portion of fresh E. Soongarica Boiss, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(2) choose fresh Leaves In Polygala Tenuifolia 60 weight portion, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(3) the little fire of the water cooled two kinds of materials being added 200 weight portions respectively decocts 2h, obtains E. Soongarica Boiss petal decoction liquor, Leaves In Polygala Tenuifolia decoction liquor respectively, for subsequent use;
(4) carry out reduced pressure concentration with Rotary Evaporators to E. Soongarica Boiss petal decoction liquor, agents useful for same is water, obtains E. Soongarica Boiss petal concentrate, adds the water of 100 weight portions, fully dissolve, and obtains E. Soongarica Boiss petal juice, for subsequent use; Carry out reduced pressure concentration with Rotary Evaporators to Leaves In Polygala Tenuifolia decoction liquor, agents useful for same is water, obtains Leaves In Polygala Tenuifolia concentrate, adds the water of 100 weight portions, fully dissolves, and obtains Leaves In Polygala Tenuifolia juice, for subsequent use;
(5) E. Soongarica Boiss petal juice obtained above, Leaves In Polygala Tenuifolia juice are fully mixed, namely obtain pearl nucleus soak;
In April, 2011, selecting diameter is that the pearl nucleus of 8mm soak 3 days in obtained pearl nucleus soak, choose the long adult hydriopsis cumingii for 160-200mm of body, its outer embrane inserts pearl nucleus, each hydriopsis cumingii inserts pearl nucleus, then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plant pearl operating technology and artificial pearl culture technology all belongs to prior art, this test is totally 300 hydriopsis cumingiis, cultivate 300 pearls altogether, be divided into three groups to carry out, namely often 100 hydriopsis cumingiis, 100 pearls are repeated, the record results pearl time, measure the diameter of every pearl and record, calculate the pearl diameter mean value often organizing repeated test, survey tool is spiral micrometer (accuracy is 0.01mm).
Result of the test is as follows:
The results pearl time is in November, 2012, and namely the pearl growth phase is 1 year about 7 months;
The pearl totally 100 that battery of tests is cultivated, average diameter is 12.53mm;
The pearl totally 100 that second group of test is cultivated, average diameter is 12.28mm;
The pearl totally 100 that 3rd group of test is cultivated, average diameter is 12.34mm;
300 pearl diameter mean values are 12.38mm.
Embodiment 12
This embodiment is check experiment
In April, 2011, selecting diameter is that the pearl nucleus of 8mm soak 3 days in clear water, choose the long adult hydriopsis cumingii for 160-200mm of body, its outer embrane inserts pearl nucleus, each hydriopsis cumingii inserts pearl nucleus, then artificial pearl culture is carried out, Cultivated water is special cultured pearl waters, plant pearl operating technology and artificial pearl culture technology all belongs to prior art, this test is totally 300 hydriopsis cumingiis, cultivate 300 pearls altogether, be divided into three groups to carry out, namely often 100 hydriopsis cumingiis, 100 pearls are repeated, the record results pearl time, measure the diameter of every pearl and record, calculate the pearl diameter mean value often organizing repeated test, survey tool is spiral micrometer (accuracy is 0.01mm).
Result of the test is as follows:
The results pearl time is in January, 2013-February, and namely the pearl growth phase is 1 year about 10 months;
The pearl totally 100 that battery of tests is cultivated, average diameter is 9.31mm;
The pearl totally 100 that second group of test is cultivated, average diameter is 9.22mm;
The pearl totally 100 that 3rd group of test is cultivated, average diameter is 9.06mm;
300 pearl diameter mean values are 9.20mm.
Claims (1)
1. one kind is shortened the pearl nucleus of producing nucleated pearls phase, it is characterized in that, comprise pearl nucleus (1), pit (2), the diameter of pearl nucleus is 8mm, pearl nucleus (1) surface uniform distribution pit (2), pit (2) aperture area is less than base area; Pearl nucleus (1) soak 3 days in pearl nucleus soak, and the preparation method of this soak, comprising:
(1) choose fresh spindleberry 32 weight portion, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(2) choose petal 20 weight portion of fresh E. Soongarica Boiss, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(3) choose fresh Leaves In Polygala Tenuifolia 55 weight portion, be placed on less than 1000 DEG C Muffle furnaces after 500 ± 25 DEG C of high temperature sintering 4h, take out and be cooled to room temperature, for subsequent use;
(4) the little fire of the water cooled three kinds of materials being added 200 weight portions respectively decocts 2h, obtains spindleberry decoction liquor, E. Soongarica Boiss petal decoction liquor, Leaves In Polygala Tenuifolia decoction liquor respectively, for subsequent use;
(5) carry out reduced pressure concentration with Rotary Evaporators to spindleberry decoction liquor, agents useful for same is water, obtains spindleberry concentrate, adds the water of 100 weight portions, fully dissolves, and obtains spindleberry juice, for subsequent use; Carry out reduced pressure concentration with Rotary Evaporators to E. Soongarica Boiss petal decoction liquor, agents useful for same is water, obtains E. Soongarica Boiss petal concentrate, adds the water of 100 weight portions, fully dissolve, and obtains E. Soongarica Boiss petal juice, for subsequent use; Carry out reduced pressure concentration with Rotary Evaporators to Leaves In Polygala Tenuifolia decoction liquor, agents useful for same is water, obtains Leaves In Polygala Tenuifolia concentrate, adds the water of 100 weight portions, fully dissolves, and obtains Leaves In Polygala Tenuifolia juice, for subsequent use;
(6) spindleberry juice obtained above, E. Soongarica Boiss petal juice, Leaves In Polygala Tenuifolia juice are fully mixed, namely obtain pearl nucleus soak.
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101036449A (en) * | 2007-04-24 | 2007-09-19 | 詹伟建 | Pearl sacs processing method for cultivating nucleated pearls |
| JP2013158251A (en) * | 2012-02-01 | 2013-08-19 | Panasonic Corp | Culturing method |
| CN103270991A (en) * | 2013-06-20 | 2013-09-04 | 北海市源龙珍珠有限公司 | Golden pearl cultivation method |
| US20140174373A1 (en) * | 2009-03-31 | 2014-06-26 | Florida Atlantic University Board Of Trustees | Methods for producing cultured pearls in conch and other gastropods |
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2015
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101036449A (en) * | 2007-04-24 | 2007-09-19 | 詹伟建 | Pearl sacs processing method for cultivating nucleated pearls |
| US20140174373A1 (en) * | 2009-03-31 | 2014-06-26 | Florida Atlantic University Board Of Trustees | Methods for producing cultured pearls in conch and other gastropods |
| JP2013158251A (en) * | 2012-02-01 | 2013-08-19 | Panasonic Corp | Culturing method |
| CN103270991A (en) * | 2013-06-20 | 2013-09-04 | 北海市源龙珍珠有限公司 | Golden pearl cultivation method |
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