CN105250177B - A kind of extracting method of passion fruit extract and its application - Google Patents
A kind of extracting method of passion fruit extract and its application Download PDFInfo
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- CN105250177B CN105250177B CN201510733794.7A CN201510733794A CN105250177B CN 105250177 B CN105250177 B CN 105250177B CN 201510733794 A CN201510733794 A CN 201510733794A CN 105250177 B CN105250177 B CN 105250177B
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- passion fruit
- hair
- immersion treatment
- warm water
- treatment
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
Abstract
The present invention, which provides a kind of extracting method of passion fruit extract, includes step:Passion fruit cleans, pulverization process, immersion treatment, broken wall treatment, warm water immersion treatment, centrifuged, filtration treatment obtain supernatant and to gained supernatant carry out concentrate filtrate handle to obtain target product, the extracting method of passion fruit extract provided by the present invention it is more traditional first fruit thing is dried or air-dried after extract again, nutritional ingredient is more rich, by the unique physical characteristic of ultrasonic wave passion fruit extracts active ingredients can be promoted more abundant, recovery rate significantly improves than traditional handicraft, extraction time greatly shortens, operation is simple for the method, it is low for equipment requirements, reduce operating cost, it is added into hair conditioner, moist moisture-keeping efficacy well can be played, supplement the nutriment needed for hair, hair barrier function can also be improved, maintain the gloss and elasticity of hair.
Description
Technical field
The present invention relates to daily cleaning chemical products technical field, and in particular to a kind of extracting method of passion fruit extract and its
Using.
Background technology
Passion fruit originates in South America, scientific name passionflower, because its pulp can give out banana, pineapple, strawberry, lichee, lemon,
The strong fragrances of ten several fruit such as mango, smoked plum and using names.Passion fruit contains 17 kinds of amino acid, abundant protein, fat,
165 kinds of sugar, vitamin, calcium, phosphorus, iron, potassium, SOD enzymes and superfluorescent fiber etc. to human body benefit materials, be more referred to as VC in fruit it
King, have the unique taste (seed is crispy and delicious, nutritious).Passion fruit has anti-inflammatory analgetic, promoting blood circulation, blood fat-reducing blood pressure-decreasing, enriching yin to mend
Kidney, refresh oneself sober up, the magical effect such as dispelling fatigue, skin-protecting face nursing.
Contain numerous superfluorescent fibers in passion fruit, the most trickle part of the deep enough stomach of energy, absorbed by its active gene
Internal harmful substance thoroughly discharges it, plays the screen-wall effect for protecting skin not absorb harmful substance, may also suppress harmful micro-
The growth of biology.Body is purified, avoids harmful substance from depositing in vivo, and then improves skin, beautify the effect of appearance.It is super
Fiber can promote to alleviate dermatitis symptom, remove and stick the excitor substance that is trapped on skin, avoid stimulating skin and by human body again
Absorb, so as to dermatitis symptom, superfluorescent fiber also has antitumor activity.
VC in passion fruit participates in cholesterol metabolic, can reduce cholesterol, purifies blood.In addition, be rich in passion fruit
VC, carrotene, SOD enzymes can remove interior free yl, play face nourishing antidebilitation.The seed of passion fruit is rich in high protein, high
Level fat, skin and hair can be given to provide abundant nutritional ingredient;Passion fruit, which can also adsorb cholesterol and bile etc, to be had
Machine molecule, suppress absorption of the skin to grease, keep skin and the dry and comfortable non-greasy of hair.
The hair top layer of health is complete by one groupHair scale pieceThe diaphragm of hair is formed with the grease of naturally secret, excessively
The natural diaphragm of this layer can all be destroyed by washing reason, boiling hot dye, exposure in sunshine, caused cortex water loss, hair is dried up, follow the string
And flexibility.Hair conditioner is only commonly used, could persistently form the diaphragm of hair, hair is escaped injury.
The impaired situation getting worse of the hair of modern, shampoo be difficult meet to repair it is all required for damaged hair
Composition.Therefore consumer is more likely to select some quick-acting products, the reparation liquid for special nursing.Hair can be made by repairing liquid
Epidermis scales closure is got up, and makes the smooth easily comb of healthy hair, health is submissive, effectively can more be supplemented the nutrients to hair, repairs impaired hair
Matter.Sun-screening agent, vitamin, protein hydrolysate, plant extraction liquid etc. can supplement the various nutriments needed for hair.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of passion fruit extraction for above-mentioned the deficiencies in the prior art
The extracting method of thing and its application in hair care product.
The present invention is that technical scheme is used by solving the above problems:
A kind of extracting method of passion fruit extract, comprises the following steps:
(1) cleaning treatment is carried out to the passion fruit;
(2) passion fruit cleaned in step (1) is positioned in disintegrating machine and carries out pulverization process;
(3) Extraction solvent is added in the passion fruit crushed, carries out immersion treatment;
(4) immersion treatment is crossed in step (3) passion fruit and solvent are added on ultrasonator and carry out ultrasonication
Processing;
(5) warm water immersion treatment is carried out to the passion fruit in step (3) by ultrasonication;
(6) passion fruit crossed to warm water immersion treatment is centrifuged, filtration treatment obtains supernatant;
(7) concentration filtrate is carried out to gained supernatant to handle to obtain target product.
Further, motor of crusher power is 800~1800W in the step (2), and it is 0.2~2min to crush the time.
Further, Extraction solvent described in the step (3) is in water, ethanol, methanol, acetone, petroleum ether, n-hexane
One or more, the weight ratio of the Extraction solvent and the passion fruit is 3:1~20:1.
Further, warm water temperature described in the step (5) is 30~50 DEG C, the warm water and the passion fruit weight
Than for 8:1~10:1.
Further, the concentration filtrate processing is thin using vacuum under the conditions of vacuum is 0.090~0.095Mpa
Film condensing device carries out flash concentration, and the feed speed for adjusting solution to be concentrated is concentrated into repeatedly with 150~250mL.min flow
The 1/5~1/6 of original volume, obtain passion fruit extract.
Application of the described passion fruit extract in hair products.
The beneficial effects of the present invention are:
The extracting method of passion fruit extract provided by the present invention it is more traditional first fruit thing is dried or air-dried after carry again
Take, nutritional ingredient is more rich, by the unique physical characteristic of ultrasonic wave passion fruit extracts active ingredients can be promoted more abundant, extraction
Rate significantly improves than traditional handicraft, and extraction time greatly shortens, and operation is simple for the method, low for equipment requirements, reduces fortune
Row cost, it is added into hair conditioner, can be played moist moisture-keeping efficacy well, be supplemented the nutriment needed for hair, also
Hair barrier function can be improved, maintain the gloss and elasticity of hair.
Brief description of the drawings
Fig. 1 is a kind of process chart of the extracting method of passion fruit extract of the present invention.
Embodiment
Embodiments of the present invention are specifically illustrated below in conjunction with the accompanying drawings, and these embodiments are only given for explanation
Purpose, limitation of the invention can not be interpreted as, including accompanying drawing is only for reference and explanation uses, and does not form to patent of the present invention
The limitation of protection domain, because without departing from the spirit and scope of the present invention, many can be carried out to the present invention and changed
Become.
Embodiment 1
As shown in figure 1, in the present embodiment, a kind of extracting method of passion fruit extract provided by the present invention, including it is following
Step:
(1) cleaning treatment is carried out to the passion fruit, described fresh passion fruit is commercially available passion fruit;
(2) passion fruit and solvent that were cleaned in step (1) are positioned in disintegrating machine and carry out pulverization process, crush electromechanics
Acc power is 800~1800W, and it is 1min to crush the time;
(3) Extraction solvent is added in the passion fruit crushed, immersion treatment is carried out, is extracted described in the step (3)
Solvent is 90% ethanol, and the weight ratio of the Extraction solvent and the passion fruit is 5:1;
(4) passion fruit that immersion treatment is crossed in step (3) is added to progress ultrasonication processing on ultrasonator;
(5) warm water immersion treatment is carried out to the passion fruit in step (3) by ultrasonication, the warm water temperature is 45
DEG C, the warm water is 10 with the passion fruit weight ratio:1;
(6) passion fruit crossed to warm water immersion treatment is centrifuged, filtration treatment obtains supernatant;
(7) carry out concentration filtrate to gained supernatant to handle to obtain target product, the concentration filtrate processing is in vacuum
Spend to use Reduced Pressure Concentration Device to carry out flash concentration under the conditions of 0.090~0.095Mpa, adjust the feed liquor of solution to be concentrated
Speed is concentrated into the 1/5 of original volume with 150~250mL.min flow repeatedly, obtains passion fruit extract.
Embodiment 2
As shown in figure 1, in the present embodiment, a kind of extracting method of passion fruit extract provided by the present invention, including it is following
Step:
(1) cleaning treatment is carried out to the passion fruit, described fresh passion fruit is commercially available passion fruit;
(2) passion fruit and solvent that were cleaned in step (1) are positioned in disintegrating machine and carry out pulverization process, crush electromechanics
Acc power is 800~1800W, and it is 1min to crush the time;
(3) Extraction solvent is added in the passion fruit crushed, immersion treatment is carried out, is extracted described in the step (3)
Solvent is 90% ethanol, and the weight ratio of the Extraction solvent and the passion fruit is 8:1;
(4) passion fruit that immersion treatment is crossed in step (3) is added to progress ultrasonication processing on ultrasonator;
(5) warm water immersion treatment is carried out to the passion fruit in step (3) by ultrasonication, the warm water temperature is 45
DEG C, the warm water is 10 with the passion fruit weight ratio:1;
(6) passion fruit crossed to warm water immersion treatment is centrifuged, filtration treatment obtains supernatant;
(7) carry out concentration filtrate to gained supernatant to handle to obtain target product, the concentration filtrate processing is in vacuum
Spend to use Reduced Pressure Concentration Device to carry out flash concentration under the conditions of 0.090~0.095Mpa, adjust the feed liquor of solution to be concentrated
Speed is concentrated into the 1/5 of original volume with 150~250mL.min flow repeatedly, obtains passion fruit extract.
Embodiment 3
As shown in figure 1, in the present embodiment, a kind of extracting method of passion fruit extract provided by the present invention, including it is following
Step:
(1) cleaning treatment is carried out to the passion fruit, described fresh passion fruit is commercially available passion fruit;
(2) passion fruit and solvent that were cleaned in step (1) are positioned in disintegrating machine and carry out pulverization process, crush electromechanics
Acc power is 800~1800W, and it is 1min to crush the time;
(3) Extraction solvent is added in the passion fruit crushed, immersion treatment is carried out, is extracted described in the step (3)
Solvent is 90% ethanol, and the weight ratio of the Extraction solvent and the passion fruit is 3:1;
(4) passion fruit that immersion treatment is crossed in step (3) is added to progress ultrasonication processing on ultrasonator;
(5) warm water immersion treatment is carried out to the passion fruit in step (3) by ultrasonication, the warm water temperature is 45
DEG C, the warm water is 20 with the passion fruit weight ratio:1;
(6) passion fruit crossed to warm water immersion treatment is centrifuged, filtration treatment obtains supernatant;
(7) carry out concentration filtrate to gained supernatant to handle to obtain target product, the concentration filtrate processing is in vacuum
Spend to use Reduced Pressure Concentration Device to carry out flash concentration under the conditions of 0.090~0.095Mpa, adjust the feed liquor of solution to be concentrated
Speed is concentrated into the 1/6 of original volume with 150~250mL.min flow repeatedly, obtains passion fruit extract.
Embodiment 4
The present embodiment is the application in hair conditioner to passion fruit extract, and the moisturizing and nourishing hair conditioner includes following weight
The component of percentage:
1%~15% surfactant;
1%~10% conditioner;
1%~10% fatting agent;
1%~10% active component;
0.05%~0.2% chelating agent;
1~10% additive;
Surplus is water,
Surfactant is at least one of cetostearyl alcohol, cetanol, beeswax.
Conditioner is hydroxyethyl cellulose, hexadecyltrimethylammonium chloride, OTAC, melon
At least one of glue, organic silicon emulsion, ring five dimethyl silicone polymer, dimethyl silicone polymer.
Fatting agent is at least one of lanolin, olive oil, argan oil, vaseline.
Active component is aloe powder, vitamin E, ties up it and orders former B5, Vitwas E, Sodium Hyaluronate, DL- pyrroles
At least one of alkanone carboxylic acid sodium (PCA-Na), passion fruit extract solution, red grape extract.
Chelating agent is at least one of disodium EDTA, tetrasodium salt of EDTA.
Additive is preservative, essence, pigment and pH adjusting agent.
The passion fruit extract that embodiment 1 to embodiment 3 is extracted is added in hair conditioner and studied, is embodied
Scheme as shown in the scheme 1 to scheme 5 in table 1,
Several triers (choosing 10 in the present embodiment) are randomly selected to try out the product of scheme 1 to scheme 5, and
The trial effect of several cases scores to more than, as shown in table 2,
Table 1
Table 2
Scheme 1 | Scheme 2 | Scheme 3 | Scheme 4 | Scheme 5 | |
Trier 1 | 6 | 7 | 9 | 8.5 | 9 |
Trier 2 | 6.5 | 7 | 9.5 | 8 | 7 |
Trier 3 | 7 | 7 | 9.5 | 8.5 | 7 |
Trier 4 | 7 | 7 | 10 | 8.5 | 7.5 |
Trier 5 | 6.5 | 8 | 9 | 8 | 6.5 |
Trier 6 | 7 | 7.5 | 8.5 | 8 | 8 |
Trier 7 | 7.5 | 7 | 9 | 8 | 8 |
Trier 8 | 6 | 7 | 9.5 | 8 | 7.5 |
Trier 9 | 6.5 | 7 | 9.5 | 7.5 | 6 |
Trier 10 | 7 | 7 | 9 | 8 | 6 |
Note:Trier evaluates obtained assessment result, resultant effect:10 points best, and 0 point worst
From the point of view of trial effect scoring by 10 triers, the hair care effect of scheme 3 is ideal, therefore case study on implementation 1
For the preferred scheme of the present invention.
The present invention puies forward the method for selecting the essence using supersonic wave wall breaking technology from fresh passion fruit compared with conventional method.Compared with
It is traditional first fruit thing is dried or air-dried after extract again, nutritional ingredient is more rich, can be promoted by the unique physical characteristic of ultrasonic wave
Make fresh passion fruit cell tissue broken wall or deformation, make that passion fruit extracts active ingredients are more abundant, and recovery rate shows than traditional handicraft
Write and improve up to 50-500%;The extraction of intensified by ultrasonic wave passion fruit can generally obtain optimum extraction rate at 20-40 minutes, extract
Time greatly shortens more than 2/3 compared with conventional method;The temperature of ultrasonic extraction passion fruit elite is at 40-60 DEG C, to having in passion fruit
Effect composition has protective effect, while saves energy consumption;Operation is simple for the method, low for equipment requirements, reduces operating cost,
The passion fruit extract prepared using the present invention is applied in hair nursing, and potent moisturizing, rescue hair core can be provided for hair,
The effect of the hair of fracture is repaired, makes hair become to moisten, rich in gloss and elasticity.
Above-described embodiment is the preferable embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment
Limitation, other any Spirit Essences without departing from the present invention with made under principle change, modification, replacement, combine, simplification,
Equivalent substitute mode is should be, is included within protection scope of the present invention.
Claims (5)
1. a kind of moisturizing and nourishing hair conditioner, include the component of following percentage by weight:
1%~15% surfactant;1%~10% conditioner;1%~10% fatting agent;1%~10%
Active component;0.05%~0.2% chelating agent;1~10% additive;Surplus is water;
Surfactant is at least one of cetostearyl alcohol, cetanol, beeswax;
Conditioner is hydroxyethyl cellulose, hexadecyltrimethylammonium chloride, OTAC, melon glue, had
At least one of machine silicon emulsion, ring five dimethyl silicone polymer, dimethyl silicone polymer;
Fatting agent is at least one of lanolin, olive oil, argan oil, vaseline;
Active component is DL- pyrrolidone sodium carboxylates;
Chelating agent is at least one of disodium EDTA, tetrasodium salt of EDTA;
Additive is preservative, essence, pigment and pH adjusting agent;
Also containing 0.5% passion fruit extract;
Wherein, the extracting method of the passion fruit extract, comprises the following steps:
(1) cleaning treatment is carried out to the passion fruit;
(2) passion fruit cleaned in step (1) is positioned in disintegrating machine and carries out pulverization process;
(3) Extraction solvent is added in the passion fruit crushed, carries out immersion treatment;
(4) immersion treatment is crossed in step (3) passion fruit and solvent are added on ultrasonator and carried out at ultrasonication
Reason;
(5) warm water immersion treatment is carried out to the passion fruit in step (3) by ultrasonication;
(6) passion fruit crossed to warm water immersion treatment is centrifuged, filtration treatment obtains supernatant;
(7) concentration filtrate is carried out to gained supernatant to handle to obtain target product.
2. moisturizing and nourishing hair conditioner according to claim 1, it is characterised in that:Motor of crusher work(in the step (2)
Rate is 800~1800W, and it is 0.2~2min to crush the time.
3. moisturizing and nourishing hair conditioner according to claim 1, it is characterised in that:Extraction solvent described in the step (3)
For 90% ethanol, the weight ratio of the Extraction solvent and the passion fruit is 3:1~20:1.
4. moisturizing and nourishing hair conditioner according to claim 1, it is characterised in that:Warm water temperature described in the step (5)
For 30~50 DEG C, the warm water is 8 with the passion fruit weight ratio:1~10:1.
5. moisturizing and nourishing hair conditioner according to claim 1, it is characterised in that:The concentration filtrate processing is in vacuum
To use Reduced Pressure Concentration Device to carry out flash concentration under the conditions of 0.090~0.095Mpa, adjust solution to be concentrated enters liquid speed
Degree is concentrated into the 1/5~1/6 of original volume with 150~250mL.min flow repeatedly, obtains passion fruit extract.
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CN106562904A (en) * | 2016-09-23 | 2017-04-19 | 广西壮族自治区中国科学院广西植物研究所 | Facial mask containing passion fruit extract and preparation method of facial mask |
CN107384680B (en) * | 2017-07-21 | 2020-10-09 | 广西壮族自治区农业科学院农产品加工研究所 | Passion fruit and longan fruit wine and brewing method thereof |
CN108685793A (en) * | 2018-08-02 | 2018-10-23 | 芜湖扬展新材料科技服务有限公司 | A kind of preparation method of the moisturizing emulsion of the extract containing passion fruit |
CN109125133B (en) * | 2018-10-24 | 2021-04-20 | 西安惟颐生物科技有限公司 | Female breast maintenance compound essential oil |
CN109568214A (en) * | 2019-01-20 | 2019-04-05 | 王忠良 | A kind of passion fruit shell extract preparation method |
CN109938303A (en) * | 2019-04-03 | 2019-06-28 | 中国热带农业科学院农产品加工研究所 | A kind of low-temperature instant passion fruit powder and preparation method thereof |
CN110819458A (en) * | 2019-11-08 | 2020-02-21 | 湖北中烟工业有限责任公司 | Preparation method and application of passion fruit tobacco essence |
CN113575943B (en) * | 2021-06-25 | 2023-12-26 | 广州泽力医药科技有限公司 | Extraction method of lycopene and related active ingredients in passion fruits |
CN113367341A (en) * | 2021-06-29 | 2021-09-10 | 华纳盛世(武汉)生物科技有限公司 | Composition for soothing nerves and improving sleep and preparation method thereof |
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