CN105209513B - 用于粉末涂料组合物的乙烯基官能化聚氨酯树脂 - Google Patents
用于粉末涂料组合物的乙烯基官能化聚氨酯树脂 Download PDFInfo
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Classifications
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- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
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- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
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- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
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- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
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- C08G18/6715—Unsaturated monofunctional alcohols or amines
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
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- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/73—Polyisocyanates or polyisothiocyanates acyclic
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- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D167/00—Coating compositions based on polyesters obtained by reactions forming a carboxylic ester link in the main chain; Coating compositions based on derivatives of such polymers
- C09D167/06—Unsaturated polyesters having carbon-to-carbon unsaturation
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/14—Polyurethanes having carbon-to-carbon unsaturated bonds
- C09D175/16—Polyurethanes having carbon-to-carbon unsaturated bonds having terminal carbon-to-carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/03—Powdery paints
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D2401/00—Form of the coating product, e.g. solution, water dispersion, powders or the like
- B05D2401/30—Form of the coating product, e.g. solution, water dispersion, powders or the like the coating being applied in other forms than involving eliminable solvent, diluent or dispersant
- B05D2401/32—Form of the coating product, e.g. solution, water dispersion, powders or the like the coating being applied in other forms than involving eliminable solvent, diluent or dispersant applied as powders
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D3/00—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials
- B05D3/02—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials by baking
- B05D3/0254—After-treatment
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C35/00—Heating, cooling or curing, e.g. crosslinking or vulcanising; Apparatus therefor
- B29C35/02—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould
- B29C35/08—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould by wave energy or particle radiation
- B29C35/0805—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould by wave energy or particle radiation using electromagnetic radiation
- B29C2035/0827—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould by wave energy or particle radiation using electromagnetic radiation using UV radiation
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- B29C35/00—Heating, cooling or curing, e.g. crosslinking or vulcanising; Apparatus therefor
- B29C35/02—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould
- B29C35/08—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould by wave energy or particle radiation
- B29C35/0866—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould by wave energy or particle radiation using particle radiation
- B29C2035/0877—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould by wave energy or particle radiation using particle radiation using electron radiation, e.g. beta-rays
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B29C37/00—Component parts, details, accessories or auxiliary operations, not covered by group B29C33/00 or B29C35/00
- B29C37/0025—Applying surface layers, e.g. coatings, decorative layers, printed layers, to articles during shaping, e.g. in-mould printing
- B29C37/0028—In-mould coating, e.g. by introducing the coating material into the mould after forming the article
- B29C2037/0039—In-mould coating, e.g. by introducing the coating material into the mould after forming the article the coating being applied in powder or particle form
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2075/00—Use of PU, i.e. polyureas or polyurethanes or derivatives thereof, as moulding material
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- C—CHEMISTRY; METALLURGY
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- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2150/00—Compositions for coatings
- C08G2150/20—Compositions for powder coatings
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
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Abstract
Description
UR | UR1 | UR2 | UR3 | UR4 | UR5 |
用于第一步的单体 | |||||
间苯二甲酸(mol) | 1.70 | ||||
对苯二甲酸(mol) | 2.87 | 2.82 | 1.83 | 3.30 | |
新戊二醇(mol) | 3.68 | 3.79 | 2.66 | ||
三羟甲基丙烷(mol) | 0.29 | 0.29 | 0.29 | ||
1,2-亚丙基二醇(mol) | 4.13 | ||||
氢化双酚A(mol) | 0.99 | ||||
己二醇(mol) | 4.03 | ||||
用于第二步的单体 | |||||
富马酸(mol) | 0.87 | 0.85 | 1.76 | 1.90 | 0.85 |
总量(mol) | 7.71 | 7.74 | 7.10 | 7.75 | 3.57 |
用于第一步的单体 | |||||
间苯二甲酸(g) | 281.7 | ||||
对苯夺甲酸(g) | 477.5 | 468.2 | 303.5 | 547.9 | |
新戊二醇(g) | 383.0 | 394.3 | 276.8 | ||
三羟甲基丙烷(g) | 38.3 | 38.3 | 39.1 | ||
1,2-亚丙基二醇(g) | 314.2 | ||||
氢化双酚A(g) | 237.7 | ||||
己二醇(g) | 475.8 | ||||
用于第二步的单体 | |||||
富马酸(g) | 101.2 | 99.2 | 203.8 | 220.7 | 98.9 |
总重量(g) | 1000.0 | 1000.0 | 1000.0 | 1000.0 | 1000.0 |
合成期间形成的水(g) | 133.6 | 132.2 | 123.4 | 134.1 | 148.2 |
所产生树脂的重量(g) | 866.4 | 867.8 | 876.6 | 865.9 | 851.8 |
UR的特征 | |||||
理论值 | |||||
AV(mg KOH/g UR) | 1 | 0 | 4 | 1 | 1 |
OHV(mg KOH/g UR) | 57 | 70 | 29 | 39 | 60 |
官能度(f) | 2.9 | 2.7 | 2.0 | 2.0 | 2.9 |
Mn(Da) | 2806 | 2164 | 3401 | 2792 | 2668 |
WPU(g/mol) | 993 | 1016 | 499 | 455 | 1000 |
测量值 | |||||
WPU(g/mol) | 1031 | 1053 | 524 | 471 | 1028 |
Tg(℃) | 48 | 48 | 53 | n.a. | 52 |
To(℃) | n.a. | n.a. | n.a. | 45 | n.a. |
ΔHo(J/g) | n.a. | n.a. | n.a. | 55 | n.a. |
Tm(℃) | n.a. | n.a. | n.a. | 67 | n.a. |
ΔHm(J/g) | n.a. | n.a. | n.a. | 39 | n.a. |
在160℃下的粘度(Pa.s) | 20.4 | 9.1 | 41.1 | 2.2 | 27 |
AV(mg KOH/g UR) | 0.7 | 5.3 | 4.7 | 1.7 | 1.5 |
OHV(mg KOH/g UR) | 49.8 | 69.8 | 35.7 | 35.6 | 56.7 |
Claims (56)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP13165556 | 2013-04-26 | ||
EP13165556.5 | 2013-04-26 | ||
PCT/EP2014/058056 WO2014173861A1 (en) | 2013-04-26 | 2014-04-22 | Vinyl functionalized urethane resins for powder coating compositions |
Publications (2)
Publication Number | Publication Date |
---|---|
CN105209513A CN105209513A (zh) | 2015-12-30 |
CN105209513B true CN105209513B (zh) | 2018-11-20 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201480026249.8A Active CN105209513B (zh) | 2013-04-26 | 2014-04-22 | 用于粉末涂料组合物的乙烯基官能化聚氨酯树脂 |
Country Status (14)
Country | Link |
---|---|
US (1) | US10072179B2 (zh) |
EP (1) | EP2989140B1 (zh) |
KR (1) | KR20160003785A (zh) |
CN (1) | CN105209513B (zh) |
AU (1) | AU2014257624B2 (zh) |
BR (1) | BR112015026696A2 (zh) |
CA (1) | CA2909325C (zh) |
DK (1) | DK2989140T3 (zh) |
EA (1) | EA030358B9 (zh) |
ES (1) | ES2634991T3 (zh) |
HK (1) | HK1219286A1 (zh) |
PL (1) | PL2989140T3 (zh) |
SI (1) | SI2989140T1 (zh) |
WO (1) | WO2014173861A1 (zh) |
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Also Published As
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PL2989140T3 (pl) | 2017-10-31 |
ES2634991T3 (es) | 2017-10-02 |
WO2014173861A1 (en) | 2014-10-30 |
KR20160003785A (ko) | 2016-01-11 |
BR112015026696A2 (pt) | 2017-07-25 |
CA2909325C (en) | 2021-01-26 |
EA030358B9 (ru) | 2018-09-28 |
SI2989140T1 (sl) | 2017-10-30 |
EA030358B1 (ru) | 2018-07-31 |
HK1219286A1 (zh) | 2017-03-31 |
EP2989140B1 (en) | 2017-05-24 |
AU2014257624B2 (en) | 2017-03-02 |
US20160068707A1 (en) | 2016-03-10 |
EP2989140A1 (en) | 2016-03-02 |
US10072179B2 (en) | 2018-09-11 |
CN105209513A (zh) | 2015-12-30 |
AU2014257624A1 (en) | 2015-11-05 |
CA2909325A1 (en) | 2014-10-30 |
EA201592059A1 (ru) | 2016-04-29 |
DK2989140T3 (en) | 2017-09-04 |
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