CN105200433A - Stainless steel liquid polishing paste and preparation method thereof - Google Patents
Stainless steel liquid polishing paste and preparation method thereof Download PDFInfo
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- CN105200433A CN105200433A CN201510571598.4A CN201510571598A CN105200433A CN 105200433 A CN105200433 A CN 105200433A CN 201510571598 A CN201510571598 A CN 201510571598A CN 105200433 A CN105200433 A CN 105200433A
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- 229910001220 stainless steel Inorganic materials 0.000 title claims abstract description 61
- 239000010935 stainless steel Substances 0.000 title claims abstract description 61
- 239000007788 liquid Substances 0.000 title claims abstract description 54
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- 238000005498 polishing Methods 0.000 title abstract description 41
- 238000003756 stirring Methods 0.000 claims abstract description 24
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000000654 additive Substances 0.000 claims abstract description 15
- 239000004094 surface-active agent Substances 0.000 claims abstract description 14
- 239000008367 deionised water Substances 0.000 claims abstract description 13
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 13
- 239000000725 suspension Substances 0.000 claims abstract description 13
- 239000011259 mixed solution Substances 0.000 claims abstract description 10
- 239000003921 oil Substances 0.000 claims abstract description 8
- 238000001816 cooling Methods 0.000 claims abstract description 7
- 239000001993 wax Substances 0.000 claims description 96
- 239000002253 acid Substances 0.000 claims description 20
- 150000002632 lipids Chemical class 0.000 claims description 20
- 238000002156 mixing Methods 0.000 claims description 16
- 230000000996 additive effect Effects 0.000 claims description 13
- 239000004519 grease Substances 0.000 claims description 12
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 11
- 239000003082 abrasive agent Substances 0.000 claims description 11
- 239000000203 mixture Substances 0.000 claims description 11
- 239000012188 paraffin wax Substances 0.000 claims description 11
- -1 sorbitol anhydride Chemical class 0.000 claims description 11
- 239000013543 active substance Substances 0.000 claims description 10
- 238000004945 emulsification Methods 0.000 claims description 8
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical group CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 6
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 6
- 238000009775 high-speed stirring Methods 0.000 claims description 6
- WGLPBDUCMAPZCE-UHFFFAOYSA-N Trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 claims description 5
- 238000013019 agitation Methods 0.000 claims description 5
- 239000004203 carnauba wax Substances 0.000 claims description 5
- 235000013869 carnauba wax Nutrition 0.000 claims description 5
- 239000004200 microcrystalline wax Substances 0.000 claims description 5
- 235000019808 microcrystalline wax Nutrition 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- 239000000377 silicon dioxide Substances 0.000 claims description 5
- 235000021355 Stearic acid Nutrition 0.000 claims description 4
- 235000013871 bee wax Nutrition 0.000 claims description 4
- 239000012166 beeswax Substances 0.000 claims description 4
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 4
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims description 4
- 239000008117 stearic acid Substances 0.000 claims description 4
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 claims description 3
- HXKKHQJGJAFBHI-UHFFFAOYSA-N 1-aminopropan-2-ol Chemical group CC(O)CN HXKKHQJGJAFBHI-UHFFFAOYSA-N 0.000 claims description 3
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 claims description 3
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 claims description 3
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 3
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 3
- 239000005642 Oleic acid Substances 0.000 claims description 3
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 claims description 3
- 229930006000 Sucrose Natural products 0.000 claims description 3
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 3
- 150000001412 amines Chemical class 0.000 claims description 3
- 229940075507 glyceryl monostearate Drugs 0.000 claims description 3
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 claims description 3
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 claims description 3
- 239000001788 mono and diglycerides of fatty acids Substances 0.000 claims description 3
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims description 3
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 3
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 3
- 239000000244 polyoxyethylene sorbitan monooleate Substances 0.000 claims description 3
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims description 3
- 229920000053 polysorbate 80 Polymers 0.000 claims description 3
- 239000000600 sorbitol Substances 0.000 claims description 3
- 239000005720 sucrose Substances 0.000 claims description 3
- 150000005846 sugar alcohols Polymers 0.000 claims description 3
- 229960004418 trolamine Drugs 0.000 claims description 3
- 238000000227 grinding Methods 0.000 abstract description 7
- 239000000463 material Substances 0.000 abstract description 6
- 238000000034 method Methods 0.000 abstract description 6
- 239000000243 solution Substances 0.000 abstract description 5
- 230000001804 emulsifying effect Effects 0.000 abstract description 3
- 235000014113 dietary fatty acids Nutrition 0.000 abstract 2
- 229930195729 fatty acid Natural products 0.000 abstract 2
- 239000000194 fatty acid Substances 0.000 abstract 2
- 150000004665 fatty acids Chemical class 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 1
- 235000013336 milk Nutrition 0.000 description 7
- 239000008267 milk Substances 0.000 description 7
- 210000004080 milk Anatomy 0.000 description 7
- 230000000694 effects Effects 0.000 description 6
- 238000004140 cleaning Methods 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 4
- 239000006061 abrasive grain Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 239000012071 phase Substances 0.000 description 3
- RNMDNPCBIKJCQP-UHFFFAOYSA-N 5-nonyl-7-oxabicyclo[4.1.0]hepta-1,3,5-trien-2-ol Chemical compound C(CCCCCCCC)C1=C2C(=C(C=C1)O)O2 RNMDNPCBIKJCQP-UHFFFAOYSA-N 0.000 description 2
- AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 238000007598 dipping method Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- IRHTZOCLLONTOC-UHFFFAOYSA-N hexacosan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCO IRHTZOCLLONTOC-UHFFFAOYSA-N 0.000 description 2
- 238000005461 lubrication Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 238000007517 polishing process Methods 0.000 description 2
- 238000007127 saponification reaction Methods 0.000 description 2
- 238000006748 scratching Methods 0.000 description 2
- 230000002393 scratching effect Effects 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000011149 active material Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 238000005282 brightening Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- ZZVUWRFHKOJYTH-UHFFFAOYSA-N diphenhydramine Chemical compound C=1C=CC=CC=1C(OCCN(C)C)C1=CC=CC=C1 ZZVUWRFHKOJYTH-UHFFFAOYSA-N 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000010685 fatty oil Substances 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- XMHIUKTWLZUKEX-UHFFFAOYSA-N hexacosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCC(O)=O XMHIUKTWLZUKEX-UHFFFAOYSA-N 0.000 description 1
- 239000005556 hormone Substances 0.000 description 1
- 229940088597 hormone Drugs 0.000 description 1
- FRVCGRDGKAINSV-UHFFFAOYSA-L iron(2+);octadecanoate Chemical compound [Fe+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O FRVCGRDGKAINSV-UHFFFAOYSA-L 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000012184 mineral wax Substances 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 238000000643 oven drying Methods 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 229910052814 silicon oxide Inorganic materials 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000008399 tap water Substances 0.000 description 1
- 235000020679 tap water Nutrition 0.000 description 1
- 230000002110 toxicologic effect Effects 0.000 description 1
- 231100000027 toxicology Toxicity 0.000 description 1
- 238000004506 ultrasonic cleaning Methods 0.000 description 1
- 239000012178 vegetable wax Substances 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Landscapes
- Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)
Abstract
The invention discloses stainless steel liquid polishing paste and a preparation method thereof. The polishing paste comprises wax, fatty acid, an emulsifier, a surface active agent, oil, a grinding material, additives and deionized water. The preparation method comprises the following steps: sequentially adding the wax, the fatty acid, the emulsifier, the oil and the additives into a thermostatic container with 80 to 90 DEG C under a stirring condition, stirring, completely dissolving to obtain a mixed solution; adding the surface active agent and the deionized water into another container, heating and stirring, and completely dissolving to obtain a surface active agent solution; slowly adding the surface active agent solution into the mixed solution, continuously stirring for 20 to 40 minutes at the temperature of 80 to 90 DEG C, and emulsifying; adding the deionized water to the grinding material to prepare a grinding material suspension; slowly adding the grinding material suspension, stirring, cooling, and then stirring for 30 to 50 minutes at a high speed to obtain a product. The polishing paste is used for mechanically polishing stainless steel, so that good surface quality and high glossiness can be obtained; moreover, a polished workpiece is simple to wash. The preparation method is simple in process and easy to operate and can produce a high-quality product.
Description
Technical field
The invention belongs to technical field of surface, relate to a kind of for stainless buffing wax and preparation method thereof, particularly relate to a kind of liquor finish wax with and preparation method thereof.
Background technology
In Stainless Steel Products or workpiece manufacturing processed, polishing is absolutely necessary operation, stainless polishing mainly adopts buffing wax to carry out physics polishing, present stage, stainless steel polishing generally adopts solid polishing wax to carry out polishing, but in polishing process, solid polishing wax can be formed residual due to instantaneous high-temperature high pressure at stainless steel surface, namely Wax removal water is used also to be difficult to clean up completely, cause Stainless Steel Products or workpiece surface cannot bright dipping or bright dipping not enough, and formed mottled at Stainless Steel Products or workpiece surface after processing.Moreover solid-state buffing wax easily forms Micro scratching at Stainless Steel Products or workpiece surface.Another kind of polishing mode adopts liquor finish wax, although liquor finish wax starts application in Stainless Steel Watch mirror polish, but containing polyoxyethylene nonylphenol ether in the emulsifying agent that the liquor finish wax found that there is adopts, polyoxyethylene nonylphenol ether is generally acknowledged environmental hormone, for material of embargoing, there is environmental security in this liquor finish wax.
Summary of the invention
The technical problem to be solved in the present invention is, for polishing in prior art easily produce Stainless Steel Products or workpiece surface glossiness after Micro scratching, polishing not, the defect of the technical problem such as cleaning is difficult, after providing a kind of polishing, Stainless Steel Products or workpiece have good surface quality, higher glossiness, and clean simple stainless steel liquid buffing wax after polishing.
The technical problem that the present invention will solve further, is to provide that a kind of technique is simple, easy to operate, the preparation method of production high-quality stainless steel liquid buffing wax.
The technical solution adopted for the present invention to solve the technical problems is:
A kind of stainless steel liquid buffing wax, comprises the feed composition of following mass percent:
In described stainless steel liquid buffing wax, preferred described wax comprises main wax and auxiliary wax, and wherein main wax is whiteruss, and auxiliary wax is beeswax, carnauba wax, Microcrystalline Wax one wherein, and the proportioning of main wax and auxiliary wax is 5 ~ 30:1.
In described stainless steel liquid buffing wax, preferred described lipid acid is at least one in palmitinic acid, oleic acid, stearic acid.
In described stainless steel liquid buffing wax, preferred described emulsifying agent is glyceryl monostearate, sorbitol anhydride monopalmitate, sucrose fatty ester one wherein.
In described stainless steel liquid buffing wax, preferred described tensio-active agent is at least one in polyoxyethylene octylphenol ether, fatty alcohol-polyoxyethylene ether, polyoxyethylene sorbitan monooleate.
In described stainless steel liquid buffing wax, preferred described grease is plam oil.
In described stainless steel liquid buffing wax, preferred described abrasive material is the one in Alpha-alumina, silica powder, chromic oxide.
In described stainless steel liquid buffing wax, preferred described additive is α-amino isopropyl alcohol, trolamine, polyalcohol amine one wherein.
A preparation method for stainless steel liquid buffing wax, comprises the following steps:
A, under agitation, successively paraffin, lipid acid, emulsifying agent, grease, additive to be added in the thermostatic container of 80 ~ 90 DEG C, be stirred to all to dissolve and obtain mixing milk sap;
B, tensio-active agent, deionized water to be added in another one 80 ~ 90 DEG C of thermostatic containers, to be stirred to and to dissolve completely, obtain surfactant soln;
C, abrasive material is added deionized water be mixed with abrasive suspension;
D, surfactant soln to be slowly added in mixing milk sap that steps A obtains, at 80 ~ 90 DEG C, to continue to stir emulsification in 20-40 minute;
E, abrasive suspension slowly added in liquid that step D obtains and stir, after cooling, within high-speed stirring 30-50 minute, namely obtains stainless steel liquid buffing wax.
In the preparation method of stainless steel liquid buffing wax, preferred described steps A is: the thermostatic container first paraffin and lipid acid being added individual 80 ~ 90 DEG C, stirring makes wax mix with lipid acid, then add emulsifying agent and continue heated and stirred to mixing, add the mixing of grease heated and stirred again, finally add additive, heated and stirred mixes, and is stirred to all to dissolve to obtain mixed solution.
Liquor finish wax of the present invention belongs to water prescription, Stainless Steel Products or workpiece can be made to obtain good surface quality, higher glossiness, and after polishing, workpiece cleaning is simple.In addition, polishing wheel surface is had to the effect of cooling, the loss of polishing wheel can be decreased simultaneously.Polishing can be carried out by automatic polishing machine, reduce cost of labor, decrease the uncertainty due to manual operation, improve working (machining) efficiency.
In stainless steel polishing wax, wax comprises main wax and auxiliary wax, and described main wax is the whiteruss of lightweight, and described auxiliary wax is that beeswax, carnauba wax, Microcrystalline Wax are wherein a kind of.Except main wax, then increase auxiliary wax, its objective is and strengthen polishing effect further.Specifically, beeswax has certain ductility and toughness, can dissolve each other, and glossiness is better with various mineral wax, vegetable wax and hot fatty oil.The particle of Microcrystalline Wax is comparatively large, when mix with liquid oils, having and preventing oil content to be separated and the characteristic of precipitation, can prevent being separated of the abrasive segments of buffing wax and lipid acid to a certain extent.Microcrystalline Wax also has good ductility, has refining effect, significantly can strengthen the smooth finish of stainless steel surface to by the lattice throwing surface.Carnauba wax contains cerinic acid, ceryl alcohol and the ester of 80% ~ 85%, is good lubricant, and has good gloss and toughness.Carnauba wax easily melts with other wax phase, and after molten mutually, the toughness of wax improves, and tackiness reduction, plasticity improves.
In stainless steel liquid buffing wax of the present invention, described abrasive material is that Alpha-alumina, silica powder, chromic oxide are wherein a kind of.Abrasive material is the main component of buffing wax, has higher hardness and good physical strength, and its hardness higher than polished workpiece hardness, thus must realize grinding.Stainless steel Mohs' hardness is 5.5, and aluminum oxide Mohs' hardness is 9, and silica powder Mohs' hardness is 7, and chromic oxide Mohs' hardness is 9, and the abrasive hardness of therefore the present invention's selection, much larger than stainless steel, perfection can realize grinding.Abrasive material also should possess good thermostability, prevents from decomposing because of polish temperature too high (can reach 400 DEG C) in polishing process.The fusing point of aluminum oxide, silica powder (silicon oxide), chromic oxide, all more than 1500 DEG C, has good thermostability.
In stainless steel liquid buffing wax of the present invention, described lipid acid is palmitinic acid, oleic acid, stearic acid wherein at least one.Lipid acid is one of organic chief component of liquor finish wax, has good oilness, is also good brightener simultaneously.Stearic acid can produce chemisorption at steel surface and form unimolecular layer iron stearate soap-film, and this film is large at metallic surface sticking power, boundary lubrication ability is improved greatly, thus can reduce or eliminate issuable fine cut in abrasive grinding process.
In stainless steel liquid buffing wax of the present invention, described emulsifying agent is that glyceryl monostearate, sorbitol anhydride monopalmitate, sucrose fatty ester are wherein a kind of.Emulsifying agent is a kind of organic compound that immiscible liquid can be made to form true emulsion, and they have surface-active material, can reduce oil water interfacial tension by a relatively large margin.Emulsifying agent described in the present invention is lipophilic emulsifying agent, is formed composite with tensio-active agent, and the HLB value (hydrophile-lipophile balance value) after composite is 9 ~ 12, and HLB value needed for emulsifying aq paraffin is 11, so can well by whiteruss emulsification.
In stainless steel liquid buffing wax of the present invention, described tensio-active agent is polyoxyethylene octylphenol ether, fatty alcohol-polyoxyethylene ether, polyoxyethylene sorbitan monooleate wherein at least one.Tensio-active agent of the present invention is environment-friendly type, toxicological harmless type, and has higher HLB value, and HLB is higher, and wetting ability is stronger, is conducive to the cleaning of workpiece after polishing.
In stainless steel liquid buffing wax provided by the invention, described additive is that α-amino isopropyl alcohol, trolamine, polyalcohol amine are wherein a kind of.Hydramine can with organic acid generation saponification reaction, the Saponification material of generation has the effect of lubrication and clean stainless steel surface.
In preparation method of the present invention, consider the physics-chem characteristic of various component, the component of steps A adopts the mode added successively, makes the lipophilicity milk sap first obtained have the effect of better mixing or emulsification, in the solution that step B is obtained, join in the mixed solution of steps A, being that aqueous phase is added oil phase, is phase conversion emulsifying, and its particle of milk sap of obtaining of method is little thus, and be uniformly dispersed, good stability.Finally abrasive suspension is joined in the wax after emulsification, high-speed stirring, make abrasive material to be dispersed in wax well.
Accompanying drawing explanation
Below in conjunction with drawings and Examples, the invention will be further described, in accompanying drawing:
Fig. 1 is the preparation technology figure of the embodiment of the present invention.
Embodiment
In order to there be understanding clearly to technical characteristic of the present invention, object and effect, now contrast accompanying drawing and describe the specific embodiment of the present invention in detail.
Embodiment 1, a kind of stainless steel liquid buffing wax, comprise the feed composition of following mass percent:
Preparation method as shown in Figure 1, comprises the following steps:
A, under agitation, successively paraffin, lipid acid, emulsifying agent, grease, additive to be added in the thermostatic container of 80 DEG C.Be specially: first paraffin and lipid acid are added thermostatic container, stir and wax is mixed with lipid acid, then add emulsifying agent and continue heated and stirred to mixing, add the mixing of grease heated and stirred again, finally add additive, heated and stirred mixes, and is stirred to all to dissolve to obtain mixed solution;
B, tensio-active agent, deionized water to be added in another one 80 DEG C of thermostatic containers, to be stirred to and to dissolve completely, obtain surfactant soln;
C, abrasive material is added deionized water, stir and be mixed with abrasive suspension;
D, surfactant soln to be slowly added in mixing milk sap that steps A obtains, at 80 DEG C, to continue stirring emulsification in 20 minutes;
E, slowly to be added by abrasive suspension in liquid that step D obtains and stir, after cooling, namely high-speed stirring obtains stainless steel liquid buffing wax for 30 minutes.
Embodiment 2, a kind of stainless steel liquid buffing wax, comprise the feed composition of following mass percent:
Preparation method as shown in Figure 1, comprises the following steps:
A, under agitation, successively paraffin, lipid acid, emulsifying agent, grease, additive to be added in the thermostatic container of 90 DEG C.Be specially: first paraffin and lipid acid are added thermostatic container, stir and wax is mixed with lipid acid, then add emulsifying agent and continue heated and stirred to mixing, add the mixing of grease heated and stirred again, finally add additive, heated and stirred mixes, and is stirred to all to dissolve to obtain mixed solution;
B, tensio-active agent, deionized water to be added in another one 90 DEG C of thermostatic containers, to be stirred to and to dissolve completely, obtain surfactant soln;
C, abrasive material is added deionized water, stir and be mixed with abrasive suspension;
D, surfactant soln to be slowly added in mixing milk sap that steps A obtains, at 90 DEG C, to continue stirring emulsification in 30 minutes;
E, slowly to be added by abrasive suspension in liquid that step D obtains and stir, after cooling, namely high-speed stirring obtains stainless steel liquid buffing wax for 40 minutes.
Embodiment 3, a kind of stainless steel liquid buffing wax, comprise the feed composition of following mass percent:
Preparation method as shown in Figure 1, comprises the following steps:
A, under agitation, successively paraffin, lipid acid, emulsifying agent, grease, additive to be added in the thermostatic container of 85 DEG C.Be specially: first paraffin and lipid acid are added thermostatic container, stir and wax is mixed with lipid acid, then add emulsifying agent and continue heated and stirred to mixing, add the mixing of grease heated and stirred again, finally add additive, heated and stirred mixes, and is stirred to all to dissolve to obtain mixed solution;
B, tensio-active agent, deionized water to be added in another one 85 DEG C of thermostatic containers, to be stirred to and to dissolve completely, obtain surfactant soln;
C, abrasive material is added deionized water, stir and be mixed with abrasive suspension;
D, surfactant soln to be slowly added in mixing milk sap that steps A obtains, at 85 DEG C, to continue stirring emulsification in 40 minutes;
E, slowly to be added by abrasive suspension in liquid that step D obtains and stir, after cooling, namely high-speed stirring obtains stainless steel liquid buffing wax for 50 minutes.
Embodiment 4, a kind of stainless steel liquid buffing wax, comprise the feed composition of following mass percent:
Preparation method, with embodiment 1-3, does not repeat them here.
Embodiment 5, a kind of stainless steel liquid buffing wax, comprise the feed composition of following mass percent:
Preparation method, with embodiment 1-3, does not repeat them here.
Embodiment 6, a kind of stainless steel liquid buffing wax, comprise the feed composition of following mass percent:
Preparation method, with embodiment 1-3, does not repeat them here.
In above-described embodiment, the selection of abrasive grain is according to procedure calls, and the abrasive grain that wherein essence is thrown is 5000-8000 order, and the abrasive grain of rough polishing is 800-1000 order.
Comparative example 1: commercial liquid buffing wax (containing 5000 order Alpha-aluminas), throws for essence.
Comparative example 2: commercial liquid buffing wax (containing 1000 order Alpha-aluminas), for rough polishing.
Polishing simultaneous test:
Adopt the stainless steel liquid buffing wax of embodiment of the present invention 1-6, the commercial liquid buffing wax of comparative example 1-2, carry out mechanical polishing to stainless steel work-piece, polishing machine is nonstandard customization Full-automatic polishing machine.
Polishing step: first use fiber crops wheel to carry out rough polishing to workpiece, rotating speed 1000 ~ 1200rpm, the amount of feed (amount of feed standard: just to have contacted with workpiece with wheel and be decided to be zero, and then provide the amount of feed forward) 10 ~ 15mm, re-use cloth wheel and essence throwing is carried out to workpiece, rotating speed 2000 ~ 2500rpm, the amount of feed 20 ~ 25mm.
Polishing judgement criteria:
(1) surfaceness:
According to GB1031-2009 standard described in testing method can record the workpiece after the stainless steel liquid buffing wax polishing of embodiment 1-6 and adopt the surfaceness of the workpiece after comparative example 1-2 liquor finish wax polishing.
(2) surface of polished glossiness:
Adopt appearance method, the luminance brightness of workpiece surface after polishing is divided into 5 grades;
1 grade: surperficial adularescent oxide film, without luminance brightness;
2 grades: slightly light, does not see profile;
3 grades: luminance brightness is better, can find out profile;
4 grades: surface-brightening, more clearly find out profile (being equivalent to the surface quality of electrochemical etching)
5 grades: light as minute surface.
(3) workpiece cleaning complexity after polishing:
To clean and moisture eliminator put into by workpiece at 80 DEG C after dry 2h, and after being cooled to room temperature, adopting Shanghai to help section's ten thousand/analytical balance and weigh, be designated as M
0; At workpiece surface uniform application buffing wax, take out after putting into 150 DEG C of aging 45min of baking oven, put into moisture eliminator and be cooled to room temperature, weigh and be designated as M
1; Workpiece is placed in 5% Wax removal water (the commercial metals surface finish wax clean-out system) solution of 70 DEG C, takes out after ultrasonic cleaning 10min, and use tap water 30s, then after putting into 80 DEG C of oven drying 2h, put into moisture eliminator, be cooled to room temperature and weigh, be designated as M
2.Dewax efficiency eta=[(M
2-M
0)/M
1-M
0)] × 100%.
η=95 ~ 100%, without dirt, surperficial moisture film is continuous, is decided to be outstanding;
η=90 ~ 95%, without obvious dirt, surperficial moisture film is discontinuous, is decided to be good;
η=80 ~ 90%, a small amount of dirt, is decided to be medium;
Below η=80%, obvious dirt, is decided to be poor;
Test-results is as shown in table 2:
Table 2
As can be seen from above table: be no matter that essence is thrown or rough polishing, stainless steel liquid buffing wax of the present invention is to after workpiece polishing, and liquor finish wax commercially available compared to existing technology, the workpiece surface of polishing is more smooth, more easy cleaning and glossiness is also higher.
Claims (10)
1. a stainless steel liquid buffing wax, is characterized in that, comprises the feed composition of following mass percent:
。
2. stainless steel liquid buffing wax according to claim 1, is characterized in that, described wax comprises main wax and auxiliary wax, and wherein main wax is whiteruss, and auxiliary wax is beeswax, carnauba wax, Microcrystalline Wax one wherein, and the proportioning of main wax and auxiliary wax is 5 ~ 30:1.
3. stainless steel liquid buffing wax according to claim 1, is characterized in that, described lipid acid is at least one in palmitinic acid, oleic acid, stearic acid.
4. stainless steel liquid buffing wax according to claim 1, is characterized in that, described emulsifying agent is glyceryl monostearate, sorbitol anhydride monopalmitate, sucrose fatty ester one wherein.
5. stainless steel liquid buffing wax according to claim 1, is characterized in that, described tensio-active agent is at least one in polyoxyethylene octylphenol ether, fatty alcohol-polyoxyethylene ether, polyoxyethylene sorbitan monooleate.
6. stainless steel liquid buffing wax according to claim 1, is characterized in that, described grease is plam oil.
7. stainless steel liquid buffing wax according to claim 1, is characterized in that, described abrasive material is the one in Alpha-alumina, silica powder, chromic oxide.
8. stainless steel liquid buffing wax according to claim 1, is characterized in that, described additive is α-amino isopropyl alcohol, trolamine, polyalcohol amine one wherein.
9. a preparation method for stainless steel liquid buffing wax, is characterized in that: comprise the following steps:
A, under agitation, successively paraffin, lipid acid, emulsifying agent, grease, additive to be added in the thermostatic container of 80 ~ 90 DEG C, be stirred to all to dissolve and obtain mixed solution;
B, tensio-active agent, deionized water to be added in another one 80 ~ 90 DEG C of thermostatic containers, to be stirred to and to dissolve completely, obtain surfactant soln;
C, abrasive material is added deionized water be mixed with abrasive suspension;
D, surfactant soln to be slowly added in mixed solution that steps A obtains, at 80 ~ 90 DEG C, to continue to stir emulsification in 20-40 minute;
E, abrasive suspension slowly added in liquid that step D obtains and stir, after cooling, within high-speed stirring 30-50 minute, namely obtains stainless steel liquid buffing wax.
10. the preparation method of stainless steel liquid buffing wax according to claim 9, it is characterized in that, described steps A is: the thermostatic container first paraffin and lipid acid being added individual 80 ~ 90 DEG C, stirring makes wax mix with lipid acid, then add emulsifying agent and continue heated and stirred to mixing, then add the mixing of grease heated and stirred, finally add additive, heated and stirred mixes, and is stirred to all to dissolve to obtain mixed solution.
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