CN105778862A - Diamond grinding paste easy to clean and preparation method thereof - Google Patents
Diamond grinding paste easy to clean and preparation method thereof Download PDFInfo
- Publication number
- CN105778862A CN105778862A CN201610214158.8A CN201610214158A CN105778862A CN 105778862 A CN105778862 A CN 105778862A CN 201610214158 A CN201610214158 A CN 201610214158A CN 105778862 A CN105778862 A CN 105778862A
- Authority
- CN
- China
- Prior art keywords
- weight portion
- diamond
- diamond paste
- weight portions
- consumption
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
- C09K3/14—Anti-slip materials; Abrasives
- C09K3/1454—Abrasive powders, suspensions and pastes for polishing
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/02—Polishing compositions containing abrasives or grinding agents
Abstract
The invention relates to a diamond grinding paste easy to clean and a preparation method thereof. The diamond grinding paste is prepared from synthetic diamond micro-powder, glycerin, glycerol monostearate and a detergent. The diamond grinding paste has good cleaning performance, is exquisite and can facilitate cleaning of grinder walls while achieving a good grinding effect.
Description
[technical field]
The invention belongs to materials processing technology field.More particularly it relates to an the diamond paste of easy cleaning, the preparation method further relating to described easy cleaning diamond paste.
[background technology]
The feature ground is that abrasive material constantly rolls in process of lapping, produces extruding and two kinds of effects of cutting, makes convex-concave surface gradually flat smooth.A kind of buffing cream that diamond abrasive pastes are made with selected gem grade diamond micron power and paste bonding agent, coloring agent, preservative, essence etc., it is adaptable to the measurer of high hardness material goods, cutlery optical instrument and the grinding of other best bright finish workpiece, the polishings such as glass, pottery, gem, hard alloy.Diamond grinds mastic and divides water-soluble and oil soluble two kinds, has well lubrication and cooling performance.Diadust intensity is high, and epigranular ground effect is good.Such as CN104017499 discloses a kind of diamond paste, aviation diesel oil or machine oil are mixed to get a kind of oil medium by this invention, polishing effect is good, this oil medium diamond paste can be adsorbed on the surface of wall when grinding and polishing, not easy cleaning, can have undesirable effect follow-up grinding and polishing.
In order to better solve the defect of prior art, the present invention is summing up in existing technical foundation, and by substantial amounts of experiment and analysis, the present inventor develops the diamond paste of a kind of easy cleaning, solves the neat and tidy of dismembyator wall surface, improves grinding efficiency.
[summary of the invention]
[solving the technical problem that]
It is an object of the invention to provide a kind of easy cleaning diamond paste.
The preparation method that it is a further object to provide described easy cleaning diamond paste.
[technical scheme]
The present invention is achieved through the following technical solutions.
The present invention relates to the diamond paste of a kind of easy cleaning.
Described diamond paste is made up of 5～15 weight portion synthetic diamond micropowders, 100～200 weight portion glycerol, 200～400 weight portion glyceryl monostearates and 115～170 weight portion liquid detergents.
A preferred embodiment of the invention, described diamond paste is made up of 7～12 weight portion synthetic diamond micropowders, 125～170 weight portion glycerol, 250～350 weight portion glyceryl monostearates and 125～160 weight portion liquid detergents.
Another kind of preferred implementation according to the present invention, described diamond paste is made up of 8～10 weight portion synthetic diamond micropowders, 140～154 weight portion glycerol, 290～320 weight portion glyceryl monostearates and 138～148 weight portion liquid detergents.
Another kind of preferred implementation according to the present invention, the particle diameter of described synthetic diamond micropowder is 1.0～0.5 microns.
The preparation method that the present invention relates to a kind of easy cleaning diamond paste.
The step of this preparation method is as follows:
A, dissolving
200～400 weight portion glyceryl monostearates are added in 100～200 weight portion glycerol, make glyceryl monostearate dissolve and obtain a kind of solution；
B, dispersion
5～15 weight portion synthetic diamond micropowders and 115～170 weight portion liquid detergents are added in the step A solution obtained, mix homogeneously, then it is placed in ultrasonoscope and carries out ultrasonic disperse 10～20min when power 120～180W and frequency 20～30KHz, obtain a kind of milky mixt；
C, cooling
The milky mixt obtained by step B is cooled to room temperature, obtains described easy cleaning diamond paste.
A preferred embodiment of the invention, in step, dissolves glyceryl monostearate when water bath heating temperature 70～80 DEG C.
Another kind of preferred implementation according to the present invention, in step, consumption 250～350 weight portion of glyceryl monostearate；The consumption of glycerol is 125～170 weight portions.
Another kind of preferred implementation according to the present invention, in step, the consumption of glyceryl monostearate is 290～320 weight portions；The consumption of glycerol is 140～154 weight portions.
Another kind of preferred implementation according to the present invention, in stepb, the consumption of synthetic diamond micropowder is 7～12 weight portions；The consumption of liquid detergent is 125～160 weight portions.
Another kind of preferred implementation according to the present invention, in stepb, the consumption of synthetic diamond micropowder is 8～10 weight portions；The consumption of liquid detergent is 138～148 weight portions.
The present invention is described in more detail below.
The present invention relates to the diamond paste of a kind of easy cleaning.
Described diamond paste is made up of 5～15 weight portion synthetic diamond micropowders, 100～200 weight portion glycerol, 200～400 weight portion glyceryl monostearates and 115～170 weight portion liquid detergents.
The synthetic diamond micropowder that the present invention uses refers to the diamond particles that particle diameter is 1.0～0.5 microns, and diadust hardness is high, wearability is good, is widely used in the technical fields such as cutting, grinding, probing.Diadust is the desirable feedstock of the high hardness materials such as grinding and polishing hard alloy, pottery, gem, optical glass.The synthetic diamond micropowder that the present invention uses is with trade name bortz powder product sold by Ya Long hard material company limited of Henan Province.
The glycerol that the present invention uses acts primarily as the effect of a kind of lubricant in the compositions of the present invention, namely plays the effect of lubrication mastic.The glycerol that the present invention uses is to be researched and developed company limited with trade name glycerol product sold by the auspicious auspiciousization glass religion instrument in Yunnan.In the compositions of the present invention, glycerol is required component, without glycerol, then mastic can be made can not to rub up together, lack certain toughness, and mastic can not play the effect of lubrication.
Glyceryl monostearate is C16-C18 long-chain fatty acid and glycerol esterification reaction product.It is a kind of non-ionic surfactant, not only contains hydrophilic group but also contain lipophilic group, and it has the several functions such as moistening, emulsifying, foaming.In the compositions of the present invention, glyceryl monostearate makes diamond lap mastic fine and smooth, mainly acts as the effect of lubricant and dispersant.The glyceryl monostearate that the present invention uses is to be researched and developed company limited with trade name glyceryl monostearate product sold by the auspicious auspiciousization glass religion instrument in Yunnan.In the compositions of the present invention, glyceryl monostearate is required component, without glyceryl monostearate, then can not form body of paste.It is of course also possible to use and glyceryl monostearate character and act on close, diamond paste performance of the present invention do not had other ester compounds dysgenic, for instance ethylene glycol stearate, pentaerythritol monostearate simultaneously；These other ester compounds are also all within scope.
Liquid detergent is a kind of daily cleaning articles for use, and it contains various active composition, and main component is surfactant, and these compositions can make various greasy spot, harmful substance dissolve, emulsifying, and dispersion suspends, thus reaching the effect of cleaning.In the compositions of the present invention, liquid detergent mainly acts as the effect of blender and lubricant, reaches the purpose of easy cleaning.The liquid detergent that the present invention uses is to be taught instrument to research and develop company limited by Yunnan auspicious auspiciousization glass to found white liquid detergent product sold with trade name.In the compositions of the present invention, liquid detergent is required component, without liquid detergent, then can not reach the purpose of easy cleaning.It is of course also possible to use close with liquid detergent character and effect, diamond paste performance of the present invention do not had other abluent dysgenic, for instance vertical white liquid detergent, blue moon handwashing liquid simultaneously；These other abluents are also all within scope.
In the compositions of the present invention, when the content of other component is in described scope, if the amount of synthetic diamond micropowder is less than 5 weight portions, then can reach the effect ground not；If the amount of synthetic diamond micropowder is more than 15 weight portions, the too high meeting of diamond content makes diadust be collected as graininess, reduces the effect of grinding and polishing；Therefore, the amount of synthetic diamond micropowder is 5～15 weight portions is rational, it is preferred that 7～12 weight portions, it is more preferred to be 8～10 weight portions.
Similarly, when the content of other component is in described scope, if the amount of glycerol is less than 100 weight portions, then diamond paste can be made not have the effect of lubrication；If the amount of glycerol is more than 200 weight portions, the then body of paste that the diamond paste of gained can be made not formed, there is certain mobility；Therefore, the amount of glycerol is 100～200 weight portions is appropriate, it is preferred that 125～170 weight portions, it is more preferred to be 140～154 weight portions.
When the content of other component is in described scope, if the amount of glyceryl monostearate less than 200 weight portions, then can make what diamond paste solidified to be not as abundant；If the amount of glyceryl monostearate is more than 400 weight portions, then diamond paste can be made well not disperse；Therefore, the amount of glyceryl monostearate is 200～400 weight portions is feasible, it is preferred that 250～350 weight portions, it is more preferred to be 290～320 weight portions.
When the content of other component is in described scope, if the amount of liquid detergent is less than 115 weight portions, the then DeGrain that can clean；If the amount of liquid detergent is more than 170 weight portions, then can on grinding and polishing time cutting effect produce impact, do not reach expected effect；Therefore, the amount of liquid detergent is 115～170 weight portions is rational, it is preferred that 125～160 weight portions, it is more preferred to be 138～148 weight portions.
According to the present invention, described diamond paste is preferably by 7～12 weight portion synthetic diamond micropowders, 125～170 weight portion glycerol, 250～350 weight portion glyceryl monostearates and what 125～160 weight portion liquid detergents formed.
It is highly preferred that described diamond paste is made up of 8～10 weight portion synthetic diamond micropowders, 140～154 weight portion glycerol, 290～320 weight portion glyceryl monostearates and 138～148 weight portion liquid detergents.
According to the present invention, the particle diameter of described diadust is 1.0～0.5 microns.
In the present invention, if the particle diameter of diadust exceedes described scope, then can jitter time long, reduce experiment efficiency.
The preparation method that the present invention relates to a kind of easy cleaning diamond paste.
The step of this preparation method is as follows:
A, dissolving
200～400 weight portion glyceryl monostearates are added in 100～200 weight portion glycerol, make glyceryl monostearate dissolve and obtain a kind of solution.
Glyceryl monostearate is preferably dissolved in glycerol by this dissolving step when water bath heating temperature 70～80 DEG C.
As described in the previous with the situation of glycerol about glyceryl monostearate, therefore do not repeat them here.
Preferably, the consumption of glyceryl monostearate is 250～350 weight portions；The consumption of glycerol is 125～170 weight portions.
It is highly preferred that consumption 290～320 weight portion of glyceryl monostearate；The consumption of glycerol is 140～154 weight portions.
B, dispersion
5～15 weight portion synthetic diamond micropowders and 115～170 parts of liquid detergents are added in the step A solution obtained, mix homogeneously, then it is placed in ultrasonoscope and carries out ultrasonic disperse 10～20min when power 120～180W and frequency 20～30KHz, obtain a kind of milky mixt.
The present invention uses the purpose of ultrasonoscope to be in that the diadust of particle diameter 1.0～0.5 microns uniformly, be quickly dispersed in liquid detergent such that it is able to obtain a kind of stable milky mixt.
Synthetic diamond micropowder dispersion is all had a huge impact by ultrasonoscope power and frequency.If its ultrasonic power is less than 120W, then can not reach scattered effect；If its ultrasonic power is more than 180W, then disperseing acutely, each component warm-up movement is violent, affects the uniformity of diadust.Therefore, its ultrasonic power is 120～180W is desirable.
Similarly, if its supersonic frequency is less than 20KHz, then can not reach scattered purpose；If its supersonic frequency is higher than 30KHz, then can disperse acutely, the impurity of air can be absorbed.Therefore, its supersonic frequency is 20～30KHz is feasible.
If its ultrasonic disperse time is shorter than 10min, then mastic dispersion can be made uneven；If its ultrasonic disperse time is more than 20min, then can be collected as the phenomenon of granule by mastic.Therefore, its ultrasonic disperse time is 10～20min is desirable.
The ultrasonoscope that the present invention uses is product sold in the market, for instance formed an alliance board ultrasonic washing unit product sold with trade name by the cleaning equipment company limited that forms an alliance of Shenzhen.
As described in the previous with the situation of liquid detergent about synthetic diamond micropowder, therefore do not repeat them here.
Preferably, the consumption of synthetic diamond micropowder is 7～12 weight portions；The consumption of liquid detergent is 125～160 weight portions.
It is highly preferred that the consumption of synthetic diamond micropowder is 8～10 weight portions；The consumption of liquid detergent is 138～148 weight portions.
C, cooling
The milky mixt obtained by step B is cooled to room temperature, obtains described easy cleaning diamond paste.
In the present invention, allowing the milky mixt type of cooling can be widely known various modes, for instance by psychrolusia or the refrigerator type of cooling, simply needs the milky mixt obtained by step B to be cooled to room temperature, just obtains described easy cleaning diamond paste.
Employing standard ZYP300 grinder, use easy cleaning diamond paste of the present invention that carborundum, corundum and carbon steel material have been carried out grinding and polishing, its grinding and polishing result is that the surface roughness of three kinds of materials all significantly reduces and material surface scratch is few, use liquid detergent abluent cleaning performance obvious, can clean at normal temperatures.
Meanwhile, use the diamond paste prepared by the same collocation method being added without liquid detergent. at identical conditions carborundum, corundum and carbon steel material having been carried out grinding and polishing, its grinding and polishing result is for using liquid detergent abluent cleaning performance and polishing effect better, more rapid.
It is clear that the addition of liquid detergent improves polishing and the efficiency cleaned by the above results.
The easy cleaning diamond paste of the present invention has following feature:
A, the present invention easy cleaning diamond paste be readily cleaned.
B, the present invention easy cleaning diamond paste in synthetic diamond micropowder be uniformly dispersed, mastic is fine and smooth.
C, the present invention the grinding effect of easy cleaning diamond paste excellent, stable performance.
[beneficial effect]
The invention has the beneficial effects as follows: it is strong that existing abrasive pastes have adsorptivity, it is easy to be adsorbed on grinding wall.Under identical grinding condition in contrast, the present invention using liquid detergent as blender and lubricant, thus having good cleaning.Glycerol as lubricant, is added glyceryl monostearate and makes mastic fine and smooth by the present invention, and ultrasound wave is more conducive to synthetic diamond micropowder to be disperseed uniformly, improves the dispersibility of diamond, is also convenient for grinding the cleaning of wall while the grinding effect reached.
[detailed description of the invention]
The present invention will be better understood when by following embodiment.
Embodiment 1: preparation easy cleaning diamond paste
The enforcement step of this embodiment is as follows:
A, dissolving
When water bath heating temperature 70 DEG C, by the auspicious auspiciousization glass religion instrument in Yunnan, 250 weight portions are researched and developed company limited be added in 100 weight portion glycerol with the glyceryl monostearate that trade name glyceryl monostearate is sold, make glyceryl monostearate dissolve and obtain a kind of solution；
B, dispersion
In the step A solution obtained, add 7 weight portions taught the synthetic diamond micropowder that instrument research and development company limited sells with trade name bortz powder to be taught instrument to research and develop company limited with 138 weight portions by Yunnan auspicious auspiciousization glass by Yunnan auspicious auspiciousization glass to found the liquid detergent of white liquid detergent sale with trade name, mix homogeneously, then be placed in by Shenzhen form an alliance cleaning equipment company limited with trade name form an alliance board ultrasonic washing unit sell ultrasonoscope in, carry out ultrasonic disperse 18min when power 140W and frequency 20KHz, obtain a kind of milky mixt；
C, cooling
Adopting the psychrolusia type of cooling, the milky mixt obtained by step B is cooled to room temperature, obtains described easy cleaning diamond paste.
Employing standard ZYP300 grinder, use easy cleaning diamond paste of the present invention that carbofrax material has been carried out grinding and polishing, its grinding and polishing, it is shown that the surface roughness Ra of carbofrax material is 0.270 μm, is 0.521 μm of obvious reduction compared to the surface roughness Ra before polishing；Using liquid detergent abluent cleaning performance to improve, material surface is clean, and almost without residue, scavenging period shortens 3 times, improves the efficiency of cleaning, easy to clean.
Meanwhile, use the diamond paste prepared by the same compound method being added without liquid detergent. at identical conditions carbofrax material is carried out grinding and polishing, its grinding and polishing result is that after polishing, the surface roughness Ra of carborundum is 0.293 μm, uses liquid detergent abluent cleaning performance and polishing effect better, more rapid.
It is clear that the addition of liquid detergent improves polishing and the efficiency cleaned by the above results.
Embodiment 2: preparation easy cleaning diamond paste
The enforcement step of this embodiment is as follows:
A, dissolving
When water bath heating temperature 75 DEG C, by the auspicious auspiciousization glass religion instrument in Yunnan, 350 weight portions are researched and developed company limited be added in 200 weight portion glycerol with the glyceryl monostearate that trade name glyceryl monostearate is sold, make glyceryl monostearate dissolve and obtain a kind of solution；
B, dispersion
The liquid detergent that synthetic diamond micropowder that 12 weight portions are sold with trade name bortz powder and 148 weight portions are sold with trade name liquid detergent by Yunnan auspicious auspiciousization glass religion instrument research and development company limited is added by Ya Long hard material company limited of Henan Province in the step A solution obtained, mix homogeneously, then be placed in by Shenzhen form an alliance cleaning equipment company limited with trade name form an alliance board ultrasonic washing unit sell ultrasonoscope in, carry out ultrasonic disperse 10min when power 120W and frequency 30KHz, obtain a kind of milky mixt；
C, cooling
Adopting the refrigerator type of cooling, the milky mixt obtained by step B is cooled to room temperature, obtains described easy cleaning diamond paste.
Employing standard ZYP300 grinder, use easy cleaning diamond paste of the present invention that corundum material has been carried out grinding and polishing, its grinding and polishing, it is shown that the surface roughness Ra of corundum material is 0.281 μm, is 0.437 μm of obvious reduction compared to the surface roughness Ra before polishing；Using liquid detergent abluent cleaning performance to improve, material surface is clean, and almost without residue, scavenging period shortens 3 times, improves the efficiency of cleaning, easy to clean.
Meanwhile, use the diamond paste prepared by the same collocation method being added without liquid detergent. at identical conditions to corundum grinding and polishing, its grinding and polishing result is that after polishing, the surface roughness Ra of corundum is 0.296 μm, uses liquid detergent abluent cleaning performance and polishing effect better, more rapid.
It is clear that the addition of liquid detergent improves polishing and the efficiency cleaned by the above results.
Embodiment 3: preparation easy cleaning diamond paste
The enforcement step of this embodiment is as follows:
A, dissolving
When water bath heating temperature 80 DEG C, by the auspicious auspiciousization glass religion instrument in Yunnan, 200 weight portions are researched and developed company limited be added in 125 weight portion glycerol with the glyceryl monostearate that trade name glyceryl monostearate is sold, make glyceryl monostearate dissolve and obtain a kind of solution；
B, dispersion
The liquid detergent that synthetic diamond micropowder that 5 weight portions are sold with trade name bortz powder and 115 weight portions are sold with trade name liquid detergent by Yunnan auspicious auspiciousization glass religion instrument research and development company limited is added by Ya Long hard material company limited of Henan Province in the step A solution obtained, mix homogeneously, then be placed in by Shenzhen form an alliance cleaning equipment company limited with trade name form an alliance board ultrasonic washing unit sell ultrasonoscope in, carry out ultrasonic disperse 12min when power 180W and frequency 25KHz, obtain a kind of milky mixt；
C, cooling
Adopting the psychrolusia type of cooling, the milky mixt obtained by step B is cooled to room temperature, obtains described easy cleaning diamond paste.
Employing standard ZYP300 grinder., use easy cleaning diamond paste of the present invention that carbon steel material has been carried out grinding and polishing, its grinding and polishing, it is shown that the surface roughness Ra of carbon steel material is 0.228 μm, is 0.346 μm of obvious reduction compared to the surface roughness Ra before polishing；Using liquid detergent abluent cleaning performance to improve, material surface is clean, and almost without residue, scavenging period shortens 3 times, improves the efficiency of cleaning, easy to clean.
Meanwhile, use the diamond paste prepared by the same collocation method being added without liquid detergent at identical conditions to carbon steel grinding and polishing, its grinding and polishing result is that after polishing, the surface roughness Ra of carbon steel is 0.236 μm, uses liquid detergent abluent cleaning performance and polishing effect better, more rapid.
It is clear that the addition of liquid detergent improves polishing and the efficiency cleaned by the above results.
Embodiment 4: preparation easy cleaning diamond paste
The enforcement step of this embodiment is as follows:
A, dissolving
When water bath heating temperature 75 DEG C, by the auspicious auspiciousization glass religion instrument in Yunnan, 400 weight portions are researched and developed company limited be added in 170 weight portion glycerol with the glyceryl monostearate that trade name glyceryl monostearate is sold, make glyceryl monostearate dissolve and obtain a kind of solution；
B, dispersion
In the step A solution obtained, add synthetic diamond micropowder that 15 weight portions are sold with trade name bortz powder by Ya Long hard material company limited of Henan Province and 170 weight portions are found, with trade name, the liquid detergent that white liquid detergent is sold by Yunnan auspicious Xiang Hua Bo Jiaoyiyan company, mix homogeneously, then be placed in by Shenzhen form an alliance cleaning equipment company limited with trade name form an alliance board ultrasonic washing unit sell ultrasonoscope in, carry out ultrasonic disperse 20min when power 160W and frequency 28KHz, obtain a kind of milky mixt；
C, cooling
Adopting the refrigerator type of cooling, the milky mixt obtained by step B is cooled to room temperature, obtains described easy cleaning diamond paste.
Employing standard ZYP300 grinder, use easy cleaning diamond paste of the present invention that carbofrax material has been carried out grinding and polishing, the surface roughness Ra of its grinding and polishing result carbofrax material is 0.273 μm, is 0.521 μm of obvious reduction compared to the surface roughness Ra before polishing；Material surface is clean, and almost without residue, scavenging period shortens 3 times, improves the efficiency of cleaning, easy to clean.
Meanwhile, the diamond paste prepared by the same collocation method being added without liquid detergent is used at identical conditions carbofrax material to be carried out grinding and polishing, its grinding and polishing result is that after polishing, the surface roughness Ra of carborundum is 0.286 μm, use liquid detergent abluent cleaning performance better, product easy cleaning, material surface cut is few.
It is clear that the addition of liquid detergent improves polishing and the efficiency cleaned by the above results.
Embodiment 5: preparation easy cleaning diamond paste
The enforcement step of this embodiment is as follows:
A, dissolving
When water bath heating temperature 72 DEG C, by the auspicious auspiciousization glass religion instrument in Yunnan, 290 weight portions are researched and developed company limited be added in 140 weight portion glycerol with the glyceryl monostearate that trade name glyceryl monostearate is sold, make glyceryl monostearate dissolve and obtain a kind of solution；
B, dispersion
Adding synthetic diamond micropowder that 8 weight portions are sold with trade name bortz powder by company of Ya Long hard material company limited of Henan Province and 125 weight portions in the step A solution obtained is taught instrument research and development company limited to found, with trade name, the liquid detergent that white liquid detergent is sold by Yunnan auspicious auspiciousization glass, mix homogeneously, then be placed in by Shenzhen form an alliance cleaning equipment company limited with trade name form an alliance board ultrasonic washing unit sell ultrasonoscope in, carry out ultrasonic disperse 16min when power 170W and frequency 22KHz, obtain a kind of milky mixt；
C, cooling
Adopting the psychrolusia type of cooling, the milky mixt obtained by step B is cooled to room temperature, obtains described easy cleaning diamond paste.
Employing standard ZYP300 grinder, use easy cleaning diamond paste of the present invention that corundum material has been carried out grinding and polishing, the surface roughness Ra of its grinding and polishing result corundum material is 0.279 μm, is 0.442 μm of obvious reduction compared to the surface roughness Ra before polishing；Using liquid detergent abluent cleaning performance to improve, material surface is clean, and almost without residue, scavenging period shortens 3 times, improves the efficiency of cleaning, easy to clean.
Meanwhile, the diamond paste prepared by the same compound method being added without liquid detergent is used at identical conditions corundum material to be carried out grinding and polishing, its grinding and polishing result is that after polishing, the surface roughness Ra of corundum is 0.283 μm, use liquid detergent abluent cleaning performance better, product easy cleaning, material surface cut is few.
It is clear that the addition of liquid detergent improves polishing and the cleaning performance of the efficiency cleaned and material surface by the above results.
Embodiment 6: preparation easy cleaning diamond paste
The enforcement step of this embodiment is as follows:
A, dissolving
When water bath heating temperature 78 DEG C, by the auspicious auspiciousization glass religion instrument in Yunnan, 320 weight portions are researched and developed company limited be added in 154 weight portion glycerol with the glyceryl monostearate that trade name glyceryl monostearate is sold, make glyceryl monostearate dissolve and obtain a kind of solution；
B, dispersion
In the step A solution obtained, add synthetic diamond micropowder that 10 weight portions are sold with trade name bortz powder by Ya Long hard material company limited of Henan Province and 160 weight portions are sent out limited and ground, by the auspicious auspiciousization glass religion instrument in Yunnan, the liquid detergent that company sells with trade name liquid detergent, mix homogeneously, then it is placed in and is formed an alliance with trade name by the cleaning equipment company limited that forms an alliance of Shenzhen the ultrasonoscope that board ultrasonoscope cleaning machine mark sells is carried out ultrasonic disperse 14min when power 150W and frequency 25KHz, obtain a kind of milky mixt；
C, cooling
Adopting the psychrolusia type of cooling, the milky mixt obtained by step B is cooled to room temperature, obtains described easy cleaning diamond paste.
Employing standard ZYP300 grinder, use easy cleaning diamond paste of the present invention that carbon steel material has been carried out grinding and polishing, the surface roughness Ra of its grinding and polishing result carbon steel material is 0.219 μm, is 0.351 μm of obvious reduction compared to the surface roughness Ra before polishing；Using liquid detergent abluent cleaning performance to improve, material surface is clean, and almost without residue, scavenging period shortens 3 times, improves the efficiency of cleaning, easy to clean.
Meanwhile, the diamond paste prepared by the same collocation method being added without liquid detergent is used at identical conditions carbon steel material to be carried out grinding and polishing, its grinding and polishing result is that after polishing, the surface roughness Ra of carbon steel is 0.232 μm, use liquid detergent abluent cleaning performance better, product easy cleaning, material surface cut is few.
It is clear that the addition of liquid detergent improves polishing and the efficiency cleaned by the above results.
Claims (10)
1. the diamond paste of an easy cleaning, it is characterised in that described diamond paste is made up of 5～15 weight portion synthetic diamond micropowders, 100～200 weight portion glycerol, 200～400 weight portion glyceryl monostearates and 115～170 weight portion liquid detergents.
2. diamond paste according to claim 1, it is characterised in that described diamond paste is made up of 7～12 weight portion synthetic diamond micropowders, 125～170 weight portion glycerol, 250～350 weight portion glyceryl monostearates and 125～160 weight portion liquid detergents.
3. diamond paste according to claim 1, it is characterised in that described diamond paste is made up of 8～10 weight portion synthetic diamond micropowders, 140～154 weight portion glycerol, 290～320 weight portion glyceryl monostearates and 138～148 weight portion liquid detergents.
4. the diamond paste described in claim any one of claim 1-3, it is characterised in that the particle diameter of described synthetic diamond micropowder is 1.0～0.5 microns.
5. the preparation method of an easy cleaning diamond paste, it is characterised in that the step of this preparation method is as follows:
A, dissolving
200～400 weight portion glyceryl monostearates are added in 100～200 weight portion glycerol, make glyceryl monostearate dissolve and obtain a kind of solution；
B, dispersion
5～15 weight portion synthetic diamond micropowders and 115～170 weight portion liquid detergents are added in the step A solution obtained, mix homogeneously, then it is placed in ultrasonoscope and carries out ultrasonic disperse 10～20min when power 120～180W and frequency 20～30KHz, obtain a kind of milky mixt；
C, cooling
The milky mixt obtained by step B is cooled to room temperature, obtains described easy cleaning diamond paste.
6. preparation method according to claim 5, it is characterised in that in step, dissolves glyceryl monostearate when water bath heating temperature 70～80 DEG C.
7. preparation method according to claim 5, it is characterised in that in step, consumption 250～350 weight portion of glyceryl monostearate；The consumption of glycerol is 125～170 weight portions.
8. preparation method according to claim 5, it is characterised in that in step, the consumption of glyceryl monostearate is 290～320 weight portions；The consumption of glycerol is 140～154 weight portions.
9. diamond paste according to claim 5, it is characterised in that in stepb, the consumption of synthetic diamond micropowder is 7～12 weight portions；The consumption of liquid detergent is 125～160 weight portions.
10. diamond paste according to claim 5, it is characterised in that in stepb, the consumption of synthetic diamond micropowder is 8～10 weight portions；The consumption of liquid detergent is 138～148 weight portions.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610214158.8A CN105778862A (en) | 2016-04-08 | 2016-04-08 | Diamond grinding paste easy to clean and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610214158.8A CN105778862A (en) | 2016-04-08 | 2016-04-08 | Diamond grinding paste easy to clean and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105778862A true CN105778862A (en) | 2016-07-20 |
Family
ID=56395041
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610214158.8A Pending CN105778862A (en) | 2016-04-08 | 2016-04-08 | Diamond grinding paste easy to clean and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105778862A (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107722933A (en) * | 2016-08-10 | 2018-02-23 | 云南民族大学 | A kind of diamond paste and preparation method thereof |
| CN108165178A (en) * | 2018-01-24 | 2018-06-15 | 合肥同佑电子科技有限公司 | A kind of mobile phone metal rear shell antiscuffing paste |
| CN108987273A (en) * | 2017-06-05 | 2018-12-11 | 宁波江丰电子材料股份有限公司 | The surface treatment method of silver evaporation material |
| CN109054746A (en) * | 2018-08-20 | 2018-12-21 | 深圳市金辉源投资有限公司 | A kind of lapping liquid and application method for steel mold surface mirror surface treatment |
| CN112937203A (en) * | 2021-01-26 | 2021-06-11 | 西安钛斗金属制品科技有限公司 | Antique polishing method for titanium product |
| CN116083052A (en) * | 2022-12-31 | 2023-05-09 | 北京国瑞升科技股份有限公司 | Diamond grinding paste and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1375383A (en) * | 2002-04-25 | 2002-10-23 | 张彩根 | Cutting making process of silicon carbide boat for chip manufacture |
| CN101224564A (en) * | 2008-02-02 | 2008-07-23 | 杨学海 | Manufacturing methods of polishing wheel base cloth and polishing wheel |
| CN101624511A (en) * | 2009-08-14 | 2010-01-13 | 上海震旦办公设备有限公司 | Sharp grinding composition of paper shredder blade, grinding sheet and grinding bag manufactured thereby and relevant manufacturing technique |
| CN102627999A (en) * | 2012-03-20 | 2012-08-08 | 南京航空航天大学 | Water-based cutting fluid for microcrystalline glass processing, and preparation method thereof |
| CN102721593A (en) * | 2012-06-27 | 2012-10-10 | 北京科技大学 | Method for displaying original austenitic grain boundary of martensitic heat-resistant steel |
-
2016
- 2016-04-08 CN CN201610214158.8A patent/CN105778862A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1375383A (en) * | 2002-04-25 | 2002-10-23 | 张彩根 | Cutting making process of silicon carbide boat for chip manufacture |
| CN101224564A (en) * | 2008-02-02 | 2008-07-23 | 杨学海 | Manufacturing methods of polishing wheel base cloth and polishing wheel |
| CN101624511A (en) * | 2009-08-14 | 2010-01-13 | 上海震旦办公设备有限公司 | Sharp grinding composition of paper shredder blade, grinding sheet and grinding bag manufactured thereby and relevant manufacturing technique |
| CN102627999A (en) * | 2012-03-20 | 2012-08-08 | 南京航空航天大学 | Water-based cutting fluid for microcrystalline glass processing, and preparation method thereof |
| CN102721593A (en) * | 2012-06-27 | 2012-10-10 | 北京科技大学 | Method for displaying original austenitic grain boundary of martensitic heat-resistant steel |
Non-Patent Citations (2)
| Title |
|---|
| 朱山民，等: "《金刚石磨具制造》", 31 March 1984 * |
| 胡世祥: "用洗洁精配制研磨剂研磨高硬材料", 《机床》 * |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107722933A (en) * | 2016-08-10 | 2018-02-23 | 云南民族大学 | A kind of diamond paste and preparation method thereof |
| CN108987273A (en) * | 2017-06-05 | 2018-12-11 | 宁波江丰电子材料股份有限公司 | The surface treatment method of silver evaporation material |
| CN108165178A (en) * | 2018-01-24 | 2018-06-15 | 合肥同佑电子科技有限公司 | A kind of mobile phone metal rear shell antiscuffing paste |
| CN109054746A (en) * | 2018-08-20 | 2018-12-21 | 深圳市金辉源投资有限公司 | A kind of lapping liquid and application method for steel mold surface mirror surface treatment |
| CN109054746B (en) * | 2018-08-20 | 2020-11-03 | 深圳市金辉源投资有限公司 | Grinding fluid for mirror surface treatment of steel die surface and use method |
| CN112937203A (en) * | 2021-01-26 | 2021-06-11 | 西安钛斗金属制品科技有限公司 | Antique polishing method for titanium product |
| CN116083052A (en) * | 2022-12-31 | 2023-05-09 | 北京国瑞升科技股份有限公司 | Diamond grinding paste and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105778862A (en) | Diamond grinding paste easy to clean and preparation method thereof | |
| CN102703232B (en) | Emulsification type car cleaning polish and preparation method of emulsification type car cleaning polish | |
| CN103342965A (en) | Ultra-fine polishing wax for stainless steel metal product | |
| CN103590044A (en) | Metal polishing agent and preparation method thereof | |
| CN105200433A (en) | Stainless steel liquid polishing paste and preparation method thereof | |
| CN100526513C (en) | Wax removal water for cleaning automobile aluminum wheel hub and preparing method thereof | |
| CN106634836A (en) | Diamond paste as well as preparation method and application thereof | |
| CN104959900A (en) | Ultra-fine polishing process of metal product | |
| CN107400499A (en) | A kind of diamond paste and preparation method thereof | |
| CN107304347A (en) | A kind of method that utilization ultrasonic wave prepares diamond paste | |
| CN104120013A (en) | Easy-clean cutting fluid with uniformly dispersed grinding material and preparation method thereof | |
| CN113667408A (en) | Multifunctional liquid wax and preparation method thereof | |
| CN107304348A (en) | A kind of method that microwave heating prepares diamond paste | |
| CN105506638A (en) | Polishing liquid for metallographic analysis and preparation method and application method thereof | |
| CN103333617B (en) | Special polishing fluid for plastic soft metallic materials and method for preparing polishing fluid | |
| CN108642498A (en) | A kind of rapid wax removing agent and preparation method thereof | |
| JP3869520B2 (en) | Water-soluble cutting fluid for wire saw | |
| CN108754507A (en) | A kind of ultrasonic cleaning agent and preparation method and application method | |
| CN103642398B (en) | Polishing liquid for stainless steel material and use thereof | |
| CN106119861A (en) | A kind of preparation method of anti-rust water-based metal wax removing agent | |
| JP3826238B2 (en) | Liquid composition for metal polishing | |
| CN108728849A (en) | A kind of stainless steel material polishing agent and preparation method thereof | |
| CN106281219A (en) | A kind of double dissolubility diamond multiple grinding cream of water oil and preparation method thereof | |
| CN105002000A (en) | Cleaning powder, and preparation method and applications thereof | |
| CN104120004A (en) | Water-based cutting fluid stable in quality and uniform to disperse and preparation method of water-based cutting fluid |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160720 |
|
| RJ01 | Rejection of invention patent application after publication |