CN105175476B - 一种从油茶饼粕中提取茶皂素的方法 - Google Patents
一种从油茶饼粕中提取茶皂素的方法 Download PDFInfo
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- CN105175476B CN105175476B CN201510554232.6A CN201510554232A CN105175476B CN 105175476 B CN105175476 B CN 105175476B CN 201510554232 A CN201510554232 A CN 201510554232A CN 105175476 B CN105175476 B CN 105175476B
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- cake
- tea saponin
- camellia oleifera
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- oleifera seeds
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- 239000001397 quillaja saponaria molina bark Substances 0.000 title claims abstract description 26
- 229930182490 saponin Natural products 0.000 title claims abstract description 26
- 150000007949 saponins Chemical class 0.000 title claims abstract description 26
- 241000526900 Camellia oleifera Species 0.000 title claims abstract description 25
- 238000000034 method Methods 0.000 title claims abstract description 19
- 241001122767 Theaceae Species 0.000 title claims abstract 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 30
- 239000000843 powder Substances 0.000 claims abstract description 23
- 239000000203 mixture Substances 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000012530 fluid Substances 0.000 claims abstract description 14
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims abstract description 13
- 238000007710 freezing Methods 0.000 claims abstract description 7
- 230000008014 freezing Effects 0.000 claims abstract description 7
- 239000013618 particulate matter Substances 0.000 claims description 18
- 239000000706 filtrate Substances 0.000 claims description 12
- 238000010792 warming Methods 0.000 claims description 11
- 239000008187 granular material Substances 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 6
- 235000014593 oils and fats Nutrition 0.000 claims description 6
- 239000002245 particle Substances 0.000 claims description 6
- 230000001105 regulatory effect Effects 0.000 claims description 6
- 239000000344 soap Substances 0.000 claims description 5
- 238000002360 preparation method Methods 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 9
- 238000000605 extraction Methods 0.000 abstract description 8
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 238000010298 pulverizing process Methods 0.000 abstract 1
- 244000269722 Thea sinensis Species 0.000 description 23
- 239000003960 organic solvent Substances 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 2
- -1 glycoside compound Chemical class 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 239000000575 pesticide Substances 0.000 description 2
- 241000371997 Eriocheir sinensis Species 0.000 description 1
- 235000006468 Thea sinensis Nutrition 0.000 description 1
- 239000003674 animal food additive Substances 0.000 description 1
- 238000009360 aquaculture Methods 0.000 description 1
- 244000144974 aquaculture Species 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 239000008396 flotation agent Substances 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 239000004088 foaming agent Substances 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- 238000005065 mining Methods 0.000 description 1
- 239000003223 protective agent Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
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- Medicines Containing Plant Substances (AREA)
- Cosmetics (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
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CN201510554232.6A CN105175476B (zh) | 2015-09-02 | 2015-09-02 | 一种从油茶饼粕中提取茶皂素的方法 |
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CN201510554232.6A CN105175476B (zh) | 2015-09-02 | 2015-09-02 | 一种从油茶饼粕中提取茶皂素的方法 |
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CN105175476A CN105175476A (zh) | 2015-12-23 |
CN105175476B true CN105175476B (zh) | 2016-12-28 |
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CN201510554232.6A Active CN105175476B (zh) | 2015-09-02 | 2015-09-02 | 一种从油茶饼粕中提取茶皂素的方法 |
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Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2017167233A1 (zh) * | 2016-03-31 | 2017-10-05 | 江苏恒瑞医药股份有限公司 | 一种奥贝胆酸的新结晶形式及其制备方法 |
CN106221500B (zh) * | 2016-08-05 | 2018-04-17 | 河北晨阳工贸集团有限公司 | 一种防电晕高阻涂料的制备方法 |
CN109293728A (zh) * | 2018-10-09 | 2019-02-01 | 中国科学院青岛生物能源与过程研究所 | 一种高纯茶皂素的绿色低成本制备方法 |
USD918654S1 (en) | 2019-06-06 | 2021-05-11 | Sharkninja Operating Llc | Grill plate |
CN111592578B (zh) * | 2020-05-29 | 2021-11-19 | 信阳师范学院 | 山茶粕中的茶皂素提取工艺及其在氨基酸洁面皂中的应用 |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101962396B (zh) * | 2009-07-21 | 2012-11-21 | 浙江大学 | 一种从油茶饼粕、茶粕或茶枯中制取茶皂素的方法 |
CN102276679B (zh) * | 2011-06-27 | 2013-03-13 | 中国林业科学研究院林产化学工业研究所 | 一种从油茶饼粕减压沸腾提取高纯度茶皂素的方法 |
CN103275164B (zh) * | 2013-05-23 | 2016-06-22 | 安徽省华银茶油有限公司 | 一种食盐促渗从油茶饼粕中提取茶皂素的方法 |
CN104530173B (zh) * | 2014-12-11 | 2016-08-24 | 晋江佶邦机械技术服务有限公司 | 一种提取油茶饼粕中茶皂素的工艺 |
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C41 | Transfer of patent application or patent right or utility model | ||
CB03 | Change of inventor or designer information |
Inventor after: Shi Shuqin Inventor before: Lei Chunsheng Inventor before: Xue Hongjuan |
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Effective date of registration: 20161013 Address after: 362300 Nanan, Fujian, the United States and the United States along the River Road, No. 97 Applicant after: Shi Shuqin Address before: 213164 Changzhou, Changzhou, new North District, the town of Paris Road, spring, No. 27, No. Applicant before: CHANGZHOU CHANGYU PRACTICAL GAS CO., LTD. |
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C41 | Transfer of patent application or patent right or utility model | ||
CB03 | Change of inventor or designer information |
Inventor after: Zhang Wencai Inventor after: Liang Wenhong Inventor after: Cai Chunxiao Inventor before: Shi Shuqin |
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Effective date of registration: 20170215 Address after: 530000 Nanning Jiangnan District, the Guangxi Zhuang Autonomous Region Road, No. 10 Patentee after: Guangxi Golden Tea Oil Co., Ltd. Address before: 362300 Nanan, Fujian, the United States and the United States along the River Road, No. 97 Patentee before: Shi Shuqin |