CN105168589A - Eye-care traditional Chinese medicine gel preparation and preparation method thereof - Google Patents
Eye-care traditional Chinese medicine gel preparation and preparation method thereof Download PDFInfo
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Abstract
The invention provides an eye-care traditional Chinese medicine gel preparation and a preparation method thereof. The traditional Chinese medicine gel preparation is prepared from, by mass, 1%-3% of liquorice, 3%-8% of safflower carthamus, 2%-6% of barbary wolfberry fruits, 6%-8% of fructus corni, 6%-10% of semen cassiae, 6%-9% of shaved cinnamon barks, 5%-9% of folium mori, 9%-12% of white chrysanthemum, 9%-12% of salvia miltiorrhiza, 12%-15% of polygala tenuifolia, 0.5%-2% of menthol, 0.5%-2% of borneol, 2%-3% of carbomer, 0.5%-1.5% of triethanolamine and 15%-30% of pure water. The traditional Chinese medicine gel preparation is obtained according to the preparation method through the steps of traditional Chinese medicine soaking, heating and decocting, concentrating, carbomer adding for gel forming and triethanolamine adding for pH value regulating. The traditional Chinese medicine gel preparation is suitable for symptoms such as shortsightedness, eye drying and aningeresting, photaesthesia and wind fear, lacrimation induced by irritation of the wind and blurred vision, can be applied to daily healthcare of conjunctivitis, trachoma and marginal blepharitis, is good in curative effect and free of toxic and side effects compared with commercially available eye drops and is suitable for being used for a long time.
Description
Technical field
The present invention relates to a kind of eye care Chinese medicine gel and preparation method thereof.
Background technology
The latex glop of homogeneous, the suspendible that gel refers to that medicine and suitable adjuvant make or emulsion-type or semi-solid preparation.Gel has water solublity or oil-soluble feature, and after topical, affected part surface skin absorbs good, and side effect is lower; Meanwhile, the easy to use and applicable various types of patient of gel, acceptance is generally higher.Along with deepening continuously of gel research, researcheres are also devoted to exploitation more different types gel, according to statistics, China has Clinical Researches of New Drugs certification or the New Drug Certificate that tens kinds of gel new drugs such as lomefloxacin hydrochloride eye gel, Azithromycin gel agent, clindamycin hydrochloride gel agent, Ta Zhaluoding gel successively obtain National Drug Administration's drug evaluation center in recent years.In ophthalmic administration, the multiple advantage in view of gel which gives application in a big way.
In recent years, the living habit of people and external environment there occurs larger change, ophthalmic diseases becomes a kind of multiple and common disease gradually, the outstanding problems such as myopia, eye xerophthalmia are puckery, photophobia aversion to wind, epiphora induced by wind, blurring of vision, conjunctival congestion and swelling pain, conjunctivitis, cause serious harmful effect to daily life and work.Containing multi-medicament composition and antiseptic in the collyrium generally used, and it is in the majority with western medicine composition, the preparation of Chinese medicine ingredients is less, may there be improvement to a certain extent at the use initial stage to above symptom, but long-time use not only can make Conjunctival Goblet Cells in eyes damage, also may increase the weight of the symptoms such as puckery, the rubescent or pain of an xerophthalmia, the serious allergy that also can cause causes the diseases such as bronchial asthma, arrhythmia, cataract.
Summary of the invention
For existing dripping eyedrop Problems existing, and the advantage of attached gel agent, a kind of eye care Chinese medicine gel of the present invention and preparation method thereof.Technical scheme of the present invention is as follows:
A kind of eye care Chinese medicine gel, according to its recipe ingredient of mass percent is: Radix Glycyrrhizae 1 ~ 3%, Flos Carthami 3 ~ 8%, Fructus Lycii 2 ~ 6%, Fructus Corni 6 ~ 8%, Semen Cassiae 6 ~ 10%, Cortex Cinnamomi 6 ~ 9%, Folium Mori 5 ~ 9%, Flos Chrysanthemi 9 ~ 12%, Radix Salviae Miltiorrhizae 9 ~ 12%, Radix Polygalae 12 ~ 15%, Mentholum 0.5 ~ 2%, Borneolum Syntheticum 0.5 ~ 2%, carbomer 2 ~ 3%, triethanolamine 0.5 ~ 1.5%, pure water 15 ~ 30%.
The preparation method of described a kind of eye care Chinese medicine gel, carry out according to following processing step:
(1) according to above-mentioned quality proportioning first extracting liquorice, Flos Carthami, Fructus Lycii, Fructus Corni, Semen Cassiae, Cortex Cinnamomi, Folium Mori, Flos Chrysanthemi, Radix Salviae Miltiorrhizae, Radix Polygalae, clean with pure water, put into and decoct container, add the pure water of all Chinese medicine gross masses 3 ~ 4 times, soak 0.5 ~ 1 hour;
(2) be heated to 90 ~ 100 ° of C decoct 1 ~ 2 hour, be cooled to room temperature, filter out medicine juice;
(3) medicine juice is proceeded to concentrator distilling under reduced pressure to dewater, reach 80 ~ 90% to drug level;
(4) under room temperature, carbomer is dissolved in pure water, stirs into clear gel and slowly add in the medicine concentrated solution of step (3) again, mix homogeneously;
(5) add triethanolamine under room temperature, control ph is 5.5 ~ 6.5, pours into packing container sealing, sterilizing, sterilization, obtain eye care Chinese medicine gel after mix homogeneously.
The decoction container of described step (1) is rustless steel, glass or ceramic vessel.
The distilling under reduced pressure condition of described step (3) is: vacuum is 0.1 ~ 0.5MPa, and vapo(u)rizing temperature is 40 ~ 60 ° of C, and distillation time is 1 ~ 2 hour.
The mixing speed of described step (4) is 100 ~ 300r/min.
Eye care Chinese medicine gel of the present invention is applicable to the symptoms such as myopia, eye xerophthalmia are puckery, photophobia aversion to wind, epiphora induced by wind, blurring of vision, conjunctival congestion and swelling pain, also can be used for conjunctivitis, sand holes, blepharitis daily health caring use.Using method is: external application near the eyes, 2 ~ 3mL/ time, 1 times/day, and serious symptom person can increase to 2 times/day, and the external application time will ensure to clean with clear water after 1 ~ 2h again, is beneficial to play drug effect better, can life-time service.
The effect of above-described each compatibility raw material of Chinese medicine is described below:
Radix Glycyrrhizae: be a kind of tonification Chinese herbal medicine, there is effect of invigorating the spleen and replenishing QI, relieving spasm to stop pain, expelling phlegm for arresting cough, heat-clearing and toxic substances removing, coordinating the actions of various ingredients in a prescription, go back Anhydroalkannin and antiallergic.Cure mainly the diseases such as laryngopharynx swelling and pain, asthma and cough, stomach abdomen pain, consumptive lung disease chronic cough, also hand-foot skin is chapped from the cold, contact dermatitis, skin ulcer etc. have good efficacy.
Flos Carthami: acrid-sweet flavor, micro-hardship, warm in nature, GUIXIN, Liver Channel, have blood vessel dilating, protection cerebral tissue, reduce the effect such as blood fat and blood pressure, anticoagulation, modern medicine study shows, Flos Carthami also has antiinflammatory antiinflammatory, immunomodulating, analgesia and sedation.
Fructus Lycii: sweet in the mouth, property is put down, and returns liver, kidney channel.What ancient Chinese medicine doctor treatment deficiency of liver-blood, deficiency of kidney-YIN caused looks thing duskization and nyctalopia, usually uses Fructus Lycii.It has immunomodulating, antitumor, resisting fatigue, adjusting blood lipid blood glucose and blood pressure, protection reproductive system, the effects such as looks improving and the skin nourishing.Shennong's Herbal is recorded: " Fructus Lycii take for a long time can hard muscles and bones, resistance to cold and summer-heat, making light of one's life by commiting suicide old, is top grade in Chinese medicine.
Fructus Corni: sour in the mouth, slightly warm in nature, returns liver, kidney channel.There is liver and kidney tonifying, arresting seminal emission gas, Gu the effect of collapse.Cure mainly soreness of waist and knee joint, have a dizzy spell, blurring of vision, deficiency of the liver cold and heat, incessant sweating due to debility, the heart shakes the diseases such as scattered pulse.
Semen Cassiae: bitter in the mouth, sweet, salty, cold nature, returns liver, kidney, large intestine channel, and have loosening bowel to relieve constipation, reduce effect of blood fat and blood pressure, liver heat removing and eyesight improving, cure mainly the puckery pain of conjunctival congestion, the many tear of photophobia, has a headache dizzy, poor vision, constipation.
Cortex Cinnamomi: Cortex Cinnamomi is the one of Cortex Cinnamomi, acrid-sweet flavor is hot in nature, can complement sun, warming the spleen and stomach, removing accumulated cold, promoting blood circulation, replenishing vital essence to improve eyesight.Cure mainly decline of the fire from the gate of life, cold extremities faint pulse, YANG-depletion is collapsed, the diseases such as stomachache is had loose bowels, chills and pain of the waist and kness.Modern medicine study proves, Cortex Cinnamomi has powerful bactericidal action, better than negative patient to the effect of Gram’s staining rigidity bacterium, can external application.
Folium Mori: bitter but sweet flavor, cold in nature, return lung, Liver Channel.There is dispelling wind and heat pathogens, clearing away lung-heat and moistening for dryness, liver heat removing and eyesight improving, effect of flat blood removing heat from blood.For anemopyretic cold, lung-heat type cough, dizziness headache, conjunctival congestion is dim-sighted.In addition, Folium Mori contain the several physiological active substances such as abundant aminoacid, cellulose, vitamin, mineral and flavone, are that a kind of well Chinese crude drug is held concurrently health food.
Flos Chrysanthemi: property is pungent, sweet, bitter, is slightly cold.Return lung, Liver Channel.Effect dispelling wind and heat pathogens, suppressing the hyperactive liver improving eyesight, heat-clearing and toxic substances removing.For anemopyretic cold, fever and headache, conjunctival congestion is dim-sighted, deficiency of the liver and kindey, and order is secretly dim-sighted, dizzy infantile convulsion, controls excessive rising of liver-YANG, has a headache dizzy, kind wind and heat dispersing, purging liver-fire, holding concurrently can tonifying YIN improving eyesight, therefore availablely controls wind-heat of liver channel, or liver-fire is attacked caused conjunctival congestion and swelling pain, the effect of long memorial wind liver heat removing and eyesight improving altogether; Also can heat-clearing and toxic substances removing, especially kindly separate furunculosis, therefore availablely control furuncle swelling toxin.
Radix Salviae Miltiorrhizae: bitter in the mouth, is slightly cold, GUIXIN, Liver Channel.Have blood circulation promoting and blood stasis dispelling, except pain granulation promoting, clear away heart-fire relieving restlessness, effect of removing heat from blood eliminating carbuncle.For obstruction of qi in the chest and cardialgia, gastral cavity abdomen hypochondriac pain, abdominal mass abdominal mass is gathered, pyretic arthralgia pain, dysphoria and insomnia, dysmenorrhea amenorrhea, and skin infection such as to swell and ache the disease.Radix Polygalae: bitter in the mouth is pungent, warm in nature, GUIXIN, kidney, lung meridian.Can happily gas and mind tranquilizing and the heart calming, kidney qi can be led to and strong will is not forgotten, therefore there is Fructus Alpiniae Oxyphyllae of calming the nerves, effect of resolving depression.Cure mainly the malaise of disarmony between the heart and kidney, palpitation with fear, forgetful, nocturnal emission, insomnia, carbuncle skin ulcer is swollen waits disease.
Beneficial effect of the present invention is:
Eye care Chinese medicine gel of the present invention, according to the theory of " liver opening at eye " in Chinese medicine, the above-mentioned each Chinese medicine of compatibility, there is liver heat removing and eyesight improving, anti-inflammatory analgetic, effect of heat-clearing and toxic substances removing, be applicable to that myopia, eye xerophthalmia are puckery, the symptom such as photophobia aversion to wind, epiphora induced by wind, blurring of vision, conjunctival congestion and swelling pain, also can be used for conjunctivitis, sand holes, blepharitis daily health caring use, more commercially available collyrium good effect and having no side effect, is applicable to life-time service; The inventive method is simple, easily controls, and has industrial value.
Detailed description of the invention
The Radix Glycyrrhizae adopted in the embodiment of the present invention, Flos Carthami, Fructus Lycii, Fructus Corni, Semen Cassiae, Cortex Cinnamomi, Folium Mori, Flos Chrysanthemi, Radix Salviae Miltiorrhizae, Radix Polygalae, Mentholum, Borneolum Syntheticum are all purchased from pharmacy.
The carbomer adopted in the embodiment of the present invention and triethanolamine are commercially available medical grade product.
Embodiment 1
A kind of eye care Chinese medicine gel, recipe ingredient is: Radix Glycyrrhizae 1g, Flos Carthami 3g, Fructus Lycii 4g, Fructus Corni 8g, Semen Cassiae 6g, Cortex Cinnamomi 7g, Folium Mori 6g, Flos Chrysanthemi 10g, Radix Salviae Miltiorrhizae 10g, Radix Polygalae 12g, Mentholum 1g, Borneolum Syntheticum 0.5g, carbomer 2g, triethanolamine 1g, pure water 18.5g.Preparation method is:
(1) according to above-mentioned quality first extracting liquorice, Flos Carthami, Fructus Lycii, Fructus Corni, Semen Cassiae, Cortex Cinnamomi, Folium Mori, Flos Chrysanthemi, Radix Salviae Miltiorrhizae, Radix Polygalae, clean with pure water, put into and decoct container, add 325g pure water, soak 1 hour;
(2) be heated to 100 ° of C and decoct 1 hour, be cooled to room temperature, filter out medicine juice;
(3) medicine juice is proceeded to concentrator distilling under reduced pressure to dewater, reach 90% to drug level;
(4) under room temperature, carbomer is dissolved in pure water, stirs into clear gel and slowly add in the medicine concentrated solution of step (3) again, mix homogeneously;
(5) add triethanolamine under room temperature, control ph is 6.0, pours into packing container sealing, sterilizing, sterilization, obtain eye care Chinese medicine gel after mix homogeneously.
The analysis result of the eye care Chinese medicine gel of the present embodiment is as shown in table 1.
Embodiment 2
A kind of eye care Chinese medicine gel, recipe ingredient is: Radix Glycyrrhizae 3g, Flos Carthami 5g, Fructus Lycii 5g, Fructus Corni 6g, Semen Cassiae 10g, Cortex Cinnamomi 7g, Folium Mori 5g, Flos Chrysanthemi 12g, Radix Salviae Miltiorrhizae 9g, Radix Polygalae 15g, Mentholum 2g, Borneolum Syntheticum 1g, carbomer 3g, triethanolamine 1g, pure water 16g.Preparation method is:
(1) according to above-mentioned quality first extracting liquorice, Flos Carthami, Fructus Lycii, Fructus Corni, Semen Cassiae, Cortex Cinnamomi, Folium Mori, Flos Chrysanthemi, Radix Salviae Miltiorrhizae, Radix Polygalae, clean with pure water, put into and decoct container, add 250g pure water, soak 2 hours;
(2) be heated to 100 ° of C and decoct 1 hour, be cooled to room temperature, filter out medicine juice;
(3) medicine juice is proceeded to concentrator distilling under reduced pressure to dewater, reach 88% to drug level;
(4) under room temperature, carbomer is dissolved in pure water, stirs into clear gel and slowly add in the medicine concentrated solution of step (3) again, mix homogeneously;
(5) add triethanolamine under room temperature, control ph is 6.5, pours into packing container sealing, sterilizing, sterilization, obtain eye care Chinese medicine gel after mix homogeneously.
The analysis result of the eye care Chinese medicine gel of the present embodiment is as shown in table 1.
Embodiment 3
A kind of eye care Chinese medicine gel, recipe ingredient is: Radix Glycyrrhizae 1g, Flos Carthami 3g, Fructus Lycii 4g, Fructus Corni 7g, Semen Cassiae 6g, Cortex Cinnamomi 6g, Folium Mori 6g, Flos Chrysanthemi 10g, Radix Salviae Miltiorrhizae 9g, Radix Polygalae 12g, Mentholum 1g, Borneolum Syntheticum 0.5g, carbomer 2g, triethanolamine 1.5g, pure water 21g.Preparation method is:
(1) according to above-mentioned quality first extracting liquorice, Flos Carthami, Fructus Lycii, Fructus Corni, Semen Cassiae, Cortex Cinnamomi, Folium Mori, Flos Chrysanthemi, Radix Salviae Miltiorrhizae, Radix Polygalae, clean with pure water, put into and decoct container, add 325g pure water, soak 2 hours;
(2) be heated to 100 ° of C and decoct 1 hour, be cooled to room temperature, filter out medicine juice;
(3) medicine juice is proceeded to concentrator distilling under reduced pressure to dewater, reach 85% to drug level;
(4) under room temperature, carbomer is dissolved in pure water, stirs into clear gel and slowly add in the medicine concentrated solution of step (3) again, mix homogeneously;
(5) add triethanolamine under room temperature, control ph is 6.5, pours into packing container sealing, sterilizing, sterilization, obtain eye care Chinese medicine gel after mix homogeneously.
The analysis result of the eye care Chinese medicine gel of the present embodiment is as shown in table 1.
Carry out outward appearance, the medicament state of 0 ~ 40 ° and the analysis of experiments of Ocular irritation to eye care Chinese medicine gel prepared by above 3 embodiments, result is as shown in table 1
Table 1 Chinese medicine gel outward appearance, the medicament state of 0 ~ 40 ° and Ocular irritation analysis of experiments result
The application case of eye care Chinese medicine gel of the present invention
Collect 50 office workers of certain IT company long campaigns computer work, wherein 48 office workers exist that eye xerophthalmia is to some extent puckery, photophobia aversion to wind, epiphora induced by wind, blurring of vision, conjunctival congestion and swelling pain problem, 2 conjunctivitis patients by name, adhere to using eye care Chinese medicine gel of the present invention 1 month, use 1 every day, after 1 month, collection result is: in 48 office workers, and 30 described symptoms of reflection are improved obviously, 15 reflections, without significant change, do not submit result to for 3; 2 conjunctivitis patients reflect that inflammation obviously alleviates, and still use in continuation.
Claims (5)
1. an eye care Chinese medicine gel, it is characterized in that according to its recipe ingredient of mass percent be: Radix Glycyrrhizae 1 ~ 3%, Flos Carthami 3 ~ 8%, Fructus Lycii 2 ~ 6%, Fructus Corni 6 ~ 8%, Semen Cassiae 6 ~ 10%, Cortex Cinnamomi 6 ~ 9%, Folium Mori 5 ~ 9%, Flos Chrysanthemi 9 ~ 12%, Radix Salviae Miltiorrhizae 9 ~ 12%, Radix Polygalae 12 ~ 15%, Mentholum 0.5 ~ 2%, Borneolum Syntheticum 0.5 ~ 2%, carbomer 2 ~ 3%, triethanolamine 0.5 ~ 1.5%, pure water 15 ~ 30%.
2. the preparation method of a kind of eye care Chinese medicine gel according to claim 1, it is characterized in that carrying out according to following processing step: (1) is according to above-mentioned quality proportioning first extracting liquorice, Flos Carthami, Fructus Lycii, Fructus Corni, Semen Cassiae, Cortex Cinnamomi, Folium Mori, Flos Chrysanthemi, Radix Salviae Miltiorrhizae, Radix Polygalae, clean with pure water, put into and decoct container, add the pure water of all Chinese medicine gross masses 3 ~ 4 times, soak 0.5 ~ 1 hour;
(2) be heated to 90 ~ 100 ° of C decoct 1 ~ 2 hour, be cooled to room temperature, filter out medicine juice;
(3) medicine juice is proceeded to concentrator distilling under reduced pressure to dewater, reach 80 ~ 90% to drug level;
(4) under room temperature, carbomer is dissolved in pure water, stirs into clear gel and slowly add in the medicine concentrated solution of step (3) again, mix homogeneously;
(5) add triethanolamine under room temperature, control ph is 5.5 ~ 6.5, pours into packing container sealing, sterilizing, sterilization, obtain eye care Chinese medicine gel after mix homogeneously.
3. the preparation method of a kind of eye care Chinese medicine gel according to claim 2, is characterized in that the decoction container of described step (1) is rustless steel, glass or ceramic vessel.
4. the preparation method of a kind of eye care Chinese medicine gel according to claim 2, it is characterized in that the distilling under reduced pressure condition of described step (3) is: vacuum is 0.1 ~ 0.5MPa, vapo(u)rizing temperature is 40 ~ 60 ° of C, and distillation time is 1 ~ 2 hour.
5. the preparation method of a kind of eye care Chinese medicine gel according to claim 2, is characterized in that the mixing speed of described step (4) is 100 ~ 300r/min.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107440975A (en) * | 2017-09-18 | 2017-12-08 | 江苏天眼医药科技股份有限公司 | A kind of composition for eye-care |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1291500A (en) * | 2000-10-12 | 2001-04-18 | 黄耀文 | Chinese patent medicine for treating myopia and amblyopia |
| CN1799619A (en) * | 2005-10-10 | 2006-07-12 | 武汉大学 | Chinese medicinal gel formulation and its preparing process |
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2015
- 2015-10-27 CN CN201510703472.8A patent/CN105168589A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1291500A (en) * | 2000-10-12 | 2001-04-18 | 黄耀文 | Chinese patent medicine for treating myopia and amblyopia |
| CN1799619A (en) * | 2005-10-10 | 2006-07-12 | 武汉大学 | Chinese medicinal gel formulation and its preparing process |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107440975A (en) * | 2017-09-18 | 2017-12-08 | 江苏天眼医药科技股份有限公司 | A kind of composition for eye-care |
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