CN105113224A - Novel plant component clothing softener - Google Patents
Novel plant component clothing softener Download PDFInfo
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- CN105113224A CN105113224A CN201510564387.8A CN201510564387A CN105113224A CN 105113224 A CN105113224 A CN 105113224A CN 201510564387 A CN201510564387 A CN 201510564387A CN 105113224 A CN105113224 A CN 105113224A
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Abstract
The invention discloses a novel plant component clothing softener, which comprises the following components in parts by weight: 1-4 parts of a plant antibiosis softening extract, 0.5-1 part of esterquats, 0.5-1 part of essence, 5-7 parts of citric acid and 100-120 parts of distilled water. The invention discloses a preparation method of the plant antibiosis softening extract. The softener can reduce the contents of the esterquats and essence; and the plant antibiosis softening extract is added, so that the softener is environmentally friendly, has effects of sterilization and disinfection and also has plant fragrance, and has well market promotion value.
Description
Technical field:
The present invention relates to fabric softener field, be specifically related to a kind of novel plant component fabric softener.
Background technology:
Clothing is in washing process, fiber fines is often wound around, intertwine, even rupture, clothing is after repeatedly washing, the alkalescence effect of washing agent more makes the intrinsic slickness of fiber, extensibility and elasticity be affected, what show is that one integral piece clothing seems to wear, do not have shape, and touch feel stiff especially, more this clothes washing number of times sensation be more obvious.Certain fabric is through the conditioning of softener, and fiber has recovered original form, and the fold on fabric also considerably reduces, and makes complicated flatiron work originally become simple, easy, time saving and energy saving.
Be defined as in " fabric softening agent industry standard ": be applicable to coordinate washing agent to use in fabric washing nursing process, play make fabric sofetening, fluffy, eliminate the washing and nursing article of electrostatic interaction.The effect of fabric softener just looks like be surface uniform ground floor diaphragm for fabric fibre; fiber surface is owing to having adsorbed softener; interfibrous coefficient of friction reduces; mobility enhances; fiber intrinsic level and smooth, extend, compression performance have also been obtained recovery, so fabric becomes more soft, fluffy, flexible.
Data according to Environmental Protection Agency (EPA) and chemical producting safety description (MSDS) show, and containing multiple hazardous chemical composition in fabric softener, comprise benzyl acetate, phenmethylol, citrene, linalool, chloroform etc.Benzyl acetate may cause cancer of pancreas, and its gas can stimulate eyes and respiratory tract, causes cough, and energy absorbing transmission from skin; Phenmethylol can stimulate the upper respiratory tract, causes central nervous system disorder, and causes the symptoms such as headache, Nausea and vomiting and blood pressure drops; Citrene is a kind of known carcinogenic substance, stimulates eyes and skin; Linalool has anesthetic effect, can cause central nervous system disorder and unsmooth breath, in animal experiment, subjects even can be caused dead; Chloroform is a kind of neurotoxic narcoticness, carcinogenic material, is listed in hazardous waste list by Environmental Protection Agency.
" naturally living " points out, when this type of chemical composition of major part heats in dryer, danger is larger.Because softener can remain in clothing, cause these chemical composition slow release out, infiltrate skin or enter air.What is worse, all with the addition of fragrance in most of fabric softener to cover chemical odor.For children, old man and patient, these chemical compositions of Long Term Contact are especially dangerous, even can cause permanent damage.Children may play fash, cry and scream or suffer from diarrhoea for a long time.Some researcher even points out, has part SIDS sudden infant death syndrome case to cause due to allergic reaction, and is likely with the children clothes of fabric softener washing and bed clothes and causes one of irritated reason.
Ester based quaternary ammonium salt soft dose of softness is stablized, and consumption is little, and outstanding biological degradability, environmental protection, more with multiple functions such as anti-yellowing change, sterilizings, is that the one of softener industry from now on dominates trend.
Chinese invention patent CN103046335B discloses a kind of marine biological sterilization fabric softener and preparation method thereof, and percentage proportioning is as follows: marine biological sterilization agent 2.0-4.0%; Ester based quaternary ammonium salt 2.0-4.0%; Citric acid 6.0-8.0%; Essence 2.0-3.5%; Surplus is water.The marine biological sterilization fabric softener of this invention can be effectively degerming and destatic, and uses that fabric can be made to feel well is clean aseptic, a softer and smoother touch, smooth docile on a small quantity, and in addition also having the advantage of environment-protecting asepsis, is of the present invention closest to prior art.
Summary of the invention:
Object of the present invention:
Softener of the present invention reduces the content of ester based quaternary ammonium salt and essence, adds the submissive extract of plants antimicrobial, has effect of sterilizing concurrently, have plant fragrance simultaneously, environmental protection, efficient energy-saving.
The invention provides following technical scheme:
A kind of novel plant component fabric softener, comprises the component of following parts by weight:
Plants antimicrobial submissive extract 1-4 part, ester based quaternary ammonium salt 0.5-1 part, essence 0.5-1 part, citric acid 5-7 part, distilled water 100-120 part;
The submissive extract of described plants antimicrobial has been prepared by following operating procedure:
The first step: pulverize after being dried by green tea tea grounds, adds green tea slag powder weight 5-10 glycerine doubly in green tea tea grounds powder, and vacuum and low temperature stirs 10-15 hour;
Second step: olive oil is mixed with aloe pulp and pulls an oar; Mixed weight 5 times of NaOH aqueous slkalis are added, stand at low temperature after agitating heating 5-7 hour, removing top layer and the insoluble composition of bottom in aloe mixing making beating liquid;
3rd step: the component first step and second step prepared is according to weight ratio 1:2-3 mixing and stirring, and it is neutral for adding hydrochloric acid solution adjust ph, and after leaving standstill, removing insoluble solids is collected liquid part and obtained the submissive extract of plants antimicrobial.
Preferably, the component of following parts by weight is comprised:
Plants antimicrobial submissive extract 3-4 part, ester based quaternary ammonium salt 0.5-0.8 part, essence 0.5-0.6 part, citric acid 5-7 part, distilled water 100-120 part.
Preferably, the submissive extract of described plants antimicrobial is prepared in the first step, adds green tea slag powder weight 8-10 glycerine doubly in green tea tea grounds powder.
Preferably, the submissive extract of described plants antimicrobial to be prepared in the first step vacuum and low temperature and is stirred 12-15 hour.
Preferably, the submissive extract of described plants antimicrobial is prepared in second step olive oil and aloe pulp to mix according to weight ratio 1:20-22 and is pulled an oar.
Preferably, the submissive extract of described plants antimicrobial prepares the molar concentration of NaOH aqueous slkali in second step is 2mol/L.
Preferably, the submissive extract of described plants antimicrobial prepares the mass fraction of hydrochloric acid solution in the 3rd step is 35-37%.
The preparation method of product of the present invention is: in 35 DEG C of water, add ester based quaternary ammonium salt and citric acid according to weight proportion, obtain mixed liquor one after being uniformly mixed 30 minutes; Add the submissive extract of plants antimicrobial and essence to mixed liquor is a kind of according to weight proportion, be uniformly mixed 30 minutes and obtain described a kind of plant component fabric softener.
Softener is the chemical substance that a class can change quiet, the coefficient of kinetic friction of fiber.When changing confficient of static friction, feel touches level and smooth sense, is easy to move on fiber or fabric; When change the coefficient of kinetic friction time, the fine structure between fiber and fiber is easy to mutual movement, namely fiber or fabric easily deformable.The comprehensive sensation of the two is exactly soft.
Glycerine, Chinese formal name used at school glycerol, miscible with any ratio with water and alcohols, amine, phenols, the aqueous solution is neutral.Be dissolved in the ethyl acetate of 11 times, the ether of about 500 times.Be insoluble to benzene, chloroform, carbon tetrachloride, carbon disulfide, benzinum, oils, long-chain fatty alcohol.Flammable, meet the strong oxidizer such as chromium dioxide, potassium chlorate and can cause burning and blast.Also be the good solvent of many inorganic salts and gas.To metal non-corrosiveness, do can be oxidized to acrolein when solvent uses.
In seasoning and colouring foods, contribute to food because glycerine has stickiness shaping.In the snap frozen of food, glycerine can be used as the heat transfer medium with direct food contact.The lubricant of glycerine or food processing and package packing machine.In addition, polyglycereol and the application of polyglycerol ester in manufacture frangible products and margarine increase just year by year.Medical industry: as softening agent, viscosity modifier and solvent.Glycerine sore wood phenol can be used as sedative, and nitroglycerine is a kind of vasodilator agent etc. in coronary spasm.Daily-use chemical industry: for the additive of cosmetics, toothpaste, flavoring essence, the antidesiccant of tobacco.Plastics industry: the initiator in producing as polyurethane foam plastics.Textile and dyeing industry: as lubricant, hygroscopic agent, crease and shrink resistance finishing agent, diffusant, bleeding agent etc.In addition, glycerine also has extensive use in industry such as pottery, photograph, leather and timber.The present invention utilizes the dissolubility to organic solution of glycerine, softening and solvent action, is dissolved by antibacterial material fat-soluble in green tea.
Green tea remains the natural materials of fresh leaf, and the Tea Polyphenols contained, catechin, chlorophyll, caffeine, amino acid, vitamins and other nutritious components are also more.These natural nutrition compositions in green tea have special effect to anti-aging, anti-cancer, anticancer, sterilization, anti-inflammatory etc., also containing non-water-soluble trophic function healthy ingredient in green tea slag, by the composite dissolving with glycerine, give the organoleptic quality of natural faint scent, be provided with good natural bacteriostatic effect simultaneously.
Olive oil is by the fresh direct cold press of olive fruit, without heating and chemical treatment, remains natural nutrient component, has light fruital, and olive oil is as oily matter simultaneously, can change quiet, the coefficient of kinetic friction of fiber.
Aloe, Aloe is Liliaceae perennial evergreen herbaceous plant, and leafage is raw, large and plump, in seat shape or be born in stem top, the normal lanceolar of leaf or leaf short wide, edge has sharp tooth to sting.Aloe integrates edible, medicinal, improves looks, views and admires plant nova.It has bactericidal action, antiinflammatory action, moistening beautification function, lets out effect under stomach invigorating, the cardiac stimulant effect of invigorating blood circulation, immunity and palingenesis, immunity and antitumor action, detoxication, anti-aging effects, analgesia, sedation, anti-sunlight function.It is secreted effluent and has been widely applied in medicine and daily use chemicals.The method of among the people also useful aloe county leaf juice beauty treatment, what be subject to people gathers around handful.Be rich in SOD, polysaccharide, protein and vitamin C in aloe, there is good performance of keeping humidity.
The present invention by by aloe pulp with add NaOH aqueous slkali after mixed with olive oil and mix, utilize NaOH and the saponification of fat, separated out by cryoprecipitation after basic hydrolysis, then pass through in HCL with rear standing desalination, obtain the submissive extract of plants antimicrobial.
Beneficial effect of the present invention:
1. softener of the present invention reduces the content of ester based quaternary ammonium salt and essence, reduces production cost.
2. the present invention adds the submissive extract of plants antimicrobial, has effect of sterilizing concurrently, has plant fragrance simultaneously, environmental protection, efficient energy-saving.
3. this invention exploits the preparation method of plants antimicrobial softener extract, there is good market popularization value.
Detailed description of the invention:
Be described in detail embodiments of the invention below, the present embodiment is implemented under premised on invention technical scheme, give detailed embodiment and concrete operating process, but protection scope of the present invention is not limited to following embodiment.The experimental program of unreceipted actual conditions in embodiment, the condition that conveniently condition or manufacturer advise usually is implemented.
Embodiment one
A kind of novel plant component fabric softener, comprises the component of following parts by weight:
The submissive extract of plants antimicrobial 1 part, ester based quaternary ammonium salt 0.5 part, 0.5 part, essence, citric acid 5 parts, distilled water 100 parts;
The submissive extract of described plants antimicrobial has been prepared by following operating procedure:
The first step: pulverize after green tea tea grounds is dried, in green tea tea grounds powder, add the glycerine of green tea slag powder weight 5 times, vacuum and low temperature stirs 10 hours;
Second step: olive oil and aloe pulp are mixed according to weight ratio 1:20 and pulls an oar; In aloe mixing making beating liquid, add mixed weight 5 times of NaOH aqueous slkalis (molar concentration is 2mol/L), agitating heating is stand at low temperature after 5 hours, removing top layer and the insoluble composition of bottom;
3rd step: the component first step and second step prepared is according to weight ratio 1:2 mixing and stirring, add hydrochloric acid solution (mass fraction is 35%) adjust ph for neutral, after leaving standstill, removing insoluble solids is collected liquid part and is obtained the submissive extract of plants antimicrobial.
Embodiment two
A kind of novel plant component fabric softener, comprises the component of following parts by weight:
The submissive extract of plants antimicrobial 4 parts, ester based quaternary ammonium salt 1 part, 1 part, essence, citric acid 7 parts, distilled water 120 parts;
The submissive extract of described plants antimicrobial has been prepared by following operating procedure:
The first step: pulverize after green tea tea grounds is dried, in green tea tea grounds powder, add the glycerine of green tea slag powder weight 10 times, vacuum and low temperature stirs 15 hours;
Second step: olive oil and aloe pulp are mixed according to weight ratio 1:22 and pulls an oar; In aloe mixing making beating liquid, add mixed weight 5 times of NaOH aqueous slkalis (molar concentration is 2mol/L), agitating heating is stand at low temperature after 7 hours, removing top layer and the insoluble composition of bottom;
3rd step: the component first step and second step prepared is according to weight ratio 1:3 mixing and stirring, add hydrochloric acid solution (mass fraction is 37%) adjust ph for neutral, after leaving standstill, removing insoluble solids is collected liquid part and is obtained the submissive extract of plants antimicrobial.
Embodiment three
A kind of novel plant component fabric softener, comprises the component of following parts by weight:
The submissive extract of plants antimicrobial 1 part, ester based quaternary ammonium salt 1 part, 0.5 part, essence, citric acid 7 parts, distilled water 100 parts;
The submissive extract of described plants antimicrobial has been prepared by following operating procedure:
The first step: pulverize after green tea tea grounds is dried, in green tea tea grounds powder, add the glycerine of green tea slag powder weight 5 times, vacuum and low temperature stirs 15 hours;
Second step: olive oil and aloe pulp are mixed according to weight ratio 1:20 and pulls an oar; In aloe mixing making beating liquid, add mixed weight 5 times of NaOH aqueous slkalis (molar concentration is 2mol/L), agitating heating is stand at low temperature after 7 hours, removing top layer and the insoluble composition of bottom;
3rd step: the component first step and second step prepared is according to weight ratio 1:2 mixing and stirring, add hydrochloric acid solution (mass fraction is 37%) adjust ph for neutral, after leaving standstill, removing insoluble solids is collected liquid part and is obtained the submissive extract of plants antimicrobial.
Embodiment four
A kind of novel plant component fabric softener, comprises the component of following parts by weight:
The submissive extract of plants antimicrobial 4 parts, ester based quaternary ammonium salt 0.5 part, 1 part, essence, citric acid 5 parts, distilled water 120 parts;
The submissive extract of described plants antimicrobial has been prepared by following operating procedure:
The first step: pulverize after green tea tea grounds is dried, in green tea tea grounds powder, add the glycerine of green tea slag powder weight 10 times, vacuum and low temperature stirs 10 hours;
Second step: olive oil and aloe pulp are mixed according to weight ratio 1:22 and pulls an oar; In aloe mixing making beating liquid, add mixed weight 5 times of NaOH aqueous slkalis (molar concentration is 2mol/L), agitating heating is stand at low temperature after 5 hours, removing top layer and the insoluble composition of bottom;
3rd step: the component first step and second step prepared is according to weight ratio 1:3 mixing and stirring, add hydrochloric acid solution (mass fraction is 35%) adjust ph for neutral, after leaving standstill, removing insoluble solids is collected liquid part and is obtained the submissive extract of plants antimicrobial.
Embodiment five
A kind of novel plant component fabric softener, comprises the component of following parts by weight:
The submissive extract of plants antimicrobial 3 parts, ester based quaternary ammonium salt 0.5 part, 0.5 part, essence, citric acid 5 parts, distilled water 100 parts;
The submissive extract of described plants antimicrobial has been prepared by following operating procedure:
The first step: pulverize after green tea tea grounds is dried, in green tea tea grounds powder, add the glycerine of green tea slag powder weight 8 times, vacuum and low temperature stirs 12 hours;
Second step: olive oil and aloe pulp are mixed according to weight ratio 1:20 and pulls an oar; In aloe mixing making beating liquid, add mixed weight 5 times of NaOH aqueous slkalis (molar concentration is 2mol/L), agitating heating is stand at low temperature after 5 hours, removing top layer and the insoluble composition of bottom;
3rd step: the component first step and second step prepared is according to weight ratio 1:2 mixing and stirring, add hydrochloric acid solution (mass fraction is 35%) adjust ph for neutral, after leaving standstill, removing insoluble solids is collected liquid part and is obtained the submissive extract of plants antimicrobial.
Embodiment six
A kind of novel plant component fabric softener, comprises the component of following parts by weight:
The submissive extract of plants antimicrobial 4 parts, ester based quaternary ammonium salt 0.8 part, 0.6 part, essence, citric acid 7 parts, distilled water 120 parts;
The submissive extract of described plants antimicrobial has been prepared by following operating procedure:
The first step: pulverize after green tea tea grounds is dried, in green tea tea grounds powder, add the glycerine of green tea slag powder weight 10 times, vacuum and low temperature stirs 15 hours;
Second step: olive oil and aloe pulp are mixed according to weight ratio 1:22 and pulls an oar; In aloe mixing making beating liquid, add mixed weight 5 times of NaOH aqueous slkalis (molar concentration is 2mol/L), agitating heating is stand at low temperature after 7 hours, removing top layer and the insoluble composition of bottom;
3rd step: the component first step and second step prepared is according to weight ratio 1:3 mixing and stirring, add hydrochloric acid solution (mass fraction is 37%) adjust ph for neutral, after leaving standstill, removing insoluble solids is collected liquid part and is obtained the submissive extract of plants antimicrobial.
Embodiment seven
A kind of novel plant component fabric softener, comprises the component of following parts by weight:
The submissive extract of plants antimicrobial 3 parts, ester based quaternary ammonium salt 0.8 part, 0.5 part, essence, citric acid 7 parts, distilled water 100 parts;
The submissive extract of described plants antimicrobial has been prepared by following operating procedure:
The first step: pulverize after green tea tea grounds is dried, in green tea tea grounds powder, add the glycerine of green tea slag powder weight 10 times, vacuum and low temperature stirs 12 hours;
Second step: olive oil and aloe pulp are mixed according to weight ratio 1:22 and pulls an oar; In aloe mixing making beating liquid, add mixed weight 5 times of NaOH aqueous slkalis (molar concentration is 2mol/L), agitating heating is stand at low temperature after 5 hours, removing top layer and the insoluble composition of bottom;
3rd step: the component first step and second step prepared is according to weight ratio 1:3 mixing and stirring, add hydrochloric acid solution (mass fraction is 35%) adjust ph for neutral, after leaving standstill, removing insoluble solids is collected liquid part and is obtained the submissive extract of plants antimicrobial.
Embodiment eight
A kind of novel plant component fabric softener, comprises the component of following parts by weight:
The submissive extract of plants antimicrobial 4 parts, ester based quaternary ammonium salt 0.5 part, 0.6 part, essence, citric acid 5 parts, distilled water 120 parts;
The submissive extract of described plants antimicrobial has been prepared by following operating procedure:
The first step: pulverize after green tea tea grounds is dried, in green tea tea grounds powder, add the glycerine of green tea slag powder weight 8 times, vacuum and low temperature stirs 15 hours;
Second step: olive oil and aloe pulp are mixed according to weight ratio 1:20 and pulls an oar; In aloe mixing making beating liquid, add mixed weight 5 times of NaOH aqueous slkalis (molar concentration is 2mol/L), agitating heating is stand at low temperature after 7 hours, removing top layer and the insoluble composition of bottom;
3rd step: the component first step and second step prepared is according to weight ratio 1:2 mixing and stirring, add hydrochloric acid solution (mass fraction is 37%) adjust ph for neutral, after leaving standstill, removing insoluble solids is collected liquid part and is obtained the submissive extract of plants antimicrobial.
Embodiment nine
A kind of novel plant component fabric softener, comprises the component of following parts by weight:
The submissive extract of plants antimicrobial 3 parts, ester based quaternary ammonium salt 0.6 part, 0.5 part, essence, citric acid 6 parts, distilled water 110 parts;
The submissive extract of described plants antimicrobial has been prepared by following operating procedure:
The first step: pulverize after green tea tea grounds is dried, in green tea tea grounds powder, add the glycerine of green tea slag powder weight 9 times, vacuum and low temperature stirs 13 hours;
Second step: olive oil and aloe pulp are mixed according to weight ratio 1:21 and pulls an oar; In aloe mixing making beating liquid, add mixed weight 5 times of NaOH aqueous slkalis (molar concentration is 2mol/L), agitating heating is stand at low temperature after 6 hours, removing top layer and the insoluble composition of bottom;
3rd step: the component first step and second step prepared is according to weight ratio 1:2 mixing and stirring, add hydrochloric acid solution (mass fraction is 36%) adjust ph for neutral, after leaving standstill, removing insoluble solids is collected liquid part and is obtained the submissive extract of plants antimicrobial.
Embodiment ten
A kind of novel plant component fabric softener, comprises the component of following parts by weight:
The submissive extract of plants antimicrobial 4 parts, ester based quaternary ammonium salt 0.7 part, 0.6 part, essence, citric acid 6 parts, distilled water 110 parts;
The submissive extract of described plants antimicrobial has been prepared by following operating procedure:
The first step: pulverize after green tea tea grounds is dried, in green tea tea grounds powder, add the glycerine of green tea slag powder weight 9 times, vacuum and low temperature stirs 13 hours;
Second step: olive oil and aloe pulp are mixed according to weight ratio 1:21 and pulls an oar; In aloe mixing making beating liquid, add mixed weight 5 times of NaOH aqueous slkalis (molar concentration is 2mol/L), agitating heating is stand at low temperature after 6 hours, removing top layer and the insoluble composition of bottom;
3rd step: the component first step and second step prepared is according to weight ratio 1:2 mixing and stirring, add hydrochloric acid solution (mass fraction is 36%) adjust ph for neutral, after leaving standstill, removing insoluble solids is collected liquid part and is obtained the submissive extract of plants antimicrobial.
The preparation method of above-mentioned enforcement product is: in 35 DEG C of water, add ester based quaternary ammonium salt and citric acid according to weight proportion, obtain mixed liquor one after being uniformly mixed 30 minutes; Add the submissive extract of plants antimicrobial and essence to mixed liquor is a kind of according to weight proportion, be uniformly mixed 30 minutes and obtain described a kind of plant component fabric softener.
The product prepared by above-described embodiment carries out bacteriostatic experiment and organoleptic test.
Ten product labellings method described in embodiment prepared are embodiment one to ten, and the softener that in a kind of marine biological sterilization fabric softener disclosed in Chinese invention patent CN103046335B, described in embodiment 6, method prepares is denoted as control group.
By above-mentioned 11 softener product dilute with waters 20 times, soaking at room temperature clothing, adds up its fungistatic effect.
Table one: to colibacillary fungistatic effect
Described data all represent with average ± variance form.
Table two: to the fungistatic effect of Staphylococcus aureus ball
Described data all represent with average ± variance form.
Organoleptic detection: (test specimen: cotton towel), by 11 product dilute with waters, 20 times of post processing test specimens, to its sense of touch, bulking intensity, fragrance comfort level, carry out evaluation marking, each sensory evaluation total score is 10 points, full marks 30 points.
Table three: sense of touch is marked
| Bulking intensity | Compliance | Fragrance comfort level | Total score | |
| Embodiment one | 9.36±0.44 | 9.39±0.05 | 9.44±0.24 | 28.19±0.56 |
| Embodiment two | 9.43±0.40 | 9.39±0.01 | 9.33±0.49 | 28.15±1.39 |
| Embodiment three | 9.34±0.01 | 9.51±0.13 | 9.40±0.50 | 28.25±1.38 |
| Embodiment four | 9.30±0.04 | 9.47±0.41 | 9.46±0.44 | 28.23±1.40 |
| Embodiment five | 9.40±0.34 | 9.40±0.15 | 9.37±0.48 | 28.17±1.62 |
| Embodiment six | 9.55±0.35 | 9.51±0.28 | 9.37±0.26 | 28.43±1.39 |
| Embodiment seven | 9.42±0.23 | 9.54±0.21 | 9.57±0.31 | 28.53±1.56 |
| Embodiment eight | 9.37±0.21 | 9.40±0.04 | 9.59±0.12 | 28.36±1.58 |
| Embodiment nine | 9.47±0.20 | 9.35±0.05 | 9.33±0.50 | 28.15±1.75 |
| Embodiment ten | 9.51±0.04 | 9.97±0.12 | 9.27±0.16 | 28.75±1.32 |
| Control group | 9.04±0.22 | 9.11±0.42 | 9.23±0.21 | 27.38±0.67 |
Described data all represent with average ± variance form.
The embodiment of the present invention is low compared with the content of its ester based quaternary ammonium salt of control group and essence, sense of touch after its test specimen process, bulking intensity, fragrance comfort level are marked simultaneously, mark higher, more obvious to the fungistatic effect of Escherichia coli and staphylococcus aureus, soak Escherichia coli and the staphylococcus aureus that within 2 minutes, just can suppress more than 99%, soak and just 100% can suppress the activity of this two strains bacterium in 4 minutes.
Above content is only better embodiment of the present invention, and for those of ordinary skill in the art, according to thought of the present invention, all will change in specific embodiments and applications, this description should not be construed as limitation of the present invention.
Claims (7)
1. a novel plant component fabric softener, is characterized in that, comprises the component of following parts by weight:
Plants antimicrobial submissive extract 1-4 part, ester based quaternary ammonium salt 0.5-1 part, essence 0.5-1 part, citric acid 5-7 part, distilled water 100-120 part;
The submissive extract of described plants antimicrobial has been prepared by following operating procedure:
The first step: pulverize after being dried by green tea tea grounds, adds green tea slag powder weight 5-10 glycerine doubly in green tea tea grounds powder, and vacuum and low temperature stirs 10-15 hour;
Second step: olive oil is mixed with aloe pulp and pulls an oar; Mixed weight 5 times of NaOH aqueous slkalis are added, stand at low temperature after agitating heating 5-7 hour, removing top layer and the insoluble composition of bottom in aloe mixing making beating liquid;
3rd step: the component first step and second step prepared is according to weight ratio 1:2-3 mixing and stirring, and it is neutral for adding hydrochloric acid solution adjust ph, and after leaving standstill, removing insoluble solids is collected liquid part and obtained the submissive extract of plants antimicrobial.
2. a kind of novel plant component fabric softener according to claim 1, is characterized in that, comprise the component of following parts by weight:
Plants antimicrobial submissive extract 3-4 part, ester based quaternary ammonium salt 0.5-0.8 part, essence 0.5-0.6 part, citric acid 5-7 part, distilled water 100-120 part.
3. a kind of novel plant component fabric softener according to claim 1, is characterized in that: the submissive extract of described plants antimicrobial is prepared in the first step, adds green tea slag powder weight 8-10 glycerine doubly in green tea tea grounds powder.
4. a kind of novel plant component fabric softener according to claim 1, is characterized in that: the submissive extract of described plants antimicrobial is prepared vacuum and low temperature in the first step and stirred 12-15 hour.
5. a kind of novel plant component fabric softener according to claim 1, is characterized in that: the submissive extract of described plants antimicrobial is prepared in second step olive oil and aloe pulp to mix according to weight ratio 1:20-22 and pulled an oar.
6. a kind of novel plant component fabric softener according to claim 1, is characterized in that: the molar concentration that the submissive extract of described plants antimicrobial prepares NaOH aqueous slkali in second step is 2mol/L.
7. a kind of novel plant component fabric softener according to claim 1, is characterized in that: the mass fraction that the submissive extract of described plants antimicrobial prepares hydrochloric acid solution in the 3rd step is 35-37%.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106833995A (en) * | 2017-03-04 | 2017-06-13 | 黄胜华 | The antibacterial laundry soap of infant plant and its production method |
| CN106906084A (en) * | 2017-03-04 | 2017-06-30 | 黄胜华 | Infant's Antibacterial laundry detergent and its production method |
| CN107177981A (en) * | 2016-03-11 | 2017-09-19 | 广州奥蓓斯化妆品有限公司 | Fabric softener and its production method |
| CN107354729A (en) * | 2017-05-26 | 2017-11-17 | 安徽肤彩生物科技有限公司 | A kind of natural plant fabric softener |
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| CN104560432A (en) * | 2013-10-15 | 2015-04-29 | 天津一橙垄达环保科技开发有限公司 | Plant-type fabric softening and cleaning agent |
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| CN103046335A (en) * | 2011-12-15 | 2013-04-17 | 青岛海芬海洋生物科技有限公司 | Marine biological antibacterial fabric softener and preparation method thereof |
| CN103409990A (en) * | 2013-08-02 | 2013-11-27 | 东华大学 | Finishing agent used for infant red butt hygiene care as well as preparation method and application thereof |
| CN104514143A (en) * | 2013-09-27 | 2015-04-15 | 青岛畅绿生物研究所 | Water lily woolen textile softener |
| CN104560432A (en) * | 2013-10-15 | 2015-04-29 | 天津一橙垄达环保科技开发有限公司 | Plant-type fabric softening and cleaning agent |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107177981A (en) * | 2016-03-11 | 2017-09-19 | 广州奥蓓斯化妆品有限公司 | Fabric softener and its production method |
| CN106833995A (en) * | 2017-03-04 | 2017-06-13 | 黄胜华 | The antibacterial laundry soap of infant plant and its production method |
| CN106906084A (en) * | 2017-03-04 | 2017-06-30 | 黄胜华 | Infant's Antibacterial laundry detergent and its production method |
| CN107354729A (en) * | 2017-05-26 | 2017-11-17 | 安徽肤彩生物科技有限公司 | A kind of natural plant fabric softener |
| CN107354729B (en) * | 2017-05-26 | 2019-03-15 | 安徽肤彩生物科技有限公司 | A kind of natural plant fabric softener |
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Application publication date: 20151202 |