CN106283644A - A kind of footgear antibacterial and deodouring finishing agent and preparation method thereof - Google Patents
A kind of footgear antibacterial and deodouring finishing agent and preparation method thereof Download PDFInfo
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- CN106283644A CN106283644A CN201610719877.5A CN201610719877A CN106283644A CN 106283644 A CN106283644 A CN 106283644A CN 201610719877 A CN201610719877 A CN 201610719877A CN 106283644 A CN106283644 A CN 106283644A
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- antibacterial
- ethanol
- finishing agent
- footgear
- ethanol extraction
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
- A41B11/00—Hosiery; Panti-hose
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention provides a kind of footgear antibacterial and deodouring finishing agent and preparation method thereof.Preparation method is as follows: (1) chitosan, acetic acid, high purity water, after stirring 10 30 minutes, stands and waits froth breaking at temperature 20 40 DEG C;(2) Herba Artemisiae Scopariae ethanol extraction, Folium Salicis Babylonicae ethanol extraction, sorbitan monooleate, coco betaine are added, stir 30 60 minutes (3) and add decanol, Herba Pogostemonis ethanol extraction, Rhizoma Zingiberis Recens ether extract, Fructus Amomi Rotundus 30wt% ethanol-water extraction thing, essence, ultrasonic shear 40 60 minutes, obtains antibacterial and deodouring finishing agent.Antibacterial and deodouring composition used in the present invention is natural animal-plant and extracts, and all has the effect of good antibacterial and deodouring.
Description
Technical field
The present invention relates to the antibiotic finish technology of footgear, be specifically related to a kind of footgear antibacterial and deodouring finishing agent and preparation thereof
Method.
Background technology
The antibacterial and deodouring of footgear is necessary for foot health.Most antibacterial shoe material is still by antibacterial
Agent arranges in various footwear material by the method for Final finishing, gives footwear with antibiotic property.At present, can be by antibacterial and aromatic
It is organized in footwear material, while suppression foot fungus, it is also possible to hide the stink of footwear intracavity, meet people to antibacterial guarantor simultaneously
The demand of strong footwear, increases value-added content of product.Most organic antibacterial agent is harmful, and organic antibacterial agent exists
About 100 DEG C meeting Deformation partition, lose antibacterial action, the therefore safety in utilization of organic anti-bacterial, Durability of antimicrobial effect, antibacterial spectrum
The aspect Shortcomings such as property and thermostability, has been rarely employed.In natural antibacterial agent, chitosan print has the light of excellence
Spectrum antibiotic property, simultaneously sucting wet air permeability, degradability, biological activity etc., its aboundresources, pollution-free in addition, the most extensively should
In antibiotic finish of the fabric.But chitosan class antibacterial can only suppress the generation of harmful bacteria to fiber own, it is difficult to susceptible
The skin of dye has bactericidal action.Make finishing agent with Chinese herbal medicine baicalin and chitosan wool fabric is processed, knit after arrangement
Thing to escherichia coli, staphylococcus aureus, bacillus subtilis antibiotic rate all more than 92%, to golden yellow Portugal after washing 20 times
Grape coccus antibiotic rate is still more than 80%, and substantially maintains the original style of fabric, also has bacteriostasis in addition to fungus.Therefore
Chinese medicine extract and chitosan are combined, the antibacterial ability of fabric can be improved.While antibacterial, footgear is carried out deodorization whole
Reason, arrives health care.
Summary of the invention
Solve the technical problem that: it is an object of the invention to provide a kind of footgear antibacterial and deodouring finishing agent, use Chinese medicine
Extract and chitosan combines, except suppressing the generation of the harmful bacteria of fiber own, skin infection is had bactericidal action simultaneously, and
There is the effect of durable antibiotic;Deodorization is played, it is achieved health care while sterilization.
Technical scheme: a kind of footgear antibacterial and deodouring finishing agent, is prepared from by weight by following component: chitosan
0.05-0.12 part, acetic acid 0.5-1.2 part, Herba Artemisiae Scopariae ethanol extraction 0.1-0.5 part, Folium Salicis Babylonicae ethanol extraction 0.2-0.8 part, mistake
Water sorbitan oleate 4-8 part, coco betaine 4-8 part, decanol 0.05-0.15 part, Herba Pogostemonis ethanol extraction 0.05-0.15
Part, Rhizoma Zingiberis Recens ether extract 0.05-0.15 part, Fructus Amomi Rotundus 30wt% ethanol-water extraction thing 0.5-1.5 part, essence 2-6 part, high-purity
Water 100-150 part.
It is further preferred that described a kind of footgear antibacterial and deodouring finishing agent, following component prepare by weight and
Become: chitosan 0.07-0.1 part, acetic acid 0.7-1.1 part, Herba Artemisiae Scopariae ethanol extraction 0.25-0.45 part, Folium Salicis Babylonicae ethanol extraction
0.4-0.6 part, sorbitan monooleate 5-7 part, coco betaine 5-7 part, decanol 0.08-0.12 part, Herba Pogostemonis ethanol carry
Take thing 0.08-0.12 part, Rhizoma Zingiberis Recens ether extract 0.08-0.12 part, Fructus Amomi Rotundus 30wt% ethanol-water extraction thing 0.9-1.1 part, perfume (or spice)
Essence 3-5 part, high purity water 120-140 part.
The preparation method of above-mentioned footgear antibacterial and deodouring finishing agent comprises the following steps:
(1) chitosan, acetic acid, high purity water, after stirring 10-30 minute, stands and waits froth breaking at temperature 20-40 DEG C;
(2) Herba Artemisiae Scopariae ethanol extraction, Folium Salicis Babylonicae ethanol extraction, sorbitan monooleate, coco betaine are added, stirring
30-60 minute;
(3) decanol, Herba Pogostemonis ethanol extraction, Rhizoma Zingiberis Recens ether extract, Fructus Amomi Rotundus 30wt% ethanol-water extraction thing, essence are added, super
Sound wave is sheared 40-60 minute, obtains antibacterial and deodouring finishing agent.
Further, the preparation method of described a kind of footgear antibacterial and deodouring finishing agent, in described step (1), temperature is
30 minutes, mixing time was 15-25 minute.
Further, the preparation method of described a kind of footgear antibacterial and deodouring finishing agent, in described step (2) during stirring
Between be 35-45 minute.
Further, the preparation method of described a kind of footgear antibacterial and deodouring finishing agent, ultrasound wave in described step (3)
Shear 45-55 minute.
Beneficial effect: the footgear antibacterial and deodouring finishing agent of the present invention is except the life except suppressing the harmful bacteria of fiber own
Becoming, have bactericidal action simultaneously to skin infection, and have the effect of durable antibiotic, before washing, bacteriostasis rate reaches 98%, washes 20 times
Remaining to reach 90%, rate of descent is 8.2% later;Using the method test deodorizing effect of shoe pad spraying, optimal deodorization rate is permissible
Reach 95%, when Final finishing, more preferably deodorizing effect when directly will arrange with finishing agent, will be reached.
Detailed description of the invention
Embodiment 1
A kind of footgear antibacterial and deodouring finishing agent, is prepared from by weight by following component: chitosan 0.05 part, acetic acid 1.2
Part, Herba Artemisiae Scopariae ethanol extraction 0.1 part, Folium Salicis Babylonicae ethanol extraction 0.2 part, sorbitan monooleate 4 parts, coco betaine 8
Part, decanol 0.15 part, Herba Pogostemonis ethanol extraction 0.05 part, Rhizoma Zingiberis Recens ether extract 0.05 part, Fructus Amomi Rotundus 30wt% ethanol-water extraction
Thing 1.5 parts, 6 parts of essence, high purity water 100 parts.
The preparation method of above-mentioned footgear antibacterial and deodouring finishing agent is: (1) chitosan, acetic acid, high purity water, temperature 20 DEG C
After lower stirring 10 minutes, stand and wait froth breaking;(2) Herba Artemisiae Scopariae ethanol extraction, Folium Salicis Babylonicae ethanol extraction, anhydrous sorbitol oil are added
Acid esters, coco betaine, stir 30 minutes;(3) decanol, Herba Pogostemonis ethanol extraction, Rhizoma Zingiberis Recens ether extract, Fructus Amomi Rotundus are added
30wt% ethanol-water extraction thing, essence, ultrasonic shear 40 minutes, obtain antibacterial and deodouring finishing agent.
Embodiment 2
A kind of footgear antibacterial and deodouring finishing agent, is prepared from by weight by following component: chitosan 0.12 part, acetic acid 0.5
Part, Herba Artemisiae Scopariae ethanol extraction 0.5 part, Folium Salicis Babylonicae ethanol extraction 0.8 part, sorbitan monooleate 8 parts, coco betaine 4
Part, decanol 0.05 part, Herba Pogostemonis ethanol extraction 0.15 part, Rhizoma Zingiberis Recens ether extract 0.15 part, Fructus Amomi Rotundus 30wt% ethanol-water extraction
Thing 0.5 part, 2 parts of essence, high purity water 150 parts.
The preparation method of above-mentioned footgear antibacterial and deodouring finishing agent is: (1) chitosan, acetic acid, high purity water, temperature 40 DEG C
After lower stirring 30 minutes, stand and wait froth breaking;(2) Herba Artemisiae Scopariae ethanol extraction, Folium Salicis Babylonicae ethanol extraction, anhydrous sorbitol oil are added
Acid esters, coco betaine, stir 60 minutes;(3) decanol, Herba Pogostemonis ethanol extraction, Rhizoma Zingiberis Recens ether extract, Fructus Amomi Rotundus are added
30wt% ethanol-water extraction thing, essence, ultrasonic shear 60 minutes, obtain antibacterial and deodouring finishing agent.
Embodiment 3
A kind of footgear antibacterial and deodouring finishing agent, is prepared from by weight by following component: chitosan 0.07 part, acetic acid 0.7
Part, Herba Artemisiae Scopariae ethanol extraction 0.45 part, Folium Salicis Babylonicae ethanol extraction 0.4 part, sorbitan monooleate 7 parts, coco betaine 7
Part, decanol 0.12 part, Herba Pogostemonis ethanol extraction 0.12 part, Rhizoma Zingiberis Recens ether extract 0.12 part, Fructus Amomi Rotundus 30wt% ethanol-water extraction
Thing 1.1 parts, 5 parts of essence, high purity water 120 parts.
The preparation method of above-mentioned footgear antibacterial and deodouring finishing agent is: (1) chitosan, acetic acid, high purity water, temperature 40 DEG C
After lower stirring 15 minutes, stand and wait froth breaking;(2) Herba Artemisiae Scopariae ethanol extraction, Folium Salicis Babylonicae ethanol extraction, anhydrous sorbitol oil are added
Acid esters, coco betaine, stir 45 minutes;(3) decanol, Herba Pogostemonis ethanol extraction, Rhizoma Zingiberis Recens ether extract, Fructus Amomi Rotundus are added
30wt% ethanol-water extraction thing, essence, ultrasonic shear 45 minutes, obtain antibacterial and deodouring finishing agent.
Embodiment 4
A kind of footgear antibacterial and deodouring finishing agent, is prepared from by weight by following component: chitosan 0.1 part, acetic acid 1.1
Part, Herba Artemisiae Scopariae ethanol extraction 0.25 part, Folium Salicis Babylonicae ethanol extraction 0.6 part, sorbitan monooleate 5 parts, coco betaine 5
Part, decanol 0.08 part, Herba Pogostemonis ethanol extraction 0.08 part, Rhizoma Zingiberis Recens ether extract 0.08 part, Fructus Amomi Rotundus 30wt% ethanol-water extraction
Thing 0.9 part, 3 parts of essence, high purity water 140 parts.
The preparation method of above-mentioned footgear antibacterial and deodouring finishing agent is: (1) chitosan, acetic acid, high purity water, temperature 30 DEG C
After lower stirring 25 minutes, stand and wait froth breaking;(2) Herba Artemisiae Scopariae ethanol extraction, Folium Salicis Babylonicae ethanol extraction, anhydrous sorbitol oil are added
Acid esters, coco betaine, stir 35 minutes;(3) decanol, Herba Pogostemonis ethanol extraction, Rhizoma Zingiberis Recens ether extract, Fructus Amomi Rotundus are added
30wt% ethanol-water extraction thing, essence, ultrasonic shear 55 minutes, obtain antibacterial and deodouring finishing agent.
Embodiment 5
A kind of footgear antibacterial and deodouring finishing agent, is prepared from by weight by following component: chitosan 0.09 part, acetic acid 1 part,
Herba Artemisiae Scopariae ethanol extraction 0.35 part, Folium Salicis Babylonicae ethanol extraction 0.5 part, sorbitan monooleate 6 parts, coco betaine 6 parts,
Decanol 0.1 part, Herba Pogostemonis ethanol extraction 0.1 part, Rhizoma Zingiberis Recens ether extract 0.1 part, Fructus Amomi Rotundus 30wt% ethanol-water extraction thing 1 part,
4 parts of essence, high purity water 130 parts.
The preparation method of above-mentioned footgear antibacterial and deodouring finishing agent is: (1) chitosan, acetic acid, high purity water, temperature 30 DEG C
After lower stirring 20 minutes, stand and wait froth breaking;(2) Herba Artemisiae Scopariae ethanol extraction, Folium Salicis Babylonicae ethanol extraction, anhydrous sorbitol oil are added
Acid esters, coco betaine, stir 40 minutes;(3) decanol, Herba Pogostemonis ethanol extraction, Rhizoma Zingiberis Recens ether extract, Fructus Amomi Rotundus are added
30wt% ethanol-water extraction thing, essence, ultrasonic shear 50 minutes, obtain antibacterial and deodouring finishing agent.
Comparative example 1
A kind of footgear antibacterial and deodouring finishing agent, is prepared from by weight by following component: chitosan 0.05 part, acetic acid 1.2
Part, sorbitan monooleate 4 parts, coco betaine 8 parts, decanol 0.15 part, Herba Pogostemonis ethanol extraction 0.05 part, Rhizoma Zingiberis Recens second
Ether extract 0.05 part, Fructus Amomi Rotundus 30wt% ethanol-water extraction thing 1.5 parts, 6 parts of essence, high purity water 100 parts.
The preparation method of above-mentioned footgear antibacterial and deodouring finishing agent is: (1) chitosan, acetic acid, high purity water, temperature 20 DEG C
After lower stirring 10 minutes, stand and wait froth breaking;(2) add sorbitan monooleate, coco betaine, stir 30 minutes;
(3) decanol, Herba Pogostemonis ethanol extraction, Rhizoma Zingiberis Recens ether extract, Fructus Amomi Rotundus 30wt% ethanol-water extraction thing, essence, ultrasound wave are added
Shear 40 minutes, obtain antibacterial and deodouring finishing agent.
Comparative example 2
A kind of footgear antibacterial and deodouring finishing agent, is prepared from by weight by following component: chitosan 0.12 part, acetic acid 0.5
Part, Herba Artemisiae Scopariae ethanol extraction 0.5 part, Folium Salicis Babylonicae ethanol extraction 0.8 part, sorbitan monooleate 8 parts, coco betaine 4
Part, decanol 0.05 part, 2 parts of essence, high purity water 150 parts.
The preparation method of above-mentioned footgear antibacterial and deodouring finishing agent is: (1) chitosan, acetic acid, high purity water, temperature 40 DEG C
After lower stirring 30 minutes, stand and wait froth breaking;(2) Herba Artemisiae Scopariae ethanol extraction, Folium Salicis Babylonicae ethanol extraction, anhydrous sorbitol oil are added
Acid esters, coco betaine, stir 60 minutes;(3) add decanol essence, ultrasonic shear 60 minutes, obtain antibacterial and deodouring whole
Reason agent.
The property indices of material of the present invention see table, it may be seen that the footgear antibacterial and deodouring of the present invention arranges
Agent has the effect of durable antibiotic, and before washing, bacteriostasis rate reaches 98%, remains to reach 90% after washing 20 times, and rate of descent is
8.2%;Using the method test deodorizing effect of shoe pad spraying, optimal deodorization rate can reach 95%.
The table 1 footgear property indices of antibacterial and deodouring finishing agent
Note: being determined as of (1) bacteriostasis rate suppresses escherichia coli
(2) the method test deodorizing effect of shoe pad spraying is used.
Claims (6)
1. a footgear antibacterial and deodouring finishing agent, it is characterised in that be prepared from by weight by following component: chitosan
0.05-0.12 part, acetic acid 0.5-1.2 part, Herba Artemisiae Scopariae ethanol extraction 0.1-0.5 part, Folium Salicis Babylonicae ethanol extraction 0.2-0.8 part, mistake
Water sorbitan oleate 4-8 part, coco betaine 4-8 part, decanol 0.05-0.15 part, Herba Pogostemonis ethanol extraction 0.05-0.15
Part, Rhizoma Zingiberis Recens ether extract 0.05-0.15 part, Fructus Amomi Rotundus 30wt% ethanol-water extraction thing 0.5-1.5 part, essence 2-6 part, high-purity
Water 100-150 part.
A kind of footgear antibacterial and deodouring finishing agent the most according to claim 1, it is characterised in that by following component by weight
Part is prepared from: chitosan 0.07-0.1 part, acetic acid 0.7-1.1 part, Herba Artemisiae Scopariae ethanol extraction 0.25-0.45 part, Folium Salicis Babylonicae ethanol
Extract 0.4-0.6 part, sorbitan monooleate 5-7 part, coco betaine 5-7 part, decanol 0.08-0.12 part, Herba Pogostemonis
Ethanol extraction 0.08-0.12 part, Rhizoma Zingiberis Recens ether extract 0.08-0.12 part, Fructus Amomi Rotundus 30wt% ethanol-water extraction thing 0.9-
1.1 parts, essence 3-5 part, high purity water 120-140 part.
3. the footgear preparation method of antibacterial and deodouring finishing agent, it is characterised in that comprise the following steps:
(1) chitosan, acetic acid, high purity water, after stirring 10-30 minute, stands and waits froth breaking at temperature 20-40 DEG C;
(2) Herba Artemisiae Scopariae ethanol extraction, Folium Salicis Babylonicae ethanol extraction, sorbitan monooleate, coco betaine are added, stirring
30-60 minute;
(3) decanol, Herba Pogostemonis ethanol extraction, Rhizoma Zingiberis Recens ether extract, Fructus Amomi Rotundus 30wt% ethanol-water extraction thing, essence are added, super
Sound wave is sheared 40-60 minute, obtains antibacterial and deodouring finishing agent.
The preparation method of a kind of footgear antibacterial and deodouring finishing agent the most according to claim 3, it is characterised in that: described step
Suddenly in (1), temperature is 30 minutes, and mixing time is 15-25 minute.
The preparation method of a kind of footgear antibacterial and deodouring finishing agent the most according to claim 3, it is characterised in that: described step
Suddenly in (2), mixing time is 35-45 minute.
The preparation method of a kind of footgear antibacterial and deodouring finishing agent the most according to claim 3, it is characterised in that: described step
Suddenly ultrasonic shear 45-55 minute in (3).
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CN201610719877.5A CN106283644A (en) | 2016-08-25 | 2016-08-25 | A kind of footgear antibacterial and deodouring finishing agent and preparation method thereof |
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Cited By (4)
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CN108425241A (en) * | 2018-04-09 | 2018-08-21 | 海宁市依丽袜业有限公司 | A kind of preparation method of socks |
CN109251256A (en) * | 2018-10-11 | 2019-01-22 | 李宁 | Modified cyclodextrin and its application in compound bacteriostasis, and deodorization liquid |
CN109457474A (en) * | 2018-10-11 | 2019-03-12 | 李宁 | A kind of high-efficiency antimicrobial deodorant socks and preparation method thereof |
CN110269284A (en) * | 2019-05-24 | 2019-09-24 | 浙江玺润服饰有限公司 | A kind of antibacterial and deodorizing socks |
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CN104094979A (en) * | 2014-07-04 | 2014-10-15 | 李钟� | Willow leaf for preparing sanitizer |
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CN1803200A (en) * | 2006-01-19 | 2006-07-19 | 武汉理工大学 | Antibiotic and deodorant agent for shoes and socks |
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CN108425241A (en) * | 2018-04-09 | 2018-08-21 | 海宁市依丽袜业有限公司 | A kind of preparation method of socks |
CN109251256A (en) * | 2018-10-11 | 2019-01-22 | 李宁 | Modified cyclodextrin and its application in compound bacteriostasis, and deodorization liquid |
CN109457474A (en) * | 2018-10-11 | 2019-03-12 | 李宁 | A kind of high-efficiency antimicrobial deodorant socks and preparation method thereof |
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