CN103409990A - Finishing agent used for infant red butt hygiene care as well as preparation method and application thereof - Google Patents
Finishing agent used for infant red butt hygiene care as well as preparation method and application thereof Download PDFInfo
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- CN103409990A CN103409990A CN2013103355171A CN201310335517A CN103409990A CN 103409990 A CN103409990 A CN 103409990A CN 2013103355171 A CN2013103355171 A CN 2013103355171A CN 201310335517 A CN201310335517 A CN 201310335517A CN 103409990 A CN103409990 A CN 103409990A
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Abstract
The invention relates to a finishing agent used for infant red butt hygiene care as well as a preparation method and application thereof. The finishing agent comprises the following components in weight percent: 0.1-0.9% of antibacterial agent, 3-6% of plant extract, 0.4-0.7% of hydrophilic agent, and the balance of distilled water. The preparation method comprises the following steps: preparing a hydrophilic agent solution, and determining the critical micelle concentration by utilizing the density method; preparing a hydrophilic agent solution, and after treatment of non-woven fabric, testing hydrophilic performance of the non-woven fabric before and after hydrophilic treatment; adding the antibacterial agent and the plant extract into the hydrophilic agent solutions, so as to obtain the finishing agent. The application of the finishing agent is to obtain the non-woven fabric with hydrophilic, antibacterial and skin care functions through treatment of the non-woven fabric. According to the invention, the non-woven fabric has the hydrophilic, antibacterial and skin care functions, and plays an extremely significant role in prevention, improvement and treatment of red butts of an infant; the used raw materials are low in cost, easy to obtain, economic and environmentally friendly, and has no toxic or side effect to the human body; the used method is quick, simple, efficient, low in cost and convenient to operate.
Description
Technical field
The invention belongs to finishing agent and preparation thereof and Application Areas, particularly the red hip hygiene care of a kind of baby finishing agent and its preparation method and application.
Background technology
Non-weaving cloth also is nonwoven fabric, Nonwovens, referred to as nonwoven fabric.Be defined as: the combination of the fiber of orientation or random alignment by friction, obvolvent or bonding or these methods mutually combine thin slice, fibre web or the batts made (do not comprise paper and woven fabric, knitted fabric, tufteds, with stitch bonded fabrics and the wet method fulling milling felted terxture of stitching yarn).At hydrophobic non-weaving cloth, when namely abandoning hygienic material, especially during the baby paper diaper surface material, must carry out hydrophilic finiss to improve its hydrophily.
In environment for human survival, the microorganisms such as mould, fungi, saccharomycete and bacterium are ubiquitous.Under suitable condition, microorganism will breed and accumulate on non-weaving cloth, thereby produce niff, color spot and indecency outward appearance, and sometimes also can affect the function of product.In order effectively to suppress microorganism, transfer in nonwoven product, maintain good sanitary condition and living environment, antibiotic finish just has very important meaning.At present, produce antibacterial non-woven and mainly contain blending method, two kinds of methods of finishing method.
Therefore, process nonwoven fabric by the mode of rear arrangement, make it have simultaneously hydrophilic and antibacterial functions, have very important significance for the red hip of control baby.
Summary of the invention
Technical problem to be solved by this invention is to provide the red hip hygiene care of a kind of baby finishing agent and its preparation method and application, this invention makes nonwoven fabric have simultaneously the function of hydrophilic, antibiotic and skin care, has very important significance for prevention, improvement and the red hip for the treatment of baby; The raw material that use are cheap and easy to get, and economic environmental protection, to human body nonhazardous or side effect; The method of using is quick, simple and direct, efficient, cheap and easy to operate.
The red hip hygiene care of a kind of baby of the present invention finishing agent, by mass percentage, finishing agent is composed of the following components: 0.1%～0.9% antiseptic, 3%～6% plant extracts, 0.4%～0.7% hydrophilizing agent, distilled water are surplus.
Described hydrophilizing agent is surfactant Lurol PP-12667(Galston scientific & technical corporation).
Described antiseptic is one or more in benzalkonium chloride, benzalkonium bromide, polyhexamethylene guanide, tannic acid.
Described plant extracts is one or more in green-tea extract, camomile extract, witch hazel extract, Honegsukle flower P.E, Indocalamus leaf extract, Radix Arnebiae extract, Gotu Kola P.E.
The red hip hygiene care of a kind of baby of the present invention preparation method of finishing agent comprises:
(1) preparation hydrophilizing agent solution, utilize densimetry to determine critical micelle concentration; Wherein hydrophilizing agent accounts for 0.1%～1% of distilled water mass fraction;
(2) preparation hydrophilizing agent solution, nonwoven fabric, after arranging, are tested the hydrophilicity of hydrophilic finiss front and back nonwoven fabric; Wherein hydrophilizing agent accounts for 0.4%～0.7% of distilled water mass fraction;
(3) antiseptic, plant extracts are added in hydrophilizing agent solution, obtain finishing agent.
Densimetry described in described step (1) is the density p of measuring the hydrophilizing agent solution of variable concentrations, draws out the relation curve of density p and concentration C, can roughly obtain critical micelle concentration by determining the flex point on curve.
In described step (2), test the hydrophilicity of hydrophilic finiss front and back nonwoven fabric by contact angle experiments, contact angle tester model is DSA30.
The red hip hygiene care of a kind of baby, with the application of finishing agent, is processed nonwoven fabric by dipping, roller coat, sprinkling or foam method with finishing agent, obtains having the nonwoven fabric of the function of hydrophilic, antibiotic and skin care.
The present invention adopts the vibrations flask method to carry out antibacterial experiment, and test strain is Escherichia coli and staphylococcus aureus.
Finishing agent formula of the present invention comprises hydrophilizing agent, antiseptic and natural plant extracts, by the concentration of adjusting hydrophilizing agent and antiseptic, successfully make nonwoven fabric have simultaneously the function of hydrophilic, antibiotic and skin care, have very important significance for the red hip of control baby.
Beneficial effect
(1) the present invention makes nonwoven fabric have simultaneously the function of hydrophilic, antibiotic and skin care, has very important significance for prevention, improvement and the red hip for the treatment of baby;
(2) raw material used in the present invention are cheap and easy to get, and economic environmental protection, to human body nonhazardous or side effect;
(3) method used in the present invention is quick, simple and direct, efficient, cheap and easy to operate.
The accompanying drawing explanation
Fig. 1 is the density p of variable concentrations hydrophilizing agent solution of embodiment 1～5, Comparative Examples 1 gained and the graph of relation of concentration C;
Fig. 2 is nonwoven fabric contact angle experiments photo after the hydrophilic finiss of embodiment 1～5, Comparative Examples 1 gained;
Fig. 3 is the stereoscan photograph of non-woven fabrics fiber after the hydrophilic finiss of embodiment 1～5, Comparative Examples 1 gained;
Fig. 4 is the survival rate column diagram of staphylococcus aureus under the different antiseptic concentration of embodiment 1～5, Comparative Examples 1 gained;
Fig. 5 is colibacillary survival rate column diagram under the different antiseptic concentration of embodiment 1～5, Comparative Examples 1 gained.
The specific embodiment
Below in conjunction with specific embodiment, further set forth the present invention.Should be understood that these embodiment only are not used in and limit the scope of the invention be used to the present invention is described.Should be understood that in addition those skilled in the art can make various changes or modifications the present invention after the content of having read the present invention's instruction, these equivalent form of values fall within the application's appended claims limited range equally.
(1) compound concentration is 0.1%, 0.2%, 0.3%, 0.4%, 0.5%, 0.6%, 0.7%, 0.8%, 0.9% and 1% hydrophilizing agent solution respectively, measures the density of variable concentrations solution, and result as shown in Figure 1;
(2) compound concentration is 0.4%, 0.5%, 0.6%, 0.7% solution respectively, nonwoven fabric through after arrange after 90 ℃ dry 5min.Non-woven fabrics fiber after hydrophilic finiss is characterized, and result as shown in Figure 2 and Figure 3;
(3) compound concentration is 0.4% solution, then in solution, adds 0.1% antiseptic, 6% plant extracts;
(4) weighing 0.80g puts into through the nonwoven fabric arranged later the conical flask that contains 80ml LB culture medium, and 121 ℃ sterilizing 20 minutes.In triangular flask, inoculate respectively Escherichia coli and staphylococcus aureus, 24h is cultivated in concussion, and every 12h takes a sample once, metric measurement optical density OD
550, result as shown in Figure 4, Figure 5.
(1) compound concentration is 0.1%, 0.2%, 0.3%, 0.4%, 0.5%, 0.6%, 0.7%, 0.8%, 0.9% and 1% hydrophilizing agent solution respectively, measures the density of variable concentrations solution, and result as shown in Figure 1;
(2) compound concentration is 0.4%, 0.5%, 0.6%, 0.7% solution respectively, after nonwoven fabric, arranges latter 90 ℃ and dries 5min.Non-woven fabrics fiber after hydrophilic finiss is characterized, and result as shown in Figure 2 and Figure 3;
(3) compound concentration is 0.4% solution, then in solution, adds 0.3% antiseptic, 6% plant extracts;
(4) weighing 0.80g puts into through the nonwoven fabric arranged later the conical flask that contains 80ml LB culture medium, and 121 ℃ sterilizing 20 minutes.In triangular flask, inoculate respectively Escherichia coli and staphylococcus aureus, 24h is cultivated in concussion, and every 12h takes a sample once, metric measurement optical density OD
550, result as shown in Figure 4, Figure 5.
(1) respectively compound concentration be and 0.1%, 0.2%, 0.3%, 0.4%, 0.5%, 0.6%, 0.7%, 0.8%, 0.9% and 1% hydrophilizing agent solution, the density of measurement variable concentrations solution, and result is as shown in Figure 1;
(2) compound concentration is 0.4%, 0.5%, 0.6%, 0.7% solution respectively, nonwoven fabric through after arrange after 90 ℃ dry 5min.Non-woven fabrics fiber after hydrophilic finiss is characterized, and result as shown in Figure 2 and Figure 3;
(3) compound concentration is 0.4% solution, then in solution, adds 0.5% antiseptic, 6% plant extracts;
(4) weighing 0.80g puts into through the nonwoven fabric arranged later the conical flask that contains 80ml LB culture medium, and 121 ℃ sterilizing 20 minutes.In triangular flask, inoculate respectively Escherichia coli and staphylococcus aureus, 24h is cultivated in concussion, and every 12h takes a sample once, metric measurement optical density OD
550, result as shown in Figure 4, Figure 5.
Embodiment 4
(1) compound concentration is 0.1%, 0.2%, 0.3%, 0.4%, 0.5%, 0.6%, 0.7%, 0.8%, 0.9% and 1% hydrophilizing agent solution respectively, measures the density of variable concentrations solution, and result as shown in Figure 1;
(2) compound concentration is 0.4%, 0.5%, 0.6%, 0.7% solution respectively, nonwoven fabric through after arrange after 90 ℃ dry 5min.Non-woven fabrics fiber after hydrophilic finiss is characterized, and result as shown in Figure 2 and Figure 3;
(3) compound concentration is 0.4% solution, then in solution, adds 0.7% antiseptic, 6% plant extracts;
(4) weighing 0.80g puts into through the nonwoven fabric arranged later the conical flask that contains 80ml LB culture medium, and 121 ℃ sterilizing 20 minutes.In triangular flask, inoculate respectively Escherichia coli and staphylococcus aureus, 24h is cultivated in concussion, and every 12h takes a sample once, metric measurement optical density OD
550, result as shown in Figure 4, Figure 5.
(1) compound concentration is 0.1%, 0.2%, 0.3%, 0.4%, 0.5%, 0.6%, 0.7%, 0.8%, 0.9% and 1% hydrophilizing agent solution respectively, measures the density of variable concentrations solution, and result as shown in Figure 1;
(2) compound concentration is 0.4%, 0.5%, 0.6%, 0.7% solution respectively, nonwoven fabric through after arrange after 90 ℃ dry 5min.Non-woven fabrics fiber after hydrophilic finiss is characterized, and result as shown in Figure 2 and Figure 3;
(3) compound concentration is 0.4% solution, then in solution, adds 0.9% antiseptic, 6% plant extracts;
(4) weighing 0.80g puts into through the nonwoven fabric arranged later the conical flask that contains 80ml LB culture medium, and 121 ℃ sterilizing 20 minutes.In triangular flask, inoculate respectively Escherichia coli and staphylococcus aureus, 24h is cultivated in concussion, and every 12h takes a sample once, metric measurement optical density OD
550, result as shown in Figure 4, Figure 5.
Comparative Examples 1
(1) compound concentration is 0.1%, 0.2%, 0.3%, 0.4%, 0.5%, 0.6%, 0.7%, 0.8%, 0.9% and 1% hydrophilizing agent solution respectively, measures the density of variable concentrations solution, and result as shown in Figure 1;
(2) compound concentration is 0.4%, 0.5%, 0.6%, 0.7% solution respectively, nonwoven fabric through one soak one roll after 90 ℃ dry 5min.Non-woven fabrics fiber after hydrophilic finiss is characterized, and result as shown in Figure 2 and Figure 3;
(3) compound concentration is 0.4% solution, and weighing 0.80g puts into through the nonwoven fabric arranged later the conical flask that contains 80ml LB culture medium, and 121 ℃ sterilizing 20 minutes.In triangular flask, inoculate respectively Escherichia coli and staphylococcus aureus, 24h is cultivated in concussion, and every 12h takes a sample once, metric measurement optical density OD
550, result as shown in Figure 4, Figure 5.
Claims (8)
1. the red hip hygiene care of baby finishing agent, it is characterized in that: by mass percentage, finishing agent is composed of the following components: 0.1%～0.9% antiseptic, 3%～6% plant extracts, 0.4%～0.7% hydrophilizing agent, distilled water are surplus.
2. the red hip hygiene care of a kind of baby according to claim 1 finishing agent, it is characterized in that: described hydrophilizing agent is surfactant Lurol PP-12667.
3. the red hip hygiene care of a kind of baby according to claim 1 finishing agent, it is characterized in that: described antiseptic is one or more in benzalkonium chloride, benzalkonium bromide, polyhexamethylene guanide, tannic acid.
4. the red hip hygiene care of a kind of baby according to claim 1 finishing agent, it is characterized in that: described plant extracts is one or more in green-tea extract, camomile extract, witch hazel extract, Honegsukle flower P.E, Indocalamus leaf extract, Radix Arnebiae extract, Gotu Kola P.E.
5. the red hip hygiene care of a baby as described as claim 1-4 by the preparation method of finishing agent, comprising:
(1) preparation hydrophilizing agent solution, utilize densimetry to determine critical micelle concentration; Wherein hydrophilizing agent accounts for 0.1%～1% of distilled water mass fraction;
(2) preparation hydrophilizing agent solution, nonwoven fabric, after arranging, are tested the hydrophilicity of hydrophilic finiss front and back nonwoven fabric; Wherein hydrophilizing agent accounts for 0.4%～0.7% of distilled water mass fraction;
(3) antiseptic, plant extracts are added in hydrophilizing agent solution, obtain finishing agent.
6. the red hip hygiene care of a kind of baby according to claim 5 is by the preparation method of finishing agent, it is characterized in that: the densimetry described in described step (1) is the density p of measuring the hydrophilizing agent solution of variable concentrations, draw out the relation curve of density p and concentration C, can roughly obtain critical micelle concentration by determining the flex point on curve.
7. the red hip hygiene care of a kind of baby according to claim 5 is by the preparation method of finishing agent, it is characterized in that: in described step (2), test the hydrophilicity of hydrophilic finiss front and back nonwoven fabric by contact angle experiments, contact angle tester model is DSA30.
8. the red hip hygiene care of a baby as claimed in claim 1 with the application of finishing agent, is characterized in that: by dipping, roller coat, sprinkling or foam method, process nonwoven fabric with finishing agent, obtain having the nonwoven fabric of the function of hydrophilic, antibiotic and skin care.
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104606552A (en) * | 2015-02-09 | 2015-05-13 | 山东三星玉米产业科技有限公司 | Rice bran oil as well as preparation method and application thereof |
| CN105113224A (en) * | 2015-09-08 | 2015-12-02 | 湖州新创丝织品有限公司 | Novel plant component clothing softener |
| CN105168321A (en) * | 2015-09-08 | 2015-12-23 | 湖州市菱湖重兆金辉丝织厂 | Lithospermum erythrorhizon-based pure vegetable diaper rash prevention lotion and infant wet tissue thereof |
| CN105854067A (en) * | 2016-03-28 | 2016-08-17 | 福建鼻涕虫婴儿用品有限公司 | Buttock-protecting chamomile paper diaper core and preparation method thereof, and buttock-protecting paper diaper with chamomile core |
| CN106012511A (en) * | 2016-05-16 | 2016-10-12 | 福建冠泓工业有限公司 | Aloe hydrophilic oil agent solution, preparing method and skin-friendly non-woven fabric |
| CN106176342A (en) * | 2016-07-08 | 2016-12-07 | 浙江优全护理用品科技有限公司 | A kind of prevention baby's red hip baby's special health wet tissue and preparation method thereof |
| CN106943454A (en) * | 2017-03-30 | 2017-07-14 | 黑龙江童医生儿童生物制药有限公司 | A kind of disposable antibacterial spraying of plant type and preparation method thereof |
| CN108815556A (en) * | 2018-06-04 | 2018-11-16 | 湖北研妆实业有限公司 | A kind of paper diaper with the red hip function of prevention |
| CN112726199A (en) * | 2020-12-28 | 2021-04-30 | 福建冠泓工业有限公司 | Cool skin-friendly non-woven fabric and preparation method thereof |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104606552A (en) * | 2015-02-09 | 2015-05-13 | 山东三星玉米产业科技有限公司 | Rice bran oil as well as preparation method and application thereof |
| CN105113224A (en) * | 2015-09-08 | 2015-12-02 | 湖州新创丝织品有限公司 | Novel plant component clothing softener |
| CN105168321A (en) * | 2015-09-08 | 2015-12-23 | 湖州市菱湖重兆金辉丝织厂 | Lithospermum erythrorhizon-based pure vegetable diaper rash prevention lotion and infant wet tissue thereof |
| CN105854067A (en) * | 2016-03-28 | 2016-08-17 | 福建鼻涕虫婴儿用品有限公司 | Buttock-protecting chamomile paper diaper core and preparation method thereof, and buttock-protecting paper diaper with chamomile core |
| CN105854067B (en) * | 2016-03-28 | 2019-03-26 | 福建鼻涕虫婴儿用品有限公司 | The preparation method and chamomile core hip pad paper diaper of chamomile hip pad paper diaper core |
| CN106012511A (en) * | 2016-05-16 | 2016-10-12 | 福建冠泓工业有限公司 | Aloe hydrophilic oil agent solution, preparing method and skin-friendly non-woven fabric |
| CN106176342A (en) * | 2016-07-08 | 2016-12-07 | 浙江优全护理用品科技有限公司 | A kind of prevention baby's red hip baby's special health wet tissue and preparation method thereof |
| CN106943454A (en) * | 2017-03-30 | 2017-07-14 | 黑龙江童医生儿童生物制药有限公司 | A kind of disposable antibacterial spraying of plant type and preparation method thereof |
| CN108815556A (en) * | 2018-06-04 | 2018-11-16 | 湖北研妆实业有限公司 | A kind of paper diaper with the red hip function of prevention |
| CN112726199A (en) * | 2020-12-28 | 2021-04-30 | 福建冠泓工业有限公司 | Cool skin-friendly non-woven fabric and preparation method thereof |
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Application publication date: 20131127 |