CN105106061A - Traditional Chinese medicine toothpaste containing calamine - Google Patents
Traditional Chinese medicine toothpaste containing calamine Download PDFInfo
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- CN105106061A CN105106061A CN201510525986.9A CN201510525986A CN105106061A CN 105106061 A CN105106061 A CN 105106061A CN 201510525986 A CN201510525986 A CN 201510525986A CN 105106061 A CN105106061 A CN 105106061A
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Abstract
The invention discloses traditional Chinese medicine toothpaste containing calamine. The traditional Chinese medicine toothpaste comprises the following raw materials in percentage by weight: 0.1-2% of calamine and 5-8% of traditional Chinese medicine extracting solution. The traditional Chinese medicine extracting solution is prepared from the following raw herbal materials in part by weight: 12-18 parts of radix glycyrrhizae, 12-18 parts of radix scutellariae and 8-12 parts of radix ophiopogonis. The traditional Chinese medicine toothpaste has effects of preventing oral ulcer and relieving symptoms of oral ulcer.
Description
Technical field
The present invention and toothpaste preparation field, especially a kind of Chinese medicinal toothpaste containing Calamina.
Background technology
Oral ulcer is commonly called as " aphtha ", is a kind of common ulcerative damages disease betiding oral mucosa, is more common in inside lip, the position such as tongue, tongue abdomen, cheek mucosa, vestibule ditch, soft palate, the mucosa at these positions lack keratinization layer or keratinization poor; Tongue ulcer refers to the oral ulcer betiding tongue, tongue abdominal part position; Sharp ache during oral ulcer outbreak, local causalgia is obvious, and severe patient also can affect diet, speak, and causes very big inconvenience to daily life; Can the General Symptoms such as concurrent halitosis, chronic pharyngitis, constipation, headache, dizziness, nauseating, weak, irritated, heating, lymphadenectasis; The Therapeutic Method of current oral ulcer normally adopts spray, or oral medicine, but oral ulcer often easily repeatedly, and spray and oral medicine cannot play the effect of prevention and therapy simultaneously.
Toothpaste is cleaning supplies conventional in daily life, if can preventing canker sore and the functional component alleviating oral ulcer symptom be added in toothpaste, so to the oral health of people by of great advantage.
Summary of the invention
The invention provides a kind of containing Calamina Chinese medicinal toothpaste, there is effect of preventing canker sore and alleviation oral ulcer symptom, and natural non-stimulated.
For achieving the above object, technical scheme of the present invention is:
Containing a Chinese medicinal toothpaste for Calamina, it is characterized in that:
Be made up of the raw material of following percentage by weight:
Calamina 0.1 ~ 2%
Chinese medicine extraction liquid 5 ~ 8%;
Stone powder 40 ~ 45%;
Sorbitol 23 ~ 30%;
Glycerol 2 ~ 5%;
Sodium lauryl sulphate 2 ~ 3%;
Binding agent 0.8 ~ 2%;
Saccharin sodium 0.1 ~ 0.3%;
Tertiary sodium phosphate 0.2 ~ 0.6%;
Essence 1 ~ 1.5%;
Water surplus;
Wherein, described Chinese medicine extraction liquid and preparation method thereof is:
(1) by following raw material of Chinese medicine by weight ratio: 12 ~ 18 parts, Radix Glycyrrhizae, Radix Scutellariae 12 ~ 18 parts, Radix Ophiopogonis 8 ~ 12 parts; After preparing, raw material of Chinese medicine is pulverized;
(2) raw material of Chinese medicine is dropped into 70% ethanol of 5 ~ 6 times of weight, heating and refluxing extraction 2 times, each extraction time is 1h, merges extracted twice liquid;
(3) 2 times that extracting solution are concentrated into Chinese medicine weight obtain Chinese medicine extraction liquid.
Further, in above-mentioned steps (1), raw material of Chinese medicine is by weight ratio: 15 parts, Radix Glycyrrhizae, Radix Scutellariae 15 parts, Radix Ophiopogonis 10 parts.
Containing a Chinese medicinal toothpaste preparation method for Calamina, it is characterized in that comprising the following steps:
(1) in cream tank processed, drop into stone powder, sodium lauryl sulphate, sodium carboxymethyl cellulose, carrageenan, saccharin sodium and tertiary sodium phosphate, stir, obtain powder A;
(2) by Calamina and sorbitol, G & W premix, suspension A is obtained;
(3) in powder A, drop into suspension A, shut cream tank processed, open vacuum pump, open scraper and agitator stirring, drop into Chinese medicine extraction liquid after 30 minutes, after 10 minutes, add essence, stir 5 minutes, close agitator, scraper successively, vacuum breaker, stops vacuum pump, makes after sampling detection is qualified.
Containing a Chinese medicinal toothpaste for Calamina, it is characterized in that:
Be made up of the raw material of following percentage by weight:
Calamina 0.1 ~ 2%
Chinese medicine extraction liquid 5 ~ 8%;
Silicon dioxide 25 ~ 35%;
Sorbitol 20 ~ 35%;
Glycerol 8 ~ 10%;
Sodium lauryl sulphate 2 ~ 3%;
Binding agent 0.8 ~ 2%;
Saccharin sodium 0.1 ~ 0.3%;
Tertiary sodium phosphate 0.1 ~ 0.5%;
Essence 1 ~ 1.5%;
Water surplus;
Wherein, the preparation method of described Chinese medicine extraction liquid is:
(1) by following raw material of Chinese medicine by weight ratio: 12 ~ 18 parts, Radix Glycyrrhizae, Radix Scutellariae 12 ~ 18 parts, Radix Ophiopogonis 8 ~ 12 parts; After preparing, raw material of Chinese medicine is pulverized;
(2) raw material of Chinese medicine is dropped into 70% ethanol of 5 ~ 6 times of weight, heating and refluxing extraction 2 times, each extraction time is 1h, merges extracted twice liquid;
(3) 2 times that extracting solution are concentrated into Chinese medicine weight obtain Chinese medicine extraction liquid.
Further, in above-mentioned steps (1), raw material of Chinese medicine is by weight ratio: 15 parts, Radix Glycyrrhizae, Radix Scutellariae 15 parts, Radix Ophiopogonis 10 parts.
Containing a Chinese medicinal toothpaste preparation method for Calamina, it is characterized in that comprising the following steps:
(1) in cream tank processed, drop into silicon dioxide, sodium lauryl sulphate, guar gum, carrageenan, saccharin sodium and tertiary sodium phosphate, stir, obtain powder material B;
(2) by Calamina and sorbitol, G & W premix, suspension B is obtained;
(3) in powder material B, drop into suspension B, shut cream tank processed, open vacuum pump, open scraper and agitator stirring, drop into Chinese medicine extraction liquid after 30 minutes, after 10 minutes, add essence, stir 5 minutes, close agitator, scraper successively, vacuum breaker, stops vacuum pump, makes after sampling detection is qualified.
The above-described Chinese medicinal toothpaste containing Calamina, comprise Calamina, Radix Glycyrrhizae, Radix Scutellariae and Radix Ophiopogonis four kinds of Chinese medicine ingredients, wherein:
Calamina: property is sweet, flat, taste is micro-puckery, and return stomach warp, function cures mainly: removing toxic substances improving acuity of vision and removing nebula, the antipruritic sore of removing dampness; For conjunctival congestion and swelling pain, marginal blepharitis, nebula film bulbar conjunctiva polyp, ulcer being unable to heal, pus is dripping, eczema, skin pruritus.Main component is zinc carbonate, still containing small amounts calcium 0.27%, and magnesium oxide 0.45%, ferrum oxide 0.58%, manganese oxide 0.01%.Zinc in this stone, often by a small amount of ferrum (bivalence) is replaced.In addition, some Calamina kinds are still containing germanium and the indium of a small amount of brill, copper, cadmium, lead and trace.Record according to " modern Practical Chinese medicinal ": " for the not easily closing in person of chronic ulcer, lower leg ulcer, have the merit of erosion prevention and muscle growing."
Radix Glycyrrhizae: property is sweet, flat; There is invigorating the spleen and replenishing QI, nourishing the lung to arrest cough, eliminating fire and detoxication, relieving spasm to stop pain, antiinflammatory, antianaphylactic effect; Radix Scutellariae: bitter in the mouth, cold in nature, has heat clearing and damp drying, eliminating fire and detoxication, hemostasis, the effect such as antiabortive.Cure mainly the diseases such as epidemic febrile disease, upper respiratory tract infection, cough due to lung-heat, damp and hot jaundice, pneumonia, dysentery, hemoptysis, conjunctival congestion, frequent fetal movement, hypertension, carbuncle furuncle; Radix Ophiopogonis: property is sweet, micro-hardship, is slightly cold; YIN nourishing and the production of body fluid promoting, lung moistening clears away heart-fire; For dryness of the lung dry cough, deficiency of YIN consumptive disease is coughed, sore throat pharyngalgia, and Tianjin wound is thirsty, and interior-heat is quenched one's thirst, vexed insomnia, dryness of the intestine constipation.
The present invention has the following advantages:
(1) select Calamina, Radix Glycyrrhizae, Radix Scutellariae and Radix Ophiopogonis four kinds of Chinese medicines, Calamina has convergence itching-relieving action, collaborative Radix Glycyrrhizae, Radix Scutellariae and Radix Ophiopogonis, there is the effect of good preventing canker sore and alleviation oral ulcer symptom, and Radix Glycyrrhizae taste is sweet, Radix Ophiopogonis promotes the production of body fluid, and can cover the astringent taste of Calamina preferably, avoids Calamina to affect the mouthfeel of toothpaste;
(2) toothpaste matrix formula and Chinese medicine extraction liquid, Calamina can stablize compatibility, and paste stability is good;
(3) toothpaste processing technology is simple, is applicable to the commercial production of scale.
Detailed description of the invention
Embodiment 1 and 2
The preparation of Chinese medicine extraction liquid:
(1) following raw material of Chinese medicine is taken by weight: 15 parts, Radix Glycyrrhizae, Radix Scutellariae 15 parts, Radix Ophiopogonis 10 parts; After preparing, raw material of Chinese medicine is pulverized;
(2) raw material of Chinese medicine is dropped into 70% ethanol of 6 times of weight, heating and refluxing extraction 2 times, each extraction time is 1h, merges extracted twice liquid;
(3) 2 times that extracting solution are concentrated into Chinese medicine weight obtain Chinese medicine extraction liquid.
Other mixed raw materials of Chinese medicine extraction liquid and toothpaste are become toothpaste, and the percentage by weight of each component is as follows:
Embodiment 3 and 4
The preparation of Chinese medicine extraction liquid:
(1) following raw material of Chinese medicine is taken by weight: 12 parts, Radix Glycyrrhizae, Radix Scutellariae 12 parts, Radix Ophiopogonis 12 parts; After preparing, raw material of Chinese medicine is pulverized;
(2) raw material of Chinese medicine is dropped into 70% ethanol of 5 times of weight, heating and refluxing extraction 2 times, each extraction time is 1h, merges extracted twice liquid;
(3) 2 times that extracting solution are concentrated into Chinese medicine weight obtain Chinese medicine extraction liquid.
Other mixed raw materials of Chinese medicine extraction liquid and toothpaste are become toothpaste, and the percentage by weight of each component is as follows:
Embodiment 5 and 6
The preparation of Chinese medicine extraction liquid:
(1) following raw material of Chinese medicine is taken by weight: 18 parts, Radix Glycyrrhizae, Radix Scutellariae 18 parts, Radix Ophiopogonis 8 parts; After preparing, raw material of Chinese medicine is pulverized;
(2) raw material of Chinese medicine is dropped into 75% ethanol of 6 times of weight, heating and refluxing extraction 2 times, each extraction time is 1h, merges extracted twice liquid;
(3) 2 times that extracting solution are concentrated into Chinese medicine weight obtain Chinese medicine extraction liquid.
Other mixed raw materials of Chinese medicine extraction liquid and toothpaste are become toothpaste, and the percentage by weight of each component is as follows:
| Raw material | Raw material weight degree (%) |
| Embodiment 5 | Embodiment 6 | |
| Calamina | 0.1 | 0.1 |
| Chinese medicine extraction liquid | 8 | 8 |
| Stone powder | 40 | 0 |
| Silicon dioxide | 0 | 25 |
| Sorbitol | 23 | 35 |
| Glycerol | 5 | 8 |
| Sodium lauryl sulphate | 2.5 | 2 |
| Sodium carboxymethyl cellulose | 0.8 | 0 |
| Guar gum | 0 | 0.3 |
| Carrageenan | 0.4 | 1 |
| Saccharin sodium | 0.25 | 0.25 |
| Tertiary sodium phosphate | 0.4 | 0.3 |
| Essence | 1 | 1 |
| Water | Surplus | Surplus |
The preparation method of embodiment 1,3 and 5 is:
(1) in cream tank processed, drop into stone powder, sodium lauryl sulphate, sodium carboxymethyl cellulose, carrageenan, saccharin sodium and tertiary sodium phosphate, stir, obtain powder A;
(2) by Calamina and sorbitol, G & W premix, suspension A is obtained;
(3) in powder A, drop into suspension A, shut cream tank processed, open vacuum pump, open scraper and agitator stirring, drop into Chinese medicine extraction liquid after 30 minutes, after 10 minutes, add essence, stir 5 minutes, close agitator, scraper successively, vacuum breaker, stops vacuum pump, makes after sampling detection is qualified.
The preparation method of embodiment 2,4 and 6 is:
(1) in cream tank processed, drop into silicon dioxide, sodium lauryl sulphate, guar gum, carrageenan, saccharin sodium and tertiary sodium phosphate, stir, obtain powder material B;
(2) by Calamina and sorbitol, G & W premix, suspension B is obtained;
(3) in powder material B, drop into suspension B, shut cream tank processed, open vacuum pump, open scraper and agitator stirring, drop into Chinese medicine extraction liquid after 30 minutes, after 10 minutes, add essence, stir 5 minutes, close agitator, scraper successively, vacuum breaker, stops vacuum pump, makes after sampling detection is qualified.
Clinical effectiveness is tested:
Test method: choose experimenter 350 people with oral ulcer symptom and test, each half of men and women, the age from 18 ~ 50 years old, 30 years old mean age, and the greatest length of experimenter's ulcer wound surface reaches more than 5mm; Experimenter is divided into 7 groups at random, use toothpaste (being added with Calamina and Chinese medicine extraction liquid) prepared by embodiment 1 ~ 6, a kind of with control sample, control sample is the toothpaste only on the market with common cleaning function, every morning, noon, evening respectively brush teeth once, Brushing time 5 minutes, brushes teeth before test, first records pain symptom and the oral ulcer situation of experimenter.
Brush teeth test after one day, and the pain of inspection experimenter slows down situation, and the canker sores situation of experimenter alleviates as effectively, and pain condition does not alleviate as invalid.
Brushed teeth test after four days, the oral ulcer recovery situation of inspection experimenter, and it is effectively that ulcer healing or ulcer area reduce more than 80%, otherwise is then invalid.
Check after experimenter uses four days, result is as follows:
Find out from result of the test, the toothpaste of embodiment 1 ~ 6 is to alleviating canker sore pain situation, helping the effective percentage of oral ulcer healing all higher than control sample, the effective percentage that embodiment 2 helps oral ulcer to heal can up to 88%, as can be seen here, the present invention has good effect to alleviation oral ulcer symptom.
Claims (6)
1., containing a Chinese medicinal toothpaste for Calamina, it is characterized in that:
Be made up of the raw material of following percentage by weight:
Calamina 0.1 ~ 2%
Chinese medicine extraction liquid 5 ~ 8%;
Stone powder 40 ~ 45%;
Sorbitol 23 ~ 30%;
Glycerol 2 ~ 5%;
Sodium lauryl sulphate 2 ~ 3%;
Binding agent 0.8 ~ 2%;
Saccharin sodium 0.1 ~ 0.3%;
Tertiary sodium phosphate 0.2 ~ 0.6%;
Essence 1 ~ 1.5%;
Water surplus;
Wherein, described Chinese medicine extraction liquid and preparation method thereof is:
(1) by following raw material of Chinese medicine by weight ratio: 12 ~ 18 parts, Radix Glycyrrhizae, Radix Scutellariae 12 ~ 18 parts, Radix Ophiopogonis 8 ~ 12 parts; After preparing, raw material of Chinese medicine is pulverized;
(2) raw material of Chinese medicine is dropped into 70% ethanol of 5 ~ 6 times of weight, heating and refluxing extraction 2 times, each extraction time is 1h, merges extracted twice liquid;
(3) 2 times that extracting solution are concentrated into Chinese medicine weight obtain Chinese medicine extraction liquid.
2. the Chinese medicinal toothpaste containing Calamina according to claim 1, is characterized in that:
In described step (1), raw material of Chinese medicine is by weight ratio: 15 parts, Radix Glycyrrhizae, Radix Scutellariae 15 parts, Radix Ophiopogonis 10 parts.
3. the Chinese medicinal toothpaste preparation method containing Calamina as claimed in claim 1 or 2, is characterized in that comprising the following steps:
(1) in cream tank processed, drop into stone powder, sodium lauryl sulphate, sodium carboxymethyl cellulose, carrageenan, saccharin sodium and tertiary sodium phosphate, stir, obtain powder A;
(2) by Calamina and sorbitol, G & W premix, suspension A is obtained;
(3) in powder A, drop into suspension A, shut cream tank processed, open vacuum pump, open scraper and agitator stirring, drop into Chinese medicine extraction liquid after 30 minutes, after 10 minutes, add essence, stir 5 minutes, close agitator, scraper successively, vacuum breaker, stops vacuum pump, makes after sampling detection is qualified.
4., containing a Chinese medicinal toothpaste for Calamina, it is characterized in that:
Be made up of the raw material of following percentage by weight:
Calamina 0.1 ~ 2%
Chinese medicine extraction liquid 5 ~ 8%;
Silicon dioxide 25 ~ 35%;
Sorbitol 20 ~ 35%;
Glycerol 8 ~ 10%;
Sodium lauryl sulphate 2 ~ 3%;
Binding agent 0.8 ~ 2%;
Saccharin sodium 0.1 ~ 0.3%;
Tertiary sodium phosphate 0.1 ~ 0.5%;
Essence 1 ~ 1.5%;
Water surplus;
Wherein, the preparation method of described Chinese medicine extraction liquid is:
(1) by following raw material of Chinese medicine by weight ratio: 12 ~ 18 parts, Radix Glycyrrhizae, Radix Scutellariae 12 ~ 18 parts, Radix Ophiopogonis 8 ~ 12 parts; After preparing, raw material of Chinese medicine is pulverized;
(2) raw material of Chinese medicine is dropped into 70% ethanol of 5 ~ 6 times of weight, heating and refluxing extraction 2 times, each extraction time is 1h, merges extracted twice liquid;
(3) 2 times that extracting solution are concentrated into Chinese medicine weight obtain Chinese medicine extraction liquid.
5. the Chinese medicinal toothpaste containing Calamina according to claim 4, is characterized in that:
In described step (1), raw material of Chinese medicine is by weight ratio: 15 parts, Radix Glycyrrhizae, Radix Scutellariae 15 parts, Radix Ophiopogonis 10 parts.
6. the Chinese medicinal toothpaste preparation method containing Calamina as described in claim 4 or 5, is characterized in that comprising the following steps:
(1) in cream tank processed, drop into silicon dioxide, sodium lauryl sulphate, guar gum, carrageenan, saccharin sodium and tertiary sodium phosphate, stir, obtain powder material B;
(2) by Calamina and sorbitol, G & W premix, suspension B is obtained;
(3) in powder material B, drop into suspension B, shut cream tank processed, open vacuum pump, open scraper and agitator stirring, drop into Chinese medicine extraction liquid after 30 minutes, after 10 minutes, add essence, stir 5 minutes, close agitator, scraper successively, vacuum breaker, stops vacuum pump, makes after sampling detection is qualified.
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| CN201510525986.9A CN105106061A (en) | 2015-08-26 | 2015-08-26 | Traditional Chinese medicine toothpaste containing calamine |
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| CN201510525986.9A CN105106061A (en) | 2015-08-26 | 2015-08-26 | Traditional Chinese medicine toothpaste containing calamine |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1554324A (en) * | 2003-09-24 | 2004-12-15 | 柳州两面针股份有限公司 | Chinese medicinal tooth-paste |
| CN102698122A (en) * | 2012-01-10 | 2012-10-03 | 刘霞 | Traditional Chinese medicinal composition for treating paradentitis, and preparation method and administration method thereof and toothpaste |
| CN103520049A (en) * | 2013-10-18 | 2014-01-22 | 柳州两面针股份有限公司 | Application of compound traditional Chinese medicine extracts in preparation of health care products for oral care |
| CN103520578A (en) * | 2013-10-25 | 2014-01-22 | 李佃场 | Traditional Chinese medicine composition for treating oral ulcer and preparation method thereof |
-
2015
- 2015-08-26 CN CN201510525986.9A patent/CN105106061A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1554324A (en) * | 2003-09-24 | 2004-12-15 | 柳州两面针股份有限公司 | Chinese medicinal tooth-paste |
| CN102698122A (en) * | 2012-01-10 | 2012-10-03 | 刘霞 | Traditional Chinese medicinal composition for treating paradentitis, and preparation method and administration method thereof and toothpaste |
| CN103520049A (en) * | 2013-10-18 | 2014-01-22 | 柳州两面针股份有限公司 | Application of compound traditional Chinese medicine extracts in preparation of health care products for oral care |
| CN103520578A (en) * | 2013-10-25 | 2014-01-22 | 李佃场 | Traditional Chinese medicine composition for treating oral ulcer and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 吴玉生等: "《常见病中医处方手册•第1版》", 31 August 2011, 化学工业出版社 * |
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Application publication date: 20151202 |