CN105088373A - Anti-bacterial fabric and preparation method thereof - Google Patents
Anti-bacterial fabric and preparation method thereof Download PDFInfo
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- CN105088373A CN105088373A CN201510594185.8A CN201510594185A CN105088373A CN 105088373 A CN105088373 A CN 105088373A CN 201510594185 A CN201510594185 A CN 201510594185A CN 105088373 A CN105088373 A CN 105088373A
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Abstract
The invention relates to anti-bacterial fabric and a preparation method thereof. The anti-bacterial fabric is mainly prepared from 82-85 parts of bamboo fibers, 2-4 parts of water-based amino acid modified polyurethane, 5-13 parts of acrylate polymer, 1-2 parts of nano-zinc oxide, 1-2 parts of nanometer jade powder, 2-5 parts of microporous lignocellulose and 0.5-1.5 parts of dispersing agents. The breathability of the textile fabric is smaller than 5 mm/s, and moisture transmission of the textile fabric is larger than or equal to 10,000 g/m<2>.d. After the fabric is washed and naturally aired 150 times, the breathability and moisture transmission are not obviously changed. In addition, the fabric is free from irritation to the skin of a human body, and is quite prominent in anti-bacterial and mould-proof function.
Description
Technical field
The present invention relates to knitted fabric and textile technical field, particularly relate to a kind of antibiotic facing material and preparation method.
Background technology
At present, due to the quickening of process of industrialization, global carbon dioxide discharge capacity increases severely, and the ozone layer in air is increasingly thin, and the uitraviolet intensity arriving ground increases year by year, and cutaneum carcinoma illness rate promotes greatly; Based on this, develop a kind of functional with practicality and the anti-ultraviolet function coating of depositing seems particularly important.Existing ultraviolet resistant is used for the processing of tent, curtain, umbrella, be generally and reach good UVResistant effect, require that webbing slurry amount is large, coating is thick and heavy, good covering with the radiation of ultraviolet blocking-up, although this kind fabric anti-ultraviolet property well changes comparatively obvious to the feel of cloth; In addition, the ultra-thin skin clothing that recent market occurs arranges fabric, although reach ultra-thin, protection effect uvioresistant, the index such as moisture-inhibiting do not possess, and cannot play good protective action.
Knit fabric, divides by weaving method, has Weft knitted fabric and warp knitted fabric two class.Weft knitted fabric often with low-elasticity terylene fibre or special-shaped terylene thread, POLYAMIDE YARNS, cotton yarn, wool yarn etc. for raw material, adopt plain stitch, change plain stitch, rib-loop plain stitch, double rib plain stitch, figured texture weave, pile stitch etc., various weft machine weave and form.
Along with the enhancing of health of people consciousness, also more and more higher to the requirement of clothing fabric, to human body skin nonirritant, there is effect of antibacterial and mouldproof.
CN104389047A discloses a kind of antibacterial and mouldproof weaving face fabric and preparation method thereof.This antibacterial and mouldproof weaving face fabric, by parts by mass, comprise bamboo fibre 60-80 part, tarragon fiber 10-30 part, Chinese yew fiber 10-20 part, fluoroacrylate polymer emulsion 5-10 part, polyvinyl alcohol 5-10 part, nano-chitosan 1-3 part, dispersant 0.5-2 part; The antibacterial and mouldproof weaving face fabric of this invention, to human body skin nonirritant, has good ventilative, antibacterial and mouldproof, health-care effect.But the fabric poisture-penetrability of this invention and fastness to washing are not good, and be not suitable for thick and heavy clothing, warming effect is also poor.
Summary of the invention
The object of the present invention is to provide a kind of antibiotic facing material, this antibiotic facing material is to human body skin nonirritant, and have good ventilative, antibacterial and mouldproof and health-care effect, in addition, vapor transfer rate is good and air penetrability is low, and fastness to washing is good, is applicable to thicker clothing.
For reaching this object, the present invention by the following technical solutions:
On the one hand, the invention provides a kind of antibiotic facing material, it is characterized in that, described antibiotic facing material prepares by primarily of following raw material:
In the present invention, described bamboo fibre is a kind of cellulose fibre extracted from the bamboo of self-sow, bamboo fibre has the characteristics such as good gas permeability, stronger ABRASION RESISTANCE and good dyeability, have again simultaneously natural antibacterial, antibacterial, except mite, deodorization and anti-ultraviolet function.Described chitin is cationic natural polymer, and have the good effect of controlling bacterium, mould, repairing, pure natural has no side effect.Be rich in amino in chitin, need become soluble chitin through de-acetyl and just present, its amino presents powerful effect adsorption-decomposition function organic pernicious gas.Chitin is high molecular weight material, and its molecular weight can reach more than 1,000,000.Molecular weight more high absorption capacity is stronger, is applicable to industry and field of Environment Protection.
Described bamboo fibre can be such as 82,82.2,82.4,82.6,82.8,83,83.2,83.4,83.6,83.8,84,84.2,84.4,84.6,84.8 or 85.
The amino-acid modified polyurethane of described water-based can be such as 2,2.2,2.4,2.6,2.8,3,3.2,3.4,3.6,3.8 or 4.
Described fluoroacrylate polymer can be such as 5,5.5,6,6.5,7,7.5,8,8.5,9,9.5,10,10.5,11,11.5,12,12.5 or 13.
Described nano zine oxide can be such as 1,1.1,1.2,1.3,1.4,1.5,1.6,1.7,1.8,1.9 or 2.
Described nanometer jade powder can be such as 1,1.1,1.2,1.3,1.4,1.5,1.6,1.7,1.8,1.9 or 2.
Described micropore ligno-cellulose can be such as 2,2.2,2.4,2.6,2.8,3,3.2,3.4,3.6,3.8,4,4.2,4.4,4.6,4.8 or 5.
Described dispersant can be such as 0.5,0.6,0.7,0.8,0.9,1,1.1,1.2,1.3,1.4 or 1.5.
Preferably, described antibiotic facing material prepares by primarily of following raw material:
Preferably, described dispersant is the mixture of any one or at least two kinds in glyceryl monostearate, lauryl sodium sulfate or polyacrylamide.
On the other hand, the invention provides a kind of method preparing antibiotic facing material as described in relation to the first aspect, comprise the following steps:
(1) bamboo fibre of formula ratio, the amino-acid modified polyurethane of water-based, fluoroacrylate polymer, nano zine oxide, nanometer jade powder, micropore ligno-cellulose and dispersant is even, obtain mixed solution;
(2) mixed solution is dropped in double screw extruder blended, obtain spinning fibre;
(3) spinning fibre is carried out washing, dry and weaving, obtain described weaving face fabric.
Preferably, the weaving of step (1) described mixing is for grind to form fiber dust by each component raw material, and then add water stirring;
Preferably, the particle diameter of described fiber dust is 300-350 order, is preferably 320-330 order.
Preferably, the temperature of described water is 60-82 DEG C, is preferably 65-75 DEG C.
Preferably, the time of described stirring is 5-10min, is preferably 7-8min.
Preferably, the detailed process of step (2) is: nano-chitosan 1 ~ 3 part and dispersant 0.5 ~ 2 part are joined in fibers mixture liquid, is heated to 50 ~ 60 DEG C and stirs 2 ~ 3min, obtained spinning solution.
Preferably, step (2) the described time blended in double screw extruder is 30-50min, is preferably 45-50min.
Preferably, temperature blended in described double screw extruder is 140-170 DEG C, is preferably 145-155 DEG C.
Preferably, the oven dry described in step (3) adopts thermograde drying tunnel.
Preferably, described thermograde is followed successively by 145-150 DEG C from drying tunnel entrance to outlet, 150-155 DEG C, 155-160 DEG C, and 160-165 DEG C, is preferably 150 DEG C-155 DEG C-160 DEG C-165 DEG C.
Preferably, the time of described oven dry is 40-60s, is preferably 40-50s.
Preferably, step (3) described weaving is melt spinning.
Preferably, the temperature of described melt spinning is 150-190 DEG C, is preferably 160-180 DEG C.
As optimal technical scheme, the preparation method of described antibiotic facing material comprises the following steps:
(1) bamboo fibre of formula ratio, the amino-acid modified polyurethane of water-based, fluoroacrylate polymer, nano zine oxide, nanometer jade powder, micropore ligno-cellulose and dispersant being ground to form particle diameter is 300-350 object powder, add the water of 60-82 DEG C and stir 5-10min, mix, obtain mixed solution;
(2) mixed solution being dropped into temperature is blended 30-50min in the double screw extruder of 140-170 DEG C, obtains spinning fibre;
(3) spinning fibre is carried out washing, dry and weaving, dry and adopt thermograde drying tunnel, be followed successively by 145-150 DEG C from drying tunnel entrance to outlet, 150-155 DEG C, 155-160 DEG C, and 160-165 DEG C, drying time is 40-60s, obtains described weaving face fabric.
Compared with prior art, the present invention has following beneficial effect:
Weaving face fabric air penetrability < 5mm/s of the present invention, vapor transfer rate>=10,000g/m
2d; After 150 times washing nature dries, air penetrability and vapor transfer rate have no significant change; In addition, fabric of the present invention is to human body skin nonirritant, and antibacterial and mouldproof effect is also very outstanding.
Detailed description of the invention
Technical scheme of the present invention is further illustrated below by detailed description of the invention.
Those skilled in the art should understand, described embodiment is only help to understand the present invention, should not be considered as concrete restriction of the present invention.
Embodiment 1
A kind of antibiotic facing material, described antibiotic facing material prepares by primarily of following raw material:
Preparation method is as follows:
(1) bamboo fibre of formula ratio, the amino-acid modified polyurethane of water-based, fluoroacrylate polymer, nano zine oxide, nanometer jade powder, micropore ligno-cellulose and dispersant being ground to form particle diameter is 300 object powder, add the water of 60 DEG C and stir 10min, mix, obtain mixed solution;
(2) mixed solution being dropped into temperature is blended 50min in the double screw extruder of 140 DEG C, obtains spinning fibre;
(3) spinning fibre is carried out washing, dry and weaving, dry and adopt thermograde drying tunnel, be followed successively by 145 DEG C from drying tunnel entrance to outlet, 150 DEG C, 155 DEG C, and 160 DEG C, drying time is 60s, obtains described weaving face fabric.
Embodiment 2
A kind of antibiotic facing material, described antibiotic facing material prepares by primarily of following raw material:
Preparation method is as follows:
(1) bamboo fibre of formula ratio, the amino-acid modified polyurethane of water-based, fluoroacrylate polymer, nano zine oxide, nanometer jade powder, micropore ligno-cellulose and dispersant being ground to form particle diameter is 350 object powder, add the water of 82 DEG C and stir 5min, mix, obtain mixed solution;
(2) mixed solution being dropped into temperature is blended 50min in the double screw extruder of 170 DEG C, obtains spinning fibre;
(3) spinning fibre is carried out washing, dry and weaving, dry and adopt thermograde drying tunnel, be followed successively by 150 DEG C from drying tunnel entrance to outlet, 155 DEG C, 160 DEG C, and 165 DEG C, drying time is 60s, obtains described weaving face fabric.
Embodiment 3
A kind of antibiotic facing material, described antibiotic facing material prepares by primarily of following raw material:
Preparation method is as follows:
(1) bamboo fibre of formula ratio, the amino-acid modified polyurethane of water-based, fluoroacrylate polymer, nano zine oxide, nanometer jade powder, micropore ligno-cellulose and dispersant being ground to form particle diameter is 325 object powder, add the water of 71 DEG C and stir 7.5min, mix, obtain mixed solution;
(2) mixed solution being dropped into temperature is blended 40min in the double screw extruder of 155 DEG C, obtains spinning fibre;
(3) spinning fibre is carried out washing, dry and weaving, dry and adopt thermograde drying tunnel, be followed successively by 147.5 DEG C from drying tunnel entrance to outlet, 152.5 DEG C, 157.5 DEG C, and 162.5 DEG C, drying time is 50s, obtains described weaving face fabric.
Embodiment 4
A kind of antibiotic facing material, described antibiotic facing material prepares by primarily of following raw material:
Preparation method is as follows:
(1) bamboo fibre of formula ratio, the amino-acid modified polyurethane of water-based, fluoroacrylate polymer, nano zine oxide, nanometer jade powder, micropore ligno-cellulose and dispersant being ground to form particle diameter is 330 object powder, add the water of 80 DEG C and stir 7min, mix, obtain mixed solution;
(2) mixed solution being dropped into temperature is blended 35min in the double screw extruder of 160 DEG C, obtains spinning fibre;
(3) spinning fibre is carried out washing, dry and weaving, dry and adopt thermograde drying tunnel, be followed successively by 148 DEG C from drying tunnel entrance to outlet, 153 DEG C, 156 DEG C, and 164 DEG C, drying time is 47s, obtains described weaving face fabric.
By the performance of the antibiotic facing material of the present invention of experiment test below.
According to ASTMD737 standard, gas permeability (taking vapor transfer rate as index) is tested; According to BSEN14119-2003 standard, mildew resistance is tested; According to GB/T20944.3-2008 standard to antibiotic property (taking bacteriostasis rate as index).Result is as shown in table 1 below:
As can be seen from the above table, antibiotic facing material prepared by the present invention, compared with existing fabric, has good ventilative, antibacterial and mouldproof performance.Simultaneously with the addition of bamboo fibre in antibiotic facing material, nano-chitosan make it also to have antibacterial and mouldproof, effect and health care that deodorization, repairing, adsorption-decomposition function are harmful to organic gas.
In sum, weaving face fabric air penetrability < 5mm/s of the present invention, vapor transfer rate >=10,000g/m2d; After 150 times washing nature dries, air penetrability and vapor transfer rate have no significant change; In addition, antibacterial and mouldproof weaving face fabric of the present invention, to human body skin nonirritant, has good ventilative, antibacterial and mouldproof, health-care effect.
It should be noted that and understand, when not departing from the spirit and scope of accompanying claim the present invention for required protection, various amendment and improvement can be made to the present invention of foregoing detailed description.Therefore, the scope of claimed technical scheme is not by the restriction of given any specific exemplary teachings.
Applicant states, the present invention illustrates process of the present invention by above-described embodiment, but the present invention is not limited to above-mentioned processing step, does not namely mean that the present invention must rely on above-mentioned processing step and could implement.Person of ordinary skill in the field should understand, any improvement in the present invention, to equivalence replacement and the interpolation of auxiliary element, the concrete way choice etc. of raw material selected by the present invention, all drops within protection scope of the present invention and open scope.
Claims (9)
1. an antibiotic facing material, is characterized in that, described antibiotic facing material prepares primarily of following raw material by weight:
2. antibiotic facing material according to claim 1, is characterized in that, described antibiotic facing material prepares by primarily of following raw material:
3. antibiotic facing material according to claim 1 and 2, is characterized in that, described dispersant is the mixture of any one or at least two kinds in glyceryl monostearate, lauryl sodium sulfate or polyacrylamide.
4. prepare a method for the antibiotic facing material according to any one of claim 1-3, it is characterized in that, comprise the following steps:
(1) bamboo fibre of formula ratio, the amino-acid modified polyurethane of water-based, fluoroacrylate polymer, nano zine oxide, nanometer jade powder, micropore ligno-cellulose and dispersant is even, obtain mixed solution;
(2) mixed solution is dropped in double screw extruder blended, obtain spinning fibre;
(3) spinning fibre is carried out washing, dry and weaving, obtain described weaving face fabric.
5. preparation method according to claim 4, is characterized in that, the weaving of step (1) described mixing is for grind to form fiber dust by each component raw material, and then add water stirring;
Preferably, the particle diameter of described fiber dust is 300-350 order, is preferably 320-330 order;
Preferably, the temperature of described water is 60-82 DEG C, is preferably 65-75 DEG C;
Preferably, the time of described stirring is 5-10min, is preferably 7-8min.
6. the method preparing antibacterial and mouldproof weaving face fabric according to claim 4, it is characterized in that, the detailed process of step (2) is: join in fibers mixture liquid by nano-chitosan 1 ~ 3 part and dispersant 0.5 ~ 2 part, be heated to 50 ~ 60 DEG C and stir 2 ~ 3min, obtained spinning solution.
Preparation method according to claim 4 or 5, is characterized in that, step (2) the described time blended in double screw extruder is 30-50min, is preferably 45-50min;
Preferably, temperature blended in described double screw extruder is 140-170 DEG C, is preferably 145-155 DEG C.
7. the preparation method according to any one of claim 4-6, is characterized in that, the oven dry described in step (3) adopts thermograde drying tunnel;
Preferably, described thermograde is followed successively by 145-150 DEG C from drying tunnel entrance to outlet, 150-155 DEG C, 155-160 DEG C, and 160-165 DEG C, is preferably 150 DEG C-155 DEG C-160 DEG C-165 DEG C;
Preferably, the time of described oven dry is 40-60s, is preferably 40-50s.
8. the preparation method according to any one of claim 4-7, is characterized in that, step (3) described weaving is melt spinning;
Preferably, the temperature of described melt spinning is 150-190 DEG C, is preferably 160-180 DEG C.
9. the preparation method according to any one of claim 4-8, is characterized in that, comprises the following steps:
(1) bamboo fibre of formula ratio, the amino-acid modified polyurethane of water-based, fluoroacrylate polymer, nano zine oxide, nanometer jade powder, micropore ligno-cellulose and dispersant being ground to form particle diameter is 300-350 object powder, add the water of 60-82 DEG C and stir 5-10min, mix, obtain mixed solution;
(2) mixed solution being dropped into temperature is blended 30-50min in the double screw extruder of 140-170 DEG C, obtains spinning fibre;
(3) spinning fibre is carried out washing, dry and weaving, dry and adopt thermograde drying tunnel, be followed successively by 145-150 DEG C from drying tunnel entrance to outlet, 150-155 DEG C, 155-160 DEG C, and 160-165 DEG C, drying time is 40-60s, obtains described weaving face fabric.
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Cited By (8)
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| CN105887239A (en) * | 2016-05-23 | 2016-08-24 | 太和县蓝翎养殖有限公司 | Hydrophobic antibacterial type artificial wig fibers containing peacock feather |
| CN106012220A (en) * | 2016-06-24 | 2016-10-12 | 广德毅维纺织有限公司 | Washable fabric for shirts |
| CN106072942A (en) * | 2016-08-24 | 2016-11-09 | 江苏中孚达科技股份有限公司 | A kind of Nano anti-bacterial fabric |
| CN107881625A (en) * | 2017-12-05 | 2018-04-06 | 合肥师范学院 | Sun-proof antibacterial weaving face fabric |
| CN108468212A (en) * | 2018-03-29 | 2018-08-31 | 王术民 | A kind of production method of the health-care deodorized material of novel antibacterial of not silver ion |
| CN109295538A (en) * | 2018-09-29 | 2019-02-01 | 浙江和也健康科技有限公司 | A kind of antibacterial and deodorizing textile fabric and preparation method thereof |
| CN114075709A (en) * | 2021-10-26 | 2022-02-22 | 广州市楠忻隆纺织品有限公司 | Zinc-containing jade fiber cold feeling cloth and preparation method and application thereof |
| CN115404695A (en) * | 2022-08-18 | 2022-11-29 | 广州市简康科技有限公司 | Multifunctional fabric |
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| CN105887239A (en) * | 2016-05-23 | 2016-08-24 | 太和县蓝翎养殖有限公司 | Hydrophobic antibacterial type artificial wig fibers containing peacock feather |
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| CN114075709A (en) * | 2021-10-26 | 2022-02-22 | 广州市楠忻隆纺织品有限公司 | Zinc-containing jade fiber cold feeling cloth and preparation method and application thereof |
| CN115404695A (en) * | 2022-08-18 | 2022-11-29 | 广州市简康科技有限公司 | Multifunctional fabric |
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Application publication date: 20151125 |