CN105086766A - Antistatic environment-friendly water-based paint and preparation method thereof - Google Patents
Antistatic environment-friendly water-based paint and preparation method thereof Download PDFInfo
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- CN105086766A CN105086766A CN201510581523.4A CN201510581523A CN105086766A CN 105086766 A CN105086766 A CN 105086766A CN 201510581523 A CN201510581523 A CN 201510581523A CN 105086766 A CN105086766 A CN 105086766A
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Abstract
The invention discloses an antistatic environment-friendly water-based paint which comprises the following raw materials in parts by weight: 53-78 parts of water-based epoxy resin, 35-55 parts of water-based unsaturated polyester acrylate resin, 18-35 parts of polyetheretherketone, 10-28 parts of lithium carbonate, 12-25 parts of sodium alkyl sulfonate, 12-26 parts of zinc acetate, 5-20 parts of talcum powder, 5-15 parts of diatomite, 6-15 parts of zinc sulfide, 4-13 parts of alumina powder, 6-15 parts of barium sulfate, 3-15 parts of zinc peroxide, 2-10 parts of film formation assistant, 2-8 parts of wetting agent, 1-6 parts of defoaming agent and 18-30 parts of deionized water. The water-based paint disclosed by the invention is green and environment-friendly, has the advantages of favorable antistatic property, favorable adhesion, favorable hardness and favorable chemical resistance stability, and has favorable application prospects.
Description
Technical field
The present invention relates to paint field, particularly a kind of anti-electrostatic environment protecting water-based paint and preparation method thereof.
Background technology
Coating a kind ofly can be coated in article surface by different construction technologies; form adhere well, there is some strength, continuous print solid film; it is widely used in industrial production and daily life, plays the active effect of protection base material and aesthetic appeal.Along with the progress of science and technology, the application of electronic equipments is more and more general, thus the electromagnetic environment produced also becomes increasingly complex, and the possibility that unpredictable static hazard is produced increases further, so become a problem in the urgent need to address already for electronic equipments anti-electrostatic.In numerous electrostatic protection measure, coating Antistatic Paint is a kind of measure of simple and fast, and because it is practical, constructability and use, enjoy liking and paying close attention to of people.Day by day now serious in environmental pollution, people more and more recognize the importance of environmental protection.But traditional coating is mostly oil paint, interior containing a large amount of organic solvents, these solvent evaporates can bring environmental pollution to a certain degree, worsen contaminate environment further, threaten living space and the environment of people; In this external coating process, people also can suction part volatilization organic solvent, also the healthy and safe of human body in serious harm.
Summary of the invention
The technical problem solved is: at least one in order to solve the problem, provides a kind of anti-electrostatic environment protecting water-based paint and preparation method thereof.
Technical scheme: in order to solve the problem, the invention provides a kind of anti-electrostatic environment protecting water-based paint, comprise the component raw material of following parts by weight: aqueous epoxy resins 53 ~ 78 parts, water-based unsaturated polyester acrylate resin 35 ~ 55 parts, polyether-ether-ketone 18 ~ 35 parts, Quilonum Retard 10 ~ 28 parts, sodium allyl sulfonate 12 ~ 25 parts, zinc acetate 12 ~ 26 parts, talcum powder 5 ~ 20 parts, 5 ~ 15 parts, diatomite, 6 ~ 15 parts, zinc sulphide, aluminum oxide powder 4 ~ 13 parts, 6 ~ 15 parts, barium sulfate, zinc peroxide 3 ~ 15 parts, film coalescence aid 2 ~ 10 parts, wetting agent 2 ~ 8 parts, defoamer 1 ~ 6 part and deionized water 18 ~ 30 parts.
Preferably, described a kind of anti-electrostatic environment protecting water-based paint, is characterized in that: aqueous epoxy resins 65 ~ 78 parts, water-based unsaturated polyester acrylate resin 42 ~ 55 parts, polyether-ether-ketone 18 ~ 26 parts, Quilonum Retard 15 ~ 24 parts, sodium allyl sulfonate 12 ~ 19 parts, zinc acetate 12 ~ 20 parts, talcum powder 5 ~ 11 parts, 5 ~ 9 parts, diatomite, 8 ~ 15 parts, zinc sulphide, aluminum oxide powder 6 ~ 13 parts, 8 ~ 15 parts, barium sulfate, zinc peroxide 6 ~ 15 parts, film coalescence aid 2 ~ 7 parts, wetting agent 2 ~ 5 parts, defoamer 1 ~ 4 part and deionized water 22 ~ 30 parts.
Preferably, described a kind of anti-electrostatic environment protecting water-based paint, is characterized in that: aqueous epoxy resins 65 parts, water-based unsaturated polyester acrylate resin 42 parts, polyether-ether-ketone 25 parts, Quilonum Retard 12 parts, sodium allyl sulfonate 18 parts, zinc acetate 15 parts, talcum powder 8 parts, 7 parts, diatomite, 11 parts, zinc sulphide, aluminum oxide powder 8 parts, 11 parts, barium sulfate, zinc peroxide 6 parts, film coalescence aid 8 parts, wetting agent 4 parts, defoamer 2 parts and deionized water 26 parts.
Preferably, described film coalescence aid is alcohol ester-12 0 or ethanol.
Preferably, described wetting agent is polyurethane aqueous wetting agent.
Preferably, described defoamer is methyl-silicone oil.
The preparation method of described a kind of anti-electrostatic environment protecting water-based paint, comprises the following steps:
(1) take Quilonum Retard, zinc acetate, talcum powder, diatomite, zinc sulphide, aluminum oxide powder, barium sulfate and zinc peroxide according to above-mentioned parts by weight, then carry out pre-dispersed mixing and grinding, cross 200 mesh sieves, obtain compound;
(2) aqueous epoxy resins taken according to above-mentioned parts by weight, water-based unsaturated polyester acrylate resin, polyether-ether-ketone, sodium allyl sulfonate, film coalescence aid, wetting agent and defoamer are placed in stirred pot, mix and blend 30min, then the compound in step (1) is added in stirred pot, continue to stir 2h with the speed of 50 ~ 200rpm;
(3) take deionized water according to above-mentioned parts by weight, and slowly added by deionized water in step (2), rate of addition is 1g/min ~ 4g/min, dropwises and obtain required coating.
Preferably, the stirring velocity in described step (2) is 100rpm; The rate of addition of the deionized water in described step (3) is 1.8g/min.
The present invention has following beneficial effect: the not only environmental protection of the water-borne coatings prepared by the present invention, has good antistatic property, sticking power, hardness and chemical-resistant stability simultaneously, possesses good application prospect.
Embodiment
In order to understand the present invention further, below in conjunction with embodiment, invention preferred embodiment is described, but should be appreciated that these describe just for further illustrating the features and advantages of the present invention, instead of limiting to the claimed invention.
Embodiment 1
A kind of anti-electrostatic environment protecting water-based paint, comprises the component raw material of following parts by weight: aqueous epoxy resins 53 parts, water-based unsaturated polyester acrylate resin 35 parts, polyether-ether-ketone 18 parts, Quilonum Retard 10 parts, sodium allyl sulfonate 12 parts, zinc acetate 12 parts, talcum powder 5 parts, 5 parts, diatomite, 6 parts, zinc sulphide, aluminum oxide powder 4 parts, 6 parts, barium sulfate, zinc peroxide 3 parts, alcohol ester-12 0 film coalescence aid 2 parts, polyurethane aqueous wetting agent 2 parts, methyl-silicone oil defoamer 1 part and deionized water 18 parts.
The preparation method of this anti-electrostatic environment protecting water-based paint, comprises the following steps:
(1) take Quilonum Retard, zinc acetate, talcum powder, diatomite, zinc sulphide, aluminum oxide powder, barium sulfate and zinc peroxide according to above-mentioned parts by weight, then carry out pre-dispersed mixing and grinding, cross 200 mesh sieves, obtain compound;
(2) aqueous epoxy resins taken according to above-mentioned parts by weight, water-based unsaturated polyester acrylate resin, polyether-ether-ketone, sodium allyl sulfonate, film coalescence aid, wetting agent and defoamer are placed in stirred pot, mix and blend 30min, then the compound in step (1) is added in stirred pot, continue to stir 2h with the speed of 50rpm;
(3) take deionized water according to above-mentioned parts by weight, and slowly added by deionized water in step (2), rate of addition is 1g/min, dropwises and obtain required coating.
Embodiment 2
A kind of anti-electrostatic environment protecting water-based paint, comprises the component raw material of following parts by weight: aqueous epoxy resins 78 parts, water-based unsaturated polyester acrylate resin 55 parts, polyether-ether-ketone 35 parts, Quilonum Retard 28 parts, sodium allyl sulfonate 25 parts, zinc acetate 26 parts, talcum powder 20 parts, 15 parts, diatomite, 15 parts, zinc sulphide, aluminum oxide powder 13 parts, 15 parts, barium sulfate, zinc peroxide 15 parts, ethanol film coalescence aid 10 parts, polyurethane aqueous wetting agent 8 parts, methyl-silicone oil defoamer 6 parts and deionized water 30 parts.
The preparation method of this anti-electrostatic environment protecting water-based paint, comprises the following steps:
(1) take Quilonum Retard, zinc acetate, talcum powder, diatomite, zinc sulphide, aluminum oxide powder, barium sulfate and zinc peroxide according to above-mentioned parts by weight, then carry out pre-dispersed mixing and grinding, cross 200 mesh sieves, obtain compound;
(2) aqueous epoxy resins taken according to above-mentioned parts by weight, water-based unsaturated polyester acrylate resin, polyether-ether-ketone, sodium allyl sulfonate, film coalescence aid, wetting agent and defoamer are placed in stirred pot, mix and blend 30min, then the compound in step (1) is added in stirred pot, continue to stir 2h with the speed of 200rpm;
(3) take deionized water according to above-mentioned parts by weight, and slowly added by deionized water in step (2), rate of addition is 4g/min, dropwises and obtain required coating.
Embodiment 3
A kind of anti-electrostatic environment protecting water-based paint, comprises the component raw material of following parts by weight: aqueous epoxy resins 65 parts, water-based unsaturated polyester acrylate resin 45 parts, polyether-ether-ketone 26 parts, Quilonum Retard 19 parts, sodium allyl sulfonate 18 parts, zinc acetate 16 parts, talcum powder 12 parts, 10 parts, diatomite, 11 parts, zinc sulphide, aluminum oxide powder 8 parts, 11 parts, barium sulfate, zinc peroxide 9 parts, ethanol film coalescence aid 6 parts, polyurethane aqueous wetting agent 5 parts, methyl-silicone oil defoamer 3 parts and deionized water 24 parts.
The preparation method of this anti-electrostatic environment protecting water-based paint, comprises the following steps:
(1) take Quilonum Retard, zinc acetate, talcum powder, diatomite, zinc sulphide, aluminum oxide powder, barium sulfate and zinc peroxide according to above-mentioned parts by weight, then carry out pre-dispersed mixing and grinding, cross 200 mesh sieves, obtain compound;
(2) aqueous epoxy resins taken according to above-mentioned parts by weight, water-based unsaturated polyester acrylate resin, polyether-ether-ketone, sodium allyl sulfonate, film coalescence aid, wetting agent and defoamer are placed in stirred pot, mix and blend 30min, then the compound in step (1) is added in stirred pot, continue to stir 2h with the speed of 125rpm;
(3) take deionized water according to above-mentioned parts by weight, and slowly added by deionized water in step (2), rate of addition is 2g/min, dropwises and obtain required coating.
Embodiment 4
A kind of anti-electrostatic environment protecting water-based paint, comprises the component raw material of following parts by weight: aqueous epoxy resins 65 parts, water-based unsaturated polyester acrylate resin 42 parts, polyether-ether-ketone 26 parts, Quilonum Retard 15 parts, sodium allyl sulfonate 19 parts, zinc acetate 20 parts, talcum powder 11 parts, 9 parts, diatomite, 8 parts, zinc sulphide, aluminum oxide powder 6 parts, 8 parts, barium sulfate, zinc peroxide 6 parts, alcohol ester-12 0 film coalescence aid 7 parts, polyurethane aqueous wetting agent 5 parts, methyl-silicone oil defoamer 4 parts and deionized water 22 parts.
The preparation method of this anti-electrostatic environment protecting water-based paint, comprises the following steps:
(1) take Quilonum Retard, zinc acetate, talcum powder, diatomite, zinc sulphide, aluminum oxide powder, barium sulfate and zinc peroxide according to above-mentioned parts by weight, then carry out pre-dispersed mixing and grinding, cross 200 mesh sieves, obtain compound;
(2) aqueous epoxy resins taken according to above-mentioned parts by weight, water-based unsaturated polyester acrylate resin, polyether-ether-ketone, sodium allyl sulfonate, film coalescence aid, wetting agent and defoamer are placed in stirred pot, mix and blend 30min, then the compound in step (1) is added in stirred pot, continue to stir 2h with the speed of 100rpm;
(3) take deionized water according to above-mentioned parts by weight, and slowly added by deionized water in step (2), rate of addition is 2g/min, dropwises and obtain required coating.
Embodiment 5
A kind of anti-electrostatic environment protecting water-based paint, comprises the component raw material of following parts by weight: aqueous epoxy resins 65 parts, water-based unsaturated polyester acrylate resin 42 parts, polyether-ether-ketone 25 parts, Quilonum Retard 12 parts, sodium allyl sulfonate 18 parts, zinc acetate 15 parts, talcum powder 8 parts, 7 parts, diatomite, 11 parts, zinc sulphide, aluminum oxide powder 8 parts, 11 parts, barium sulfate, zinc peroxide 6 parts, ethanol film coalescence aid 8 parts, polyurethane aqueous wetting agent 4 parts, methyl-silicone oil defoamer 2 parts and deionized water 26 parts.
The preparation method of this anti-electrostatic environment protecting water-based paint, comprises the following steps:
(1) take Quilonum Retard, zinc acetate, talcum powder, diatomite, zinc sulphide, aluminum oxide powder, barium sulfate and zinc peroxide according to above-mentioned parts by weight, then carry out pre-dispersed mixing and grinding, cross 200 mesh sieves, obtain compound;
(2) aqueous epoxy resins taken according to above-mentioned parts by weight, water-based unsaturated polyester acrylate resin, polyether-ether-ketone, sodium allyl sulfonate, film coalescence aid, wetting agent and defoamer are placed in stirred pot, mix and blend 30min, then the compound in step (1) is added in stirred pot, continue to stir 2h with the speed of 100rpm;
(3) take deionized water according to above-mentioned parts by weight, and slowly added by deionized water in step (2), rate of addition is 1.8g/min, dropwises and obtain required coating.
By above-mentioned prepared paint on base material, carry out every test after drying, refer to following table:
The not only environmental protection of water-borne coatings prepared by the present invention, has good antistatic property, sticking power, hardness and chemical-resistant stability simultaneously, possesses good application prospect.
The foregoing is only the specific embodiment of the present invention; but these are the simple description to mentality of designing of the present invention; instead of the restriction to mentality of designing of the present invention, any do not exceed mentality of designing of the present invention combination, increase or amendment, all fall into protection scope of the present invention.
Claims (8)
1. an anti-electrostatic environment protecting water-based paint, is characterized in that: the component raw material comprising following parts by weight: aqueous epoxy resins 53 ~ 78 parts, water-based unsaturated polyester acrylate resin 35 ~ 55 parts, polyether-ether-ketone 18 ~ 35 parts, Quilonum Retard 10 ~ 28 parts, sodium allyl sulfonate 12 ~ 25 parts, zinc acetate 12 ~ 26 parts, talcum powder 5 ~ 20 parts, 5 ~ 15 parts, diatomite, 6 ~ 15 parts, zinc sulphide, aluminum oxide powder 4 ~ 13 parts, 6 ~ 15 parts, barium sulfate, zinc peroxide 3 ~ 15 parts, film coalescence aid 2 ~ 10 parts, wetting agent 2 ~ 8 parts, defoamer 1 ~ 6 part and deionized water 18 ~ 30 parts.
2. a kind of anti-electrostatic environment protecting water-based paint according to claim 1, is characterized in that: aqueous epoxy resins 65 ~ 78 parts, water-based unsaturated polyester acrylate resin 42 ~ 55 parts, polyether-ether-ketone 18 ~ 26 parts, Quilonum Retard 15 ~ 24 parts, sodium allyl sulfonate 12 ~ 19 parts, zinc acetate 12 ~ 20 parts, talcum powder 5 ~ 11 parts, 5 ~ 9 parts, diatomite, 8 ~ 15 parts, zinc sulphide, aluminum oxide powder 6 ~ 13 parts, 8 ~ 15 parts, barium sulfate, zinc peroxide 6 ~ 15 parts, film coalescence aid 2 ~ 7 parts, wetting agent 2 ~ 5 parts, defoamer 1 ~ 4 part and deionized water 22 ~ 30 parts.
3. a kind of anti-electrostatic environment protecting water-based paint according to claim 1, is characterized in that: aqueous epoxy resins 65 parts, water-based unsaturated polyester acrylate resin 42 parts, polyether-ether-ketone 25 parts, Quilonum Retard 12 parts, sodium allyl sulfonate 18 parts, zinc acetate 15 parts, talcum powder 8 parts, 7 parts, diatomite, 11 parts, zinc sulphide, aluminum oxide powder 8 parts, 11 parts, barium sulfate, zinc peroxide 6 parts, film coalescence aid 8 parts, wetting agent 4 parts, defoamer 2 parts and deionized water 26 parts.
4. a kind of anti-electrostatic environment protecting water-based paint according to claim 1, is characterized in that: described film coalescence aid is alcohol ester-12 0 or ethanol.
5. a kind of anti-electrostatic environment protecting water-based paint according to claim 1, is characterized in that: described wetting agent is polyurethane aqueous wetting agent.
6. a kind of anti-electrostatic environment protecting water-based paint according to claim 1, is characterized in that: described defoamer is methyl-silicone oil.
7. the preparation method of a kind of anti-electrostatic environment protecting water-based paint as claimed in claim 1, is characterized in that: comprise the following steps:
(1) take Quilonum Retard, zinc acetate, talcum powder, diatomite, zinc sulphide, aluminum oxide powder, barium sulfate and zinc peroxide according to above-mentioned parts by weight, then carry out pre-dispersed mixing and grinding, cross 200 mesh sieves, obtain compound;
(2) aqueous epoxy resins taken according to above-mentioned parts by weight, water-based unsaturated polyester acrylate resin, polyether-ether-ketone, sodium allyl sulfonate, film coalescence aid, wetting agent and defoamer are placed in stirred pot, mix and blend 30min, then the compound in step (1) is added in stirred pot, continue to stir 2h with the speed of 50 ~ 200rpm;
(3) take deionized water according to above-mentioned parts by weight, and slowly added by deionized water in step (2), rate of addition is 1g/min ~ 4g/min, dropwises and obtain required coating.
8. the preparation method of a kind of anti-electrostatic environment protecting water-based paint according to claim 7, is characterized in that: the stirring velocity in described step (2) is 100rpm; The rate of addition of the deionized water in described step (3) is 1.8g/min.
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN106049046A (en) * | 2016-07-29 | 2016-10-26 | 吴国强 | Novel textile water-based coating and preparation method thereof |
CN106554629A (en) * | 2016-11-02 | 2017-04-05 | 墨宝股份有限公司 | A kind of antistatic environment friendly plastic rubber sheet material and preparation method thereof |
CN108485466A (en) * | 2018-04-03 | 2018-09-04 | 白山市和硅藻科技有限公司 | A kind of environment-friendly liquid anti-static coatings |
CN109485836A (en) * | 2018-09-27 | 2019-03-19 | 合众(佛山)化工有限公司 | A kind of polyether-ether-ketone modified water-based alkyd resin and preparation method thereof |
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CN101921528A (en) * | 2010-08-11 | 2010-12-22 | 池州学院 | Calcium carbonate/nickel composite conductive material matrix antistatic coating and preparation method thereof |
CN104631106A (en) * | 2015-02-05 | 2015-05-20 | 江苏华艺服饰有限公司 | Antistatic finishing agent, and preparation method and application thereof |
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2015
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Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101921528A (en) * | 2010-08-11 | 2010-12-22 | 池州学院 | Calcium carbonate/nickel composite conductive material matrix antistatic coating and preparation method thereof |
CN104631106A (en) * | 2015-02-05 | 2015-05-20 | 江苏华艺服饰有限公司 | Antistatic finishing agent, and preparation method and application thereof |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106049046A (en) * | 2016-07-29 | 2016-10-26 | 吴国强 | Novel textile water-based coating and preparation method thereof |
CN106554629A (en) * | 2016-11-02 | 2017-04-05 | 墨宝股份有限公司 | A kind of antistatic environment friendly plastic rubber sheet material and preparation method thereof |
CN108485466A (en) * | 2018-04-03 | 2018-09-04 | 白山市和硅藻科技有限公司 | A kind of environment-friendly liquid anti-static coatings |
CN109485836A (en) * | 2018-09-27 | 2019-03-19 | 合众(佛山)化工有限公司 | A kind of polyether-ether-ketone modified water-based alkyd resin and preparation method thereof |
CN109485836B (en) * | 2018-09-27 | 2020-11-17 | 合众(佛山)化工有限公司 | Polyether-ether-ketone modified waterborne alkyd resin and preparation method thereof |
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