CN106554629A - A kind of antistatic environment friendly plastic rubber sheet material and preparation method thereof - Google Patents
A kind of antistatic environment friendly plastic rubber sheet material and preparation method thereof Download PDFInfo
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- CN106554629A CN106554629A CN201610945933.7A CN201610945933A CN106554629A CN 106554629 A CN106554629 A CN 106554629A CN 201610945933 A CN201610945933 A CN 201610945933A CN 106554629 A CN106554629 A CN 106554629A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K13/00—Use of mixtures of ingredients not covered by one single of the preceding main groups, each of these compounds being essential
- C08K13/02—Organic and inorganic ingredients
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G81/00—Macromolecular compounds obtained by interreacting polymers in the absence of monomers, e.g. block polymers
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/04—Carbon
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/05—Alcohols; Metal alcoholates
- C08K5/053—Polyhydroxylic alcohols
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/13—Phenols; Phenolates
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/16—Nitrogen-containing compounds
- C08K5/17—Amines; Quaternary ammonium compounds
- C08K5/19—Quaternary ammonium compounds
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/36—Sulfur-, selenium-, or tellurium-containing compounds
- C08K5/41—Compounds containing sulfur bound to oxygen
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/36—Sulfur-, selenium-, or tellurium-containing compounds
- C08K5/41—Compounds containing sulfur bound to oxygen
- C08K5/42—Sulfonic acids; Derivatives thereof
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/49—Phosphorus-containing compounds
- C08K5/51—Phosphorus bound to oxygen
- C08K5/52—Phosphorus bound to oxygen only
- C08K5/524—Esters of phosphorous acids, e.g. of H3PO3
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/04—Antistatic
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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Abstract
The invention discloses a kind of antistatic environment friendly plastic rubber sheet material, including the raw material of following weight portion：80～100 parts of epoxy resin, 40～50 parts of polyurethane resin, 10～30 parts of ethylene glycol, 2～8 parts of dodecylbenzene sodium sulfonate, 3～10 parts of sodium lauryl sulphate, N, 2～8 parts of N dimethyl N Ethylbenzyls quaternary ammonium salt, 3～12 parts of white carbon black, 3～8 parts of antioxidant, 10～20 parts of coloring agent, 2～8 parts of dispersant, 2～6 parts of plasticizer, 3～9 parts of thickening agent, 3～6 parts of cross-linking agent, 2～4 parts of emulsifying agent.Environment friendly plastic rubber sheet material proposed by the present invention, water resistance and resistance to elevated temperatures it is good, anti-static ability significantly, can isolation ultraviolet, and oxidation resistance is strong, and rate of ageing is slow, the invention allows for a kind of preparation method of simple antistatic environment friendly plastic rubber sheet material.
Description
Technical field
The present invention relates to plastic material technical field, more particularly to a kind of antistatic environment friendly plastic rubber sheet material and its preparation side
Method.
Background technology
The range of application of plastic cement is wider, is seen everywhere in daily life, such as household electrical appliances, automobile, mobile phone, medical apparatus and instruments,
Dirt-proof boot, cutting ferrule etc..After the product long-time use of some plastic cement materials, often there is color because environment or illumination etc. affect and send out
Huang, situations such as product ftractures, can also be produced electrostatic between people sometimes, bring worry to user.
The content of the invention
The invention aims to shortcoming present in prior art is solved, and a kind of antistatic environment friendly plastic rubber for proposing
Sheet material and preparation method thereof.
A kind of antistatic environment friendly plastic rubber sheet material, including the raw material of following weight portion：50～100 parts of epoxy resin, polyurethane
40～50 parts of resin, 10～30 parts of ethylene glycol, 2～8 parts of dodecylbenzene sodium sulfonate, 3～10 parts of sodium lauryl sulphate, N, N-
2～8 parts of dimethyl-N-ethyl benzyl quaternary ammonium salt, 3～12 parts of white carbon black, 3～8 parts of antioxidant, 10～20 parts of coloring agent, dispersion
2～8 parts of agent, 2～6 parts of plasticizer, 3～9 parts of thickening agent, 3～6 parts of cross-linking agent, 2～4 parts of emulsifying agent.
Preferably, a kind of described antistatic environment friendly plastic rubber sheet material, including the raw material of following weight portion：Epoxy resin 85～
95 parts, 40～50 parts of polyurethane resin, 15～25 parts of ethylene glycol, 3～7 parts of dodecylbenzene sodium sulfonate, sodium lauryl sulphate 4
～10 parts, 4～6 parts of N, N- dimethyl-N-ethyl benzyl quaternary ammonium salt, 4～12 parts of white carbon black, 3～6 parts of antioxidant, coloring agent 12
～18 parts, 4～6 parts of dispersant, 2～6 parts of plasticizer, 4～8 parts of thickening agent, 3～6 parts of cross-linking agent, 2～4 parts of emulsifying agent.
Preferably, a kind of described antistatic environment friendly plastic rubber sheet material, including the raw material of following weight portion：Epoxy resin 90
Part, 45 parts of polyurethane resin, 20 parts of ethylene glycol, 5 parts of dodecylbenzene sodium sulfonate, 7 parts of sodium lauryl sulphate, N, N- diformazan
5 parts of base-N- Ethylbenzyls quaternary ammonium salt, 8 parts of white carbon black, 5 parts of antioxidant, 15 parts of coloring agent, 5 parts of dispersant, 4 parts of plasticizer increase
Thick dose 6 parts, 4 parts of cross-linking agent, 3 parts of emulsifying agent.
Preferably, the antioxidant includes main anti-oxidant and auxiliary antioxidant, and main anti-oxidant and auxiliary are anti-
The weight part ratio of oxidant is 1～2:1.
Preferably, the primary antioxidant is hydroquinone or phenol.
Preferably, the auxiliary antioxidant is NSC 5284.
The invention allows for a kind of preparation method of antistatic environment friendly plastic rubber sheet material, comprises the following steps：
S1：The epoxy resin of corresponding weight portion, polyurethane resin, cross-linking agent and emulsifying agent are added in kneader, and
It is 80～100 DEG C by temperature setting, carries out high-temperature stirring, obtain the copolymer of epoxy resin and polyurethane resin；
S2：To above-mentioned epoxy resin and the ethylene glycol that corresponding weight portion is added in the copolymer of polyurethane resin, dodecane
Base benzene sulfonic acid sodium salt, sodium lauryl sulphate, N, N- dimethyl-N-ethyl benzyl quaternary ammonium salt, white carbon black, antioxidant, coloring agent, point
Powder, plasticizer and thickening agent, continue high-temperature stirring, obtain final product plastic cement sizing material；
S3：Above-mentioned sizing material is reinjected in mould, and extrusion molding obtains final product antistatic environment friendly plastic rubber sheet material.
Plastic sheet proposed by the present invention, using epoxy resin and polyurethane resin copolymerization, improves the overall waterproof of plastic cement
Performance and resistance to elevated temperatures, add kinds of surface activating agent significantly increase can the anti-static ability of plastic sheet, white carbon black and
Isolation ultraviolet is played in the addition of antioxidant again, is improved plastic cement oxidation resistance, is delayed plastic cement rate of ageing, it is to avoid modeling occurs
The phenomenon that glue product turns yellow, and a kind of the invention allows for preparation method of simple antistatic environment friendly plastic rubber sheet material.
Specific embodiment
The present invention is further explained with reference to specific embodiment.
Embodiment one
A kind of antistatic environment friendly plastic rubber sheet material proposed by the present invention, including the raw material of following weight portion：90 parts of epoxy resin,
45 parts of polyurethane resin, 20 parts of ethylene glycol, 5 parts of dodecylbenzene sodium sulfonate, 7 parts of sodium lauryl sulphate, N, N- dimethyl-N-
5 parts of Ethylbenzyl quaternary ammonium salt, 8 parts of white carbon black, 3 parts of hydroquinone, 2 parts of NSC 5284,15 parts of coloring agent, 5 parts of dispersant increase
4 parts of agent of modeling, 6 parts of thickening agent, 4 parts of cross-linking agent, 3 parts of emulsifying agent.
Its preparation method, comprises the following steps：
S1：The epoxy resin of corresponding weight portion, polyurethane resin, cross-linking agent and emulsifying agent are added in kneader, and
It is 90 DEG C by temperature setting, carries out high-temperature stirring, obtain the copolymer of epoxy resin and polyurethane resin；
S2：To above-mentioned epoxy resin and the ethylene glycol that corresponding weight portion is added in the copolymer of polyurethane resin, dodecane
Base benzene sulfonic acid sodium salt, sodium lauryl sulphate, N, N- dimethyl-N-ethyl benzyl quaternary ammonium salt, white carbon black, hydroquinone, phosphorous acid three
Ethyl ester, coloring agent, dispersant, plasticizer and thickening agent, continue high-temperature stirring, obtain final product plastic cement sizing material；
S3：Above-mentioned sizing material is reinjected in mould, and extrusion molding obtains final product antistatic environment friendly plastic rubber sheet material.
Embodiment two
A kind of antistatic environment friendly plastic rubber sheet material proposed by the present invention, including the raw material of following weight portion：Epoxy resin 100
Part, 50 parts of polyurethane resin, 30 parts of ethylene glycol, 8 parts of dodecylbenzene sodium sulfonate, 3 parts of sodium lauryl sulphate, N, N- diformazan
8 parts of base-N- Ethylbenzyls quaternary ammonium salt, 12 parts of white carbon black, 5 parts of phenol, 3 parts of NSC 5284,10 parts of coloring agent, 5 parts of dispersant,
6 parts of plasticizer, 6 parts of thickening agent, 3 parts of cross-linking agent, 4 parts of emulsifying agent.
Its preparation method, comprises the following steps：
S1：The epoxy resin of corresponding weight portion, polyurethane resin, cross-linking agent and emulsifying agent are added in kneader, and
It is 100 DEG C by temperature setting, carries out high-temperature stirring, obtain the copolymer of epoxy resin and polyurethane resin；
S2：To above-mentioned epoxy resin and the ethylene glycol that corresponding weight portion is added in the copolymer of polyurethane resin, dodecane
Base benzene sulfonic acid sodium salt, sodium lauryl sulphate, N, N- dimethyl-N-ethyl benzyl quaternary ammonium salt, white carbon black, phenol, NSC 5284,
Coloring agent, dispersant, plasticizer and thickening agent, continue high-temperature stirring, obtain final product plastic cement sizing material；
S3：Above-mentioned sizing material is reinjected in mould, and extrusion molding obtains final product antistatic environment friendly plastic rubber sheet material.
Embodiment three
A kind of antistatic environment friendly plastic rubber sheet material proposed by the present invention, including the raw material of following weight portion：80 parts of epoxy resin,
45 parts of polyurethane resin, 10 parts of ethylene glycol, 5 parts of dodecylbenzene sodium sulfonate, 10 parts of sodium lauryl sulphate, N, N- dimethyl-
2 parts of N- Ethylbenzyls quaternary ammonium salt, 10 parts of white carbon black, 3 parts of phenol, 3 parts of NSC 5284,20 parts of coloring agent, 8 parts of dispersant increase
2 parts of agent of modeling, 9 parts of thickening agent, 6 parts of cross-linking agent, 3 parts of emulsifying agent.
Its preparation method, comprises the following steps：
S1：The epoxy resin of corresponding weight portion, polyurethane resin, cross-linking agent and emulsifying agent are added in kneader, and
It is 80 DEG C by temperature setting, carries out high-temperature stirring, obtain the copolymer of epoxy resin and polyurethane resin；
S2：To above-mentioned epoxy resin and the ethylene glycol that corresponding weight portion is added in the copolymer of polyurethane resin, dodecane
Base benzene sulfonic acid sodium salt, sodium lauryl sulphate, N, N- dimethyl-N-ethyl benzyl quaternary ammonium salt, white carbon black, phenol, NSC 5284,
Coloring agent, dispersant, plasticizer and thickening agent, continue high-temperature stirring, obtain final product plastic cement sizing material；
S3：Above-mentioned sizing material is reinjected in mould, and extrusion molding obtains final product antistatic environment friendly plastic rubber sheet material.
Example IV
A kind of antistatic environment friendly plastic rubber sheet material proposed by the present invention, including the raw material of following weight portion：50 parts of epoxy resin,
50 parts of polyurethane resin, 30 parts of ethylene glycol, 2 parts of dodecylbenzene sodium sulfonate, 3 parts of sodium lauryl sulphate, N, N- dimethyl-N-
8 parts of Ethylbenzyl quaternary ammonium salt, 3 parts of white carbon black, 2 parts of hydroquinone, 1 part of NSC 5284,14 parts of coloring agent, 4 parts of dispersant increase
4 parts of agent of modeling, 3 parts of thickening agent, 3 parts of cross-linking agent, 2 parts of emulsifying agent.
Its preparation method, comprises the following steps：
S1：The epoxy resin of corresponding weight portion, polyurethane resin, cross-linking agent and emulsifying agent are added in kneader, and
It is 80 DEG C by temperature setting, carries out high-temperature stirring, obtain the copolymer of epoxy resin and polyurethane resin；
S2：To above-mentioned epoxy resin and the ethylene glycol that corresponding weight portion is added in the copolymer of polyurethane resin, dodecane
Base benzene sulfonic acid sodium salt, sodium lauryl sulphate, N, N- dimethyl-N-ethyl benzyl quaternary ammonium salt, white carbon black, hydroquinone, phosphorous acid three
Ethyl ester, coloring agent, dispersant, plasticizer and thickening agent, continue high-temperature stirring, obtain final product plastic cement sizing material；
S3：Above-mentioned sizing material is reinjected in mould, and extrusion molding obtains final product antistatic environment friendly plastic rubber sheet material.
Plastic sheet proposed by the present invention, using epoxy resin and polyurethane resin copolymerization, improves the overall waterproof of plastic cement
Performance and resistance to elevated temperatures, add kinds of surface activating agent significantly increase can the anti-static ability of plastic sheet, white carbon black and
Isolation ultraviolet is played in the addition of antioxidant again, is improved plastic cement oxidation resistance, is delayed plastic cement rate of ageing, it is to avoid modeling occurs
The phenomenon that glue product turns yellow, and a kind of the invention allows for preparation method of simple antistatic environment friendly plastic rubber sheet material.
The above, the only present invention preferably specific embodiment, but protection scope of the present invention is not limited thereto,
Any those familiar with the art the invention discloses technical scope in, technology according to the present invention scheme and its
Inventive concept equivalent or change in addition, should all be included within the scope of the present invention.
Claims (7)
1. a kind of antistatic environment friendly plastic rubber sheet material, it is characterised in that including the raw material of following weight portion：Epoxy resin 80～100
Part, 40～50 parts of polyurethane resin, 10～30 parts of ethylene glycol, 2～8 parts of dodecylbenzene sodium sulfonate, sodium lauryl sulphate 3～
10 parts, 2～8 parts of N, N- dimethyl-N-ethyl benzyl quaternary ammonium salt, 3～12 parts of white carbon black, 3～8 parts of antioxidant, coloring agent 10～
20 parts, 2～8 parts of dispersant, 2～6 parts of plasticizer, 3～9 parts of thickening agent, 3～6 parts of cross-linking agent, 2～4 parts of emulsifying agent.
2. a kind of antistatic environment friendly plastic rubber sheet material according to claim 1, it is characterised in that including the original of following weight portion
Material：85～95 parts of epoxy resin, 40～50 parts of polyurethane resin, 15～25 parts of ethylene glycol, 3～7 parts of dodecylbenzene sodium sulfonate,
4～10 parts of sodium lauryl sulphate, 4～6 parts of N, N- dimethyl-N-ethyl benzyl quaternary ammonium salt, 4～12 parts of white carbon black, antioxidant 3
～6 parts, 12～18 parts of coloring agent, 4～6 parts of dispersant, 2～6 parts of plasticizer, 4～8 parts of thickening agent, 3～6 parts of cross-linking agent, emulsifying
2～4 parts of agent.
3. a kind of antistatic environment friendly plastic rubber sheet material according to claim 1, it is characterised in that including the original of following weight portion
Material：90 parts of epoxy resin, 45 parts of polyurethane resin, 20 parts of ethylene glycol, 5 parts of dodecylbenzene sodium sulfonate, sodium lauryl sulphate 7
Part, 5 parts of N, N- dimethyl-N-ethyl benzyl quaternary ammonium salt, 8 parts of white carbon black, 5 parts of antioxidant, 15 parts of coloring agent, 5 parts of dispersant increase
4 parts of agent of modeling, 6 parts of thickening agent, 4 parts of cross-linking agent, 3 parts of emulsifying agent.
4. a kind of antistatic environment friendly plastic rubber sheet material according to claim 1, it is characterised in that the antioxidant includes master
Antioxidant and auxiliary antioxidant, and the weight part ratio of main anti-oxidant and auxiliary antioxidant is 1～2:1.
5. a kind of antistatic environment friendly plastic rubber sheet material according to claim 4, it is characterised in that the primary antioxidant is to benzene
Diphenol or phenol.
6. a kind of antistatic environment friendly plastic rubber sheet material according to claim 4, it is characterised in that the auxiliary antioxidant is
NSC 5284.
7. a kind of preparation method of antistatic environment friendly plastic rubber sheet material, it is characterised in that comprise the following steps：
S1：The epoxy resin of corresponding weight portion, polyurethane resin, cross-linking agent and emulsifying agent are added in kneader, and by temperature
Degree is set to 80～100 DEG C, carries out high-temperature stirring, obtains the copolymer of epoxy resin and polyurethane resin；
S2：To above-mentioned epoxy resin and the ethylene glycol that corresponding weight portion is added in the copolymer of polyurethane resin, detergent alkylate
Sodium sulfonate, sodium lauryl sulphate, N, N- dimethyl-N-ethyl benzyl quaternary ammonium salt, white carbon black, antioxidant, coloring agent, dispersion
Agent, plasticizer and thickening agent, continue high-temperature stirring, obtain final product plastic cement sizing material；
S3：Above-mentioned sizing material is reinjected in mould, and extrusion molding obtains final product antistatic environment friendly plastic rubber sheet material.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610945933.7A CN106554629A (en) | 2016-11-02 | 2016-11-02 | A kind of antistatic environment friendly plastic rubber sheet material and preparation method thereof |
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| CN201610945933.7A CN106554629A (en) | 2016-11-02 | 2016-11-02 | A kind of antistatic environment friendly plastic rubber sheet material and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2018188493A (en) * | 2017-04-28 | 2018-11-29 | 竹本油脂株式会社 | Conductive agent for synthetic resin, conductive resin composition and conductive floor material |
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| CN1220284A (en) * | 1998-11-13 | 1999-06-23 | 湖北省化学研究所 | Epoxy resin compound for electrostatic prevention and its preparation |
| CN1664035A (en) * | 2005-02-22 | 2005-09-07 | 大庆石油管理局 | Composite electric conductor static-conducting coating and method for making same |
| CN105086766A (en) * | 2015-09-14 | 2015-11-25 | 苏州法斯特信息科技有限公司 | Antistatic environment-friendly water-based paint and preparation method thereof |
| CN106010118A (en) * | 2016-06-27 | 2016-10-12 | 北京理工大学珠海学院 | Epoxy resin paint with antistatic property and preparation method thereof |
| CN106047081A (en) * | 2016-07-28 | 2016-10-26 | 苏州明轩地坪涂料有限公司 | Efficient antistatic paint |
-
2016
- 2016-11-02 CN CN201610945933.7A patent/CN106554629A/en active Pending
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| CN1220284A (en) * | 1998-11-13 | 1999-06-23 | 湖北省化学研究所 | Epoxy resin compound for electrostatic prevention and its preparation |
| CN1664035A (en) * | 2005-02-22 | 2005-09-07 | 大庆石油管理局 | Composite electric conductor static-conducting coating and method for making same |
| CN105086766A (en) * | 2015-09-14 | 2015-11-25 | 苏州法斯特信息科技有限公司 | Antistatic environment-friendly water-based paint and preparation method thereof |
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| Title |
|---|
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| 马虹 主编: "《教育部高职高专规划教材 化学实验技术 二》", 31 July 2002, 化学工业出版社 * |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| JP2018188493A (en) * | 2017-04-28 | 2018-11-29 | 竹本油脂株式会社 | Conductive agent for synthetic resin, conductive resin composition and conductive floor material |
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Application publication date: 20170405 |