CN105077473B - A kind of honeysuckle beverage concentrate and preparation method thereof - Google Patents
A kind of honeysuckle beverage concentrate and preparation method thereof Download PDFInfo
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- CN105077473B CN105077473B CN201510433386.XA CN201510433386A CN105077473B CN 105077473 B CN105077473 B CN 105077473B CN 201510433386 A CN201510433386 A CN 201510433386A CN 105077473 B CN105077473 B CN 105077473B
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- 235000008504 concentrate Nutrition 0.000 title claims abstract description 53
- 238000002360 preparation method Methods 0.000 title claims abstract description 23
- 241000205585 Aquilegia canadensis Species 0.000 title claims abstract 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 59
- 239000007788 liquid Substances 0.000 claims abstract description 49
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 30
- 238000001914 filtration Methods 0.000 claims abstract description 29
- 238000003756 stirring Methods 0.000 claims abstract description 23
- 238000001556 precipitation Methods 0.000 claims abstract description 22
- 235000012907 honey Nutrition 0.000 claims abstract description 18
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims abstract description 17
- 229930006000 Sucrose Natural products 0.000 claims abstract description 17
- 239000005720 sucrose Substances 0.000 claims abstract description 17
- 150000003839 salts Chemical class 0.000 claims abstract description 12
- UQZIYBXSHAGNOE-USOSMYMVSA-N Stachyose Natural products O(C[C@H]1[C@@H](O)[C@H](O)[C@H](O)[C@@H](O[C@@]2(CO)[C@H](O)[C@@H](O)[C@@H](CO)O2)O1)[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@H](CO[C@@H]2[C@@H](O)[C@@H](O)[C@@H](O)[C@H](CO)O2)O1 UQZIYBXSHAGNOE-USOSMYMVSA-N 0.000 claims abstract description 11
- UQZIYBXSHAGNOE-XNSRJBNMSA-N stachyose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO[C@@H]2[C@@H]([C@@H](O)[C@@H](O)[C@@H](CO[C@@H]3[C@@H]([C@@H](O)[C@@H](O)[C@@H](CO)O3)O)O2)O)O1 UQZIYBXSHAGNOE-XNSRJBNMSA-N 0.000 claims abstract description 11
- 239000006071 cream Substances 0.000 claims description 38
- 235000013361 beverage Nutrition 0.000 claims description 28
- 238000004821 distillation Methods 0.000 claims description 16
- 239000008213 purified water Substances 0.000 claims description 9
- 239000006228 supernatant Substances 0.000 claims description 9
- 239000000706 filtrate Substances 0.000 claims description 8
- 239000002994 raw material Substances 0.000 claims description 7
- 239000000470 constituent Substances 0.000 claims description 6
- 238000002386 leaching Methods 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 5
- 238000004140 cleaning Methods 0.000 claims description 4
- 230000006837 decompression Effects 0.000 claims description 4
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims description 4
- 229910052737 gold Inorganic materials 0.000 claims description 4
- 239000010931 gold Substances 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 239000012535 impurity Substances 0.000 claims description 4
- 239000012982 microporous membrane Substances 0.000 claims description 4
- 239000002893 slag Substances 0.000 claims description 4
- 239000000341 volatile oil Substances 0.000 claims description 4
- 238000004062 sedimentation Methods 0.000 claims description 3
- 238000005292 vacuum distillation Methods 0.000 claims description 3
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 2
- 238000001816 cooling Methods 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- 229910052709 silver Inorganic materials 0.000 claims description 2
- 239000004332 silver Substances 0.000 claims description 2
- 240000000111 Saccharum officinarum Species 0.000 claims 1
- 235000007201 Saccharum officinarum Nutrition 0.000 claims 1
- 238000009835 boiling Methods 0.000 claims 1
- 238000004064 recycling Methods 0.000 claims 1
- 239000002023 wood Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 7
- 210000000936 intestine Anatomy 0.000 abstract description 6
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- 241000894006 Bacteria Species 0.000 abstract description 4
- 238000009395 breeding Methods 0.000 abstract description 4
- 230000001488 breeding effect Effects 0.000 abstract description 4
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract description 4
- 239000011707 mineral Substances 0.000 abstract description 4
- 239000003053 toxin Substances 0.000 abstract description 4
- 231100000765 toxin Toxicity 0.000 abstract description 4
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 abstract description 3
- 239000011575 calcium Substances 0.000 abstract description 3
- 229910052791 calcium Inorganic materials 0.000 abstract description 3
- 235000009508 confectionery Nutrition 0.000 abstract description 3
- 206010012601 diabetes mellitus Diseases 0.000 abstract description 3
- 238000010790 dilution Methods 0.000 abstract description 3
- 239000012895 dilution Substances 0.000 abstract description 3
- 238000007599 discharging Methods 0.000 abstract description 3
- 230000035622 drinking Effects 0.000 abstract description 3
- 239000006041 probiotic Substances 0.000 abstract description 3
- 235000018291 probiotics Nutrition 0.000 abstract description 3
- 230000001737 promoting effect Effects 0.000 abstract description 3
- 230000009102 absorption Effects 0.000 abstract description 2
- 238000010521 absorption reaction Methods 0.000 abstract description 2
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- 241001122767 Theaceae Species 0.000 abstract 1
- 241001570521 Lonicera periclymenum Species 0.000 description 73
- 230000001954 sterilising effect Effects 0.000 description 20
- 239000000243 solution Substances 0.000 description 17
- 238000001514 detection method Methods 0.000 description 13
- 238000007689 inspection Methods 0.000 description 11
- 235000013616 tea Nutrition 0.000 description 6
- 241001391944 Commicarpus scandens Species 0.000 description 5
- 239000012141 concentrate Substances 0.000 description 4
- 238000011049 filling Methods 0.000 description 4
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- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
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- 239000007938 effervescent tablet Substances 0.000 description 2
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- 230000036039 immunity Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 241000186000 Bifidobacterium Species 0.000 description 1
- 241000208828 Caprifoliaceae Species 0.000 description 1
- 206010007247 Carbuncle Diseases 0.000 description 1
- 206010010774 Constipation Diseases 0.000 description 1
- 206010012735 Diarrhoea Diseases 0.000 description 1
- 201000000297 Erysipelas Diseases 0.000 description 1
- 244000184734 Pyrus japonica Species 0.000 description 1
- 206010044565 Tremor Diseases 0.000 description 1
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- 235000018927 edible plant Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 239000012943 hotmelt Substances 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
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- 235000013406 prebiotics Nutrition 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Non-Alcoholic Beverages (AREA)
Abstract
The invention provides a kind of honeysuckle beverage concentrate and preparation method, wherein dry honeysuckle 66.2%~76.6%, stachyose 23.0%~33.4%, salt 0.3%~0.8%；By distilling, extracting, be concentrated under reduced pressure, alcohol precipitation, water sink, preparation produces honeysuckle beverage concentrate；Or the sucrose of gross mass 5% or the honey of relative density >=1.349 are added in the honeysuckle beverage concentrate prepared, stirring and dissolving, filtering produces the honeysuckle beverage concentrate for adding sucrose or honey.The present invention is faint yellow to fallow clear liquid, has the peculiar fragrance of honeysuckle, the micro- sweet tea of taste.With clearing heat and detoxicating, dispelling wind and heat from the body effect, also there is protection, promote the breeding of intestines and stomach probiotics; suppress harmful bacteria growing; toxin expelling lead discharging, the effect for promoting the mineral absorptions such as calcium, are not only suitable and are drunk in adult, be also adapted for pregnant, puerpera, infant, weakling, patients with diabetes mellitus.This product was both capable of direct drinking, was drunk after can also adding 20ml~100ml pure water, mineral water, warm water dilution.
Description
Technical field
The invention belongs to technical field of beverage processing, more particularly to a kind of honeysuckle beverage manufacture field, and in particular to one
Plant honeysuckle beverage concentrate and preparation method thereof.
Background technology
Honeysuckle is recorded in Chinese Pharmacopoeia（Version in 2010）One, page 205, are caprifoliaceae plant honeysuckle Lonicer
Japonica Thunb. dry flowers or with the flower just opened.Summer and autumn the flowers are in blossom hair before harvest, dry.It is sweet, tremble with fear.The thoughts of returning home, lung, stomach footpath.
It is clearing heat and detoxicating, dispelling wind and heat from the body.Sore, larynx numbness, erysipelas, heat toxin blood profit, anemopyretic cold, warm disease heating are treated for carbuncle swells.
Commercially the beverage of honeysuckle is more at present,
A kind of plant cold tea decompressed concentrates of the B of CN 102578331 are preparation method；
A kind of plant cold teas of the B of CN 101292692 are concentrated under reduced pressure juice；
A kind of internal heat lowering cool teas of the B of CN 101147510 and preparation method；
A kind of honeysuckle health-care beverages of the B of CN 101288485；
A kind of preparation methods of honeysuckle beverage of the B of CN 101720962；
A kind of honeysuckle leaf distillate beverages of the B of CN 101785568 and preparation method；
The B honeysuckle effervescent tablets of CN 101828745 and preparation method；
A kind of Chinese medicinal herb cold teas of the A of CN 102793038 and preparation method；
A kind of honeysuckle tea powders of the A of CN 104171198 and preparation method, honeysuckle effervescent tablet and preparation method；
A kind of solid particle beverages of the A of CN 104489847 and preparation method；
A kind of honeysuckle health-care beverages of the A of CN 104432381 and preparation method；
A kind of honeysuckle health-care beverages of the A of CN 104544440 and preparation method；
The materials containing honeysuckle are refer in 12 disclosed patent documents of the above, but for honeysuckle beverage concentrate
Above there is not yet reporting for work.
Relevant production technology and literature survey result show that composition containing Honegsukle flower P.E is dense in the market honeysuckle beverage
Degree is low, and volume is big, and net content is usually the not Portable belt in more than 200ml；Do not possess the breeding for promoting the preferably raw bacterium of intestines and stomach, change
The effect of kind gastro-intestinal tract and function.
The content of the invention
The technical problem to be solved in the present invention is to overcome above-mentioned deficiency, studies a kind of features good taste, extracted containing honeysuckle
Thing constituent concentration is high, small volume, honeysuckle beverage concentrate easy to carry.
The invention provides a kind of honeysuckle beverage concentrate, it is not only suitable and is drunk in adult, is more suitable for pregnant, puerpera, baby
Child, weakling, patients with diabetes mellitus, it is both capable of direct drinking, also it can add 2 again by honeysuckle beverage concentrate volume~5 times of amounts
Drunk after pure water, mineral water, warm water dilution；Can packing with small volume, it is easy to carry.
To realize the purpose of the present invention, following technical scheme is taken：A kind of honeysuckle beverage concentrate, it is characterised in that：
It is comprised the following raw materials by weight percent：Dry honeysuckle 66.2%~76.6%, stachyose 23.0%~33.4%, salt 0.3%
~0.8%；By distilling, extracting, be concentrated under reduced pressure, alcohol precipitation, water sink, preparation produces honeysuckle beverage concentrate；Or preparing
Honeysuckle beverage concentrate in add the sucrose of gross mass 5% or the honey of relative density >=1.349, stirring and dissolving, filtering,
Produce the honeysuckle beverage concentrate for adding sucrose or honey.
A kind of preparation method of honeysuckle beverage concentrate, it is characterised in that：
Comprise the following steps,
1）Selection cleaning：Dry honeysuckle is taken, impurity is rejected in selection, after water wash 3~5 minutes, drip water remaining to the greatest extent；
2）Distillation：The honeysuckle eluted is put into multifunctional extracting pot, added water, distillation is collected in heating temperature leaching, distillation
Liquid, is cooled down, and is stood, and score by weight takes the upper strata distillate filtering rich in volatile oil, obtains the distillate of dry honeysuckle weight 70%
Upper liquid；
3）Extract：After distillation procedure terminates, raffinate after the raffinate not distilled in multifunctional extracting pot must distill is collected；Multipotency
Honeysuckle slag, which is added water, in extractor decocts 1 time to obtain decocting liquid, merges raffinate and decocting liquid after distillation, filters to obtain extract solution；
4）It is concentrated under reduced pressure：By extract solution be concentrated under reduced pressure relative density be 1.10~1.26 extract solution clear cream；
5）Alcohol precipitation：Ethanol in proper amount is slowly added into extract solution clear cream, is stirred evenly, is stood, sedimentation takes supernatant liquid filtering, filters
Liquid reclaim ethanol, be concentrated under reduced pressure relative density be 1.08~1.22 precipitation solution clear cream；
6）Water sinks：Add purified water into precipitation solution clear cream, stir evenly, cool down, stand, settle, take supernatant liquid filtering, filtrate subtracts
It is the heavy liquid clear cream of 1.06~1.14 water that pressure, which is concentrated to give relative density,；
7）Prepare：Take the heavy liquid clear cream of distillate upper liquid, water successively to put into preparing tank to stir evenly, add stachyose, food
Salt, is stirred to dissolve, plus purified water, to total amount is prepared after 0.8~3.2 times of dry honeysuckle weight, to stir evenly, filtering produces gold
Honeysuckle flower beverage concentrate；Or added in the honeysuckle beverage concentrate prepared gross mass 5% sucrose or relative density >=
1.349 honey, stirring and dissolving, filtering produces the honeysuckle beverage concentrate for adding sucrose or honey.
Beneficial effect：
The invention provides a kind of honeysuckle beverage concentrate, raw material honeysuckle has clearing heat and detoxicating, dispelling wind and heat from the body function；It is former
Expect stachyose, purity is extracted, can protect and remarkably promote Bifidobacterium etc. has more than 85% from the edible plants such as kobold
Beneficial bacteria is bred, and can effectively be prevented and be alleviated constipation of infantile and diarrhoea, suppresses the immunity energy of intestines problem, comprehensively enhancing infant
Power and body's resistance to disease.Also with gut purge road, the minerals absorbing effect such as toxin expelling lead discharging, promotion calcium, is a kind of prebiotic sugar；Raw material
Salt is material needed by human, and three kinds of material composition synergies make this product not only there is clearing heat and detoxicating, dispelling wind and heat from the body to make
With, also have and promote the breeding of intestines and stomach probiotics, improvement gastrointestinal tract environment and functions of intestines and stomach, the effect of enhancing body immunity.
The honeysuckle beverage concentrate as made from this method, is faint yellow to fallow clear liquid, and tool honeysuckle is peculiar
Fragrance, the micro- sweet tea of taste.With clearing heat and detoxicating, dispelling wind and heat from the body effect, also there is protection, promote the breeding of intestines and stomach probiotics, suppress harmful
Bacteria growing, toxin expelling lead discharging, the effect for promoting the mineral absorptions such as calcium, there is preferable healthcare function；It is not only suitable and is drunk in adult,
It is also adapted for pregnant, puerpera, infant, weakling, patients with diabetes mellitus；Both it is capable of direct drinking, can also it add 20ml~100ml pure
Drunk after water purification, mineral water, warm water dilution；According to《Plant beverage hygienic requirements, DBJ440100/T 30-2009（Guangzhou
Administration of Quality and Technology Supervision of city issues）》Check, comply fully with standard requirement.
Embodiment
In order to more clearly state the present invention, there is provided preferably embodiment.
A kind of honeysuckle beverage concentrate, the raw material composition matched containing following weight percent：Dry honeysuckle 66.2%~
76.6%, stachyose 23.0%~33.4%, the % of salt 0.3%~0.8；By distilling, extracting, be concentrated under reduced pressure, alcohol precipitation, water sinks, matches somebody with somebody
System produces honeysuckle beverage concentrate；Or the sucrose or phase of gross mass 5% are added in the honeysuckle beverage concentrate prepared
To the honey of density >=1.349, stirring and dissolving, filtering produces the honeysuckle beverage concentrate for adding sucrose or honey.
The raw material group of optimum weight per distribution ratio when a kind of honeysuckle beverage concentrate of the present invention is drunk for infant
Turn into：Dry honeysuckle 74.4%, stachyose 24.8%, salt 0.8%；By distilling, extracting, be concentrated under reduced pressure, alcohol precipitation, water are heavy, prepare
Produce honeysuckle beverage concentrate；Or the sucrose or relative of gross mass 5% is added in the honeysuckle beverage concentrate prepared
The honey of density >=1.349, stirring and dissolving, filtering produces the honeysuckle beverage concentrate for adding sucrose or honey.
A kind of honeysuckle beverage concentrate of the present invention is used for the raw material composition of optimum weight per distribution ratio when adult drinks
For：Dry honeysuckle 74.7%, stachyose 25%, salt 0.3%.
A kind of preparation method of honeysuckle beverage concentrate, it includes successively：Selection clean, distill, extracting, being concentrated under reduced pressure,
The operation step such as alcohol precipitation, water are heavy, preparation, filling and sealing, sterilizing, leak detection, quality examination is poly-.
1）Selection cleaning：Concrete operations include taking dry honeysuckle, and impurity is rejected in selection；Weigh gross weight 66.2%~76.6%
Dry honeysuckle, with water wash 3~5 minutes.
2）Distillation：Concrete operations include putting into the honeysuckle eluted in multifunctional extracting pot, by weight, plus dry gold
The water of 8~10 times of honeysuckle flower weight amount, after being heated to 50 DEG C~60 DEG C temperature leachings 30 minutes, in -0.02Mpa~-0.04Mpa conditions
Lower vacuum distillation, by weight, collects the distillate of dry 1~1.5 times of honeysuckle weight, distillate is cooled into 2 DEG C~12 DEG C,
And standing is after 6~12 hours at such a temperature, by weight, divides from the distillate after standing and take dry honeysuckle weight 70%
Upper strata distillate rich in volatile oil, distillate upper liquid is obtained with 0.45~1.0 μm of membrane filter, and distillate upper liquid is collected
In clean container, store under the conditions of 2 DEG C~12 DEG C standby.
3）Extract：After concrete operations terminate including distillation procedure, collecting the raffinate not distilled in multifunctional extracting pot must steam
Evaporate rear raffinate；Honeysuckle slag after being distilled in multifunctional extracting pot add water decoction 1 time decocting liquid, amount of water is by weight during decoction
Meter, for 6~8 times of the weight of dry honeysuckle, decocting time is 30~60 minutes, after decoction terminates, merge after distillation raffinate and
Decocting liquid, filters to obtain extract solution.
4）It is concentrated under reduced pressure：Concrete operations include extract solution is placed in decompression concentrator, vacuum be -0.02~-
Under the conditions of 0.06Mpa, it is concentrated under reduced pressure into relative density to obtain extract solution clear cream after 1.10~1.26 clear creams.
5）Alcohol precipitation：Concrete operations include moving into extract solution clear cream in clean settling tank, are slowly added into ethanol, side edged is stirred
Mixing makes concentration of alcohol reach 60%~80%（g/g）, room temperature is cooled to, 48~72 hours are stood, Aspirate supernatant filtering, filtrate is returned
Ethanol is received, and is concentrated under reduced pressure into the clear cream that relative density is 1.08~1.22 and obtains precipitation solution clear cream.
6）Water sinks：Concrete operations include moving to precipitation solution clear cream in clean settling tank, under conditions of stirring while adding,
By dry weight, the purified water of dry 0.7~1.5 times of honeysuckle weight is added into precipitation solution clear cream, stirs evenly, is cooled to 2~10 DEG C
And 12~24 hours are stood at such a temperature, it is 0.45~1.0 μm of filtering with microporous membrane to take supernatant aperture, and filtrate is in vacuum
Spend and obtain the heavy liquid clear cream of water under the conditions of -0.02~-0.06Mpa, to be concentrated under reduced pressure into the clear cream that relative density is 1.06~1.14,
Store under the conditions of 2 DEG C~12 DEG C standby.
7）Prepare：Concrete operations include taking in distillate upper liquid and the heavy liquid clear cream input preparing tank of water, stir evenly, add three
The stachyose and 0.3%~0.8% salt of constituent gross weight 23.0%~33.4% are planted, is stirred to dissolve, by weight, plus it is pure
It is 0.8~3.2 times of dry honeysuckle weight to change water to total amount is prepared, and is stirred evenly, and stands 15~30 minutes, is first 0.45 μm with aperture
~1.0 μm of filtering with microporous membrane, then with aperture be 0.22 μm of filtering with microporous membrane produce honeysuckle beverage concentrate, wherein 0.8 times
Water be adapted to adult, 3.2 times of water is adapted to young child；Or added in the honeysuckle beverage concentrate prepared total
The sucrose of quality 5% or the honey of relative density >=1.349, stirring and dissolving, filtering, is produced plus the honeysuckle of sucrose or honey is dense
Contracting beverage.
8）Filling and sealing：Concrete operations include preparation liquid is filling in 10ml, 20ml cleaning PET bottles easy to break respectively, dress
Amount respectively every bottle of 10.3ml~10.8ml, every bottle of 20.5ml~21.0ml, plus the tight envelope of bottom hot melt produce beverage subject to sterilization.
9）Sterilizing：By beverage bottle bottom subject to sterilization down, just stand in vehicle of sterilization, in the isobaric sterilizing leak detection cabinet of feeding, close
Cabinet door, the pressure control device such as opens, inside and outside control PET bottles easy to break under conditions of equipressure, flowing steam is heated to 100~105
DEG C sterilizing 45~60 minutes, after purified water spraying cooling to room temperature, close isobaric sterilizing leak detection cabinet etc. pressure control device, i.e.,
Obtain sterilising drink.
10）Leak detection：Isobaric sterilizing leak detection cabinet pumped vacuum systems is opened, -0.006~-0.01Mpa is evacuated to, and at this
Under the conditions of kept for 15 minutes after, close isobaric sterilizing leak detection cabinet pumped vacuum systems, open isobaric sterilizing leak detection cabinet cabinet door and take out drink
Material, produces beverage of having hunted leak.
11）Quality examination：Concrete operations include the beverage taking-up from sterilizing leak detection cabinet that will hunt leak, and send in darkroom, put
In being checked under canopy type lamp inspection cabinet, canopy type lamp inspection cabinet illumination is adjusted to 3000Lx, and background is white not return light.During inspection, inspection
Human hand is looked into by beverage bottle bottleneck, beverage bottle is just being stood on shadow shield lower edge, scrutineer's adjustment eye it is fine away from beverage bottle about 25cm at
Carefully inspect liquid level in bottle, and compared with qualified reference substance liquid level, reject empty bottle and loading amount undesirable half into
Product, concentrate and destroy；Beverage bottle is overturn with slow action again, beverage bottle is stood upside down respectively, is just standing on the continuation inspection of shadow shield lower edge
Look into, sight is first from beverage bottle bottom successively into top pan bottle in liquid and bottle inwall, observation bottle in liquid and bottle during inspection
Wall whether there is visible foreign matters, rejects the semi-finished product for having visible foreign matters in bottle, concentrates and destroys, and satisfactory semi finished package produces gold
Honeysuckle flower beverage concentrate.
Above-mentioned production operation preferred scheme is：
Perform step poly- 1）When, the impurity in honeysuckle is rejected in selection；Weigh dry honeysuckle weight total for three kinds of constituents
Weight 66.2%~76.6%, is 3~5 minutes with the water wash time.
Performing step poly- 2）When, distillation procedure amount of water is 8~10 times of dry honeysuckle weight, temperature leaching temperature is 50 DEG C~
60 DEG C, the warm 30 minutes leaching time, vacuum is -0.02Mpa~-0.04Mpa during vacuum distillation, and distillate collecting amount is dry silver
1~1.5 times of flower weight, temperature is 2 DEG C~12 DEG C when distillate is stood, and time of repose is 6~12 hours；From the steaming after standing
Divide in distillate and take the amount of distillate upper liquid to be the 70% of dry honeysuckle weight, the filter aperture of filtering distillate upper liquid is
0.45~1.0 μm, distillate upper liquid storage temperature is 2~12 DEG C.
Performing step poly- 3）When, it is 6~8 times of dry honeysuckle weight to decoct amount of water, and decocting time is 30~60 minutes.
Performing step poly- 4）When, the vacuum that is concentrated under reduced pressure is -0.02~-0.06Mpa, the control of extract solution clear cream relative density
1.10~1.26.
Performing step poly- 5）When, precipitation solution concentration of alcohol is controlled 60%~80%（g/g）, precipitation solution is cooled to quiet after room temperature
The time is put for 48~72 hours, is reclaimed after ethanol, it is 1.08~1.22 that precipitation solution clear cream, which is concentrated under reduced pressure into relative density,.
Performing step poly- 6）When, it is 0.7~1.5 times of dry honeysuckle weight, standing sedimentation that purifying water is added into clear cream
Temperature is 2~10 DEG C, time of repose 12~24 hours, and porous filtering-diaphragm filter aperture is 0.45~1.0 μm when taking supernatant liquid filtering,
The vacuum of filtrate decompression concentration is -0.02~-0.06Mpa, water sink liquid clear cream be concentrated under reduced pressure into relative density for 1.06~
1.14, water sinks immersion cream storage temperature for 2 DEG C~12 DEG C.
Performing step poly- 7）When, distillate upper liquid and water sink liquid clear cream addition for full dose, and stachyose addition is three
The 23.0%~33.4% of constituent gross weight is planted, salt addition is the 0.3%~0.8% of three kinds of constituent gross weights, is matched somebody with somebody
Total amount processed is 0.8~3.2 times of dry honeysuckle weight, prepares liquid time of repose 15 minutes~30 minutes, prepares the 1st filtering of liquid
Porous filtering-diaphragm filter aperture be 0.45 μm~1.0 μm, the 2nd time filtering porous filtering-diaphragm filter also footpath be 0.22 μm.
Performing step poly- 8）When, container filling is 10ml, 20ml PET bottles easy to break, and loading amount controls easy in 10ml PET respectively
Every bottle of 10.3ml~10.8ml of bottle, 20ml PET every bottle of 20.5ml~21.0ml of bottle easy to break are rolled over, must sternly be sealed during sealing.
Performing step poly- 9）When, sterilize using isobaric sterilizing leak detection cabinet, in pressure control systems such as unlatchings, control PET is easy to break
Sterilized and cooled down under conditions of bottle external and internal pressure is equal；Sterilizing heating medium for circulation steam, sterilising temp be 100~
105 DEG C, sterilization time 45~60 minutes uses purified water spraying method by beverage but to room temperature after sterilizing.
Performing step poly- 10）When, hunted leak with equipressure sterilizing leak detection cabinet, should first close the equipressure control of isobaric sterilizing leak detection cabinet
System, leak detection vacuum degree control scope is -0.006~-0.01Mpa, and the leak detection time is 15 minutes.
Performing step poly- 11）When, inspection chamber should be darkroom, and canopy type lamp inspection cabinet is non-reflective white background, and illumination is
3000Lx, checks that human hand takes beverage bottle bottleneck, and canopy type lamp inspection cabinet shadow shield lower edge, scrutineer are placed in by beverage bottle during inspection
The fine distance about 25cm with light source of eye, should reject that empty bottle, loading amount be not enough, have visible foreign matters etc. undesirable in bottle during inspection
Beverage, undesirable beverage should concentrate destruction, and satisfactory beverage concentrates packaging to produce.
Claims (7)
1. a kind of honeysuckle beverage concentrate, it is characterised in that：It is comprised the following raw materials by weight percent：Dry honeysuckle
66.2%~76.6%, stachyose 23.0%~33.4%, salt 0.3%~0.8%；By distilling, extracting, be concentrated under reduced pressure, alcohol precipitation, water
Heavy, preparation produces honeysuckle beverage concentrate；Or the sugarcane of gross mass 5% is added in the honeysuckle beverage concentrate prepared
Sugar or the honey of relative density >=1.349, stirring and dissolving, filtering produce the honeysuckle beverage concentrate for adding sucrose or honey；
Its preparation method comprises the following steps：
1）Selection cleaning：Dry honeysuckle is taken, impurity is rejected in selection, after water wash 3~5 minutes, drip water remaining to the greatest extent；
2）Distillation：The honeysuckle eluted is put into multifunctional extracting pot, added water, distillate is collected in heating temperature leaching, distillation,
Cooling, is stood, and score by weight is taken on the upper strata distillate filtering rich in volatile oil, the distillate for obtaining dry honeysuckle weight 70%
Layer liquid；
3）Extract：After distillation procedure terminates, raffinate after the raffinate not distilled in multifunctional extracting pot must distill is collected；Multipotency is extracted
Honeysuckle slag, which is added water, in tank decocts 1 time to obtain decocting liquid, merges raffinate and decocting liquid after distillation, filters to obtain extract solution；
4）It is concentrated under reduced pressure：By extract solution be concentrated under reduced pressure relative density be 1.10~1.26 extract solution clear cream；
5）Alcohol precipitation：Ethanol in proper amount is slowly added into extract solution clear cream, is stirred evenly, is stood, sedimentation takes supernatant liquid filtering, and filtrate is returned
Receive ethanol, be concentrated under reduced pressure relative density be 1.08~1.22 precipitation solution clear cream；
6）Water sinks：Add purified water into precipitation solution clear cream, stir evenly, cool down, stand, settle, take supernatant liquid filtering, filtrate decompression is dense
Contract relative density is 1.06~1.14 heavy liquid clear creams；
7）Prepare：Take the heavy liquid clear cream of distillate upper liquid, water successively to put into preparing tank to stir evenly, add stachyose, salt, stir
Mixing makes dissolving, plus purified water, to total amount is prepared after 0.8~3.2 times of dry honeysuckle weight, to stir evenly, it is dense that filtering produces honeysuckle
Contracting beverage；Or sucrose or relative density >=1.349 of gross mass 5% are added in the honeysuckle beverage concentrate prepared
Honey, stirring and dissolving, filtering, produce plus sucrose or honey honeysuckle beverage concentrate.
2. a kind of honeysuckle beverage concentrate according to claim 1, it is characterised in that：Described step 2）It is middle to have eluted
Honeysuckle put into multifunctional extracting pot, by weight, plus 8~10 times of dry honeysuckle weight amount water, be heated to 50 DEG C~
60 DEG C of temperature are soaked 30 minutes, the vacuum distillation under the conditions of -0.02Mpa~-0.04Mpa, by weight, collect dry honeysuckle weight
1~1.5 times of distillate, 2 DEG C~12 DEG C are cooled to by distillate, and stand 6~12 hours at such a temperature, after standing
In distillate, divide the upper strata distillate rich in volatile oil for taking dry honeysuckle weight 70%, filter to obtain distillate upper liquid, distill
Liquid upper liquid is collected in clean container, is stored under the conditions of 2 DEG C~12 DEG C standby.
3. a kind of honeysuckle beverage concentrate according to claim 1, it is characterised in that：Described step 3）Distillation terminates
Afterwards, raffinate after the raffinate not distilled in collection multifunctional extracting pot must distill；Honeysuckle slag after distillation adds water decoction 1 time,
Amount of water by weight, for 6~8 times of dry honeysuckle weight, is heated to decocting 30~60 minutes after boiling, decoction terminates during decoction
Decocting liquid is obtained afterwards, merges raffinate and decocting liquid after distillation, and filtering produces filtering extract solution.
4. a kind of honeysuckle beverage concentrate according to claim 1, it is characterised in that：Described step 4）Extract solution is put
In decompression concentrator, under the conditions of vacuum is -0.02~-0.06Mpa, it is 1.10~1.26 to be concentrated under reduced pressure into relative density
Clear cream produces extract solution clear cream.
5. a kind of honeysuckle beverage concentrate according to claim 1, it is characterised in that：Described step 5）Extract solution is clear
Cream is moved into clean settling tank, is slowly added into ethanol, and stirring while adding, concentration of alcohol is cooled to room after reaching 60%~80%
Temperature, stands 48~72 hours, Aspirate supernatant filtering, filtrate recycling ethanol, and be concentrated under reduced pressure into relative density for 1.08~
1.22 clear cream produces precipitation solution clear cream.
6. a kind of honeysuckle beverage concentrate according to claim 1, it is characterised in that：Described step 6）Precipitation solution is clear
Cream is placed in clean settling tank, under conditions of stirring while adding, by weight, and dry honeysuckle weight is added into precipitation solution clear cream
0.7~1.5 times of purified water after, stir evenly, be cooled to 2~10 DEG C, and stand 12~24 hours at such a temperature, take supernatant to use
Aperture is 0.45~1.0 μm of filtering with microporous membrane, and filtrate is concentrated under reduced pressure under the conditions of vacuum is -0.02~-0.06Mpa
Relative density produces the heavy liquid clear cream of water for 1.06~1.14 clear cream, stores under the conditions of 2 DEG C~12 DEG C standby.
7. a kind of honeysuckle beverage concentrate according to claim 1, it is characterised in that：Described step 7）Take on distillate
Layer liquid and water sink in liquid clear cream input preparing tank, stir evenly, add the wood of three kinds of constituent gross weights 23.0%~33.4%
Sugar and 0.3%~0.8% salt, are stirred to dissolve, by weight, plus purified water is the 0.8 of dry honeysuckle weight to total amount is prepared
Stirred evenly after~3.2 times, after standing 15~30 minutes, refilter and produce honeysuckle beverage concentrate；Or in the gold and silver prepared
The sucrose of gross mass 5% or the honey of relative density >=1.349 are added in flower beverage concentrate, stirring and dissolving, filtering is produced and added
The honeysuckle beverage concentrate of sucrose or honey.
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| CN106173729A (en) * | 2016-07-12 | 2016-12-07 | 湖北楚天舒药业有限公司 | A kind of Flos Lonicerae compound beverage and preparation method thereof |
| CN106616191A (en) * | 2016-11-15 | 2017-05-10 | 叶芳健 | Honeysuckle flower and radix puerariae powder effervescent tablets and preparation method |
| CN107950845A (en) * | 2017-11-16 | 2018-04-24 | 湖北瀚思生物科技有限公司 | Honeysuckle functional beverage and its production method |
| CN108095108A (en) * | 2017-12-09 | 2018-06-01 | 天旺科技股份有限公司 | A kind of preparation method of Pitaya Flower health promoting liquid |
| CN109007491A (en) * | 2018-06-05 | 2018-12-18 | 湖北华信制药有限公司 | A kind of honeysuckle herbaceous plant beverage and preparation method thereof |
| CN109221850A (en) * | 2018-09-21 | 2019-01-18 | 泉州黄章智能科技有限公司 | A kind of preparation method of watt of Wei beverage |
| CN109645289A (en) * | 2018-12-28 | 2019-04-19 | 康美新开河（吉林）药业有限公司 | A kind of fresh ginseng solid beverage and preparation method thereof of no sugar addition |
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| CN102578662A (en) * | 2012-02-23 | 2012-07-18 | 武斌 | Preparation method of Flos Lonicerae beverage |
| CN102772573A (en) * | 2012-08-10 | 2012-11-14 | 广东太阳神集团有限公司 | Oral liquid for strengthening immunity and resisting virus and preparation method thereof |
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| CN104432381A (en) * | 2014-12-12 | 2015-03-25 | 广州中国科学院先进技术研究所 | Honeysuckle health beverage and preparation method thereof |
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| CN102578662A (en) * | 2012-02-23 | 2012-07-18 | 武斌 | Preparation method of Flos Lonicerae beverage |
| CN102793038A (en) * | 2012-08-01 | 2012-11-28 | 广州王老吉药业股份有限公司 | Concentrated solution of Chinese herbal tea and preparation method thereof |
| CN102772573A (en) * | 2012-08-10 | 2012-11-14 | 广东太阳神集团有限公司 | Oral liquid for strengthening immunity and resisting virus and preparation method thereof |
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Denomination of invention: Honeysuckle concentrated beverage and its preparation method Effective date of registration: 20210610 Granted publication date: 20171031 Pledgee: Shiyan Tianditong Health Products Co.,Ltd. Pledgor: Hubei Wudang Biopharmaceutical Science and Technology Co.,Ltd. Registration number: Y2021980004664 |
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