CN105077473A - Honeysuckle concentrating beverage and preparation method thereof - Google Patents
Honeysuckle concentrating beverage and preparation method thereof Download PDFInfo
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- CN105077473A CN105077473A CN201510433386.XA CN201510433386A CN105077473A CN 105077473 A CN105077473 A CN 105077473A CN 201510433386 A CN201510433386 A CN 201510433386A CN 105077473 A CN105077473 A CN 105077473A
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- 241000205585 Aquilegia canadensis Species 0.000 title claims 32
- 235000013361 beverage Nutrition 0.000 title abstract description 41
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- 239000007788 liquid Substances 0.000 claims abstract description 47
- 238000003756 stirring Methods 0.000 claims abstract description 25
- 238000001556 precipitation Methods 0.000 claims abstract description 24
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims abstract description 20
- 229930006000 Sucrose Natural products 0.000 claims abstract description 20
- 238000004821 distillation Methods 0.000 claims abstract description 20
- 235000012907 honey Nutrition 0.000 claims abstract description 20
- 238000001914 filtration Methods 0.000 claims abstract description 15
- UQZIYBXSHAGNOE-XNSRJBNMSA-N stachyose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO[C@@H]2[C@@H]([C@@H](O)[C@@H](O)[C@@H](CO[C@@H]3[C@@H]([C@@H](O)[C@@H](O)[C@@H](CO)O3)O)O2)O)O1 UQZIYBXSHAGNOE-XNSRJBNMSA-N 0.000 claims abstract description 12
- UQZIYBXSHAGNOE-USOSMYMVSA-N Stachyose Natural products O(C[C@H]1[C@@H](O)[C@H](O)[C@H](O)[C@@H](O[C@@]2(CO)[C@H](O)[C@@H](O)[C@@H](CO)O2)O1)[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@H](CO[C@@H]2[C@@H](O)[C@@H](O)[C@@H](O)[C@H](CO)O2)O1 UQZIYBXSHAGNOE-USOSMYMVSA-N 0.000 claims abstract description 11
- 239000008213 purified water Substances 0.000 claims abstract description 11
- 239000006228 supernatant Substances 0.000 claims abstract description 11
- 235000008504 concentrate Nutrition 0.000 claims description 50
- 239000006071 cream Substances 0.000 claims description 38
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 29
- 238000000151 deposition Methods 0.000 claims description 19
- 239000005720 sucrose Substances 0.000 claims description 16
- 150000003839 salts Chemical class 0.000 claims description 11
- 239000000706 filtrate Substances 0.000 claims description 9
- 239000000470 constituent Substances 0.000 claims description 7
- 239000002994 raw material Substances 0.000 claims description 7
- 238000002386 leaching Methods 0.000 claims description 6
- 230000006837 decompression Effects 0.000 claims description 5
- 238000000605 extraction Methods 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 5
- 238000004062 sedimentation Methods 0.000 claims description 5
- 238000009835 boiling Methods 0.000 claims description 4
- 238000004140 cleaning Methods 0.000 claims description 4
- 238000001816 cooling Methods 0.000 claims description 4
- 239000012535 impurity Substances 0.000 claims description 4
- 239000012982 microporous membrane Substances 0.000 claims description 4
- 238000004064 recycling Methods 0.000 claims description 4
- 239000002893 slag Substances 0.000 claims description 4
- 239000000341 volatile oil Substances 0.000 claims description 4
- 238000005406 washing Methods 0.000 claims description 4
- 241001570521 Lonicera periclymenum Species 0.000 abstract description 86
- 230000000694 effects Effects 0.000 abstract description 7
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- 241000894006 Bacteria Species 0.000 abstract description 4
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract description 4
- 239000011707 mineral Substances 0.000 abstract description 4
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 abstract description 3
- 239000011575 calcium Substances 0.000 abstract description 3
- 229910052791 calcium Inorganic materials 0.000 abstract description 3
- 206010012601 diabetes mellitus Diseases 0.000 abstract description 3
- 239000003053 toxin Substances 0.000 abstract description 3
- 231100000765 toxin Toxicity 0.000 abstract description 3
- 241000245240 Lonicera Species 0.000 abstract description 2
- 238000010521 absorption reaction Methods 0.000 abstract description 2
- 239000003205 fragrance Substances 0.000 abstract description 2
- 229960004793 sucrose Drugs 0.000 abstract 4
- 238000012869 ethanol precipitation Methods 0.000 abstract 3
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract 2
- 235000010755 mineral Nutrition 0.000 abstract 2
- 230000001737 promoting effect Effects 0.000 abstract 2
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- 239000011780 sodium chloride Substances 0.000 abstract 2
- 238000013329 compounding Methods 0.000 abstract 1
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- 235000019605 sweet taste sensations Nutrition 0.000 abstract 1
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- 231100000419 toxicity Toxicity 0.000 abstract 1
- 108700012359 toxins Proteins 0.000 abstract 1
- 230000001954 sterilising effect Effects 0.000 description 22
- 238000001514 detection method Methods 0.000 description 13
- 238000007689 inspection Methods 0.000 description 10
- 239000000243 solution Substances 0.000 description 8
- 241001391944 Commicarpus scandens Species 0.000 description 6
- 241001122767 Theaceae Species 0.000 description 5
- 210000000936 intestine Anatomy 0.000 description 5
- 210000002784 stomach Anatomy 0.000 description 5
- 239000012141 concentrate Substances 0.000 description 4
- 238000011049 filling Methods 0.000 description 4
- 238000011068 loading method Methods 0.000 description 4
- 238000004659 sterilization and disinfection Methods 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 3
- 238000009395 breeding Methods 0.000 description 3
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- 238000005516 engineering process Methods 0.000 description 3
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- 239000000463 material Substances 0.000 description 3
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- 230000009286 beneficial effect Effects 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 239000007938 effervescent tablet Substances 0.000 description 2
- 238000005286 illumination Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000004806 packaging method and process Methods 0.000 description 2
- 239000011265 semifinished product Substances 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 241000186000 Bifidobacterium Species 0.000 description 1
- 241000208828 Caprifoliaceae Species 0.000 description 1
- 206010007247 Carbuncle Diseases 0.000 description 1
- 206010010774 Constipation Diseases 0.000 description 1
- YTBSYETUWUMLBZ-QWWZWVQMSA-N D-threose Chemical compound OC[C@@H](O)[C@H](O)C=O YTBSYETUWUMLBZ-QWWZWVQMSA-N 0.000 description 1
- 206010012735 Diarrhoea Diseases 0.000 description 1
- 201000000297 Erysipelas Diseases 0.000 description 1
- 230000009102 absorption Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 235000018927 edible plant Nutrition 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 230000036449 good health Effects 0.000 description 1
- 239000012943 hotmelt Substances 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 210000000867 larynx Anatomy 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 231100000862 numbness Toxicity 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 235000013406 prebiotics Nutrition 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 239000013558 reference substance Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Non-Alcoholic Beverages (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention provides a honeysuckle concentrating beverage and a preparation method thereof. The honeysuckle concentrating beverage comprises 66.2%-76.6% of dried honeysuckle, 23.0%-33.4% of stachyose and 0.3%-0.8% of table salt. The honeysuckle concentrating beverage is obtained through the steps of distilling the dried honeysuckle to obtain distillate supernatant, filtering a residual distillation solution and a water decoction solution to obtain an extracting solution, decompressing and concentrating the extracting solution to obtain clear paste of the extracting solution, performing ethanol precipitation on the clear paste of the extracting solution to obtain clear paste of an ethanol precipitation solution, performing water precipitation on the clear paste of the ethanol precipitation solution to obtain clear paste of a water precipitation solution, and compounding the distillate supernatant, the clear paste of the water precipitation solution, lupeose, table salt and purified water into the honeysuckle concentrating beverage; or the honeysuckle concentrating beverage is obtained through the steps of adding cane sugar of which the weight accounts for 5% of the total weight of the honeysuckle concentrating beverage, or the honey of which the relative density is larger than or equal to 1.349 to the prepared honeysuckle concentrating beverage, stirring the prepared honeysuckle concentrating beverage with the cane sugar or the honey until the cane sugar or the honey is dissolved, and performing filtration so as to obtain the honeysuckle concentrating beverage added with the cane sugar or the honey. The honeysuckle concentrating beverage disclosed by the invention is yellowish clear liquid or light yellowish-brown clear liquid, and has the peculiar fragrance of the honeysuckles and slightly sweet taste. The honeysuckle concentrating beverage has the efficacies of clearing heat, removing toxicity and dispelling wind and heat, has the effects of protecting gastrointestinal tracts, promoting the propagation of probiotics in the gastrointestinal tracts, restraining the growth of harmful bacteria, expelling toxins, expelling lead and promoting the absorption of mineral substances such as calcium, is suitable for adults to drink, and is also suitable for pregnant women, lying-in women, babies, weak people and diabetes patients to drink. The honeysuckle concentrating beverage can be directly drunk, and can be drunk after being diluted with 20-100 ml of pure water, or 20-100 ml of mineral water or 20-100 ml of warm boiled water.
Description
Technical field
The invention belongs to technical field of beverage processing, particularly relate to a kind of honeysuckle beverage manufacture field, be specifically related to a kind of honeysuckle beverage concentrate and preparation method thereof.
Background technology
Honeysuckle is recorded in Chinese Pharmacopoeia (version in 2010), 205 pages, is the flower that caprifoliaceae plant honeysuckle Lonicer japonicaThunb. dry flower or band are just opened.Autumn in summer, the flowers are in blossom send out before gather, dry.Sweet, cold.The thoughts of returning home, lung, stomach footpath.Clearing heat and detoxicating, dispelling wind and heat from the body.Treat sore, larynx numbness, erysipelas for carbuncle is swollen, hot malicious blood profit, anemopyretic cold, warm disease is generated heat.
Commercially the beverage of honeysuckle is more at present,
CN102578331B plant cold tea decompressed concentrate and preparation method;
CN101292692B plant cold tea reduced pressure concentration juice;
CN101147510B internal heat lowering cool tea and preparation method;
CN101288485B honeysuckle health-care beverage;
The preparation method of a CN101720962B honeysuckle beverage;
CN101785568B honeysuckle leaf distillate beverage and preparation method;
CN101828745B honeysuckle effervescent tablet and preparation method;
CN102793038A Chinese medicinal herb cold tea and preparation method;
CN104171198A Lonicera flower tea powder and preparation method, honeysuckle effervescent tablet and preparation method;
CN104489847A solid particle beverage and preparation method;
CN104432381A honeysuckle health-care beverage and preparation method;
CN104544440A honeysuckle health-care beverage and preparation method;
Refer to the materials containing honeysuckle in above 12 disclosed patent documents, but report for work for honeysuckle beverage concentrate there is not yet.
Relevant production technology and literature survey result show, low containing Honegsukle flower P.E constituent concentration in honeysuckle beverage on market, volume is large, and net content is generally at more than 200ml, not Portable belt; Do not possess and promote that intestines and stomach should the breeding of raw bacterium, improve the effect of gastro-intestinal tract and function.
Summary of the invention
The technical problem to be solved in the present invention is to overcome above-mentioned deficiency, studies a kind of features good taste, and high containing Honegsukle flower P.E constituent concentration, volume is little, honeysuckle beverage concentrate easy to carry.
The invention provides a kind of honeysuckle beverage concentrate, not only be suitable for adult to drink, be more suitable for pregnant, puerpera, infant, weakling, patients with diabetes mellitus, both capable of direct drinking, drink after also can adding 2 ~ 5 times amount pure water, mineral water, warm water dilution again by honeysuckle beverage concentrate volume; The packaging of available little volume, easy to carry.
For realizing the object of the present invention, take following technical scheme: a kind of honeysuckle beverage concentrate, is characterized in that: it is made up of the raw material of following percentage by weight: dry honeysuckle 66.2% ~ 76.6%, stachyose 23.0% ~ 33.4%, salt 0.3% ~ 0.8%; Namely honeysuckle beverage concentrate is obtained through distillation, extraction, reduced pressure concentration, alcohol precipitation, depositing in water, preparation; Or in the honeysuckle beverage concentrate prepared, add the sucrose of gross mass 5% or the honey of relative density >=1.349 again, stirring and dissolving, filter, must with the honeysuckle beverage concentrate of sucrose or honey.
A preparation method for honeysuckle beverage concentrate, is characterized in that:
Comprise the following steps,
1) selection cleaning: get dry honeysuckle, impurity is rejected in selection, with water wash after 3 ~ 5 minutes, the remaining to the greatest extent water of drop;
2) distill: put in multifunctional extracting pot by the honeysuckle of drip washing, add water, add hot temperature leaching, distill, collect distillate, cooling, leave standstill, the upper strata distillate filtration of being rich in volatile oil is got in score by weight, obtains the distillate upper liquid of dry honeysuckle weight 70%;
3) extract: after distillation procedure terminates, collect the raffinate do not distilled in multifunctional extracting pot and must distill rear raffinate; In multifunctional extracting pot honeysuckle slag again boiling 1 time decocting liquid, merge raffinate and decocting liquid after distillation, filter to obtain extract;
4) reduced pressure concentration: extract reduced pressure concentration is obtained the clear cream of extract that relative density is 1.10 ~ 1.26;
5) alcohol precipitation: slowly add ethanol in proper amount in the clear cream of extract, stir evenly, leave standstill, sedimentation, gets supernatant liquid filtering, filtrate recycling ethanol, and reduced pressure concentration obtains the clear cream of precipitation solution that relative density is 1.08 ~ 1.22;
6) depositing in water: add purified water in the clear cream of precipitation solution, stir evenly, cool, leave standstill, sedimentation, get supernatant liquid filtering, it is the clear cream of 1.06 ~ 1.14 depositing in water liquid that filtrate reduced in volume obtains relative density;
7) prepare: get distillate upper liquid, the clear cream of depositing in water liquid is successively put in preparing tank and stirred evenly, add stachyose, salt, be stirred to dissolve, adding purified water to preparation total amount is after 0.8 ~ 3.2 times of dry honeysuckle weight, stir evenly, filter and obtain honeysuckle beverage concentrate; Or in the honeysuckle beverage concentrate prepared, add the sucrose of gross mass 5% or the honey of relative density >=1.349 again, stirring and dissolving, filter, must with the honeysuckle beverage concentrate of sucrose or honey.
Beneficial effect:
The invention provides a kind of honeysuckle beverage concentrate, raw material honeysuckle has clearing heat and detoxicating, dispelling wind and heat from the body function; Raw water threose, purity, more than 85%, is extracted from the edible plants such as kobold; can protect and significantly promote the beneficial bacterium propagation such as Bifidobacterium; effectively can prevent and alleviate constipation of infantile and diarrhoea, suppressing intestines problem, strengthening immunocompetence and the body disease-resistant power of infant comprehensively.Also have gut purge road, the minerals absorbing effects such as toxin expelling lead discharging, promotion calcium are a kind of prebiotic sugar; Raw material salt is the material of needed by human, and three kinds of material composition synergies, make this product not only have clearing heat and detoxicating, dispelling wind and heat from the body effect, also have and promote the breeding of intestines and stomach probio, improve gastrointestinal tract environment and functions of intestines and stomach, strengthen the effect of body immunity.
By the honeysuckle beverage concentrate that this method is obtained, for faint yellow to fallow clear liquid, the peculiar fragrance of tool honeysuckle, taste is micro-sweet.Have clearing heat and detoxicating, dispelling wind and heat from the body effect, also have protection, promote the breeding of intestines and stomach probio, suppress harmful bacteria growth, the effect of the mineral absorptions such as toxin expelling lead discharging, promotion calcium, has good health care; Not only be suitable for adult to drink, be also suitable for pregnant, puerpera, infant, weakling, patients with diabetes mellitus; Both capable of direct drinking, drink after also can adding 20ml ~ 100ml pure water, mineral water, warm water dilution; According to " plant beverage hygienic requirements, DBJ440100/T30-2009(Administration of Quality and Technology Supervision of Guangzhou City issues) " check, meet standard-required completely.
Detailed description of the invention
In order to more clearly state the present invention, provide preferably embodiment.
A kind of honeysuckle beverage concentrate, the raw material composition containing following weight percent proportioning: dry honeysuckle 66.2% ~ 76.6%, stachyose 23.0% ~ 33.4%, salt 0.3% ~ 0.8%; Namely honeysuckle beverage concentrate is obtained through distillation, extraction, reduced pressure concentration, alcohol precipitation, depositing in water, preparation; Or in the honeysuckle beverage concentrate prepared, add the sucrose of gross mass 5% or the honey of relative density >=1.349 again, stirring and dissolving, filter, must with the honeysuckle beverage concentrate of sucrose or honey.
The raw material of the optimum weight per distribution ratio that a kind of honeysuckle beverage concentrate of the present invention is used for when infant drinks consists of: dry honeysuckle 74.4%, stachyose 24.8%, salt 0.8%; Namely honeysuckle beverage concentrate is obtained through distillation, extraction, reduced pressure concentration, alcohol precipitation, depositing in water, preparation; Or in the honeysuckle beverage concentrate prepared, add the sucrose of gross mass 5% or the honey of relative density >=1.349 again, stirring and dissolving, filter, must with the honeysuckle beverage concentrate of sucrose or honey.
A kind of honeysuckle beverage concentrate of the present invention consists of for the raw material of optimum weight per distribution ratio when drinking of being grown up: dry honeysuckle 74.7%, stachyose 25%, salt 0.3%.
A preparation method for honeysuckle beverage concentrate, it comprises successively: the operation steps such as selection cleaning, distillation, extraction, reduced pressure concentration, alcohol precipitation, depositing in water, preparation, filling and sealing, sterilizing, leak detection, quality examination are poly-.
1) selection cleaning: concrete operations comprise gets dry honeysuckle, impurity is rejected in selection; Take the dry honeysuckle of gross weight 66.2% ~ 76.6%, with water wash 3 ~ 5 minutes.
2) distill: concrete operations comprise to be put in multifunctional extracting pot by the honeysuckle of drip washing, by weight, add the water of dry honeysuckle weight 8 ~ 10 times amount, be heated to 50 DEG C ~ 60 DEG C temperature leachings after 30 minutes, decompression distillation under-0.02Mpa ~-0.04Mpa condition, by weight, collect the distillate of dry honeysuckle weight 1 ~ 1.5 times, distillate is cooled to 2 DEG C ~ 12 DEG C, and leave standstill at such a temperature after 6 ~ 12 hours, by weight, the upper strata distillate being rich in volatile oil of dry honeysuckle weight 70% point is got from the distillate after leaving standstill, distillate upper liquid is obtained with 0.45 ~ 1.0 μm of membrane filter, distillate upper liquid is collected in clean container, store for subsequent use under 2 DEG C ~ 12 DEG C conditions.
3) extract: concrete operations comprise after distillation procedure terminates, and collect the raffinate do not distilled in multifunctional extracting pot and must distill rear raffinate; Honeysuckle slag in multifunctional extracting pot after distillation again boiling obtains decocting liquid 1 time, and during decoction, amount of water by weight, is 6 ~ 8 times of the weight of dry honeysuckle, decocting time is 30 ~ 60 minutes, after decoction terminates, merge the rear raffinate of distillation and decocting liquid, filter to obtain extract.
4) reduced pressure concentration: concrete operations comprise extract is placed in decompression concentrator, under vacuum is-0.02 ~-0.06Mpa condition, reduced pressure concentration become relative density be after 1.10 ~ 1.26 clear cream the clear cream of extract.
5) alcohol precipitation: concrete operations comprise and move in clean settling tank by clear for extract cream, slowly add ethanol, limit edged stirs and makes concentration of alcohol reach 60% ~ 80%(g/g), be cooled to room temperature, leave standstill 48 ~ 72 hours, Aspirate supernatant filter, filtrate recycling ethanol, and reduced pressure concentration become relative density be 1.08 ~ 1.22 clear cream obtain the clear cream of precipitation solution.
6) depositing in water: concrete operations comprise and move in clean settling tank by clear for precipitation solution cream, under the condition that limit edged stirs, by dry weight, the purified water of dry honeysuckle weight 0.7 ~ 1.5 times is added in the clear cream of precipitation solution, stir evenly, be cooled to 2 ~ 10 DEG C and leave standstill 12 ~ 24 hours at such a temperature, getting supernatant aperture is 0.45 ~ 1.0 μm of filtering with microporous membrane, filtrate is under vacuum is-0.02 ~-0.06Mpa condition, reduced pressure concentration become relative density be 1.06 ~ 1.14 clear cream obtain the clear cream of depositing in water liquid, store for subsequent use under 2 DEG C ~ 12 DEG C conditions.
7) prepare: concrete operations comprise gets in distillate upper liquid and depositing in water liquid clear cream input preparing tank, stir evenly, add stachyose and 0.3% ~ 0.8% salt of three kinds of constituent gross weights 23.0% ~ 33.4%, be stirred to dissolve, by weight, add 0.8 ~ 3.2 times that purified water to preparation total amount is dry honeysuckle weight, stir evenly, leave standstill 15 ~ 30 minutes, be first 0.45 μm ~ 1.0 μm filtering with microporous membrane with aperture, be that namely 0.22 μm of filtering with microporous membrane obtains honeysuckle beverage concentrate with aperture again, wherein the water of 0.8 times is applicable to adult, the water of 3.2 times is applicable to young child, or in the honeysuckle beverage concentrate prepared, add the sucrose of gross mass 5% or the honey of relative density >=1.349 again, stirring and dissolving, filter, must with the honeysuckle beverage concentrate of sucrose or honey.
8) filling and sealing: concrete operations comprise preparation liquid filling in the clean PET of 10ml, 20ml bottle easy to break respectively, and loading amount is respectively every bottle of 10.3ml ~ 10.8ml, every bottle of 20.5ml ~ 21.0ml, adds bottom hot melt and sternly seals and obtain beverage subject to sterilization.
9) sterilizing: by the bottom of beverage bottle subject to sterilization down, just standing in vehicle of sterilization, send in isobaric sterilizing leak detection cabinet, close cabinet door, the pressure control device such as unlatching, under condition isobaric inside and outside control PET bottle easy to break, flowing steam is heated to 100 ~ 105 DEG C of sterilizings 45 ~ 60 minutes, after purified water spraying cooling to room temperature, close isobaric sterilizing leak detection cabinet etc. pressure control device, obtain sterilising drink.
10) hunt leak: open isobaric sterilizing leak detection cabinet pumped vacuum systems, be evacuated to-0.006 ~-0.01Mpa, and keep under this condition after 15 minutes, close isobaric sterilizing leak detection cabinet pumped vacuum systems, open isobaric sterilizing leak detection cabinet cabinet door and take out beverage, obtain beverage of hunting leak.
11) quality examination: concrete operations comprise takes out beverage of hunting leak from sterilizing leak detection cabinet, and send in darkroom, check under being placed in canopy type lamp inspection cabinet, canopy type lamp inspection cabinet illumination is adjusted to 3000Lx, and background is not for return light white.During inspection, the hand-held beverage bottle bottleneck of scrutineer, makes beverage bottle just stand on shadow shield lower edge, scrutineer adjusts that eye is fine to be about 25cm place carefully to inspect liquid level in bottle apart from beverage bottle, and compare with qualified reference substance liquid level, reject empty bottle and the undesirable semi-finished product of loading amount, concentrate and destroy; Again with slow action upset beverage bottle, beverage bottle is stood upside down respectively, is just standing on shadow shield lower edge continuation inspection, during inspection, sight line first sweeps liquid and bottle inwall in bottle to top successively from beverage bottle bottom, in observation bottle, liquid and bottle inwall are with or without visible foreign matters, reject the semi-finished product having visible foreign matters in bottle, concentrate and destroy, namely satisfactory semi finished package obtains honeysuckle beverage concentrate.
Above-mentioned production operation preferred version is:
Perform step poly-1) time, the impurity in honeysuckle is rejected in selection; Taking dry honeysuckle weight is three kinds of constituent gross weights 66.2% ~ 76.6%, is 3 ~ 5 minutes with the water wash time.
In execution step poly-2) time, distillation procedure amount of water is 8 ~ 10 times of dry honeysuckle weight, temperature leaching temperature is 50 DEG C ~ 60 DEG C, the 30 minutes leaching time of temperature, during decompression distillation, vacuum is-0.02Mpa ~-0.04Mpa, distillate collecting amount is 1 ~ 1.5 times of dry honeysuckle flower weight, and when distillate leaves standstill, temperature is 2 DEG C ~ 12 DEG C, and time of repose is 6 ~ 12 hours; The amount of point to get distillate upper liquid from the distillate after leaving standstill is 70% of dry honeysuckle weight, and the filter aperture of filtering distillate upper liquid is 0.45 ~ 1.0 μm, and distillate upper liquid storage temperature is 2 ~ 12 DEG C.
In execution step poly-3) time, decoct 6 ~ 8 times that amount of water is dry honeysuckle weight, decocting time is 30 ~ 60 minutes.
In execution step poly-4) time, reduced pressure concentration vacuum is-0.02 ~-0.06Mpa, and the clear cream relative density of extract controls 1.10 ~ 1.26.
In execution step poly-5) time, precipitation solution concentration of alcohol controls at 60% ~ 80%(g/g), after precipitation solution is cooled to room temperature, time of repose is 48 ~ 72 hours, and after reclaiming ethanol, it is 1.08 ~ 1.22 that the clear cream of precipitation solution is evaporated to relative density.
In execution step poly-6) time, 0.7 ~ 1.5 times that the purifying water yield is dry honeysuckle weight is added in clear cream, standing sedimentation temperature is 2 ~ 10 DEG C, time of repose 12 ~ 24 hours, when getting supernatant liquid filtering, porous filtering-diaphragm filter aperture is 0.45 ~ 1.0 μm, the vacuum of filtrate reduced in volume is-0.02 ~-0.06Mpa, and it is 1.06 ~ 1.14 that the clear cream of depositing in water liquid is evaporated to relative density, and depositing in water immersion cream storage temperature is 2 DEG C ~ 12 DEG C.
In execution step poly-7) time, distillate upper liquid and the clear cream addition of depositing in water liquid are full dose, stachyose addition is 23.0% ~ 33.4% of three kinds of constituent gross weights, salt addition is 0.3% ~ 0.8% of three kinds of constituent gross weights, preparation total amount is 0.8 ~ 3.2 times of dry honeysuckle weight, preparation liquid time of repose 15 minutes ~ 30 minutes, the porous filtering-diaphragm filter aperture that preparation liquid filters for the 1st time is 0.45 μm ~ 1.0 μm, and the porous filtering-diaphragm filter filtered for the 2nd time also footpath is 0.22 μm.
In execution step poly-8) time, container filling is 10ml, 20mlPET bottle easy to break, and loading amount controls at 10mlPET every bottle, bottle easy to break 10.3ml ~ 10.8ml, 20mlPET every bottle, bottle 20.5ml ~ 21.0ml easy to break respectively, must sternly seal during sealing.
In execution step poly-9) time, sterilizing adopts isobaric sterilizing leak detection cabinet, at pressure control systems such as unlatchings, carries out sterilizing and cooling under the condition that control PET bottle easy to break external and internal pressure is equal; Sterilizing heat medium is circulation steam, and sterilising temp is 100 ~ 105 DEG C, sterilization time 45 ~ 60 minutes, adopts purified water spraying method by beverage but to room temperature after sterilizing.
Performing step poly-10) time, with the leak detection of isobaric sterilizing leak detection cabinet, that first should close isobaric sterilizing leak detection cabinet waits pressure control system, and leak detection vacuum degree control scope is-0.006 ~-0.01Mpa, and the leak detection time is 15 minutes.
In execution step poly-11) time, inspection chamber should be darkroom, canopy type lamp inspection cabinet is opaque white background, illumination is 3000Lx, scrutineer's hand-held beverage bottle bottleneck during inspection, beverage bottle is placed in canopy type lamp inspection cabinet shadow shield lower edge, check that human eye is fine and be about 25cm with the distance of light source, should reject during inspection in empty bottle, loading amount deficiency, bottle and have the undesirable beverages such as visible foreign matters, undesirable beverage should concentrate destruction, and satisfactory beverage is concentrated packaging and be get final product.
Claims (8)
1. a honeysuckle beverage concentrate, is characterized in that: it is made up of the raw material of following percentage by weight: dry honeysuckle 66.2% ~ 76.6%, stachyose 23.0% ~ 33.4%, salt 0.3% ~ 0.8%; Namely honeysuckle beverage concentrate is obtained through distillation, extraction, reduced pressure concentration, alcohol precipitation, depositing in water, preparation; Or in the honeysuckle beverage concentrate prepared, add the sucrose of gross mass 5% or the honey of relative density >=1.349 again, stirring and dissolving, filter, must with the honeysuckle beverage concentrate of sucrose or honey.
2. a preparation method for honeysuckle beverage concentrate, is characterized in that comprising the following steps:
1) selection cleaning: get dry honeysuckle, impurity is rejected in selection, with water wash after 3 ~ 5 minutes, the remaining to the greatest extent water of drop;
2) distill: put in multifunctional extracting pot by the honeysuckle of drip washing, add water, add hot temperature leaching, distill, collect distillate, cooling, leave standstill, the upper strata distillate filtration of being rich in volatile oil is got in score by weight, obtains the distillate upper liquid of dry honeysuckle weight 70%;
3) extract: after distillation procedure terminates, collect the raffinate do not distilled in multifunctional extracting pot and must distill rear raffinate; In multifunctional extracting pot honeysuckle slag again boiling 1 time decocting liquid, merge raffinate and decocting liquid after distillation, filter to obtain extract;
4) reduced pressure concentration: extract reduced pressure concentration is obtained the clear cream of extract that relative density is 1.10 ~ 1.26;
5) alcohol precipitation: slowly add ethanol in proper amount in the clear cream of extract, stir evenly, leave standstill, sedimentation, gets supernatant liquid filtering, filtrate recycling ethanol, and reduced pressure concentration obtains the clear cream of precipitation solution that relative density is 1.08 ~ 1.22;
6) depositing in water: add purified water in the clear cream of precipitation solution, stir evenly, cool, leave standstill, sedimentation, get supernatant liquid filtering, it is the clear cream of 1.06 ~ 1.14 depositing in water liquid that filtrate reduced in volume obtains relative density;
7) prepare: get distillate upper liquid, the clear cream of depositing in water liquid is successively put in preparing tank and stirred evenly, add stachyose, salt, be stirred to dissolve, adding purified water to preparation total amount is after 0.8 ~ 3.2 times of dry honeysuckle weight, stir evenly, filter and obtain honeysuckle beverage concentrate; Or in the honeysuckle beverage concentrate prepared, add the sucrose of gross mass 5% or the honey of relative density >=1.349 again, stirring and dissolving, filter, must with the honeysuckle beverage concentrate of sucrose or honey.
3. the preparation method of a kind of honeysuckle beverage concentrate according to claim 2, it is characterized in that: described step 2) in the honeysuckle of drip washing is put in multifunctional extracting pot, by weight, add the water of dry honeysuckle weight 8 ~ 10 times amount, be heated to 50 DEG C ~ 60 DEG C temperature leachings 30 minutes, decompression distillation under-0.02Mpa ~-0.04Mpa condition, by weight, collect the distillate of dry honeysuckle weight 1 ~ 1.5 times, distillate is cooled to 2 DEG C ~ 12 DEG C, and leave standstill 6 ~ 12 hours at such a temperature, from leave standstill after distillate, divide the upper strata distillate being rich in volatile oil getting dry honeysuckle weight 70%, filter to obtain distillate upper liquid, distillate upper liquid is collected in clean container, store for subsequent use under 2 DEG C ~ 12 DEG C conditions.
4. a kind of honeysuckle beverage concentrate preparation method according to claim 2, is characterized in that: after described step 3) distillation terminates, collect the raffinate do not distilled in multifunctional extracting pot and must distill rear raffinate; The boiling 1 time again of honeysuckle slag after distillation, during decoction, amount of water is by weight, is 6 ~ 8 times of dry honeysuckle weight, decoct 30 ~ 60 minutes after being heated to boil, obtain decocting liquid after decoction terminates, merge the rear raffinate of distillation and decocting liquid, filter and obtain filtration extract.
5. the preparation method of a kind of honeysuckle beverage concentrate according to claim 2, it is characterized in that: extract is put in decompression concentrator by described step 4), under vacuum is-0.02 ~-0.06Mpa condition, reduced pressure concentration become relative density be 1.10 ~ 1.26 clear cream namely obtain the clear cream of extract.
6. the preparation method of a kind of honeysuckle beverage concentrate according to claim 2 or 5, it is characterized in that: clear for extract cream moves in clean settling tank by described step 5), slowly add ethanol, and limit edged stirs, be cooled to room temperature after making concentration of alcohol reach 60% ~ 80%, leave standstill 48 ~ 72 hours, Aspirate supernatant filters, filtrate recycling ethanol, and reduced pressure concentration become relative density be 1.08 ~ 1.22 clear cream namely obtain the clear cream of precipitation solution.
7. the preparation method of a kind of honeysuckle beverage concentrate according to claim 6, it is characterized in that: clear for precipitation solution cream is placed in clean settling tank by described step 6), under the condition that limit edged stirs, by weight, add 0.7 ~ 1.5 times of purified water of dry honeysuckle weight in the clear cream of precipitation solution after, stir evenly, be cooled to 2 ~ 10 DEG C, and leave standstill 12 ~ 24 hours at such a temperature, getting supernatant aperture is 0.45 ~ 1.0 μm of filtering with microporous membrane, filtrate is under vacuum is-0.02 ~-0.06Mpa condition, reduced pressure concentration become relative density be 1.06 ~ 1.14 clear cream namely obtain the clear cream of depositing in water liquid, store for subsequent use under 2 DEG C ~ 12 DEG C conditions.
8. the preparation method of a kind of honeysuckle beverage concentrate according to claim 7, it is characterized in that: described step 7) gets distillate upper liquid and the clear cream of depositing in water liquid drops in preparing tank, stir evenly, add stachyose and 0.3% ~ 0.8% salt of three kinds of constituent gross weights 23.0% ~ 33.4% again, be stirred to dissolve, by weight, adding purified water to preparation total amount is stir evenly after 0.8 ~ 3.2 times of dry honeysuckle weight, leave standstill after 15 ~ 30 minutes, refilter and obtain honeysuckle beverage concentrate; Or in the honeysuckle beverage concentrate prepared, add the sucrose of gross mass 5% or the honey of relative density >=1.349 again, stirring and dissolving, filter, must with the honeysuckle beverage concentrate of sucrose or honey.
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| CN106616191A (en) * | 2016-11-15 | 2017-05-10 | 叶芳健 | Honeysuckle flower and radix puerariae powder effervescent tablets and preparation method |
| CN107950845A (en) * | 2017-11-16 | 2018-04-24 | 湖北瀚思生物科技有限公司 | Honeysuckle functional beverage and its production method |
| CN108095108A (en) * | 2017-12-09 | 2018-06-01 | 天旺科技股份有限公司 | A kind of preparation method of Pitaya Flower health promoting liquid |
| CN109007491A (en) * | 2018-06-05 | 2018-12-18 | 湖北华信制药有限公司 | A kind of honeysuckle herbaceous plant beverage and preparation method thereof |
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| CN109645289A (en) * | 2018-12-28 | 2019-04-19 | 康美新开河（吉林）药业有限公司 | A kind of fresh ginseng solid beverage and preparation method thereof of no sugar addition |
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Denomination of invention: Honeysuckle concentrated beverage and its preparation method Effective date of registration: 20210610 Granted publication date: 20171031 Pledgee: Shiyan Tianditong Health Products Co.,Ltd. Pledgor: Hubei Wudang Biopharmaceutical Science and Technology Co.,Ltd. Registration number: Y2021980004664 |