CN105070769A - 一种具有仿生凸起结构SiO2减反射膜的制备方法 - Google Patents
一种具有仿生凸起结构SiO2减反射膜的制备方法 Download PDFInfo
- Publication number
- CN105070769A CN105070769A CN201510476397.6A CN201510476397A CN105070769A CN 105070769 A CN105070769 A CN 105070769A CN 201510476397 A CN201510476397 A CN 201510476397A CN 105070769 A CN105070769 A CN 105070769A
- Authority
- CN
- China
- Prior art keywords
- sio
- preparation
- sio2
- coating
- antireflective coating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims abstract description 32
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 239000000377 silicon dioxide Substances 0.000 title claims abstract description 16
- 235000012239 silicon dioxide Nutrition 0.000 title claims abstract description 16
- 229910052681 coesite Inorganic materials 0.000 title abstract description 11
- 229910052906 cristobalite Inorganic materials 0.000 title abstract description 11
- 229910052682 stishovite Inorganic materials 0.000 title abstract description 11
- 229910052905 tridymite Inorganic materials 0.000 title abstract description 11
- 239000011521 glass Substances 0.000 claims abstract description 19
- 239000000843 powder Substances 0.000 claims abstract description 19
- 239000000758 substrate Substances 0.000 claims abstract description 16
- 238000000034 method Methods 0.000 claims abstract description 9
- 238000003756 stirring Methods 0.000 claims description 25
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 21
- 239000006117 anti-reflective coating Substances 0.000 claims description 21
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 16
- 229910001868 water Inorganic materials 0.000 claims description 14
- 241001502050 Acis Species 0.000 claims description 13
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 13
- 150000002148 esters Chemical class 0.000 claims description 13
- 229910052710 silicon Inorganic materials 0.000 claims description 13
- 239000010703 silicon Substances 0.000 claims description 13
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 claims description 10
- 239000003921 oil Substances 0.000 claims description 10
- 239000011248 coating agent Substances 0.000 claims description 8
- 238000000576 coating method Methods 0.000 claims description 8
- 238000010792 warming Methods 0.000 claims description 8
- 238000006460 hydrolysis reaction Methods 0.000 claims description 7
- 239000000243 solution Substances 0.000 claims description 7
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 6
- 239000003093 cationic surfactant Substances 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 5
- 230000032683 aging Effects 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 5
- 238000005406 washing Methods 0.000 claims description 5
- YYLGKUPAFFKGRQ-UHFFFAOYSA-N dimethyldiethoxysilane Chemical compound CCO[Si](C)(C)OCC YYLGKUPAFFKGRQ-UHFFFAOYSA-N 0.000 claims description 4
- 230000007062 hydrolysis Effects 0.000 claims description 4
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims description 4
- LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 claims description 4
- 150000004703 alkoxides Chemical class 0.000 claims description 2
- 150000007942 carboxylates Chemical class 0.000 claims description 2
- 150000001734 carboxylic acid salts Chemical class 0.000 claims description 2
- 125000002091 cationic group Chemical group 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 claims description 2
- 230000014759 maintenance of location Effects 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 239000002245 particle Substances 0.000 claims description 2
- 230000008569 process Effects 0.000 claims description 2
- 238000007761 roller coating Methods 0.000 claims description 2
- 239000012266 salt solution Substances 0.000 claims description 2
- 238000004528 spin coating Methods 0.000 claims description 2
- 230000002378 acidificating effect Effects 0.000 abstract description 9
- 238000004140 cleaning Methods 0.000 abstract description 6
- 238000006243 chemical reaction Methods 0.000 abstract description 4
- 238000002834 transmittance Methods 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract 1
- 239000007888 film coating Substances 0.000 abstract 1
- 238000009501 film coating Methods 0.000 abstract 1
- 230000002265 prevention Effects 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- 230000003667 anti-reflective effect Effects 0.000 description 10
- 230000003592 biomimetic effect Effects 0.000 description 7
- 238000009413 insulation Methods 0.000 description 6
- 230000005540 biological transmission Effects 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000012528 membrane Substances 0.000 description 4
- BDKLKNJTMLIAFE-UHFFFAOYSA-N 2-(3-fluorophenyl)-1,3-oxazole-4-carbaldehyde Chemical compound FC1=CC=CC(C=2OC=C(C=O)N=2)=C1 BDKLKNJTMLIAFE-UHFFFAOYSA-N 0.000 description 3
- 108010022579 ATP dependent 26S protease Proteins 0.000 description 3
- 206010013786 Dry skin Diseases 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 238000006482 condensation reaction Methods 0.000 description 3
- 239000008367 deionised water Substances 0.000 description 3
- 229910021641 deionized water Inorganic materials 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 235000017281 sodium acetate Nutrition 0.000 description 3
- 229940087562 sodium acetate trihydrate Drugs 0.000 description 3
- 230000003373 anti-fouling effect Effects 0.000 description 2
- 239000011664 nicotinic acid Substances 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- 229910002808 Si–O–Si Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 229910052755 nonmetal Inorganic materials 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L31/00—Semiconductor devices sensitive to infrared radiation, light, electromagnetic radiation of shorter wavelength or corpuscular radiation and specially adapted either for the conversion of the energy of such radiation into electrical energy or for the control of electrical energy by such radiation; Processes or apparatus specially adapted for the manufacture or treatment thereof or of parts thereof; Details thereof
- H01L31/02—Details
- H01L31/0216—Coatings
- H01L31/02161—Coatings for devices characterised by at least one potential jump barrier or surface barrier
- H01L31/02167—Coatings for devices characterised by at least one potential jump barrier or surface barrier for solar cells
- H01L31/02168—Coatings for devices characterised by at least one potential jump barrier or surface barrier for solar cells the coatings being antireflective or having enhancing optical properties for the solar cells
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E10/00—Energy generation through renewable energy sources
- Y02E10/50—Photovoltaic [PV] energy
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Sustainable Development (AREA)
- Engineering & Computer Science (AREA)
- Sustainable Energy (AREA)
- Physics & Mathematics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- Electromagnetism (AREA)
- General Physics & Mathematics (AREA)
- Computer Hardware Design (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Power Engineering (AREA)
- Surface Treatment Of Glass (AREA)
- Chemically Coating (AREA)
- Paints Or Removers (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510476397.6A CN105070769B (zh) | 2015-08-06 | 2015-08-06 | 一种具有仿生凸起结构SiO2减反射膜的制备方法 |
Applications Claiming Priority (1)
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---|---|---|---|
CN201510476397.6A CN105070769B (zh) | 2015-08-06 | 2015-08-06 | 一种具有仿生凸起结构SiO2减反射膜的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN105070769A true CN105070769A (zh) | 2015-11-18 |
CN105070769B CN105070769B (zh) | 2016-11-16 |
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CN201510476397.6A Active CN105070769B (zh) | 2015-08-06 | 2015-08-06 | 一种具有仿生凸起结构SiO2减反射膜的制备方法 |
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CN (1) | CN105070769B (zh) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108957598A (zh) * | 2018-07-13 | 2018-12-07 | 李志刚 | 可见光区域二氧化硅双纳米空心球冠状结构增透膜及其制备方法 |
CN109659375A (zh) * | 2019-01-31 | 2019-04-19 | 中建材蚌埠玻璃工业设计研究院有限公司 | 一种仿生结构空心纳米二氧化硅粒子减反膜的制备方法 |
CN110373050A (zh) * | 2019-07-19 | 2019-10-25 | 北京科技大学 | 一种疏水SiO2纳米混合液、功能涂层及制备 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20080185041A1 (en) * | 2007-02-02 | 2008-08-07 | Guardian Industries Corp. | Method of making a photovoltaic device with antireflective coating containing porous silica and resulting product |
CN101609859A (zh) * | 2009-07-09 | 2009-12-23 | 上海交大泰阳绿色能源有限公司 | 一种晶体硅太阳能电池双层减反射膜的制作方法 |
CN101866959A (zh) * | 2010-05-14 | 2010-10-20 | 中国科学院上海微系统与信息技术研究所 | 宽谱宽角吸收太阳电池类蛾眼减反结构及其制作方法 |
CN101866958A (zh) * | 2010-05-14 | 2010-10-20 | 河海大学常州校区 | 太阳能电池仿生抗反射膜及其制备方法 |
CN102222704A (zh) * | 2011-06-27 | 2011-10-19 | 光为绿色新能源有限公司 | 一种晶体硅太阳能电池三层减反射膜及其制备方法 |
-
2015
- 2015-08-06 CN CN201510476397.6A patent/CN105070769B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20080185041A1 (en) * | 2007-02-02 | 2008-08-07 | Guardian Industries Corp. | Method of making a photovoltaic device with antireflective coating containing porous silica and resulting product |
CN101609859A (zh) * | 2009-07-09 | 2009-12-23 | 上海交大泰阳绿色能源有限公司 | 一种晶体硅太阳能电池双层减反射膜的制作方法 |
CN101866959A (zh) * | 2010-05-14 | 2010-10-20 | 中国科学院上海微系统与信息技术研究所 | 宽谱宽角吸收太阳电池类蛾眼减反结构及其制作方法 |
CN101866958A (zh) * | 2010-05-14 | 2010-10-20 | 河海大学常州校区 | 太阳能电池仿生抗反射膜及其制备方法 |
CN102222704A (zh) * | 2011-06-27 | 2011-10-19 | 光为绿色新能源有限公司 | 一种晶体硅太阳能电池三层减反射膜及其制备方法 |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108957598A (zh) * | 2018-07-13 | 2018-12-07 | 李志刚 | 可见光区域二氧化硅双纳米空心球冠状结构增透膜及其制备方法 |
CN108957598B (zh) * | 2018-07-13 | 2020-04-07 | 李志刚 | 可见光区域二氧化硅双纳米空心球冠状结构增透膜及其制备方法 |
CN109659375A (zh) * | 2019-01-31 | 2019-04-19 | 中建材蚌埠玻璃工业设计研究院有限公司 | 一种仿生结构空心纳米二氧化硅粒子减反膜的制备方法 |
CN110373050A (zh) * | 2019-07-19 | 2019-10-25 | 北京科技大学 | 一种疏水SiO2纳米混合液、功能涂层及制备 |
CN110373050B (zh) * | 2019-07-19 | 2020-12-04 | 北京科技大学 | 一种疏水SiO2纳米混合液、功能涂层及制备 |
Also Published As
Publication number | Publication date |
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CN105070769B (zh) | 2016-11-16 |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CP01 | Change in the name or title of a patent holder | ||
CP01 | Change in the name or title of a patent holder |
Address after: 233010 Tushan Road 1047, Yuhui District, Bengbu City, Anhui Province Patentee after: China Building Materials Glass New Materials Research Institute Group Co.,Ltd. Address before: 233010 Tushan Road 1047, Yuhui District, Bengbu City, Anhui Province Patentee before: BENGBU DESIGN & Research Institute FOR GLASS INDUSTRY |
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PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A preparation method of SiO2antireflection film with bionic convex structure Effective date of registration: 20221013 Granted publication date: 20161116 Pledgee: Agricultural Bank of China Limited Bengbu Branch Pledgor: China Building Materials Glass New Materials Research Institute Group Co.,Ltd. Registration number: Y2022980018261 |
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Application publication date: 20151118 Assignee: CHINA NATIONAL BUILDING MATERIALS (HEFEI) NEW ENERGY RESOURCES CO.,LTD. Assignor: China Building Materials Glass New Materials Research Institute Group Co.,Ltd. Contract record no.: X2022980022021 Denomination of invention: A preparation method of SiO2antireflection film with bionic convex structure Granted publication date: 20161116 License type: Common License Record date: 20221130 |
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Application publication date: 20151118 Assignee: CNBM (YIXING) NEW ENERGY RESOURCES CO.,LTD. Assignor: China Building Materials Glass New Materials Research Institute Group Co.,Ltd. Contract record no.: X2022980024430 Denomination of invention: A preparation method of SiO2antireflection film with bionic convex structure Granted publication date: 20161116 License type: Common License Record date: 20221216 |
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Application publication date: 20151118 Assignee: CHINA BUILDING MATERIAL TONGCHENG NEW MATERIAL Co.,Ltd. Assignor: China Building Materials Glass New Materials Research Institute Group Co.,Ltd. Contract record no.: X2023980032105 Denomination of invention: A preparation method of SiO2 antireflection film with bionic convex structure Granted publication date: 20161116 License type: Common License Record date: 20230213 |
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Date of cancellation: 20231115 Granted publication date: 20161116 Pledgee: Agricultural Bank of China Limited Bengbu Branch Pledgor: China Building Materials Glass New Materials Research Institute Group Co.,Ltd. Registration number: Y2022980018261 |