CN105010348A - Agricultural chemical composition containing fluorine-azole cyelafuramid, fludioxonil and fluorine-pyrrole furanone - Google Patents
Agricultural chemical composition containing fluorine-azole cyelafuramid, fludioxonil and fluorine-pyrrole furanone Download PDFInfo
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- CN105010348A CN105010348A CN201510404438.0A CN201510404438A CN105010348A CN 105010348 A CN105010348 A CN 105010348A CN 201510404438 A CN201510404438 A CN 201510404438A CN 105010348 A CN105010348 A CN 105010348A
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- fluorine
- fludioxonil
- pyrrole furanone
- bacterium amine
- azoles ring
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Abstract
The invention discloses an agricultural chemical composition containing fluorine-azole cyelafuramid, fludioxonil and fluorine-pyrrole furanone, wherein the fluorine azole cyelafuramid accounts for 0.1-40wt% of the agricultural chemical composition, the fludioxonil accounts for 0.1-40wt% of the agricultural chemical composition, and the fluorine-pyrrole furanone accounts for 0.1-70wt% of the agricultural chemical composition. The agricultural chemical composition disclosed by the invention can effectively prevent and treat various diseases and insect pests on potatoes, and has many advantages of broad preventing and treating spectrum, slow resistance development, notable synergistic effects, low preventing and treating cost and the like.
Description
Technical field
The present invention relates to composition pesticide and application thereof, specifically with the composition pesticide that fluorine azoles ring bacterium amine and fludioxonil and fluorine pyrrole furanone are active ingredient, be applied to the control of damage by disease and insect on potato.
Background technology
Fluorine azoles ring bacterium amine (Sedaxane): mainly suppress mitochondria, to the Be very effective of rhizoctonia, the lasting period is long, other kind of biography and soil-borne disease is also had to the control of wide spectrum.
Fludioxonil (Fludioxonil): be non-interior suction benzene pyroles contact killing type bactericide; by the transfer suppressing glucose phosphorylated relevant, and the mycelial growth of Antifungi, finally cause germ dead; the mechanism of action is unique, with existing bactericide without cross resistance.High-efficiency broad spectrum, passes the microbial kind of many cause of diseases such as sac fungi, basidiomycetes, imperfect fungus and soil-borne disease has extraordinary preventive effect.
Fluorine pyrrole furanone (Flupyradifurone): be novel nicotinamide insecticide, acts on the central nervous system of insect, is the antagonist of insect nAChR.Mainly effective to sucking pest, harmless to honeybee, application restriction of not bloomed, to crop safety.
For the extermination of disease and insect pest agriculturally easily developed immunity to drugs, the use mechanism of action is different, the different pesticide species of control spectrum carries out the selection that mixture is a kind of the best.If reasonable mixture ratio, then can produce significant synergistic effect, make field control effect significantly be better than the effect of each single dose, expanding prevention is composed.Disease and the insect pest of large Tanaka often mix generation, as the damage by disease and insect such as the aphid on potato, tar spot mix generation throughout the year, peasant needs to buy insecticide and bactericide simultaneously, the edge of a field mixes temporarily, random large, is not often Use out of range, cause waste, increase environmental pollution, use quantity not sufficient exactly, impact prevents and treats quality.And part bactericide and insecticide are due to reasons such as chemical reactions, and are not suitable for mixture and use together, mixture is improper also easily causes degradation problem under control efficiency.
Summary of the invention
The object of the invention is for above-mentioned Problems existing, a kind of composition pesticide containing fluorine azoles ring bacterium amine and fludioxonil and fluorine pyrrole furanone is provided, for preventing and treating the multiple damage by disease and insect such as aphid on potato, grub, late blight and tar spot, a drug can parasitosis be double controls, simplify farming, joint medicine cost, reduces environmental pollution, improves and prevent and treat quality.
Technical scheme of the present invention: a kind of composition pesticide containing fluorine azoles ring bacterium amine and fludioxonil and fluorine pyrrole furanone, active ingredient is fluorine azoles ring bacterium amine, fludioxonil, fluorine pyrrole furanone, the percentage by weight of fluorine azoles ring bacterium amine in composition pesticide is 0.1% ~ 40%, the percentage by weight of fludioxonil in composition pesticide is 0.1% ~ 40%, and the percentage by weight of fluorine pyrrole furanone in composition pesticide is herbal medicine 0.1% ~ 70%.
Composition pesticide of the present invention is also containing the auxiliary element needed for pesticidal preparations, comprise emulsifier, dispersant, antifreezing agent, preservative, film forming agent, defoamer, colouring agent etc., it is all composition that is conventional in pesticidal preparations or permission use, be not particularly limited, concrete composition and consumption are determined by simple test according to recipe requirements.
Composition pesticide of the present invention according to well known to a person skilled in the art method, can be processed into suspension seed-coating agent.
The production technology of described composition pesticide application forms all belongs to existing known technology, does not repeat them here.
Composition pesticide of the present invention, is applicable to control potato disease insect pest aphid, grub, late blight, tar spot.
Composition pesticide described in the invention, can finished product preparation form provide, namely in composition, each material mixes, and the composition of composition also can provide by unit dose form, directly mixes in bucket or tank, be then diluted to desired concn before using.
Composition pesticide provided by the invention, usually adopts dressing methods to use, also can adopt other operation techniques agriculturally applied as required.
Compared with prior art, the invention has the advantages that:
1, fluorine azoles ring bacterium amine, fludioxonil and fluorine pyrrole furanone ternary built have significant synergistic function, the control efficiency significantly improved damage by disease and insect is used than single dose or binary built, expand control spectrum simultaneously, accomplished that a medicine is controlled, damage by disease and insect is planted by Zhiduo County of holding concurrently more.
2, fluorine azoles ring bacterium amine, fludioxonil and fluorine pyrrole furanone ternary built, the service life decreasing Pesticide use amount, reduce use cost, alleviate pollution to environment, delayed the drug-fast generation of damage by disease and insect, extended agricultural chemicals.
Embodiment
In order to understand essence of the present invention better; below in conjunction with embodiment, content of the present invention is described further; but can not limitation of the present invention be considered as; the following stated is only for explaining the present invention; for not departing from amendment that the present invention's spirit and principle make, replacement or improvement, all belong to the scope of protection of present invention.
Embodiment one
Following material is all weight percentage: fluorine azoles ring bacterium amine 2%, fludioxonil 1%, fluorine pyrrole furanone 10%, agriculture breast No. 500 10%, lignin sodium iodate 1.5%, Sodium Benzoate 1.5%, polyvinyl acetate 0.5%, silicone oil 1%, glycerine 1.5%, Rosa Damascana 0.5%, add water and complement to 100%.Each component is pre-mixed, then adds in sand mill and grind, after high shear mixing, add film forming agent and colouring agent allotment, 13% fluorine azoles ring bacterium amine fludioxonil fluorine pyrrole furanone suspension seed-coating agent can be obtained.
This embodiment is for preventing and treating aphid on potato, grub, late blight and tar spot: 13% fluorine azoles ring bacterium amine fludioxonil fluorine pyrrole furanone suspension seed-coating agent is by 130g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 86.42%, 83.17%, 84.58%, 85.95%; 30% fluorine azoles ring bacterium amine 20% fludioxonil suspension seed-coating agent presses 40g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 0.84%, 0.92%, 51.37%, 57.89%; 44% fluorine azoles ring bacterium amine suspension seed-coating agent presses 30g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 0.37%, 0.75%, 39.74%, 54.53%; 25 grams per liter fludioxonil suspension seed-coating agents press 20g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 0.58%, 0.62%, 48.65%, 52.58%; 50% fluorine pyrrole furanone suspension seed-coating agent presses 150g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 66.78%, 58.93%, 0.56%, 0.78%.Visible, after fluorine azoles ring bacterium amine, fludioxonil and fluorine pyrrole furanone ternary built, synergistic effect is remarkable, lasting period is long, expand control spectrum, to the preventive effect of the damage by disease and insect such as the aphid on potato, grub, late blight and tar spot significantly better than single dose or binary built, obviously reduce when in ternary built medicament, the amount ratio single dose of active ingredient or binary built use, thus alleviate carrying capacity of environment, reduce use cost, meanwhile, in process of the test, do not find that ternary built medicament germinates to seed potato and plant strain growth produces poisoning.
Embodiment two
Following material is all weight percentage: fluorine azoles ring bacterium amine 3%, fludioxonil 1%, fluorine pyrrole furanone 30%, agriculture breast No. 400 10%, lauryl sodium sulfate 1.5%, Sodium Benzoate 1.5%, polyvinyl acetate 0.5%, silicone oil 1%, glycerine 1.5%, rose-red 0.5%, add water and complement to 100%.Each component is pre-mixed, then adds in sand mill and grind, after high shear mixing, add film forming agent and colouring agent allotment, 34% fluorine azoles ring bacterium amine fludioxonil fluorine pyrrole furanone suspension seed-coating agent can be obtained.
This embodiment is for preventing and treating aphid on potato, grub, late blight and tar spot: 34% fluorine azoles ring bacterium amine fludioxonil fluorine pyrrole furanone suspension seed-coating agent is by 130g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 84.78%, 83.66%, 85.53%, 82.47%; 30% fluorine azoles ring bacterium amine 20% fludioxonil suspension seed-coating agent presses 40g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 0.93%, 0.77%, 50.75%, 58.17%; 44% fluorine azoles ring bacterium amine suspension seed-coating agent presses 30g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 0.64%, 0.48%, 40.76%, 52.69%; 25 grams per liter fludioxonil suspension seed-coating agents press 20g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 0.59%, 0.38%, 47.82%, 54.67%; 50% fluorine pyrrole furanone suspension seed-coating agent presses 150g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 63.31%, 52.05%, 0.46%, 0.82%.Visible, after fluorine azoles ring bacterium amine, fludioxonil and fluorine pyrrole furanone ternary built, synergistic effect is remarkable, lasting period is long, expand control spectrum, to the preventive effect of the damage by disease and insect such as the aphid on potato, grub, late blight and tar spot significantly better than single dose or binary built, obviously reduce when in ternary built medicament, the amount ratio single dose of active ingredient or binary built use, thus alleviate carrying capacity of environment, reduce use cost, meanwhile, in process of the test, do not find that ternary built medicament germinates to seed potato and plant strain growth produces poisoning.
Embodiment three
Following material is all weight percentage: fluorine azoles ring bacterium amine 1%, fludioxonil 1%, fluorine pyrrole furanone 20%, agriculture breast No. 400 10%, aryl alkyl APEO 1.5%, Sodium Benzoate 1.5%, polyvinyl alcohol 0.5%, silicone oil 1%, glycerine 1.5%, rose-red 0.5%, add water and complement to 100%.Each component is pre-mixed, then adds in sand mill and grind, after high shear mixing, add film forming agent and colouring agent allotment, 22% fluorine azoles ring bacterium amine fludioxonil fluorine pyrrole furanone suspension seed-coating agent can be obtained.
This embodiment is for preventing and treating aphid on potato, grub, late blight and tar spot: 22% fluorine azoles ring bacterium amine fludioxonil fluorine pyrrole furanone suspension seed-coating agent is by 130g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 81.32%, 80.25%, 81.64%, 83.06%; 30% fluorine azoles ring bacterium amine 20% fludioxonil suspension seed-coating agent presses 40g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 1.13%, 0.65%, 50.97%, 59.13%; 44% fluorine azoles ring bacterium amine suspension seed-coating agent presses 30g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 0.29%, 0.47%, 43.21%, 55.64%; 25 grams per liter fludioxonil suspension seed-coating agents press 20g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 0.83%, 0.36%, 47.53%, 53.66%; 50% fluorine pyrrole furanone suspension seed-coating agent presses 150g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 65.52%, 56.78%, 0.49%, 0.71%.Visible, after fluorine azoles ring bacterium amine, fludioxonil and fluorine pyrrole furanone ternary built, synergistic effect is remarkable, lasting period is long, expand control spectrum, to the preventive effect of the damage by disease and insect such as the aphid on potato, grub, late blight and tar spot significantly better than single dose or binary built, obviously reduce when in ternary built medicament, the amount ratio single dose of active ingredient or binary built use, thus alleviate carrying capacity of environment, reduce use cost, meanwhile, in process of the test, do not find that ternary built medicament germinates to seed potato and plant strain growth produces poisoning.
Embodiment four
Following material is all weight percentage: fluorine azoles ring bacterium amine 1%, fludioxonil 1%, fluorine pyrrole furanone 10%, agriculture breast No. 602 10%, polycarboxylate 1.5%, phenmethylol 1.5%, polyvinyl alcohol 0.5%, silicone oil 1%, glycerine 1.5%, water-based rose-red 0.5%, add water and complement to 100%.Each component is pre-mixed, then adds in sand mill and grind, after high shear mixing, add film forming agent and colouring agent allotment, 12% fluorine azoles ring bacterium amine fludioxonil fluorine pyrrole furanone suspension seed-coating agent can be obtained.
This embodiment is for preventing and treating aphid on potato, grub, late blight and tar spot: 12% fluorine azoles ring bacterium amine fludioxonil fluorine pyrrole furanone suspension seed-coating agent is by 130g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 83.86%, 81.14%, 80.96%, 82.33%; 30% fluorine azoles ring bacterium amine 20% fludioxonil suspension seed-coating agent presses 40g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 0.98%, 0.71%, 48.89%, 55.67%; 44% fluorine azoles ring bacterium amine suspension seed-coating agent presses 30g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 0.52%, 0.49%, 41.38%, 50.25%; 25 grams per liter fludioxonil suspension seed-coating agents press 20g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 0.65%, 0.58%, 46.61%, 53.48%; 50% fluorine pyrrole furanone suspension seed-coating agent presses 150g a.i./100kg seed Dressing, and after planting the preventive effect of 40d to the aphid on potato, grub, late blight and tar spot is respectively 67.64%, 58.32%, 0.39%, 0.42%.Visible, after fluorine azoles ring bacterium amine, fludioxonil and fluorine pyrrole furanone ternary built, synergistic effect is remarkable, lasting period is long, expand control spectrum, to the preventive effect of the damage by disease and insect such as the aphid on potato, grub, late blight and tar spot significantly better than single dose or binary built, obviously reduce when in ternary built medicament, the amount ratio single dose of active ingredient or binary built use, thus alleviate carrying capacity of environment, reduce use cost, meanwhile, in process of the test, do not find that ternary built medicament germinates to seed potato and plant strain growth produces poisoning.
Embodiment five
Be the composite synergy type of active ingredient to understand fluorine azoles ring bacterium amine, fludioxonil and fluorine pyrrole furanone further, to be that active ingredient is composite to fluorine azoles ring bacterium amine, fludioxonil and fluorine pyrrole furanone carried out a large amount of Toxicity Determination tests to the present inventor.
1, the composite Toxicity Determination to Potato Aphid of fluorine azoles ring bacterium amine, fludioxonil and fluorine pyrrole furanone
Carry out statistical analysis with DPS statistical analysis software, calculate the LC of each medicament
50, and calculating the co-toxicity coefficient (CTC) of mixture: co-toxicity coefficient (CTC)>=120 shows as synergistic effect; Co-toxicity coefficient (CTC)≤80 shows as antagonism; 80 < co-toxicity coefficient (CTC) < 120 show as summation action.
Table 1, Toxicity Determination result to Potato Aphid
| Medicament | LC 50 | ATI | TTI | CTC |
| Fluorine azoles ring bacterium amine (A) | 2569.82 | 100.00 | - | - |
| Fludioxonil (B) | 2177.97 | 117.99 | - | - |
| Fluorine pyrrole furanone (C) | 1.26 | 203953.97 | - | - |
| A:B:C(3:1:30) | 0.72 | 356919.44 | 179971.68 | 198.32 |
| A:B:C(3:1:20) | 0.93 | 276324.73 | 169979.06 | 162.56 |
| A:B:C(3:1:10) | 1.02 | 251943.14 | 145711.26 | 172.91 |
| A:B:C(2:1:30) | 0.94 | 273385.11 | 185422.33 | 147.44 |
| A:B:C(2:1:20) | 0.85 | 302331.76 | 177365.10 | 170.46 |
| A:B:C(2:1:10) | 0.79 | 325293.67 | 156912.13 | 207.31 |
| A:B:C(1:1:30) | 0.83 | 309616.87 | 191213.66 | 161.92 |
| A:B:C(1:1:20) | 0.77 | 333742.86 | 185422.61 | 179.99 |
| A:B:C(1:1:10) | 0.91 | 282397.80 | 169979.81 | 166.14 |
As can be seen from Table 1, when fluorine azoles ring bacterium amine, fludioxonil and fluorine pyrrole furanone are composite in a certain proportion of scope, co-toxicity coefficient (CTC) is all greater than 120, shows synergistic function to Potato Aphid; Especially composite with 2:1:10 (by quality), synergistic function is the most remarkable, and co-toxicity coefficient (CTC) is 207.31.Visible, fluorine azoles ring bacterium amine, fludioxonil and fluorine pyrrole furanone is composite has reasonability and feasibility.
2, the composite Toxicity Determination to potato black scurf of fluorine azoles ring bacterium amine, fludioxonil and fluorine pyrrole furanone
Carry out statistical analysis with DPS statistical analysis software, calculate the EC of each medicament
50, and calculating the interactional synergism value of mixture (SR): synergism value (SR) < 0.5 is antagonism; Synergism value (SR)=0.5 ~ 1.5 is additions; Synergism value (SR) > 1.5 is synergistic effects.
Table 2, Toxicity Determination result to potato black scurf
| Medicament | EC 50(ob) | EC 50(th) | SR |
| Fluorine azoles ring bacterium amine (A) | 5.28 | - | - |
| Fludioxonil (B) | 7.96 | - | - |
| Fluorine pyrrole furanone (C) | 803.95 | - | - |
| A:B:C(3:1:30) | 17.42 | 46.50 | 2.67 |
| A:B:C(3:1:20) | 14.28 | 33.39 | 2.34 |
| A:B:C(3:1:10) | 11.67 | 19.82 | 1.70 |
| A:B:C(2:1:30) | 19.39 | 60.92 | 3.14 |
| A:B:C(2:1:20) | 23.94 | 43.45 | 1.82 |
| A:B:C(2:1:10) | 7.68 | 25.15 | 3.28 |
| A:B:C(1:1:30) | 38.46 | 90.82 | 2.36 |
| A:B:C(1:1:20) | 35.97 | 64.73 | 1.80 |
| A:B:C(1:1:10) | 16.79 | 36.65 | 2.18 |
As can be seen from Table 2, when fluorine azoles ring bacterium amine, fludioxonil and fluorine pyrrole furanone are composite in a certain proportion of scope, synergism value (SR) is all greater than 1.5, shows synergistic function to potato black scurf; Especially composite with 2:1:10 (by quality), synergistic function is the most remarkable, and synergism value (SR) is 3.28.Visible, fluorine azoles ring bacterium amine, fludioxonil and fluorine pyrrole furanone is composite has reasonability and feasibility.
In sum, the present invention adopts fluorine azoles ring bacterium amine, fludioxonil and fluorine pyrrole furanone to be the composite ternary complex of active ingredient, obvious synergy, a drug can parasitosis be double controls, and expands control spectrum, compared with existing single dose or binary built preparation, prevention and elimination of disease and pests successful improves, and the lasting period is long, to crop safety, be worth applying in agricultural production.
Claims (4)
1. one kind contains the composition pesticide of fluorine azoles ring bacterium amine and fludioxonil and fluorine pyrrole furanone, it is characterized in that: active ingredient is fluorine azoles ring bacterium amine, fludioxonil, fluorine pyrrole furanone, the percentage by weight of fluorine azoles ring bacterium amine in composition pesticide is 0.1% ~ 40%, the percentage by weight of fludioxonil in composition pesticide is 0.1% ~ 40%, and the percentage by weight of fluorine pyrrole furanone in composition pesticide is 0.1% ~ 70%.
2. a kind of composition pesticide containing fluorine azoles ring bacterium amine and fludioxonil and fluorine pyrrole furanone according to claim 1, is characterized in that: its formulation is suspension seed-coating agent.
3. a kind of composition pesticide containing fluorine azoles ring bacterium amine and fludioxonil and fluorine pyrrole furanone according to claim 1 is preventing and treating the application in potato disease insect pest.
4. a kind of composition pesticide containing fluorine azoles ring bacterium amine and fludioxonil and fluorine pyrrole furanone according to claim 3, is characterized in that: described potato disease insect pest is aphid, grub, late blight, tar spot.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107467030A (en) * | 2017-08-30 | 2017-12-15 | 佛山市盈辉作物科学有限公司 | Seed treatment compositions containing fludioxonil, Metalaxyl-M and fluorine pyrrole furanone |
| CN107771811A (en) * | 2017-08-24 | 2018-03-09 | 广东和利农种业股份有限公司 | A kind of seed of bitter gourd inorganic agent and its method for handling seed of bitter gourd |
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| CN101466705A (en) * | 2006-03-31 | 2009-06-24 | 拜尔农作物科学股份公司 | Substituted enaminocarbonyl compounds |
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| CN104719304A (en) * | 2013-12-20 | 2015-06-24 | 陕西美邦农药有限公司 | Sedaxane-containing bactericidal composition |
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| CN101466705A (en) * | 2006-03-31 | 2009-06-24 | 拜尔农作物科学股份公司 | Substituted enaminocarbonyl compounds |
| DE102007045953A1 (en) * | 2007-09-26 | 2009-04-02 | Bayer Cropscience Ag | Active substance combination, useful for combating animal pest, treating seed, transgenic plant and seeds of transgenic plant, comprises a 5H-furan-2-one compound and other active agent comprising e.g. acrinathrin and alpha-cypermethrin |
| CN102365018A (en) * | 2009-03-25 | 2012-02-29 | 拜尔农作物科学股份公司 | Synergistic combinations of active ingredients |
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| CN107771811A (en) * | 2017-08-24 | 2018-03-09 | 广东和利农种业股份有限公司 | A kind of seed of bitter gourd inorganic agent and its method for handling seed of bitter gourd |
| CN107771811B (en) * | 2017-08-24 | 2020-10-09 | 广东和利农种业股份有限公司 | Bitter gourd seed treating agent and method for treating bitter gourd seeds by using same |
| CN107467030A (en) * | 2017-08-30 | 2017-12-15 | 佛山市盈辉作物科学有限公司 | Seed treatment compositions containing fludioxonil, Metalaxyl-M and fluorine pyrrole furanone |
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| CN105010348B (en) | 2018-08-14 |
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